CN108314321A - The double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze - Google Patents
The double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze Download PDFInfo
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- CN108314321A CN108314321A CN201810158027.1A CN201810158027A CN108314321A CN 108314321 A CN108314321 A CN 108314321A CN 201810158027 A CN201810158027 A CN 201810158027A CN 108314321 A CN108314321 A CN 108314321A
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- glaze
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- slurry
- reaction
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Links
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 49
- 239000002184 metal Substances 0.000 title claims abstract description 49
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 239000000463 material Substances 0.000 claims abstract description 37
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- CNLWCVNCHLKFHK-UHFFFAOYSA-N aluminum;lithium;dioxido(oxo)silane Chemical group [Li+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O CNLWCVNCHLKFHK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000010453 quartz Substances 0.000 claims abstract description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 8
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical group [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 7
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910021532 Calcite Inorganic materials 0.000 claims abstract description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical group [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 4
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical group [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052656 albite Inorganic materials 0.000 claims abstract description 4
- 229910052796 boron Inorganic materials 0.000 claims abstract description 4
- 230000004907 flux Effects 0.000 claims abstract description 4
- 239000000376 reactant Substances 0.000 claims abstract description 4
- 229910052623 talc Inorganic materials 0.000 claims abstract description 4
- 239000000454 talc Substances 0.000 claims abstract description 4
- 239000002002 slurry Substances 0.000 claims description 51
- 239000000203 mixture Substances 0.000 claims description 16
- 238000000498 ball milling Methods 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 10
- 238000007873 sieving Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 238000010304 firing Methods 0.000 claims description 7
- 239000002689 soil Substances 0.000 claims description 6
- 229910052642 spodumene Inorganic materials 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical group O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 239000011787 zinc oxide Substances 0.000 claims description 3
- 239000004927 clay Substances 0.000 abstract 2
- 210000003298 dental enamel Anatomy 0.000 abstract 2
- 235000012222 talc Nutrition 0.000 abstract 1
- 239000002932 luster Substances 0.000 description 5
- 238000005034 decoration Methods 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 241000692783 Chylismia claviformis Species 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 238000001465 metallisation Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/18—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing free metals
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Structural Engineering (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a kind of double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze, containing reaction glaze and metal glaze ground-coat enamel material in glaze used in the double-deck glaze that reaction glaze is combined with metal glaze;Wherein, the component and each component mass parts that the reaction glaze contains are as follows:High boron frit:30 parts;Spodumene:30 parts;Quartz:28 parts;Calcite:10 parts;Zinc oxide:10 parts;Reactant:10 parts;Talcum:5 parts;Guizhou clay:3 parts;Iron oxide red:3 parts;Manganese powder:3 parts;The component and each component mass parts that the metal glaze ground-coat enamel material contains are as follows:Iron powder:35 parts;Metal flux:20 parts;Albite:30 parts;Spodumene:15 parts;Quartz:8 parts;Guizhou clay:2 parts;Wash mud:10 parts.The glaze of the present invention does not contain lead, and more environmentally friendly, color is gorgeous, deep to be liked by client.
Description
Technical Field
The invention relates to a double-layer glaze combining reaction glaze and metal glaze and a preparation method thereof.
Background
At present, the color of the whole body of the dish product in the prior art is single, along with the improvement of the living level of people and the requirement on the living environment, the glaze of the dish product has higher decoration requirement, and because the metal decoration material has elegant and luxurious artistic effect, the glaze with metal luster is more and more popular. At present, three manufacturing methods for realizing the metallic luster glaze are available: 1 directly sputtering a molten metal coating on the blank; 2. coating a coat containing metal or metal compound powder on the glaze surface of the product, and performing reduction heat treatment to form a metallized decorative layer; 3. preparing glaze components with specific compositions, and firing to produce the metal luster imitating glaze with similar appearance of metal luster such as color tone, luster and the like. The first two technologies have high requirements on equipment and high decoration cost: in the third method, by preparing glaze components, the glaze with the metallization effect is directly formed without changing the firing system of the existing tunnel kiln. At present, the glaze is only applied to wall and floor tiles, and batch production is not seen in the field of dish products; similar studies are not ideal and the main problems are: 1. the metallic effect of the glaze is not particularly outstanding; 2. the wear resistance and corrosion resistance of the metal glaze surface are not related; 3. lead is generally used for preparing the glaze, so that the lead content of the glaze surface exceeds the standard, and the health of a human body is influenced when the glaze is used; 4. the glaze has more defects of pinholes and brown eyes.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the double-layer glaze combining the reaction glaze and the metal glaze, and the glaze surface of the double-layer glaze does not contain lead, is relatively environment-friendly and bright in color and is deeply favored by customers.
In order to solve the technical problems, the technical scheme of the invention is as follows: a reaction glaze and metal glaze combined double-layer glaze, wherein the glaze used in the double-layer glaze comprises a reaction glaze material and a metal glaze bottom glaze material; wherein,
the reaction glaze material comprises the following components in parts by mass:
high boron frit: 30 parts of (1);
spodumene: 30 parts of (1);
quartz: 28 parts of (1);
calcite: 10 portions of
Zinc oxide: 10 parts of (A);
the reaction agent: 10 parts of (A);
talc: 5 parts of a mixture;
guizhou soil: 3 parts of a mixture;
iron oxide red: 3 parts of a mixture;
manganese powder: 3 parts of a mixture;
the metal glaze bottom glaze material comprises the following components in parts by mass:
iron powder: 35 parts of (B);
metal flux: 20 parts of (1);
albite: 30 parts of (1);
spodumene: 15 parts of (1);
quartz: 8 parts of a mixture;
guizhou soil: 2 parts of (1);
washing mud: 10 parts.
Further, the reactant is rutile titanium dioxide.
The invention also provides a preparation method of the double-layer glaze combining the reaction glaze and the metal glaze, which comprises the following steps:
s1: respectively preparing surface glaze slurry and bottom glaze slurry; wherein the overglaze slurry is made of reactive glaze; the ground glaze slurry is made of metal ground glaze;
s2: taking a clean blank body and applying bottom glaze slurry;
s3: after the bottom glaze slurry is dried, applying surface glaze slurry;
s4: and firing the blank body coated with the overglaze slurry at 1170-1200 ℃.
Further, a method for preparing the cover slip is provided, in step S1, the method for preparing the cover slip is as follows:
preparing materials according to the components and all components of the reactive glaze;
according to the material: ball: and (3) performing wet ball milling for 12-18 hours with the mass ratio of water being 1:2:0.7, then sieving with a 250-mesh sieve, and modulating to 47-49 Baume degrees to obtain the surface glaze slurry.
Further provides a method for preparing the ground glaze slip, in step S1, the method for preparing the ground glaze slip comprises the following steps:
preparing materials according to the components of the metal glaze bottom glaze and each component;
according to the material: ball: and (3) performing wet ball milling for 12-15 hours with the mass ratio of water being 1:2:0.8, then sieving with a 250-mesh sieve, and modulating to 42-47 Baume degrees to obtain the final glaze slurry.
After the technical scheme is adopted, the metal glaze bottom glaze material adopted by the invention is the lead-free metal glaze, is relatively environment-friendly, is widely suitable for the production of household porcelain, has the sintering temperature lower than that of the traditional metal glaze, and is titanium crystal as the reaction glaze material, so that the prepared glaze is bright in color and is deeply favored by customers.
Detailed Description
In order that the present invention may be more clearly understood, the following detailed description of the present invention is given with reference to specific examples.
Example one
A reaction glaze and metal glaze combined double-layer glaze, wherein the glaze used in the double-layer glaze comprises a reaction glaze material and a metal glaze bottom glaze material; wherein,
the reaction glaze material comprises the following components in parts by mass:
high boron frit: 30 parts of (1);
spodumene: 30 parts of (1);
quartz: 28 parts of (1);
calcite: 10 portions of
Zinc oxide: 10 parts of (A);
the reaction agent: 10 parts of (A);
talc: 5 parts of a mixture;
guizhou soil: 3 parts of a mixture;
iron oxide red: 3 parts of a mixture;
manganese powder: 3 parts of a mixture;
the metal glaze bottom glaze material comprises the following components in parts by mass:
iron powder: 35 parts of (B);
metal flux: 20 parts of (1);
albite: 30 parts of (1);
spodumene: 15 parts of (1);
quartz: 8 parts of a mixture;
guizhou soil: 2 parts of (1);
washing mud: 10 parts.
The reactant is rutile titanium dioxide.
The preparation method of the double-layer glaze combining the reaction glaze and the metal glaze comprises the following steps:
s1: respectively preparing surface glaze slurry and bottom glaze slurry; wherein the overglaze slurry is made of reactive glaze; the ground glaze slurry is made of metal ground glaze;
s2: taking a clean blank body and applying bottom glaze slurry;
s3: after the bottom glaze slurry is dried, applying surface glaze slurry;
s4: and firing the blank body coated with the overglaze slurry at 1180 ℃.
In step S1, the cover slip is prepared as follows:
preparing materials according to the components and all components of the reactive glaze;
according to the material: ball: and (3) performing wet ball milling for 13 hours with the mass ratio of water being 1:2:0.7, then sieving with a 250-mesh sieve, and modulating to 47 Baume degrees to obtain the overglaze slurry.
In step S1, the method of preparing the glaze slurry is as follows:
preparing materials according to the components of the metal glaze bottom glaze and each component;
according to the material: ball: and (3) performing wet ball milling for 12 hours when the mass ratio of water is 1:2:0.8, then sieving by a 250-mesh sieve, and modulating to 42 Baume degrees to obtain the glaze slip.
Example two
The formula components of the reaction glaze and metal glaze combined double-layer glaze of the embodiment are the same as those in the first embodiment.
The preparation method of the double-layer glaze combining the reaction glaze and the metal glaze of the embodiment comprises the following steps:
s1: respectively preparing surface glaze slurry and bottom glaze slurry; wherein the overglaze slurry is made of reactive glaze; the ground glaze slurry is made of metal ground glaze;
s2: taking a clean blank body and applying bottom glaze slurry;
s3: applying the bottom glaze slurry after the bottom glaze slurry is dried;
s4: and firing the blank body coated with the ground glaze slurry at the temperature of 1190 ℃.
In step S1, the cover slip is prepared as follows:
preparing materials according to the components and all components of the reactive glaze;
according to the material: ball: and (3) performing wet ball milling for 17 hours with the mass ratio of water being 1:2:0.7, then sieving with a 250-mesh sieve, and modulating to 48 Baume degrees to obtain the overglaze slurry.
In step S1, the method of preparing the glaze slurry is as follows:
preparing materials according to the components of the metal glaze bottom glaze and each component;
according to the material: ball: and (3) performing wet ball milling for 13 hours when the mass ratio of water is 1:2:0.8, then sieving by a 250-mesh sieve, and modulating to 47 Baume degrees to obtain the glaze slip.
EXAMPLE III
The formula components of the reaction glaze and metal glaze combined double-layer glaze of the embodiment are the same as those in the first embodiment.
The preparation method of the double-layer glaze combining the reaction glaze and the metal glaze of the embodiment comprises the following steps:
s1: respectively preparing surface glaze slurry and bottom glaze slurry; wherein the overglaze slurry is made of reactive glaze; the ground glaze slurry is made of metal ground glaze;
s2: taking a clean blank body and applying bottom glaze slurry;
s3: applying the bottom glaze slurry after the bottom glaze slurry is dried;
s4: and firing the blank body coated with the ground glaze slurry at the temperature of 1170 ℃ to obtain the finished product.
In step S1, the cover slip is prepared as follows:
preparing materials according to the components and all components of the reactive glaze;
according to the material: ball: and (3) performing wet ball milling for 16 hours with the mass ratio of water being 1:2:0.7, then sieving with a 250-mesh sieve, and modulating to 48 Baume degrees to obtain the overglaze slurry.
In step S1, the method of preparing the glaze slurry is as follows:
preparing materials according to the components of the metal glaze bottom glaze and each component;
according to the material: ball: and (3) performing wet ball milling for 14 hours when the mass ratio of water is 1:2:0.8, then sieving by a 250-mesh sieve, and modulating to 45 Baume degrees to obtain the glaze slip.
The observation shows that the product of the double-layer glaze prepared by the three embodiments has bright color and meets the design requirements.
The above embodiments are described in further detail to solve the technical problems, technical solutions and advantages of the present invention, and it should be understood that the above embodiments are only examples of the present invention and are not intended to limit the present invention, and any modifications, equivalent substitutions, improvements and the like made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (5)
1. A reaction glaze and metal glaze combined double-layer glaze is characterized in that the glaze used in the reaction glaze and metal glaze combined double-layer glaze contains a reaction glaze material and a metal glaze bottom glaze material; wherein,
the reaction glaze material comprises the following components in parts by mass:
high boron frit: 30 parts of (1);
spodumene: 30 parts of (1);
quartz: 28 parts of (1);
calcite: 10 portions of
Zinc oxide: 10 parts of (A);
the reaction agent: 10 parts of (A);
talc: 5 parts of a mixture;
guizhou soil: 3 parts of a mixture;
iron oxide red: 3 parts of a mixture;
manganese powder: 3 parts of a mixture;
the metal glaze bottom glaze material comprises the following components in parts by mass:
iron powder: 35 parts of (B);
metal flux: 20 parts of (1);
albite: 30 parts of (1);
spodumene: 15 parts of (1);
quartz: 8 parts of a mixture;
guizhou soil: 2 parts of (1);
washing mud: 10 parts.
2. The reactive glaze-metal glaze combined double-layer glaze according to claim 1, wherein: the reactant is rutile titanium dioxide.
3. A process for the preparation of a double-layer glaze of the reactive glaze according to claim 1 or 2 in combination with a metallic glaze, characterized in that it comprises the steps of:
s1: respectively preparing surface glaze slurry and bottom glaze slurry; wherein the overglaze slurry is made of reactive glaze; the ground glaze slurry is made of metal ground glaze;
s2: taking a clean blank body and applying bottom glaze slurry;
s3: after the bottom glaze slurry is dried, applying surface glaze slurry;
s4: and firing the blank body coated with the overglaze slurry at 1170-1200 ℃.
4. The production method according to claim 3, characterized in that: in step S1, the cover slip is prepared as follows:
preparing materials according to the components and all components of the reactive glaze;
according to the material: ball: and (3) performing wet ball milling for 12-18 hours with the mass ratio of water being 1:2:0.7, then sieving with a 250-mesh sieve, and modulating to 47-49 Baume degrees to obtain the surface glaze slurry.
5. The production method according to claim 3, characterized in that: in step S1, the method of preparing the glaze slurry is as follows:
preparing materials according to the components of the metal glaze bottom glaze and each component;
according to the material: ball: and (3) performing wet ball milling for 12-15 hours with the mass ratio of water being 1:2:0.8, then sieving with a 250-mesh sieve, and modulating to 42-47 Baume degrees to obtain the final glaze slurry.
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Cited By (9)
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CN108975699A (en) * | 2018-08-17 | 2018-12-11 | 湖南德兴瓷业有限公司 | Furnace transmutation glaze and preparation method thereof |
CN109133647A (en) * | 2018-09-30 | 2019-01-04 | 湖南益嘉瓷业有限公司 | Starry sky reacts blue glaze and preparation method thereof |
CN110790506A (en) * | 2019-12-18 | 2020-02-14 | 湖南华联瓷业股份有限公司 | Granular double-layer reaction glaze and preparation method thereof |
CN111170635A (en) * | 2020-01-14 | 2020-05-19 | 湖南泰鑫瓷业有限公司 | Matt reaction glaze with metallic luster and preparation method thereof |
CN111233330A (en) * | 2020-02-21 | 2020-06-05 | 醴陵嘉诚陶瓷有限公司 | Corrosion glaze and preparation method thereof |
CN111453992A (en) * | 2020-03-18 | 2020-07-28 | 湖南陶润会文化传播有限公司 | Refractory mortar titanium dioxide reaction glaze and preparation method thereof |
CN113429221A (en) * | 2021-07-28 | 2021-09-24 | 广东中印陶瓷科技有限公司 | Antibacterial wear-resistant glaze and preparation method thereof |
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CN104016722A (en) * | 2014-05-13 | 2014-09-03 | 醴陵陶润实业发展有限公司 | Reactive glaze with embossment effect and preparation method thereof |
CN105753515A (en) * | 2016-04-01 | 2016-07-13 | 江苏高淳陶瓷股份有限公司 | Preparation method of speckled glaze |
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