CN108314321A - The double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze - Google Patents
The double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze Download PDFInfo
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- CN108314321A CN108314321A CN201810158027.1A CN201810158027A CN108314321A CN 108314321 A CN108314321 A CN 108314321A CN 201810158027 A CN201810158027 A CN 201810158027A CN 108314321 A CN108314321 A CN 108314321A
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- glaze
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- metal
- coat enamel
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/18—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing free metals
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Structural Engineering (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a kind of double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze, containing reaction glaze and metal glaze ground-coat enamel material in glaze used in the double-deck glaze that reaction glaze is combined with metal glaze；Wherein, the component and each component mass parts that the reaction glaze contains are as follows：High boron frit：30 parts；Spodumene：30 parts；Quartz：28 parts；Calcite：10 parts；Zinc oxide：10 parts；Reactant：10 parts；Talcum：5 parts；Guizhou clay：3 parts；Iron oxide red：3 parts；Manganese powder：3 parts；The component and each component mass parts that the metal glaze ground-coat enamel material contains are as follows：Iron powder：35 parts；Metal flux：20 parts；Albite：30 parts；Spodumene：15 parts；Quartz：8 parts；Guizhou clay：2 parts；Wash mud：10 parts.The glaze of the present invention does not contain lead, and more environmentally friendly, color is gorgeous, deep to be liked by client.
Description
Technical field
The present invention relates to a kind of double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze.
Background technology
Currently, the dish class product of the prior art, whole body color is relatively simple, with people's living standard and to living
The raising of environmental requirement has higher finishing requirements to the glaze of dish class product, due to metal decorative material have it is graceful,
Luxurious artistic effect, therefore the glaze with metallic luster is becoming increasingly popular.The making side of metal-lustrous glaze is realized at present
There are three types of methods：1 directly sputters molten metal coating on green body；2. being applied on product glaze and containing metal or metallic compound powder
The coating at end forms metallization decorative layer by reductive heat treatment；3. preparing the glaze point of specific composition, by firing, color is generated
The imitative metal-lustrous glaze of the appearances metalloid gloss such as reconciliation gloss.More demanding and trimming cost of preceding two technologies to equipment
It is high：The third method is by preparing glaze component, under the calcining system for not changing existing tunnel kiln, directly forms metallization
The glaze of effect.Current this glaze is only applied in Wall or floor tile, was seen having not yet in dish class product scope and be criticized
Amount production；Similar research is all less desirable, and the problem of being primarily present is：1. the metal effect of glaze is not especially outstanding；
2. the wearability and corrosion resistance of metal glaze are unqualified；3. lead will be used by generally doing this glaze, cause glaze lead content super
Mark, when use, influence whether the health of human body；4. the pin hole of glaze, pinhole defect are more.
Invention content
The technical problem to be solved by the present invention is to overcome the deficiencies of existing technologies, a kind of reaction glaze and metal glaze knot are provided
The double-deck glaze of conjunction, its glaze do not contain lead, and more environmentally friendly, color is gorgeous, deep to be liked by client.
In order to solve the above-mentioned technical problem, the technical scheme is that：A kind of bilayer that reaction glaze is combined with metal glaze
Glaze contains reaction glaze and metal glaze ground-coat enamel material in glaze used in it；Wherein,
The component and each component mass parts that the reaction glaze contains are as follows：
High boron frit：30 parts；
Spodumene：30 parts；
Quartz：28 parts；
Calcite：10 parts
Zinc oxide：10 parts；
Reactant：10 parts；
Talcum：5 parts；
Guizhou clay：3 parts；
Iron oxide red：3 parts；
Manganese powder：3 parts；
The component and each component mass parts that the metal glaze ground-coat enamel material contains are as follows：
Iron powder：35 parts；
Metal flux：20 parts；
Albite：30 parts；
Spodumene：15 parts；
Quartz：8 parts；
Guizhou clay：2 parts；
Wash mud：10 parts.
Further, the reactant is rutile type titanium white.
The present invention also provides a kind of preparation method of the double-deck glaze that reaction glaze is combined with metal glaze, the step of method in contain
Have：
S1：Overglaze slurry and ground-coat enamel slurry are prepared respectively；Wherein, overglaze slurry is made of reaction glaze；Ground-coat enamel is starched by metal
Glaze ground-coat enamel material is made；
S2：Clean green body is taken to apply ground-coat enamel slurry；
S3：Overglaze slurry is applied again after ground-coat enamel slurry is dry；
S4：The green body that first-class overglaze is starched is burnt under 1170 DEG C~1200 DEG C of temperature environment.
A kind of preparation method of overglaze slurry is further provided, in step sl, the preparation method of overglaze slurry is as follows：
According to the component and each component stock of reaction glaze；
By material：Ball：Mass ratio=1 of water:2:0.7, wet ball grinding 12~18 hours, then cross 250 mesh sieve, re-modulation at
47~49 Baume degrees obtain overglaze slurry.
A kind of preparation method of ground-coat enamel slurry is further provided, in step sl, the preparation method of ground-coat enamel slurry is as follows：
It stocks up according to the component and each component of metal glaze ground-coat enamel material；
By material：Ball：Mass ratio=1 of water:2:0.8, wet ball grinding 12~15 hours, then cross 250 mesh sieve, re-modulation at
42~47 Baume degrees obtain ground-coat enamel slurry.
After using above-mentioned technical proposal, the metal glaze ground-coat enamel material that the present invention uses is more environmentally friendly for unleaded metal glaze, extensively
It is general to be adapted to household china production, and firing temperature is lower than conventional metals glaze temperature, reaction glaze is that titanium tying is brilliant so that system
Standby obtained glaze face color is gorgeous, deep to be liked by client.
Specific implementation mode
In order that the present invention can be more clearly and readily understood, below according to specific embodiment, to the present invention make into
One step is described in detail.
Embodiment one
A kind of double-deck glaze for being combined with metal glaze of reaction glaze contains in glaze used in it and reacts glaze and metal
Glaze ground-coat enamel material；Wherein,
The component and each component mass parts that the reaction glaze contains are as follows：
High boron frit：30 parts；
Spodumene：30 parts；
Quartz：28 parts；
Calcite：10 parts
Zinc oxide：10 parts；
Reactant：10 parts；
Talcum：5 parts；
Guizhou clay：3 parts；
Iron oxide red：3 parts；
Manganese powder：3 parts；
The component and each component mass parts that the metal glaze ground-coat enamel material contains are as follows：
Iron powder：35 parts；
Metal flux：20 parts；
Albite：30 parts；
Spodumene：15 parts；
Quartz：8 parts；
Guizhou clay：2 parts；
Wash mud：10 parts.
The reactant is rutile type titanium white.
Contain in the step of preparation method for the double-deck glaze that the reaction glaze is combined with metal glaze, method：
S1：Overglaze slurry and ground-coat enamel slurry are prepared respectively；Wherein, overglaze slurry is made of reaction glaze；Ground-coat enamel is starched by metal
Glaze ground-coat enamel material is made；
S2：Clean green body is taken to apply ground-coat enamel slurry；
S3：Overglaze slurry is applied again after ground-coat enamel slurry is dry；
S4：The green body that first-class overglaze is starched is burnt under 1180 DEG C of temperature environment.
In step sl, the preparation method of overglaze slurry is as follows：
According to the component and each component stock of reaction glaze；
By material：Ball：Mass ratio=1 of water:2:0.7, then wet ball grinding 13 hours crosses 250 mesh sieve, re-modulation is at 47 waves
U.S. degree obtains overglaze slurry.
In step sl, the preparation method of ground-coat enamel slurry is as follows：
It stocks up according to the component and each component of metal glaze ground-coat enamel material；
By material：Ball：Mass ratio=1 of water:2:0.8, then wet ball grinding 12 hours crosses 250 mesh sieve, re-modulation is at 42 waves
U.S. degree obtains ground-coat enamel slurry.
Embodiment two
The recipe ingredient for the double-deck glaze that the reaction glaze and metal glaze of the present embodiment combine is identical as in embodiment one.
Contain in the step of preparation method for the double-deck glaze that the reaction glaze of the present embodiment is combined with metal glaze, method：
S1：Overglaze slurry and ground-coat enamel slurry are prepared respectively；Wherein, overglaze slurry is made of reaction glaze；Ground-coat enamel is starched by metal
Glaze ground-coat enamel material is made；
S2：Clean green body is taken to apply ground-coat enamel slurry；
S3：Ground-coat enamel slurry is applied again after ground-coat enamel slurry is dry；
S4：The green body that first-class ground-coat enamel is starched is burnt under 1190 DEG C of temperature environment.
In step sl, the preparation method of overglaze slurry is as follows：
According to the component and each component stock of reaction glaze；
By material：Ball：Mass ratio=1 of water:2:0.7, then wet ball grinding 17 hours crosses 250 mesh sieve, re-modulation is at 48 waves
U.S. degree obtains overglaze slurry.
In step sl, the preparation method of ground-coat enamel slurry is as follows：
It stocks up according to the component and each component of metal glaze ground-coat enamel material；
By material：Ball：Mass ratio=1 of water:2:0.8, then wet ball grinding 13 hours crosses 250 mesh sieve, re-modulation is at 47 waves
U.S. degree obtains ground-coat enamel slurry.
Embodiment three
The recipe ingredient for the double-deck glaze that the reaction glaze and metal glaze of the present embodiment combine is identical as in embodiment one.
Contain in the step of preparation method for the double-deck glaze that the reaction glaze of the present embodiment is combined with metal glaze, method：
S1：Overglaze slurry and ground-coat enamel slurry are prepared respectively；Wherein, overglaze slurry is made of reaction glaze；Ground-coat enamel is starched by metal
Glaze ground-coat enamel material is made；
S2：Clean green body is taken to apply ground-coat enamel slurry；
S3：Ground-coat enamel slurry is applied again after ground-coat enamel slurry is dry；
S4：The green body that first-class ground-coat enamel is starched is burnt under 1170 DEG C of temperature environment.
In step sl, the preparation method of overglaze slurry is as follows：
According to the component and each component stock of reaction glaze；
By material：Ball：Mass ratio=1 of water:2:0.7, then wet ball grinding 16 hours crosses 250 mesh sieve, re-modulation is at 48 waves
U.S. degree obtains overglaze slurry.
In step sl, the preparation method of ground-coat enamel slurry is as follows：
It stocks up according to the component and each component of metal glaze ground-coat enamel material；
By material：Ball：Mass ratio=1 of water:2:0.8, then wet ball grinding 14 hours crosses 250 mesh sieve, re-modulation is at 45 waves
U.S. degree obtains ground-coat enamel slurry.
The product of the double-deck glaze prepared by three above embodiment, by it has been observed that its is bright-colored, meeting design and wanting
It asks.
Particular embodiments described above, pair present invention solves the technical problem that, technical solution and advantageous effect carry out
It is further described, it should be understood that the above is only a specific embodiment of the present invention, is not limited to this
Invention, all within the spirits and principles of the present invention, any modification, equivalent substitution, improvement and etc. done should be included in this hair
Within bright protection domain.
Claims (5)
1. a kind of double-deck glaze that reaction glaze is combined with metal glaze, it is characterised in that contain reaction glaze overglaze in glaze used in it
Material and metal glaze ground-coat enamel material；Wherein,
The component and each component mass parts that the reaction glaze contains are as follows：
High boron frit：30 parts；
Spodumene：30 parts；
Quartz：28 parts；
Calcite：10 parts
Zinc oxide：10 parts；
Reactant：10 parts；
Talcum：5 parts；
Guizhou clay：3 parts；
Iron oxide red：3 parts；
Manganese powder：3 parts；
The component and each component mass parts that the metal glaze ground-coat enamel material contains are as follows：
Iron powder：35 parts；
Metal flux：20 parts；
Albite：30 parts；
Spodumene：15 parts；
Quartz：8 parts；
Guizhou clay：2 parts；
Wash mud：10 parts.
2. the double-deck glaze that reaction glaze according to claim 1 is combined with metal glaze, it is characterised in that：The reactant is gold
Red stone-type titanium dioxide.
3. a kind of preparation method for the double-deck glaze that reaction glaze as claimed in claim 1 or 2 is combined with metal glaze, it is characterised in that
Contain in the step of method：
S1：Overglaze slurry and ground-coat enamel slurry are prepared respectively；Wherein, overglaze slurry is made of reaction glaze；Ground-coat enamel is starched by metal glaze bottom
Glaze is made；
S2：Clean green body is taken to apply ground-coat enamel slurry；
S3：Overglaze slurry is applied again after ground-coat enamel slurry is dry；
S4：The green body that first-class overglaze is starched is burnt under 1170 DEG C~1200 DEG C of temperature environment.
4. preparation method according to claim 3, it is characterised in that：In step sl, the preparation method of overglaze slurry is as follows：
According to the component and each component stock of reaction glaze；
By material：Ball：Mass ratio=1 of water:2:0.7, then wet ball grinding 12~18 hours crosses 250 mesh sieve, re-modulation at 47~
49 Baume degrees obtain overglaze slurry.
5. preparation method according to claim 3, it is characterised in that：In step sl, the preparation method of ground-coat enamel slurry is as follows：
It stocks up according to the component and each component of metal glaze ground-coat enamel material；
By material：Ball：Mass ratio=1 of water:2:0.8, then wet ball grinding 12~15 hours crosses 250 mesh sieve, re-modulation at 42~
47 Baume degrees obtain ground-coat enamel slurry.
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|---|---|---|---|
| CN201810158027.1A CN108314321A (en) | 2018-02-25 | 2018-02-25 | The double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810158027.1A CN108314321A (en) | 2018-02-25 | 2018-02-25 | The double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze |
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| CN108314321A true CN108314321A (en) | 2018-07-24 |
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| CN201810158027.1A Pending CN108314321A (en) | 2018-02-25 | 2018-02-25 | The double-deck glaze and preparation method thereof that reaction glaze is combined with metal glaze |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108975699A (en) * | 2018-08-17 | 2018-12-11 | 湖南德兴瓷业有限公司 | Furnace transmutation glaze and preparation method thereof |
| CN109133647A (en) * | 2018-09-30 | 2019-01-04 | 湖南益嘉瓷业有限公司 | Starry sky reacts blue glaze and preparation method thereof |
| CN110790506A (en) * | 2019-12-18 | 2020-02-14 | 湖南华联瓷业股份有限公司 | Granular double-layer reaction glaze and preparation method thereof |
| CN111170635A (en) * | 2020-01-14 | 2020-05-19 | 湖南泰鑫瓷业有限公司 | Matt reaction glaze with metallic luster and preparation method thereof |
| CN111233330A (en) * | 2020-02-21 | 2020-06-05 | 醴陵嘉诚陶瓷有限公司 | Corrosion glaze and preparation method thereof |
| CN111453992A (en) * | 2020-03-18 | 2020-07-28 | 湖南陶润会文化传播有限公司 | Refractory mortar titanium dioxide reaction glaze and preparation method thereof |
| CN113429221A (en) * | 2021-07-28 | 2021-09-24 | 广东中印陶瓷科技有限公司 | Antibacterial wear-resistant glaze and preparation method thereof |
| CN113547869A (en) * | 2021-08-04 | 2021-10-26 | 德化县新佳兴印刷有限公司 | In-glaze color paper and preparation method thereof |
| CN114716147A (en) * | 2022-04-21 | 2022-07-08 | 醴陵千汇实业有限公司 | Crocodile skin-imitated glaze material formed by organic matter and preparation process thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108975699A (en) * | 2018-08-17 | 2018-12-11 | 湖南德兴瓷业有限公司 | Furnace transmutation glaze and preparation method thereof |
| CN109133647A (en) * | 2018-09-30 | 2019-01-04 | 湖南益嘉瓷业有限公司 | Starry sky reacts blue glaze and preparation method thereof |
| CN110790506A (en) * | 2019-12-18 | 2020-02-14 | 湖南华联瓷业股份有限公司 | Granular double-layer reaction glaze and preparation method thereof |
| CN111170635A (en) * | 2020-01-14 | 2020-05-19 | 湖南泰鑫瓷业有限公司 | Matt reaction glaze with metallic luster and preparation method thereof |
| CN111233330A (en) * | 2020-02-21 | 2020-06-05 | 醴陵嘉诚陶瓷有限公司 | Corrosion glaze and preparation method thereof |
| CN111453992A (en) * | 2020-03-18 | 2020-07-28 | 湖南陶润会文化传播有限公司 | Refractory mortar titanium dioxide reaction glaze and preparation method thereof |
| CN113429221A (en) * | 2021-07-28 | 2021-09-24 | 广东中印陶瓷科技有限公司 | Antibacterial wear-resistant glaze and preparation method thereof |
| CN113547869A (en) * | 2021-08-04 | 2021-10-26 | 德化县新佳兴印刷有限公司 | In-glaze color paper and preparation method thereof |
| CN114716147A (en) * | 2022-04-21 | 2022-07-08 | 醴陵千汇实业有限公司 | Crocodile skin-imitated glaze material formed by organic matter and preparation process thereof |
| CN114716147B (en) * | 2022-04-21 | 2023-11-21 | 醴陵千汇实业有限公司 | Crocodile-like Pi Youliao formed by organic matters and preparation process thereof |
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Application publication date: 20180724 |