CN104609899B - There is the congregational rate of crystal and glaze of flowing diffusion effect and preparation method thereof - Google Patents
There is the congregational rate of crystal and glaze of flowing diffusion effect and preparation method thereof Download PDFInfo
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- CN104609899B CN104609899B CN201410829355.1A CN201410829355A CN104609899B CN 104609899 B CN104609899 B CN 104609899B CN 201410829355 A CN201410829355 A CN 201410829355A CN 104609899 B CN104609899 B CN 104609899B
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- 230000000694 effects Effects 0.000 title claims abstract description 25
- 238000009792 diffusion process Methods 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 210000003298 Dental Enamel Anatomy 0.000 claims abstract description 61
- XLOMVQKBTHCTTD-UHFFFAOYSA-N zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 24
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L Calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims abstract description 12
- 229910052925 anhydrite Inorganic materials 0.000 claims abstract description 12
- 229910052904 quartz Inorganic materials 0.000 claims abstract description 12
- 239000010453 quartz Substances 0.000 claims abstract description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000011787 zinc oxide Substances 0.000 claims abstract description 12
- PZZYQPZGQPZBDN-UHFFFAOYSA-N Aluminium silicate Chemical compound O=[Al]O[Si](=O)O[Al]=O PZZYQPZGQPZBDN-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 6
- OGIDPMRJRNCKJF-UHFFFAOYSA-N TiO Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 6
- QORWJWZARLRLPR-UHFFFAOYSA-H Tricalcium phosphate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims abstract description 6
- GFQYVLUOOAAOGM-UHFFFAOYSA-N Zirconium(IV) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 claims abstract description 6
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 6
- 239000010459 dolomite Substances 0.000 claims abstract description 6
- 229910000514 dolomite Inorganic materials 0.000 claims abstract description 6
- 229910000460 iron oxide Inorganic materials 0.000 claims abstract description 6
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910001929 titanium oxide Inorganic materials 0.000 claims abstract description 6
- 239000010456 wollastonite Substances 0.000 claims abstract description 6
- 229910052882 wollastonite Inorganic materials 0.000 claims abstract description 6
- 239000002002 slurry Substances 0.000 claims description 20
- 238000000498 ball milling Methods 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 10
- 239000000758 substrate Substances 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 5
- 230000001590 oxidative Effects 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 239000003973 paint Substances 0.000 abstract description 17
- 239000000835 fiber Substances 0.000 abstract description 5
- 241000233855 Orchidaceae Species 0.000 abstract description 3
- 238000009825 accumulation Methods 0.000 abstract description 3
- 238000007665 sagging Methods 0.000 abstract description 3
- 229910052573 porcelain Inorganic materials 0.000 description 3
- 206010039897 Sedation Diseases 0.000 description 2
- 230000003796 beauty Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000010304 firing Methods 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 210000000697 sensory organs Anatomy 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Abstract
The invention discloses glaze of a kind of congregational rate with crystal and flowing diffusion effect and preparation method thereof, the glaze of the congregational rate and flowing diffusion effect with crystal includes ground-coat enamel and cover-coat enamel, and component and each component mass parts of described ground-coat enamel are as follows: Anhydrite: 25 parts～35 parts；Quartz: 25 parts～28 parts；Bone ash: 10 parts～15 parts；Kaolin: 3 parts～5 parts；Zinc oxide: 5 parts～8 parts；Titanium oxide: 3 parts～5 parts；Zirconium orthosilicate.: 8 parts～10 parts；Dolomite: 7 parts～11 parts；Wollastonite: 6 parts～8 parts；Iron oxide red 12 parts～18 parts；Component and each component mass parts of described cover-coat enamel are as follows: Anhydrite: 23 parts～25 parts；Quartz: 12 parts～15 parts；Calcite: 10 parts～15 parts；6 parts～8 parts of mud is washed in Yichuan；Zinc oxide: 12 parts～15 parts；Rutile 8 parts～13 parts.The present invention has the brilliant flower of crystal accumulation, has again the effect of sagging and diffusion so that whole glaze paint palm fibre, red, and orchid is trichroism alternately, magnificent mansion.
Description
Technical field
The present invention relates to glaze of a kind of congregational rate with crystal and flowing diffusion effect and preparation method thereof.
Background technology
At present, in ceramic industry, the allotment that the moulding of porcelain base is the base glaze of quality product makes porcelain more dazzling brilliant, the porcelain base of same moulding, often because glaze paint is different, and make the vision of consumer produce different impacts, and the brilliant flower of the existing crystal accumulation of glaze paint, there is again the effect of sagging and diffusion, make whole glaze paint palm fibre, red, orchid is trichroism alternately, magnificent mansion.Wherein within mobility, glaze is main, and collar extension limit is auxiliary.Outer glaze is mainly with the master that is collected as of crystal, the inside and outside sharp contrast of formation so that inside and outside sense organ contrast is big.The product produced is not complicated on producing but make sense organ more complicates, be favorably improved the class of product so that in the competition industry of reaction glaze, there is competitiveness more.
Summary of the invention
The technical problem to be solved is to overcome the deficiencies in the prior art, it is provided that the glaze of a kind of congregational rate with crystal and flowing diffusion effect, and it has the brilliant flower of crystal accumulation, there is again the effect of sagging and diffusion so that whole glaze paint palm fibre, red, orchid is trichroism alternately, magnificent mansion.
In order to solve above-mentioned technical problem, the technical scheme is that the glaze of a kind of congregational rate with crystal and flowing diffusion effect, it includes ground-coat enamel and cover-coat enamel, and component and each component mass parts of described ground-coat enamel are as follows: Anhydrite: 25 parts～35 parts；Quartz: 25 parts～28 parts；Bone ash: 10 parts～15 parts；Kaolin: 3 parts～5 parts；Zinc oxide: 5 parts～8 parts；Titanium oxide: 3 parts～5 parts；Zirconium orthosilicate.: 8 parts～10 parts；Dolomite: 7 parts～11 parts；Wollastonite: 6 parts～8 parts；Iron oxide red 12 parts～18 parts；Component and each component mass parts of described cover-coat enamel are as follows: Anhydrite: 23 parts～25 parts；Quartz: 12 parts～15 parts；Calcite: 10 parts～15 parts；6 parts～8 parts of mud is washed in Yichuan；Zinc oxide: 12 parts～15 parts；Rutile 8 parts～13 parts.
The preparation method that present invention also offers a kind of congregational rate with crystal and the glaze of flowing diffusion effect, the step of the method is as follows:
A) get the raw materials ready according to each component and each component mass parts:
B) ground-coat enamel presses ground-coat enamel material: ball: water=1:1.5:0.55, wet ball grinding 11～13 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the ground-coat enamel slurry of furnishing 50～65 Baume degrees, take the bright and clean base substrate of appearance and immerse this ground-coat enamel slurry, stand-by after drying；
C) glaze material pressed by cover-coat enamel: ball: water=1:1.6:0.5, wet ball grinding 11～13 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the cover-coat enamel slurry of furnishing 50～60 Baume degrees, the base substrate of upper base glaze slip is sprayed this cover-coat enamel slurry, under the oxidizing atmosphere of 1280～1300 DEG C, fires finished product.
After have employed technique scheme, the gathering making crystal is made more stable with flowing diffusion glaze effect by adopting new technology, by double-deck reaction effect, glaze paint is made to present the congregational rate of crystal, simultaneously plus flowing diffusion effect, the glaze paint making dullness is more lively, glaze paint is made to seem more magnificent mansion, make glaze paint colorful, feel to people, both complicated good-looking, color aspect is due to palm fibre, red, blue collocation display, it is made more to have figure beauty, and be not incubated in the shuttle kiln of 1280～1300 DEG C and to burn till, make glaze paint novel, and firing range is wide, glaze paint is attractive in appearance, do things creatively, it is well received by consumers.
Detailed description of the invention
Being clearly understood to make present disclosure be easier to, below according to specific embodiment, the present invention is further detailed explanation.
Embodiment one
The glaze of a kind of congregational rate with crystal and flowing diffusion effect, including ground-coat enamel and cover-coat enamel, component and each component mass parts of described ground-coat enamel are as follows: Anhydrite: 27 parts；Quartz: 28 parts；Bone ash: 12 parts；Kaolin: 5 parts；Zinc oxide: 8 parts；Titanium oxide: 5 parts；Zirconium orthosilicate.: 10 parts；Dolomite: 11 parts；Wollastonite: 6 parts；Iron oxide red 15 parts；Component and each component mass parts of described cover-coat enamel are as follows: Anhydrite: 25 parts；Quartz: 15 parts；Calcite: 13 parts；8 parts of mud is washed in Yichuan；Zinc oxide: 15 parts；Rutile 10 parts.
It is as follows with the step of the preparation method of the glaze of flowing diffusion effect that this has the congregational rate of crystal:
A) get the raw materials ready according to each component and each component mass parts:
B) ground-coat enamel presses ground-coat enamel material: ball: water=1:1.5:0.55, wet ball grinding 12 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the ground-coat enamel slurry of furnishing 50～65 Baume degrees, take the bright and clean base substrate of appearance and immerse this ground-coat enamel slurry, stand-by after drying；
C) glaze material pressed by cover-coat enamel: ball: water=1:1.6:0.5, wet ball grinding 13 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the cover-coat enamel slurry of furnishing 50～60 Baume degrees, the base substrate of upper base glaze slip is sprayed this cover-coat enamel slurry, under the oxidizing atmosphere of 1280～1300 DEG C, fires finished product.
Embodiment two
The glaze of a kind of congregational rate with crystal and flowing diffusion effect, including ground-coat enamel and cover-coat enamel, component and each component mass parts of described ground-coat enamel are as follows: Anhydrite: 35 parts；Quartz: 25 parts；Bone ash: 15 parts；Kaolin: 3 parts；Zinc oxide: 8 parts；Titanium oxide: 5 parts；Zirconium orthosilicate.: 10 parts；Dolomite: 8 parts；Wollastonite: 7 parts；Iron oxide red 12 parts；Component and each component mass parts of described cover-coat enamel are as follows: Anhydrite: 25 parts；Quartz: 15 parts；Calcite: 15 parts；8 parts of mud is washed in Yichuan；Zinc oxide: 15 parts；Rutile 13 parts.
It is as follows with the step of the preparation method of the glaze of flowing diffusion effect that this has the congregational rate of crystal:
A) get the raw materials ready according to each component and each component mass parts:
B) ground-coat enamel presses ground-coat enamel material: ball: water=1:1.5:0.55, wet ball grinding 12 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the ground-coat enamel slurry of furnishing 50～65 Baume degrees, take the bright and clean base substrate of appearance and immerse this ground-coat enamel slurry, stand-by after drying；
C) glaze material pressed by cover-coat enamel: ball: water=1:1.5:0.5, wet ball grinding 13 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the cover-coat enamel slurry of furnishing 50～60 Baume degrees, the base substrate of upper base glaze slip is sprayed this cover-coat enamel slurry, under the oxidizing atmosphere of 1280～1300 DEG C, fires finished product.
Embodiment three
The glaze of a kind of congregational rate with crystal and flowing diffusion effect, including ground-coat enamel and cover-coat enamel, component and each component mass parts of described ground-coat enamel are as follows: Anhydrite: 30 parts；Quartz: 25 parts；Bone ash: 15 parts；Kaolin: 5 parts；Zinc oxide: 8 parts；Titanium oxide: 3 parts；Zirconium orthosilicate.: 10 parts；Dolomite: 11 parts；Wollastonite: 6 parts；Iron oxide red 18 parts；Component and each component mass parts of described cover-coat enamel are as follows: Anhydrite: 25 parts；Quartz: 13 parts；Calcite: 13 parts；8 parts of mud is washed in Yichuan；Zinc oxide: 15 parts；Rutile 12 parts.
It is as follows with the step of the preparation method of the glaze of flowing diffusion effect that this has the congregational rate of crystal:
A) get the raw materials ready according to each component and each component mass parts:
B) ground-coat enamel presses ground-coat enamel material: ball: water=1:1.5:0.55, wet ball grinding 12 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the ground-coat enamel slurry of furnishing 50～65 Baume degrees, take the bright and clean base substrate of appearance and immerse this ground-coat enamel slurry, stand-by after drying；
C) glaze material pressed by cover-coat enamel: ball: water=1:1.6:0.5, wet ball grinding 13 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the cover-coat enamel slurry of furnishing 50～60 Baume degrees, the base substrate of upper base glaze slip is sprayed this cover-coat enamel slurry, under the oxidizing atmosphere of 1280～1300 DEG C, fires finished product.
The glaze of the congregational rate with crystal of crystal prepared by above three embodiment and flowing diffusion effect, its glaze paint all presents the congregational rate of crystal, it is respectively provided with flowing diffusion effect simultaneously, the glaze paint making dullness is more lively, glaze paint is made to seem more magnificent mansion, make glaze paint colorful, feel to people, both complicated good-looking, color aspect is due to palm fibre, red, blue collocation display, it is made more to have figure beauty, and be not incubated in the shuttle kiln of 1280～1300 DEG C and to burn till, make glaze paint novel, and firing range is wide, glaze paint is attractive in appearance, do things creatively, it is well received by consumers.
Ground-coat enamel and cover-coat enamel in the present invention all adopt the conventional mode by each component stirring mixing.
Particular embodiments described above; to present invention solves the technical problem that, technical scheme and beneficial effect further described; it is it should be understood that; the foregoing is only specific embodiments of the invention; it is not limited to the present invention; all within the spirit and principles in the present invention, any amendment of making, equivalent replacement, improvement etc., should be included within protection scope of the present invention.
Claims (2)
1. the glaze of a congregational rate with crystal and flowing diffusion effect, it is characterised in that: it includes ground-coat enamel and cover-coat enamel, and component and each component mass parts of described ground-coat enamel are as follows: Anhydrite: 25 parts～35 parts；Quartz: 25 parts～28 parts；Bone ash: 10 parts～15 parts；Kaolin: 3 parts～5 parts；Zinc oxide: 5 parts～8 parts；Titanium oxide: 3 parts～5 parts；Zirconium orthosilicate.: 8 parts～10 parts；Dolomite: 7 parts～11 parts；Wollastonite: 6 parts～8 parts；Iron oxide red 12 parts～18 parts；Component and each component mass parts of described cover-coat enamel are as follows: Anhydrite: 23 parts～25 parts；Quartz: 12 parts～15 parts；Calcite: 10 parts～15 parts；6 parts～8 parts of mud is washed in Yichuan；Zinc oxide: 12 parts～15 parts；Rutile 8 parts～13 parts.
2. the preparation method of a congregational rate as claimed in claim 1 with crystal and the glaze of flowing diffusion effect, it is characterised in that the step of the method is as follows:
A) get the raw materials ready according to each component and each component mass parts:
B) ground-coat enamel presses ground-coat enamel material: ball: water=1:1.5:0.55, wet ball grinding 11～13 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the ground-coat enamel slurry of furnishing 50～65 Baume degrees, take the bright and clean base substrate of appearance and immerse this ground-coat enamel slurry, stand-by after drying；
C) glaze material pressed by cover-coat enamel: ball: water=1:1.6:0.5, wet ball grinding 11～13 hours, after 160 mesh sieves crossed by the glaze after ball milling, then the cover-coat enamel slurry of furnishing 50～60 Baume degrees, the base substrate of upper base glaze slip is sprayed this cover-coat enamel slurry, under the oxidizing atmosphere of 1280～1300 DEG C, fires finished product.
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| CN201410829355.1A CN104609899B (en) | 2014-12-25 | 2014-12-25 | There is the congregational rate of crystal and glaze of flowing diffusion effect and preparation method thereof |
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| CN201410829355.1A CN104609899B (en) | 2014-12-25 | 2014-12-25 | There is the congregational rate of crystal and glaze of flowing diffusion effect and preparation method thereof |
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| CN104609899B true CN104609899B (en) | 2016-06-29 |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107382068A (en) * | 2017-07-24 | 2017-11-24 | 李经文 | Mobile graphic technique glaze and preparation method thereof |
| CN109437565B (en) * | 2018-12-19 | 2021-10-01 | 禹州市正玉钧窑有限公司 | Jade and gold glaze |
| CN112174523A (en) * | 2020-09-10 | 2021-01-05 | 醴陵陶润实业发展有限公司 | Ceramic clay titanium series ultra-white crystal glaze and preparation method thereof |
| CN112125520A (en) * | 2020-09-24 | 2020-12-25 | 福建省春秋陶瓷实业有限公司 | Ceramic product with flowing pattern glaze and preparation method thereof |
| CN112226818B (en) * | 2020-11-03 | 2021-08-31 | 中国地质大学（武汉） | Method for growing nano material in feldspar crystal |
| CN112479588A (en) * | 2020-12-31 | 2021-03-12 | 湖南旭日陶瓷有限公司 | Smooth glazed tile and production process thereof |
| CN112645597B (en) * | 2021-01-05 | 2022-08-05 | 湖南华联瓷业股份有限公司 | Double-layer flow difference reaction glaze and preparation method thereof |
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| CN101306955A (en) * | 2008-07-03 | 2008-11-19 | 醴陵腾瑞工贸有限公司 | Method of making cedar glaze |
| CN101786904A (en) * | 2009-12-22 | 2010-07-28 | 咸阳陶瓷研究设计院 | Color-changing glaze for metallic luster ceramics and preparation method thereof |
| CN102633535A (en) * | 2012-03-26 | 2012-08-15 | 湖南省醴陵市楚华陶瓷实业有限公司 | Method for preparing gemstone fancy glaze |
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- 2014-12-25 CN CN201410829355.1A patent/CN104609899B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101306955A (en) * | 2008-07-03 | 2008-11-19 | 醴陵腾瑞工贸有限公司 | Method of making cedar glaze |
| CN101786904A (en) * | 2009-12-22 | 2010-07-28 | 咸阳陶瓷研究设计院 | Color-changing glaze for metallic luster ceramics and preparation method thereof |
| CN102633535A (en) * | 2012-03-26 | 2012-08-15 | 湖南省醴陵市楚华陶瓷实业有限公司 | Method for preparing gemstone fancy glaze |
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