CN108309866A - A kind of adult's shower cream containing licorice - Google Patents
A kind of adult's shower cream containing licorice Download PDFInfo
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- CN108309866A CN108309866A CN201810383885.6A CN201810383885A CN108309866A CN 108309866 A CN108309866 A CN 108309866A CN 201810383885 A CN201810383885 A CN 201810383885A CN 108309866 A CN108309866 A CN 108309866A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The present invention relates to bath article fields, and in particular to arrives a kind of adult's shower cream containing licorice.A kind of adult's shower cream containing licorice includes at least following components in parts by weight：7~14 parts of laureth sodium sulfovinate, 2~7 parts of betaine type amphoteric ionic surface active agent, 1~5 part of N acylsarcosines salt, 0.3~6 part of alkyl glycosides, 1~5 part of cocounut oil acid methyl single ethanol amide, 0.6~3 part of trehalose fatty acid ester, 0.1~5 part of hydrolysed corn starch, 0.5~2 part of licorice, 0.1~2 part of dipotassium glycyrrhizinate, 0.1~8 part of polyalcohol moisturizer, 0.1~0.5 part of fungicide, 0.1~2 part of viscosity modifier, 0~0.1 part of essence, 55~75 parts of purified water.
Description
Technical field
The present invention relates to bath article fields, and in particular to arrives a kind of adult's shower cream containing licorice.
Background technology
Since the environment with surrounding contacts and the sebum secretion of skin itself, the skin of people can be dirty, it is therefore desirable to pass through
Often cleaning skin.Shower cream is one of domestic bathing articles for use, by removing dirt and grease come cleaning skin.But it existing washes one's hair
Bath lotion product pursues high cleaning power and the ability of deoiling adds the ingredients such as extremely strong surfactant, the foaming agent of a large amount of alkalinity, long
Phase is using can cause the skin problems such as to have dry skin, peel, itch.Therefore, the highly desirable one kind of developing of people contains Chinese medicine
The good bath product of skin sense after low irritant, the cleaning effect of extract be good and use.
Invention content
In order to solve the above-mentioned technical problem, the first aspect of the invention provides a kind of adult containing licorice
Shower cream includes at least following components in parts by weight：7~14 parts of laureth sodium sulfovinate, betaine type amphoteric ion
2~7 parts of surfactant, 1~5 part of N- acylsarcosines salt, 0.3~6 part of alkyl glycosides, cocounut oil acid methyl single ethanol amide 1~5
Part, 0.6~3 part of trehalose fatty acid ester, 0.1~5 part of hydrolysed corn starch, 0.5~2 part of licorice, dipotassium glycyrrhizinate
0.1~2 part, 0.1~8 part of polyalcohol moisturizer, 0.1~0.5 part of fungicide, 0.1~2 part of viscosity modifier, essence 0~0.1
Part, 55~75 parts of purified water.
In a preferred embodiment, adult's shower cream containing licorice, in parts by weight, until
Include following components less：10~14 parts of laureth sodium sulfovinate, 3~5 parts of betaine type amphoteric ionic surface active agent, N-
1~3 part of acylsarcosine salt, 0.5~3 part of alkyl glycosides, 2~4 parts of cocounut oil acid methyl single ethanol amide, trehalose fatty acid ester
0.6~2.4 part, 0.6~3 part of hydrolysed corn starch, 0.5~2 part of licorice, 0.1~1 part of dipotassium glycyrrhizinate, polyalcohol
1~3 part of moisturizer, 0.1~0.3 part of fungicide, 0.1~2 part of viscosity modifier, 0~0.1 part of essence, 60~70 parts of purified water.
In a preferred embodiment, the betaine type amphoteric ionic surface active agent is selected from coco dimethyl
Glycine betaine, Cocoamidopropyl betaine, lauroylamidopropyl betaine, cocamidopropyl propyl amide hydroxyl sulphur glycine betaine, lauramide
At least one of hydroxyl sulphur glycine betaine.
In a preferred embodiment, the N- acylsarcosine salt is selected from N- sodium lauroyl sarcosines, N- bays
At least one of acylsarcosine ammonium, N- Hamposyl Cs sodium, N- myristoyl-N-methylaminoacetic acid sodium.
In a preferred embodiment, the alkyl in the alkyl glycosides contains 10~12 carbon atoms.
In a preferred embodiment, the alkyl glycosides is selected from Plantacare 818, undecyl glucoside, the moon
Osmanthus base glucoside, decyl maltoside, undecyl maltoside, lauryl maltoside any one or more of.
In a preferred embodiment, the trehalose fatty acid ester is trehalose fatty-acid monoester, is prepared
Raw material includes trehalose, the aliphatic acid containing 8~16 carbon atoms.
In a preferred embodiment, the preparation method of the licorice, at least includes the following steps：
Using Radix Glycyrrhizae as raw material, using in warm leaching, diacolation, decoction, reflux, ultrasound, microwave or super-critical fluid extraction
One or more of method extractions；Solid-liquid ratio w/v (g/mL) is 1：5~10；Extraction time is 1~3 time, and extraction time is each
0.5~2h repeatedly merges extracting solution when extraction；The solution that extraction obtains is concentrated, concentrated solution density is 20 DEG C of proportions
1.05~1.20, obtain the licorice.
In a preferred embodiment, the polyalcohol moisturizer is selected from glycerine, 1,3-BDO, 1,2- the third two
At least one of alcohol, sorbierite；The fungicide is selected from methylisothiazolinone, methylchloroisothiazandnone, benzene oxygen second
At least one of the smooth caprylate of alcohol, methyl hydroxybenzoate, sorb, Kathon CG；The viscosity-controlling agent is selected from cellulose derivative, nothing
At least one of machine salt, polyethylene glycol, acrylate copolymer, glucoside analog derivative, polyethylene glycol stearate diester.
The second aspect of the invention provides the preparation method of adult's shower cream containing licorice, until
Include the following steps less：
Purified water is added into reaction kettle, is warming up to 60~70 DEG C, laureth sodium sulfovinate, betaine type two is added
It is property ionic surface active agent, N- acylsarcosines salt, alkyl glycosides, cocounut oil acid methyl single ethanol amide, trehalose fatty acid ester, more
First alcohol moisturizer, stirs evenly, and is cooled to 45~50 DEG C, pH adjusting agent is added, pH is adjusted to 6.5~7.2, hydrolysed corn is added
Starch, licorice, dipotassium glycyrrhizinate, fungicide, viscosity modifier, essence, stir evenly, and are cooled to 40 DEG C, discharging；
The pH adjusting agent be selected from niter cake, potassium acid sulfate, acetic acid, citric acid, tartaric acid, maleic acid, clothing it is antiacid,
At least one of lactic acid, succinic acid, anisic acid.
The above-mentioned of the application and other features, aspect and advantage is more readily understood with reference to following detailed description.
The shower cream stability of the present invention is good, and irritation is low, and foaming abundancy is fine and smooth, rinses speed and clearly moistens soon, after bath
Effect is good, and various skin quality is suitble to use, and pruitus, long-time service can effectively be inhibited to have maintenance action to skin.
Specific implementation mode
The detailed description for preferred implementation method of the invention below of participating in the election of and including embodiment this hair can be more easily understood
Bright content.Unless otherwise defined, all technologies used herein and scientific terminology have common with fields of the present invention
The normally understood identical meaning of technical staff.When there is a conflict, the definition in this specification shall prevail.
As used herein term " by ... prepare " it is synonymous with "comprising".Term "comprising" used herein, " comprising ",
" having ", " containing " or its any other deformation, it is intended that cover non-exclusionism includes.For example, the combination comprising listed elements
Object, step, method, product or device are not necessarily limited to those elements, but may include not expressly listed other elements or
Such composition, step, method, product or the intrinsic element of device.
Conjunction " Consists of " excludes any element that do not point out, step or component.If in claim, this
Phrase will make claim be closed, so that it is not included the material in addition to the material of those descriptions, but relative normal
Except rule impurity.When being rather than immediately following after theme in the clause that phrase " Consists of " appears in claim main body,
It is only limited to the element described in the clause；Other elements are not excluded except the claim as a whole.
Equivalent, concentration or other values or parameter are excellent with range, preferred scope or a series of upper limit preferred values and lower limit
When the Range Representation that choosing value limits, this, which should be understood as, specifically discloses by any range limit or preferred value and any range
Any pairing of lower limit or preferred value is formed by all ranges, regardless of whether the range separately discloses.For example, when open
When range " 1 to 5 ", described range should be interpreted as including range " 1 to 4 ", " 1 to 3 ", " 1 to 2 ", " 1 to 2 and 4 to
5 ", " 1 to 3 and 5 " etc..When numberical range is described herein, unless otherwise stated, otherwise range intention includes its end
Value and all integers and score in the range.
Singulative includes that plural number discusses object, unless the context clearly dictates otherwise." optional " or it is " arbitrary
It is a kind of " refer to that the item described thereafter or event may or may not occur, and the description include situation that event occurs and
The situation that event does not occur.
Approximate term in specification and claims is used for modifying quantity, and it is specific to indicate that the present invention is not limited to this
Quantity further includes the modified part of the acceptable change without lead to related basic function close to the quantity.Phase
It answers, modifies a numerical value with " about ", " about " etc., mean that the present invention is not limited to the exact numericals.In some examples, approximate
Term likely corresponds to the precision of the instrument of measured value.In present specification and claims, range limits can be with
Combination and/or exchange, these ranges include all subranges contained therebetween if not stated otherwise.
In addition, indefinite article "an" before element of the present invention or component and "one" quantitative requirement to element or component
(i.e. occurrence number) unrestriction.Therefore "one" or "an" should be read as including one or at least one, and odd number
The element or component of form also include plural form, unless the apparent purport of the quantity refers to singulative.
" polymer " means the polymerizable compound prepared by the monomer by the identical or different type of polymerization.Generic term
" polymer " includes term " homopolymer ", " copolymer ", " terpolymer " and " copolymer ".
" copolymer " means the polymer prepared by polymerizeing at least two different monomers.Generic term " copolymer " includes
(it is general with term " terpolymer " for term " copolymer " (its generally to refer to the polymer prepared by two kinds of different monomers)
To refer to the polymer prepared by three kinds of different monomers).It also includes the polymerization manufactured by polymerization four or more monomer
Object." blend " means the polymerization that two or more polymer is formed by mixing jointly by physics or chemical method
Object.
In order to solve the above-mentioned technical problem, the first aspect of the invention provides a kind of adult containing licorice
Shower cream includes at least following components in parts by weight：7~14 parts of laureth sodium sulfovinate, betaine type amphoteric ion
2~7 parts of surfactant, 1~5 part of N- acylsarcosines salt, 0.3~6 part of alkyl glycosides, cocounut oil acid methyl single ethanol amide 1~5
Part, 0.6~3 part of trehalose fatty acid ester, 0.1~5 part of hydrolysed corn starch, 0.5~2 part of licorice, dipotassium glycyrrhizinate
0.1~2 part, 0.1~8 part of polyalcohol moisturizer, 0.1~0.5 part of fungicide, 0.1~2 part of viscosity modifier, essence 0~0.1
Part, 55~75 parts of purified water.
In a preferred embodiment, adult's shower cream containing licorice, in parts by weight, until
Include following components less：10~14 parts of laureth sodium sulfovinate, 3~5 parts of betaine type amphoteric ionic surface active agent, N-
1~3 part of acylsarcosine salt, 0.5~3 part of alkyl glycosides, 2~4 parts of cocounut oil acid methyl single ethanol amide, trehalose fatty acid ester
0.6~2.4 part, 0.6~3 part of hydrolysed corn starch, 0.5~2 part of licorice, 0.1~1 part of dipotassium glycyrrhizinate, polyalcohol
1~3 part of moisturizer, 0.1~0.3 part of fungicide, 0.1~2 part of viscosity modifier, 0~0.1 part of essence, 60~70 parts of purified water.
Laureth sodium sulfovinate
Laureth sodium sulfovinate, english abbreviation：AES, CAS：9004-82-4 is a kind of white or light yellow gel
Shape lotion or colourless or light yellow liquid.Water and alcohol can be dissolved in.There is excellent washing performance.It is also easy to produce a large amount of foams.Pairing
There is antistatic, smooth, soft effect at fiber.Belong to anion active agent.Be widely used in daily-use chemical industry, weaving, oil, leather,
The industries such as printing and dyeing.For washing, emulsifying, soak, assisting-dyeing, diffusion the effects that.There are excellent biological degradability and cryogenic property, it is living
Property object content is higher, is not influenced by the water hardness.Especially in terms of as detergent raw material, it is not only applicable to various powdery washings
Product more adapts to various detergent, such as the washing cream (agent) of various models and every purposes, detergent, dry cleaning agent, cleaning agent,
Remover, washing cream, shampoo (dew) and various shampoos etc..
Laureth sodium sulfovinate, CAS：9004-82-4 is purchased from the Shanghai bio tech ltd Hong Fan.
Betaine type amphoteric ionic surface active agent
The characteristics of zwitterionic surfactant is that toxicity is low and low irritant to skin, eyes；It is good anti-hard
It is aqueous, it can acid and alkali resistance and each metal ion species；Good biological degradability, non-toxic, low stain；Emulsifiability and dispersibility
It can be excellent；Good bactericidal properties and suppression mouldiness；As wetting agent and foaming agent, good effect can be played；With other types table
Face activity compatibility is good, has excellent synergistic effect.
In a preferred embodiment, the betaine type amphoteric ionic surface active agent is carboxy betaine type two
Property ionic surface active agent or sulfobetaine type zwitterionic surfactant.
The carboxy betaine type zwitterionic surfactant is specifiable alpha-alkyl beet alkali, N- alkyl betaines
Alkali, N- long-chain alkoxy bases glycine betaine, N- amido betaines etc..
The sulfobetaine type zwitterionic surfactant is specifiable sulfonyl alkyl glycine betaine, weight ratio
Glycine betaine etc..
In a preferred embodiment, the betaine type amphoteric ionic surface active agent is selected from coco dimethyl
Glycine betaine, Cocoamidopropyl betaine, lauroylamidopropyl betaine, cocamidopropyl propyl amide hydroxyl sulphur glycine betaine, lauramide
At least one of hydroxyl sulphur glycine betaine.
N- acylsarcosine salt
N- acylsarcosine salt is a kind of anionic amino acids surfactant, has low toxicity, low irritant, good life
The advantages that object degradability, preferable compatibility, compounds with other anion surfactants, can reduce conventional surfactant
Generated irritation simultaneously improves foaming capacity；Amide groups in its molecular structure can form special association body, have chelating
Performance and antioxygenic property, it is good to epidermal permeability, and potential irritation solute such as sodium ion can be inhibited to pass through human body skin
The infiltration of skin, therefore will not make dry skin after using.But after shower cream system is added in N- amide sarcosinates, system exists difficult
The problem of to thicken.
In a preferred embodiment, the N- acylsarcosine salt is selected from N- sodium lauroyl sarcosines, N- bays
At least one of acylsarcosine ammonium, N- Hamposyl Cs sodium, N- myristoyl-N-methylaminoacetic acid sodium.
Alkyl glycosides
Alkyl glycosides (Alkyl Polyglycoside, APG for short) is natural high surface and high biological degradability
A kind of environment-friendly type nonionic surfactant is the hemiacetal hydroxyl by glucose and fatty alcoholic extract hydroxyl group, is lost under the catalysis of acid
Remove product obtained from a molecular water.White solid powder or pale yellow oily liquid under APG room temperature, in water solubility
Greatly, it is more difficult to be dissolved in that there are commonly solvents.
APG is nontoxic, safety small to skin irritatin, and thickening, thickening, detergency are notable.With APG substitute part AES, LAS,
6501, AEO, peregal, K12, AOS prepare meal wash agent, bath foam, hair-washing preparations, hard surface cleaner, facial cleanser, washing powder etc.,
Significant effect.The detergent made of APG has good dissolubility, mildness and degreasing power, nothing small to skin irritatin
Poison and easily rinse.In addition, also having the characteristics that sterilizing, reducing stimulation, the pure white exquisiteness of foam.APG is in highly basic, strong acid
Stablize with performance in high concentration electrolyte, corrosivity is small, and is readily biodegradable, and will not cause the pollution to environment.
In a preferred embodiment, the alkyl in the alkyl glycosides contains 10~12 carbon atoms.
In a preferred embodiment, the alkyl glycosides is selected from Plantacare 818, undecyl glucoside, the moon
Osmanthus base glucoside, decyl maltoside, undecyl maltoside, lauryl maltoside any one or more of.
Cocounut oil acid methyl single ethanol amide
Cocounut oil acid methyl single ethanol amide, abbreviation CMMEA belong to alkylol amide type surfactant, are with natural materials
Raw material, performance is mild, and irritation is small, easily biological-degradable, is to substitute cocounut oil without containing diethanol amine and nitrosamine that European Union limits the use of
The optimal selection of amide DEA.It in the alcohol ether system compounded with anion, and contains alcohol ether with good thickening effect
The various liquid of component are washed in product, and thickening properties are substantially better than coconut oleoyl amine DEA.It also has superior frost resistance, product
It is more than zero degree not muddy, do not solidify, be mobility liquid, can be more rapidly soluble in table live body system, while it also can be effective
Improve the temperature tolerance of formula.And with traditional 6501 and CMEA, there is superior thickening, foaming and foam stability energy, height
Warm viscosity change is steady, and low temperature is not easily formed jelly, small by pH value variation system viscosity fluctuation.It also has good tax fat
Effect has splendid skin sense and soothing effect.Cocounut oil acid methyl single ethanol amide be widely used in liquid detergent, shampoo, hand cleanser,
The liquid such as shower cream wash product, especially suitable for being difficult to the system thickened.
The cocounut oil acid methyl single ethanol amide of the present invention is purchased from Shanghai Mai Lun daily use chemicals Co., Ltd.
Trehalose fatty acid ester
Trehalose fatty acid ester is a kind of Glycolipids Biosurfactantss, it is using trehalose as hydrophilic radical, with fat
Fat acid has the irrational surfactant of amphiphilic structure as one kind of hydrophobic grouping.It is non-compared to common ethylene oxide
Ionic surfactant has the characteristics that hypotoxicity, good biocompatibility and outstanding biological degradability.Trehalose
Aliphatic ester has multifunction surface activity, including emulsification, dispersion, solubilising, foaming, infiltration, wetting function, and it also has
Very high chemical stability can adapt to wider temperature range, pH value and salt concentration.Trehalose fatty acid ester also has very
The effects that corrosion resistance well, radiation resistance, resist drying dehydration protection is biomolecule, cell membrane, organelle and medical life
Preservation, transport and the use of Tetramune bring great convenience.
In a preferred embodiment, the trehalose fatty acid ester is trehalose fatty-acid monoester, is prepared
Raw material includes trehalose, the aliphatic acid containing 8~16 carbon atoms.
As a kind of preferred technical solution of the present invention, the preparation method of the trehalose fatty acid ester includes at least
Following steps：
20mL pyridines, 2.63mmol trehaloses, 2.87mmol aliphatic acid, 2.87mmol2- are added into dry container
(1H- benzo trisazo- L-1- yls) -1,1,3,3- tetramethylurea tetrafluoro boric acid ester leads to nitrogen protection, 72h is stirred at 40 DEG C,
Cooling is isolated and purified to obtain the trehalose fatty acid ester using silica gel column chromatography.
Anhydrous pyridine, CAS：110-86-1 is purchased from Shanghai Mike's woods biochemical technology Co., Ltd.
Trehalose, CAS：99-20-7 is purchased from Suzhou Southeast Pharmaceuticals Co., Ltd., purity 99%.
2- (1H- benzo trisazo- L-1- yls) -1,1,3,3- tetramethylurea tetrafluoro boric acid ester, abbreviation TBTU, CAS：
125700-67-6 composes the biology that shakes purchased from the Shanghai (carat Ma Er).
Trehalose fatty acid ester in the present invention is by carboxyl in the hydroxyl and aliphatic acid in trehalose, in the work of catalyst
The composite biosurfactant obtained from lower esterification.Itself and anion surfactant laureth sodium sulfovinate and N-
Acylsarcosine salt, nonionic surfactant alkyl glycosides and cocounut oil acid methyl single ethanol amide and betaine type amphoteric ion
Surfactant has excellent compatibility, can effectively enhance system stability, and can significantly reduce anion surface active
Agent is to the irritation of skin, and obtained shower cream is mild to skin, not allergy, and foaming abundancy is fine and smooth, is easy to rinse, washes rear skin
Not dry, satiny, skin sense is comfortable, salubrious, and long-time service has repair to dry skin.
Hydrolysed corn starch
INCI：Hydrolysed corn starch (Hydrolyzed Corn Starch).The hydrolysed corn starch it is main
Ingredient is maltotetraose.Maltotetraose appearance is in colourless, transparent, viscous liquid, and mouthfeel is slightly sweet, without any smell.It
Moisture retention is good, hygroscopicity is low, thickening property is strong, there is certain acidproof and heat resistance, and freezing point effect is small, easily forms the spies such as gloss epithelium
Point, therefore there is good practicability and antibacterial activity.The researcher of Japan has found that maltotetraose can be used as hair or body
The antipruritic of skin is used in cosmetics, and can be used in higher concentration.Drying the reason of allergic skin generates itch is
Gargalesthesia nerve (C nerves) is upheld so that skin sensitivity, easy itch.And the maltotetraose with optimization molecular dimension is to gargalesthesia
Nerve has good shielding action, to reduce the susceptibility of skin.
The hydrolysed corn starch is purchased from Science and Technology Ltd. of Beijing Lingbao City.
Licorice
Glycyrrhiza uralensis fisch is glycyrrhizic legume Glycyrrhiza uralensis Fisch., swollen fruit Radix
The drying root and rhizome of Glycyrrhiza inflata Bat. or glycyrrhiza glabra Glycyrrhiza glabra L..Main product in
The ground such as the Inner Mongol, Shanxi, Gansu, Xinjiang.Radix Glycyrrhizae has tonifying spleen, QI invigorating, clearing heat and detoxicating, expelling phlegm and arresting coughing, relieving spasm to stop pain, reconciliation all
The effect of medicine.For weakness of the spleen and the stomach, lassitude hypodynamia, palpitaition, shortness of breath, coughing with a lot of sputum, gastral cavity abdomen, four limbs contraction, carbuncle sore tumefacting virus,
Alleviate drug toxicity, strong.
Radix Glycyrrhizae main chemical compositions have three classes：Saponins, flavonoids and polysaccharide.Glycyrrhizin constituents are mainly a system
Row are using oleanane as the compound of structure parent nucleus, such as glycyrrhizic acid, enoxolone.Licoflavone constituents include mainly Radix Glycyrrhizae
The compounds such as glycosides, glycyrrhizin, isoliquiritin, isoliquiritigenin, these compounds are belonging respectively to flavones, flavonols, flavanone, two
The derivatives such as hydrogen flavonols, chalcone, isoflavones, isoflavanone, isoflavan.Glycyrrhizin has removing toxic substances, relieving cough and asthma work
With, anti-inflammatory and anti-allergic effects, anti-liver injury and reduce cholesterol effect.Licoflavone has antibacterial, antitumor, antioxygen
The effects that change, anti-arrhythmia, it is mainly used for pharmacy, cosmetics etc..Licorice polysaccharide has immunological regulation, antitumor, antiviral
The effects that, it is mainly used for pharmacy and food such as candy etc..
In a preferred embodiment, the preparation method of the licorice, at least includes the following steps：
Using Radix Glycyrrhizae as raw material, using in warm leaching, diacolation, decoction, reflux, ultrasound, microwave or super-critical fluid extraction
One or more of method extractions；Solid-liquid ratio w/v (g/mL) is 1：5~10；Extraction time is 1~3 time, and extraction time is each
0.5~2h repeatedly merges extracting solution when extraction；The solution that extraction obtains is concentrated, concentrated solution density is 20 DEG C of proportions
1.05~1.20, obtain the licorice.
Solvent used in licorice is prepared as any one of solvent once：Water；The mixture of first alcohol and water mixes
The content for closing methanol in object is 10~70wt%；The mixture of second alcohol and water, the content of ethyl alcohol is 10~60wt% in mixture；
The mixture of acetone and water, the content of acetone is 10~50wt% in mixture；The mixture of ammonia and water, ammonia contains in mixture
Amount is 0.1~2wt%；The mixture of ethyl alcohol and ammonium hydroxide, the content of ethyl alcohol is 10~60wt% in mixture, remaining contains for ammonium hydroxide
It measures, the content of ammonia is 0.1~2wt% in ammonium hydroxide.
The method for concentration includes but not limited to that one or more of following methods are used in combination, as normal heating is dense
Contracting, heating under reduced pressure concentration, spraying heat drying concentration etc..
Licorice of the present invention is concentrate, and organic reagent is not remained in preferred concentrate.
Licorice of the present invention can be commercial product, such as licorice root ointment, and it is 20 to be then modulated into density with water
DEG C proportion 1.05~1.20 obtains the licorice.
In a preferred embodiment, the Radix Glycyrrhizae be Radix Glycyrrhizae Glycyrrhiza uralensis Fisch.,
Any one of swollen fruit Radix Glycyrrhiza inflata Bat. or glycyrrhiza glabra Glycyrrhiza glabra L. or more
The dry root and/or stem of kind.
Dipotassium glycyrrhizinate
Dipotassium glycyrrhizinate, CAS：68039-19-0, molecular formula are C42H61KO16.It is safe and non-toxic, there is stronger health care
Effect is mainly used for cosmetic industry.Dipotassium glycyrrhizinate has high sugariness, and low calorie, foaming characteristic and haemocylolysis are very low, safe nothing
Malicious and stronger medicinal health care function.There are anti-inflammatory, antioxygen, antibacterial, treatment wound, effectively removing superoxide ion and hydroxyl free
Base, the effect for significantly inhibiting liposome peroxidation object.There is extensive compatibility in cosmetics, often shared with other activating agents,
Can accelerate skin to their absorption and synergy, can be used for it is sun-proof, brighten, improve, antipruritic and hair-growing and hair care etc..
In a preferred embodiment, the polyalcohol moisturizer is selected from glycerine, 1,3-BDO, 1,2- the third two
At least one of alcohol, sorbierite.
In a preferred embodiment, the fungicide is selected from methylisothiazolinone, methyl chloride isothiazoline
At least one of the smooth caprylate of ketone, Phenoxyethanol, methyl hydroxybenzoate, sorb, Kathon CG.
In a preferred embodiment, the viscosity-controlling agent is selected from cellulose derivative, inorganic salts, poly- second two
At least one of alcohol, acrylate copolymer, glucoside analog derivative, polyethylene glycol stearate diester.
The cellulose derivative includes hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, hydroxypropyl first
Base cellulose etc.；The inorganic salts include sodium chloride, ammonium chloride, magnesium chloride, magnesium nitrate, sodium sulphate etc.；The acrylic acid is poly-
It includes Carbopol series, C to close object10~30Alkyl acrylic cross-linked copolymer, C10~30Alkyl acrylate cross-linked copolymer etc.；
The glucoside derivative is PEG-120 methyl glucoside dioleic acid esters.
In a preferred embodiment, the viscosity-controlling agent is the mixture of polyethylene glycol and inorganic salts,
The mass ratio of middle polyethylene glycol and inorganic salts is 1~3：1.
Surfactant forms micella in aqueous solution, and the presence of electrolyte makes the association number of micella increase, leads to spherical shape
Micella is converted to rod-shaped micelle, to make the viscosity of system increase.But micellar structure can be influenced when electrolyte excess, reduce fortune
Dynamic resistance reduces system viscosity, that is, so-called " saltouing " phenomenon occurs.Therefore the control of electrolyte addition is extremely important,
And system can be made more to stablize using electrolyte and other kinds of thickener collective effect.
In a preferred embodiment, the polyethylene glycol is the polyethylene glycol -14M of DOW Chemical.
Polyethylene glycol-the 14M of DOW Chemical corresponds to the polyethylene glycol of country's 4000-8000 molecular weight.There is thickening effect.Solely
Special long-chain linear structure imparts the physical and chemical performance of polymer synthesis：Silky smooth gracefulness is left to hair or skin
Feel；The performance of the remarkable improvement wet comb of product, makes the smooth easy combing of hair；The foam density of improvement surfactant system,
Richness, stability and persistence；Improve the lubricity and liquid form product low temperature flow of product, and it is thick to help to improve product
Degree；Feel after the coating property of improvement cream and painting, sun-screening agent can be helped to form a film for sunscreen product；Packaging Bottle is helped to maintain to go out
Mouth cleaning；Nonionic is stablized in the broad range of pH2~11, with electrolyte compatibility；Low cost, GOOD TASTE.Suitable for washing
All kinds of personal care products such as shampoo, shower cream, Cleansing Foam, hair conditioner, treatment waxes, face cream, hair gel, hair gel cream, lipstick.
Essence is used to adjust the smell of shower cream, such as the fragrance of a flower, root of Aucklandia lappa Decne, fruity.
The second aspect of the invention provides the preparation method of adult's shower cream containing licorice, until
Include the following steps less：
Purified water is added into reaction kettle, is warming up to 60~70 DEG C, laureth sodium sulfovinate, betaine type two is added
It is property ionic surface active agent, N- acylsarcosines salt, alkyl glycosides, cocounut oil acid methyl single ethanol amide, trehalose fatty acid ester, more
First alcohol moisturizer, stirs evenly, and is cooled to 45~50 DEG C, pH adjusting agent is added, pH is adjusted to 6.5~7.2, hydrolysed corn is added
Starch, licorice, dipotassium glycyrrhizinate, fungicide, viscosity modifier, stir evenly, and are cooled to 40 DEG C, discharging.
In a preferred embodiment, the pH adjusting agent is selected from niter cake, potassium acid sulfate, acetic acid, lemon
Acid, tartaric acid, maleic acid, clothing be antiacid, at least one of lactic acid, succinic acid, anisic acid.
The present invention a variety of surfactants with more than using licorice, comprehensive by each component are allocated, and have reached
Moderate cleaning force, foam type and comfort, and injury of the surfactant to skin can be eliminated, and there is whitening, moisten, is anti-
Stimulation and oil-control move back redness, anti-inflammatory, promote Healing；Can effectively prevent skin it is stimulated when sensitivity inflammation phenomenon；To skin
Gargalesthesia nerve have good shielding action, to reduce the susceptibility of skin.The shower cream foaming abundancy of the present invention is fine and smooth, goes
Dirty power is moderate, non-stimulated to hair, skin, eyes, the skin smooth after washing, especially feeling cool, pleasant, there is antipruritic work(
Effect, and shower cream pH value of the present invention is close with human skin, mild pro-skin, it includes allergic skin to be suitble to various skin quality, and long
Phase using to small pox flesh, pore is coarse, coarse skin quality has improvement result.
Although the Cucumber used is substance common in shampoo, shower cream configuration process, the present invention passes through each
The synergistic effect that the combination of kind different component and its content limit, achieves and is difficult to expect effect in the prior art, simultaneously
The excellent performance of shower cream is ensured.
The present invention is specifically described below by embodiment.It is necessarily pointed out that following embodiment is only used
In the invention will be further described, it should not be understood as limiting the scope of the invention, professional and technical personnel in the field
Some the nonessential modifications and adaptations made according to the content of aforementioned present invention, still fall within protection scope of the present invention.
In addition, if without other explanations, it is raw materials used to be all commercially available.
Embodiment 1：
Embodiment 1 provides a kind of adult's shower cream containing licorice, in parts by weight, includes at least with the following group
Point：7 parts of laureth sodium sulfovinate, 2 parts of betaine type amphoteric ionic surface active agent, 1 part of N- acylsarcosines salt, alkyl sugar
0.3 part of glycosides, 1 part of cocounut oil acid methyl single ethanol amide, 0.6 part of trehalose fatty acid ester, 0.1 part of hydrolysed corn starch, Radix Glycyrrhizae carry
Take 0.5 part of object, 0.1 part of dipotassium glycyrrhizinate, 0.1 part of polyalcohol moisturizer, 0.1 part of fungicide, 0.1 part of viscosity modifier, purifying
55 parts of water.
The betaine type amphoteric ionic surface active agent is coco dimethyl betaines；The N- acylsarcosine salt
For N- sodium lauroyl sarcosines；The alkyl glycosides is Plantacare 818.
The preparation method of the trehalose sodium soap, at least includes the following steps：
20mL pyridines, 2.63mmol trehaloses, 2.87mmol aliphatic acid, 2.87mmol2- are added into dry container
(1H- benzo trisazo- L-1- yls) -1,1,3,3- tetramethylurea tetrafluoro boric acid ester leads to nitrogen protection, 72h is stirred at 40 DEG C.
After reaction, response situation is detected with thin-layered chromatography.Thin-layered chromatography condition is as follows：Lamellae is self-control silica GF254
Plate；Solvent is acetate-methanol (7：3, v/v)；Color developing agent is 10% ethanol solution of sulfuric acid.
Mixed liquor after above-mentioned reaction is isolated and purified with silica gel column chromatography.Methylene chloride-methanol is applied first
(10：1, v/v) it is eluted, and eluent is monitored with thin-layered chromatography, set and inspected under ultraviolet lamp (256nm), 2-
(1H- benzo trisazo- L-1- yls) -1,1,3,3- tetramethylurea tetrafluoro boric acid ester contains conjugation group, occurs in the UV lamp bright
Aobvious spot is eluted to the appearance of thin-layer chromatography immaculate, 2- (1H- benzo trisazo- L-1- yls) -1,1,3,3- tetramethylurea tetrafluoro
Borate is eluted completely.The polarity of aliphatic acid is strong, will be in 2- (1H- benzo trisazo- L-1- yls) -1,1,3,3- tetramethyl
Be eluted before urea tetrafluoro boric acid ester, lamellae can be soaked in bromocresol green test solution (0.1g bromocresol greens be dissolved in 500mL ethyl alcohol and
5mL0.1mol/L sodium hydroxide solutions are made) in the several seconds, observed on lamellae after taking-up whether there is or not yellow spotting, proved if without if
Aliphatic acid is all eluted.Then methylene chloride-methanol (5 is used instead：1, v/v) continue to elute, eluent is with thin-layered chromatography
It is detected (solvent：Acetate-methanol (7：3, v/v)；Color developing agent：10% ethanol solution of sulfuric acid).In the reaction can
Trehalose fatty-acid monoester and trehalose fatty acid diester are generated, but the present invention only collects the elution of trehalose fatty-acid monoester
Liquid merges the elution fractions, and amalgamation liquid is rotated at 60 DEG C removes solvent, collects dry product.
The aliphatic acid is caprylic acid；The polyalcohol moisturizer is glycerine；The fungicide is the different thiophene of methyl
Oxazoline ketone；The viscosity-controlling agent is hydroxymethyl cellulose.
The preparation method of the licorice, at least includes the following steps：
100g licorice powders are taken, add 20wt% ethyl alcohol by solid-liquid ratio 1：10、1：8 and 1：8 ultrasonic extractions 3 times, each 1h, mistake
Filter merges extracting solution, and recycling ethyl alcohol is concentrated under reduced pressure, and concentrate proportion 1.15 (20 DEG C) obtains the licorice.
The preparation method of adult's shower cream containing licorice, at least includes the following steps：
Purified water is added into reaction kettle, is warming up to 70 DEG C, be added laureth sodium sulfovinate, betaine type amphoteric from
Sub- surfactant, N- acylsarcosines salt, alkyl glycosides, cocounut oil acid methyl single ethanol amide, trehalose fatty acid ester, polyalcohol
Moisturizer stirs evenly, and is cooled to 50 DEG C, pH adjusting agent citric acid is added, pH is adjusted to 6.5~7.2, and hydrolysed corn is added and forms sediment
Powder, licorice, dipotassium glycyrrhizinate, fungicide, viscosity modifier, stir evenly, and are cooled to 40 DEG C, discharging.
Embodiment 2：
Embodiment 2 provides a kind of adult's shower cream containing licorice, in parts by weight, includes at least with the following group
Point：14 parts of laureth sodium sulfovinate, 7 parts of betaine type amphoteric ionic surface active agent, 5 parts of N- acylsarcosines salt, alkyl
6 parts of glucosides, 5 parts of cocounut oil acid methyl single ethanol amide, 3 parts of trehalose fatty acid ester, 5 parts of hydrolysed corn starch, licorice 2
Part, 2 parts of dipotassium glycyrrhizinate, 8 parts of polyalcohol moisturizer, 0.5 part of fungicide, 2 parts of viscosity modifier, 0.1 part of essence, purified water 75
Part.
The betaine type amphoteric ionic surface active agent is Cocoamidopropyl betaine；The N- acylsarcosines
Salt is N- Hamposyl L ammoniums；The alkyl glycosides is undecyl glucoside.
The preparation method is the same as that of Example 1 for the trehalose sodium soap.
The aliphatic acid is lauric acid；The polyalcohol moisturizer is 1,3 butylene glycol；The fungicide is first
Base chloroisothiazole quinoline ketone；The viscosity-controlling agent is the polyethylene glycol -14M of DOW Chemical.
The preparation method is the same as that of Example 1 for the licorice.
The preparation method is the same as that of Example 1 for adult's shower cream containing licorice.
Embodiment 3：
Embodiment 3 provides a kind of adult's shower cream containing licorice, in parts by weight, includes at least with the following group
Point：10 parts of laureth sodium sulfovinate, 3 parts of betaine type amphoteric ionic surface active agent, 3 parts of N- acylsarcosines salt, alkyl
0.5 part of glucosides, 2 parts of cocounut oil acid methyl single ethanol amide, 2.4 parts of trehalose fatty acid ester, 0.6 part of hydrolysed corn starch, Radix Glycyrrhizae
0.5 part of extract, 0.1 part of dipotassium glycyrrhizinate, 3 parts of polyalcohol moisturizer, 0.1 part of fungicide, 0.1 part of viscosity modifier, essence
0.1 part, 70 parts of purified water.
The betaine type amphoteric ionic surface active agent is lauroylamidopropyl betaine；The N- acylsarcosines
Salt is N- Hamposyl C sodium；The alkyl glycosides is lauryl glucoside.
The preparation method is the same as that of Example 1 for the trehalose sodium soap.
The aliphatic acid is lauric acid；The polyalcohol moisturizer is 1,2- propylene glycol；The fungicide is benzene
Oxyethanol；The viscosity-controlling agent is PEG-120 methyl glucoside dioleic acid esters.
The preparation method is the same as that of Example 1 for the licorice.
The preparation method is the same as that of Example 1 for adult's shower cream containing licorice.
Embodiment 4：
Embodiment 4 provides a kind of adult's shower cream containing licorice, in parts by weight, includes at least with the following group
Point：12 parts of laureth sodium sulfovinate, 4 parts of betaine type amphoteric ionic surface active agent, 2 parts of N- acylsarcosines salt, alkyl
1.5 parts of glucosides, 3.5 parts of cocounut oil acid methyl single ethanol amide, 2 parts of trehalose fatty acid ester, 1.5 parts of hydrolysed corn starch, Radix Glycyrrhizae
2 parts of extract, 0.6 part of dipotassium glycyrrhizinate, 3 parts of polyalcohol moisturizer, 0.1 part of fungicide, 1.4 parts of viscosity modifier, essence 0.1
Part, 65 parts of purified water.
The betaine type amphoteric ionic surface active agent is cocamidopropyl propyl amide hydroxyl sulphur glycine betaine；The N- acyl fleshes
Propylhomoserin salt is N- myristoyl-N-methylaminoacetic acid sodium；The alkyl glycosides is decyl maltoside.
The preparation method is the same as that of Example 1 for the trehalose sodium soap.
The aliphatic acid is 2- n-hexyl capric acid；The polyalcohol moisturizer is sorbierite；The fungicide is
Kathon CG；The viscosity-controlling agent is the mixture of polyethylene glycol and inorganic salts, the wherein mass ratio of polyethylene glycol and inorganic salts
It is 1：1, the polyethylene glycol is the polyethylene glycol -14M of DOW Chemical, the inorganic salts be magnesium chloride, magnesium nitrate it is mixed
Close object, mass ratio 2：1.
The preparation method is the same as that of Example 1 for the licorice.
The preparation method is the same as that of Example 1 for adult's shower cream containing licorice.
Embodiment 5：
Embodiment 5 provides a kind of adult's shower cream containing licorice, in parts by weight, includes at least with the following group
Point：12 parts of laureth sodium sulfovinate, 4 parts of betaine type amphoteric ionic surface active agent, 2 parts of N- acylsarcosines salt, alkyl
1.5 parts of glucosides, 3.5 parts of cocounut oil acid methyl single ethanol amide, 2 parts of trehalose fatty acid ester, 1.5 parts of hydrolysed corn starch, Radix Glycyrrhizae
2 parts of extract, 0.6 part of dipotassium glycyrrhizinate, 3 parts of polyalcohol moisturizer, 0.1 part of fungicide, 1.4 parts of viscosity modifier, essence 0.1
Part, 65 parts of purified water.
The betaine type amphoteric ionic surface active agent is lauramide hydroxyl sulphur glycine betaine；The N- acylsarcosines
Salt is N- myristoyl-N-methylaminoacetic acid sodium；The alkyl glycosides is lauryl maltoside.
The preparation method is the same as that of Example 1 for the trehalose sodium soap.
The aliphatic acid is 4- ethyl-hexanoics；The polyalcohol moisturizer is the mixing of glycerine and 1,3 butylene glycol
Object, mass ratio 4：1；The fungicide be methylisothiazolinone, methylchloroisothiazandnone mixture, mass ratio
It is 1：1；The viscosity-controlling agent is the mixture of polyethylene glycol and inorganic salts, the wherein mass ratio of polyethylene glycol and inorganic salts
It is 1：2.5, the polyethylene glycol is the polyethylene glycol -14M of DOW Chemical, and the inorganic salts are magnesium chloride, magnesium nitrate
Mixture, mass ratio 2：1.
The preparation method is the same as that of Example 1 for the licorice.
The preparation method is the same as that of Example 1 for adult's shower cream containing licorice.
Embodiment 6：
Embodiment 6 provides a kind of adult's shower cream containing licorice, in parts by weight, includes at least with the following group
Point：12 parts of laureth sodium sulfovinate, 4 parts of betaine type amphoteric ionic surface active agent, 2 parts of N- acylsarcosines salt, alkyl
1.5 parts of glucosides, 3.5 parts of cocounut oil acid methyl single ethanol amide, 2 parts of trehalose fatty acid ester, 1.5 parts of hydrolysed corn starch, Radix Glycyrrhizae
2 parts of extract, 0.6 part of dipotassium glycyrrhizinate, 3 parts of polyalcohol moisturizer, 0.1 part of fungicide, 1.4 parts of viscosity modifier, essence 0.1
Part, 65 parts of purified water.
The betaine type amphoteric ionic surface active agent is coco dimethyl betaines and cocamidopropyl propyl amide hydroxyl sulphur
The mixture of glycine betaine, the wherein mass ratio of coco dimethyl betaines and cocamidopropyl propyl amide hydroxyl sulphur glycine betaine are 1：2；It is described
N- acylsarcosine salt be N- sodium lauroyl sarcosines；The alkyl glycosides is Plantacare 818.
The preparation method is the same as that of Example 1 for the trehalose sodium soap.
The aliphatic acid is diamyl guanidine-acetic acid；The polyalcohol moisturizer is the mixing of glycerine and 1,3 butylene glycol
Object, mass ratio 4：1；The fungicide be methylisothiazolinone, methylchloroisothiazandnone mixture, mass ratio
It is 1：1；The viscosity-controlling agent is the mixture of polyethylene glycol and inorganic salts, the wherein mass ratio of polyethylene glycol and inorganic salts
It is 1：2.5, the polyethylene glycol is the polyethylene glycol -14M of DOW Chemical, and the inorganic salts are magnesium chloride, magnesium nitrate
Mixture, mass ratio 2：1.
The preparation method is the same as that of Example 1 for the licorice.
The preparation method is the same as that of Example 1 for adult's shower cream containing licorice.
Comparative example 1：
The specific implementation mode of comparative example 1 with embodiment 6, the difference is that, include licorice.
Comparative example 2：
The specific implementation mode of comparative example 2 with embodiment 6, the difference is that, include laureth sodium sulfovinate.
Comparative example 3：
The specific implementation mode of comparative example 3 with embodiment 6, the difference is that, include betaine type amphoteric ion table
Face activating agent.
Comparative example 4：
The specific implementation mode of comparative example 4 with embodiment 6, the difference is that, include N- acylsarcosine salt.
Comparative example 5：
The specific implementation mode of comparative example 5 with embodiment 6, the difference is that, include alkyl glycosides.
Comparative example 6：
The specific implementation mode of comparative example 6 with embodiment 6, the difference is that, include trehalose fatty acid ester.
Comparative example 7：
The specific implementation mode of comparative example 7 with embodiment 6, the difference is that, include hydrolysed corn starch.
Performance evaluation：
1. stability
Two parts of sample for measuring 100mL Examples 1 to 6 and comparative example 1~7, is respectively placed in the colourless tool plug wide-mouth of 250mL
It is a to be placed one month in the incubator of (40 ± 2) DEG C in vial, it is observed after taking out recovery to room temperature；Another is in (- 5
± 2) it is placed 1 month in refrigerator DEG C, takes out and restore to room temperature to observe its character.Observe its appearance whether have layering, precipitation,
Suspended matter or other variations, are used in combination whether smell identification sample has peculiar smell or other variations, if its appearance and smell are hair
Changing then is recorded as stablizing, and is otherwise recorded as unstable.
2. irritation
It selects rabbit as animal subject, carries out acute skin irritation experiment.Test method, judgment criteria according to《Change
Cosmetic hygienic practice》The pertinent regulations of (2015 editions) skin irritation/corrosion test carry out, and test the shower cream to skin
The irritation of skin.
3. spumescence
The bubbling ability and foam stabilizing ability of the shower cream are measured using Roche foam meter.
1 performance characterization of table is tested
4. performance
By embodiment 4~6 three kind shower cream each 100 sets and subsidiary shower cream wetting soothing effect questionnaire, issue not
With the other citizen of Age-related, skin sense after asking citizen dry to skin sense after the appearance of institute's Evaluation product, foam, flushing speed, bath and water
Etc. carry out the five-grade marking system evaluation marking, withdraw questionnaire survey after 3 months, and for statistical analysis to questionnaire, data such as following table
It is shown.
Marking explanation：1 point-bad；2 points-general；3 points-good；4 points-very well；5 points-outstanding.
| Embodiment 4 | Embodiment 5 | Embodiment 6 | |
| Appearance | 4.1 | 4.3 | 4.6 |
| Foam | 3.4 | 3.6 | 4.1 |
| Rinse speed | 3.1 | 3.6 | 3.8 |
| Skin sense after bath | 3.1 | 3.4 | 3.9 |
| Skin sense after water is dry | 3.9 | 4.0 | 4.2 |
The shower cream stability of the present invention is good, and irritation is low, and foaming abundancy is fine and smooth, rinses speed and clearly moistens soon, after bath
Effect is good, and various skin quality is suitble to use, and pruitus, long-time service can effectively be inhibited to have maintenance action to skin.
Example above-mentioned is merely illustrative, some features for explaining the method for the invention.Appended right is wanted
The range as wide as possible for being intended to require to be contemplated that is sought, and embodiments as presented herein is only according to all possible implementation
The explanation of the embodiment of the selection of the combination of example.Therefore, the purpose of applicant is that the attached claims are not illustrated this hair
The exemplary selectional restriction of bright feature.Some numberical ranges used also include sub- model in the claims
It encloses, the variation in these ranges should also be construed to be covered by the attached claims in the conceived case.
Claims (10)
1. a kind of adult's shower cream containing licorice, which is characterized in that in parts by weight, include at least following components：
7~14 parts of laureth sodium sulfovinate, 2~7 parts of betaine type amphoteric ionic surface active agent, N- acylsarcosines salt 1~5
Part, 0.3~6 part of alkyl glycosides, 1~5 part of cocounut oil acid methyl single ethanol amide, 0.6~3 part of trehalose fatty acid ester, hydrolysis are beautiful
0.1~5 part of rice starch, 0.1~2 part of dipotassium glycyrrhizinate, 0.1~8 part of polyalcohol moisturizer, kills at 0.5~2 part of licorice
0.1~0.5 part of microbial inoculum, 0.1~2 part of viscosity modifier, 0~0.1 part of essence, 55~75 parts of purified water.
2. adult's shower cream containing licorice as described in claim 1, which is characterized in that in parts by weight, at least
Including following components：10~14 parts of laureth sodium sulfovinate, 3~5 parts of betaine type amphoteric ionic surface active agent, N- acyls
1~3 part of sarcosinate, 0.5~3 part of alkyl glycosides, 2~4 parts of cocounut oil acid methyl single ethanol amide, trehalose fatty acid ester 0.6
~2.4 parts, 0.6~3 part of hydrolysed corn starch, 0.5~2 part of licorice, 0.1~1 part of dipotassium glycyrrhizinate, polyalcohol moisturizing
1~3 part of agent, 0.1~0.3 part of fungicide, 0.1~2 part of viscosity modifier, 0~0.1 part of essence, 60~70 parts of purified water.
3. adult's shower cream containing licorice as described in claim 1, which is characterized in that the betaine type two
Property ionic surface active agent be selected from coco dimethyl betaines, Cocoamidopropyl betaine, lauroylamidopropyl betaine, coconut palm
At least one of oleamide propyl hydroxyl sulphur glycine betaine, lauramide hydroxyl sulphur glycine betaine.
4. adult's shower cream containing licorice as described in claim 1, which is characterized in that the N- acylsarcosines
Salt is in N- sodium lauroyl sarcosines, N- Hamposyl Ls ammonium, N- Hamposyl Cs sodium, N- myristoyl-N-methylaminoacetic acid sodium
At least one.
5. adult's shower cream containing licorice as described in claim 1, which is characterized in that in the alkyl glycosides
Alkyl contain 10~12 carbon atoms.
6. adult's shower cream containing licorice as claimed in claim 5, which is characterized in that the alkyl glycosides choosing
From Plantacare 818, undecyl glucoside, lauryl glucoside, decyl maltoside, undecyl maltoside, lauryl
Maltoside any one or more of.
7. adult's shower cream containing licorice as described in claim 1, which is characterized in that the trehalose fat
Acid esters is trehalose fatty-acid monoester, and it includes trehalose, the aliphatic acid containing 8~16 carbon atoms to prepare raw material.
8. adult's shower cream containing licorice as described in claim 1, which is characterized in that the licorice
Preparation method, at least include the following steps：
Using Radix Glycyrrhizae as raw material, using one kind in warm leaching, diacolation, decoction, reflux, ultrasound, microwave or super-critical fluid extraction
Or several method extraction；Solid-liquid ratio w/v (g/mL) is 1：5~10；Extraction time is 1~3 time, extraction time is every time 0.5~
2h repeatedly merges extracting solution when extraction；The obtained solution of extraction is concentrated, concentrated solution density be 20 DEG C of proportions 1.05~
1.20, obtain the licorice.
9. adult's shower cream containing licorice as described in claim 1, which is characterized in that the polyalcohol moisturizing
Agent is selected from least one of glycerine, 1,3 butylene glycol, 1,2- propylene glycol, sorbierite；The fungicide is selected from the different thiophene of methyl
At least one of the smooth caprylate of oxazoline ketone, methylchloroisothiazandnone, Phenoxyethanol, methyl hydroxybenzoate, sorb, Kathon CG；It is described
Viscosity-controlling agent be selected from cellulose derivative, inorganic salts, polyethylene glycol, acrylate copolymer, glucoside analog derivative, poly-
At least one of ethylene glycol double stearate.
10. as claim 1~9 any one of them contains the preparation method of adult's shower cream of licorice, feature
It is, at least includes the following steps：
Purified water is added into reaction kettle, is warming up to 60~70 DEG C, be added laureth sodium sulfovinate, betaine type amphoteric from
Sub- surfactant, N- acylsarcosines salt, alkyl glycosides, cocounut oil acid methyl single ethanol amide, trehalose fatty acid ester, polyalcohol
Moisturizer stirs evenly, and is cooled to 45~50 DEG C, pH adjusting agent is added, pH is adjusted to 6.5~7.2, be added hydrolysed corn starch,
Licorice, dipotassium glycyrrhizinate, fungicide, viscosity modifier, essence, stir evenly, and are cooled to 40 DEG C, discharging；
It is antiacid, newborn that the pH adjusting agent is selected from niter cake, potassium acid sulfate, acetic acid, citric acid, tartaric acid, maleic acid, clothing
At least one of acid, succinic acid, anisic acid.
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| CN201810383885.6A CN108309866B (en) | 2018-04-26 | 2018-04-26 | Adult shower gel containing licorice extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109276494A (en) * | 2018-09-30 | 2019-01-29 | 江门职业技术学院 | A kind of inflammation-resisting itch-stopping shower cream and preparation method thereof |
| CN110840773A (en) * | 2019-11-04 | 2020-02-28 | 广东丽臣奥威实业有限公司 | High-viscosity high-foam surfactant composition |
| CN111297744A (en) * | 2019-12-14 | 2020-06-19 | 上海妆尚生物科技有限公司 | Efficient moisturizing mask liquid and preparation method thereof |
| EP4023209A4 (en) * | 2020-05-15 | 2023-12-27 | Guangzhou Keneng Cosmetics Research Co. Ltd | Anti-dry and anti-sensitivity composition and preparation method therefor |
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| CN102949438A (en) * | 2011-08-18 | 2013-03-06 | 上海中邦斯瑞生物药业技术有限公司 | Licorice root extract and preparation method thereof |
| CN107095816A (en) * | 2017-05-26 | 2017-08-29 | 贵州苗歌生态纳米科技有限公司 | A kind of shower cream based on plant extracts |
| CN107669565A (en) * | 2017-11-22 | 2018-02-09 | 内蒙古伊草恋生物科技有限责任公司 | A kind of natural antibacterial bath foam containing radix glycyrrhizae |
| CN107929095A (en) * | 2017-12-29 | 2018-04-20 | 广州慈康生物科技有限公司 | A kind of gentle amino acid shower cream |
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2018
- 2018-04-26 CN CN201810383885.6A patent/CN108309866B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102949438A (en) * | 2011-08-18 | 2013-03-06 | 上海中邦斯瑞生物药业技术有限公司 | Licorice root extract and preparation method thereof |
| CN107095816A (en) * | 2017-05-26 | 2017-08-29 | 贵州苗歌生态纳米科技有限公司 | A kind of shower cream based on plant extracts |
| CN107669565A (en) * | 2017-11-22 | 2018-02-09 | 内蒙古伊草恋生物科技有限责任公司 | A kind of natural antibacterial bath foam containing radix glycyrrhizae |
| CN107929095A (en) * | 2017-12-29 | 2018-04-20 | 广州慈康生物科技有限公司 | A kind of gentle amino acid shower cream |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109276494A (en) * | 2018-09-30 | 2019-01-29 | 江门职业技术学院 | A kind of inflammation-resisting itch-stopping shower cream and preparation method thereof |
| CN110840773A (en) * | 2019-11-04 | 2020-02-28 | 广东丽臣奥威实业有限公司 | High-viscosity high-foam surfactant composition |
| CN111297744A (en) * | 2019-12-14 | 2020-06-19 | 上海妆尚生物科技有限公司 | Efficient moisturizing mask liquid and preparation method thereof |
| EP4023209A4 (en) * | 2020-05-15 | 2023-12-27 | Guangzhou Keneng Cosmetics Research Co. Ltd | Anti-dry and anti-sensitivity composition and preparation method therefor |
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