CN108094823A - A kind of safe and efficient liquid-state feed mould inhibitor and preparation method thereof - Google Patents
A kind of safe and efficient liquid-state feed mould inhibitor and preparation method thereof Download PDFInfo
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- CN108094823A CN108094823A CN201810121699.5A CN201810121699A CN108094823A CN 108094823 A CN108094823 A CN 108094823A CN 201810121699 A CN201810121699 A CN 201810121699A CN 108094823 A CN108094823 A CN 108094823A
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- 239000003112 inhibitor Substances 0.000 title claims abstract description 39
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 41
- 244000037364 Cinnamomum aromaticum Species 0.000 claims abstract description 28
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 claims abstract description 28
- 241000723346 Cinnamomum camphora Species 0.000 claims abstract description 25
- 229930008380 camphor Natural products 0.000 claims abstract description 25
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims abstract description 22
- 229960000846 camphor Drugs 0.000 claims abstract description 22
- ZGXJTSGNIOSYLO-UHFFFAOYSA-N 88755TAZ87 Chemical compound NCC(=O)CCC(O)=O ZGXJTSGNIOSYLO-UHFFFAOYSA-N 0.000 claims abstract description 20
- 229960002749 aminolevulinic acid Drugs 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 20
- 239000004094 surface-active agent Substances 0.000 claims abstract description 14
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 13
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 13
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 13
- 241000207199 Citrus Species 0.000 claims abstract description 12
- 235000020971 citrus fruits Nutrition 0.000 claims abstract description 12
- LDCRTTXIJACKKU-ONEGZZNKSA-N dimethyl fumarate Chemical compound COC(=O)\C=C\C(=O)OC LDCRTTXIJACKKU-ONEGZZNKSA-N 0.000 claims abstract description 12
- 229960004419 dimethyl fumarate Drugs 0.000 claims abstract description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 107
- 235000019441 ethanol Nutrition 0.000 claims description 52
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 36
- 238000001914 filtration Methods 0.000 claims description 29
- 238000000605 extraction Methods 0.000 claims description 28
- 239000004575 stone Substances 0.000 claims description 15
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 14
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 14
- 241000723353 Chrysanthemum Species 0.000 claims description 14
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 14
- 241000305548 Pterocarya stenoptera Species 0.000 claims description 14
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 14
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 14
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 14
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims description 14
- 238000001035 drying Methods 0.000 claims description 14
- 229910052901 montmorillonite Inorganic materials 0.000 claims description 14
- 239000000661 sodium alginate Substances 0.000 claims description 14
- 235000010413 sodium alginate Nutrition 0.000 claims description 14
- 229940005550 sodium alginate Drugs 0.000 claims description 14
- 241001233914 Chelidonium majus Species 0.000 claims description 13
- 235000003956 Luffa Nutrition 0.000 claims description 13
- 244000046146 Pueraria lobata Species 0.000 claims description 13
- 235000010575 Pueraria lobata Nutrition 0.000 claims description 13
- 239000004113 Sepiolite Substances 0.000 claims description 13
- 229940068560 greater celandine Drugs 0.000 claims description 13
- 229910052624 sepiolite Inorganic materials 0.000 claims description 13
- 235000019355 sepiolite Nutrition 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 12
- 238000001354 calcination Methods 0.000 claims description 10
- 239000012467 final product Substances 0.000 claims description 10
- 238000010992 reflux Methods 0.000 claims description 10
- 238000009835 boiling Methods 0.000 claims description 9
- 239000000469 ethanolic extract Substances 0.000 claims description 9
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 7
- 230000018044 dehydration Effects 0.000 claims description 7
- 238000006297 dehydration reaction Methods 0.000 claims description 7
- 239000000284 extract Substances 0.000 claims description 7
- 238000000703 high-speed centrifugation Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 6
- -1 sucrose fatty ester Chemical class 0.000 claims description 6
- 238000010828 elution Methods 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 238000004064 recycling Methods 0.000 claims description 5
- 239000011347 resin Substances 0.000 claims description 5
- 229920005989 resin Polymers 0.000 claims description 5
- 239000000654 additive Substances 0.000 claims description 4
- 230000000996 additive effect Effects 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 4
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 4
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 3
- 241000208689 Eucommia ulmoides Species 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000012141 concentrate Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 229920001213 Polysorbate 20 Polymers 0.000 claims description 2
- 229930006000 Sucrose Natural products 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 claims description 2
- 235000010486 polyoxyethylene sorbitan monolaurate Nutrition 0.000 claims description 2
- 239000005720 sucrose Substances 0.000 claims description 2
- 244000050983 Luffa operculata Species 0.000 claims 3
- JOOXCMJARBKPKM-UHFFFAOYSA-N 4-oxopentanoic acid Chemical compound CC(=O)CCC(O)=O JOOXCMJARBKPKM-UHFFFAOYSA-N 0.000 claims 2
- NIQCNGHVCWTJSM-UHFFFAOYSA-N Dimethyl phthalate Chemical compound COC(=O)C1=CC=CC=C1C(=O)OC NIQCNGHVCWTJSM-UHFFFAOYSA-N 0.000 claims 2
- 244000241257 Cucumis melo Species 0.000 claims 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims 1
- 230000003213 activating effect Effects 0.000 claims 1
- FBSAITBEAPNWJG-UHFFFAOYSA-N dimethyl phthalate Natural products CC(=O)OC1=CC=CC=C1OC(C)=O FBSAITBEAPNWJG-UHFFFAOYSA-N 0.000 claims 1
- 229960001826 dimethylphthalate Drugs 0.000 claims 1
- 238000007710 freezing Methods 0.000 claims 1
- 230000008014 freezing Effects 0.000 claims 1
- 229940040102 levulinic acid Drugs 0.000 claims 1
- 239000002893 slag Substances 0.000 claims 1
- 238000002604 ultrasonography Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 241000219138 Luffa Species 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 5
- 230000003449 preventive effect Effects 0.000 description 5
- NAOLWIGVYRIGTP-UHFFFAOYSA-N 1,3,5-trihydroxyanthracene-9,10-dione Chemical compound C1=CC(O)=C2C(=O)C3=CC(O)=CC(O)=C3C(=O)C2=C1 NAOLWIGVYRIGTP-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 241000208688 Eucommia Species 0.000 description 3
- 241000287828 Gallus gallus Species 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 3
- 241000209140 Triticum Species 0.000 description 3
- 235000021307 Triticum Nutrition 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 235000012054 meals Nutrition 0.000 description 3
- 235000019629 palatability Nutrition 0.000 description 3
- 244000144977 poultry Species 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 241000251468 Actinopterygii Species 0.000 description 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 241000272525 Anas platyrhynchos Species 0.000 description 1
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 description 1
- 241001672694 Citrus reticulata Species 0.000 description 1
- 241000238557 Decapoda Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241001494479 Pecora Species 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- 241000219780 Pueraria Species 0.000 description 1
- 241000282898 Sus scrofa Species 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- XJMWHXZUIGHOBA-UHFFFAOYSA-N azane;propanoic acid Chemical compound N.CCC(O)=O XJMWHXZUIGHOBA-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 239000004330 calcium propionate Substances 0.000 description 1
- 235000010331 calcium propionate Nutrition 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 235000021393 food security Nutrition 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- OJURWUUOVGOHJZ-UHFFFAOYSA-N methyl 2-[(2-acetyloxyphenyl)methyl-[2-[(2-acetyloxyphenyl)methyl-(2-methoxy-2-oxoethyl)amino]ethyl]amino]acetate Chemical compound C=1C=CC=C(OC(C)=O)C=1CN(CC(=O)OC)CCN(CC(=O)OC)CC1=CC=CC=C1OC(C)=O OJURWUUOVGOHJZ-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/111—Aromatic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/142—Amino acids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/163—Sugars; Polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/28—Silicates, e.g. perlites, zeolites or bentonites
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3481—Organic compounds containing oxygen
- A23L3/3508—Organic compounds containing oxygen containing carboxyl groups
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3481—Organic compounds containing oxygen
- A23L3/3508—Organic compounds containing oxygen containing carboxyl groups
- A23L3/3517—Carboxylic acid esters
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3562—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/358—Inorganic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Animal Husbandry (AREA)
- Zoology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Nutrition Science (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Molecular Biology (AREA)
- Mycology (AREA)
- Physiology (AREA)
- Inorganic Chemistry (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of safe and efficient liquid-state feed mould inhibitors and preparation method thereof, are related to mould inhibitor technical field, which includes following raw material：Camphor extracting solution, cassia bark extracting solution, Cortex Eucommiae extracting solution, dimethyl fumarate, aminolevulinic acid (ALA), sodium benzoate, caryophyllus oil, citrus dry hide powder, slow-released carrier and surfactant.This kind of mould inhibitor passes through operation is simply mixed can prepare completion to raw material.The mould inhibitor low production cost of the present invention has the characteristics that green safe nonhazardous, anti-mold effect are good, mould proof timeliness is long, dosage is few.
Description
Technical field
The present invention relates to mould inhibitor technical fields, and in particular to a kind of safe and efficient liquid-state feed mould inhibitor and its preparation side
Method.
Background technology
Feed goes mouldy during storage in order to prevent, and mould inhibitor is generally added in feed formula.At present, raise
Expect industry mainly using using organic acid salt (such as calcium propionate), composite organic acid (such as propionic acid) and propionic acid ammonium system as
Main single or composite type mouldproof agent, anti-mold effect are different.Although existing mould inhibitor kind is more, following three are primarily present
A deficiency：First, there are certain irritation and corrosivity, be affected to the palatability of feed, especially with to feed palatability ratio
More sensitive animal (such as breast, piglet and shrimp, crab) is the most prominent；2nd, additive amount is larger, commonly reaches 1000~2000 g tons
Feed, addition cost are higher；3rd, existing mould inhibitor is mostly the drug of chemical synthesis, and medicament residue can serious threat people
Food security.
The content of the invention
For problems of the prior art, the present invention provides a kind of safe and efficient liquid-state feed mould inhibitor and its systems
Preparation Method, this kind of mould inhibitor is of low cost, has the spy that green safe nonhazardous, anti-mold effect are good, mould proof timeliness is long, dosage is few
Point.
In order to achieve the above object, the present invention is achieved through the following technical solutions：
A kind of safe and efficient liquid-state feed mould inhibitor, including following raw material by weight：Camphor extracting solution 30-40
Part, 30-40 parts of cassia bark extracting solution, 20-30 parts of Cortex Eucommiae extracting solution, 1-3 parts of dimethyl fumarate, 4-6 parts of aminolevulinic acid (ALA), benzene first
1-3 parts of sour sodium 1-2 parts, 3-5 parts of caryophyllus oil, 8-12 parts of citrus dry hide powder, 60-80 parts of slow-released carrier and surfactant；
Above-mentioned slow-released carrier is made by following steps：Take the following raw material counted in parts by weight：Medical stone 20-30
Part, 20-30 parts of sepiolite, 0-30 parts of montmorillonite 2,3-5 parts of chrysanthemum cinesariaefolium, 3-5 parts of pueraria lobata, 2-4 parts of greater celandine, Chinese wingnut leaf 1-
1-2 parts of 3 parts, 1-3 parts of luffa vine, 1-2 parts of carboxymethyl cellulose and sodium alginate；Medical stone, sepiolite and montmorillonite are mixed
Uniformly, it is 580-620 DEG C of calcining 60-80min in temperature, is air-cooled to room temperature and is placed on the hydrogen peroxide solution that concentration is 15-20%
Middle immersion 50-60min, taking-up are washed to neutrality, and drying, ground 120-140 mesh sieves obtain powder；By chrysanthemum cinesariaefolium, Pueraria lobota
Root, greater celandine, Chinese wingnut leaf and luffa vine chopping are uniformly mixed, and add in the 8-10 times of clear water boiling and extraction 50-60min measured, filtering
Afterwards, filter residue is added into the 6-8 times of clear water measured, decocts extraction 40-50min, filtering merges decoction liquor, and concentration is freeze-dried into
Powder；The powder, powder are mixed into addition carboxymethyl cellulose and sodium alginate stirs evenly, adds the 3-4 times of water measured
Ultrasonic wave disperses, afterwards high speed centrifugation, dehydration, drying.
Further, above-mentioned mould inhibitor includes following raw material by weight：35 parts of camphor extracting solution, cassia bark extraction
35 parts of object, 25 parts of eucommia ulmoides extracts, 2 parts of dimethyl fumarate, 5 parts of aminolevulinic acid (ALA), 1.5 parts of sodium benzoate, 4 parts of caryophyllus oil,
2 parts of 10 parts of citrus dry hide powder, 70 parts of slow-released carrier and surfactant.
Further, above-mentioned slow-released carrier is made by following steps：Take the following raw material counted in parts by weight：Wheat meal
25 parts of stone, 25 parts of sepiolite, 5 parts of montmorillonite 2,4 parts of chrysanthemum cinesariaefolium, 4 parts of pueraria lobata, 3 parts of greater celandine, 2 parts of Chinese wingnut leaf, luffa vine
1.5 parts of 2 parts, 1.5 parts of carboxymethyl cellulose and sodium alginate；Medical stone, sepiolite and montmorillonite are uniformly mixed, are in temperature
600 DEG C of calcining 70min are air-cooled to room temperature and are placed in the hydrogen peroxide solution that concentration is 15% and impregnate 55min, during taking-up is washed to
Property, drying, ground 130 mesh sieve obtain powder；Chrysanthemum cinesariaefolium, pueraria lobata, greater celandine, Chinese wingnut leaf and luffa vine are shredded and mixed
Uniformly, the clear water boiling and extraction 55min of 9 times of amounts is added in, after filtering, filter residue is added to the clear water of 7 times of amounts, decocts extraction
45min, filtering merge decoction liquor, and concentration is freeze-dried into powder；The powder, powder are mixed and add in carboxymethyl cellulose
It is stirred evenly with sodium alginate, the water ultrasonic wave for adding 3 times of amounts disperses, afterwards high speed centrifugation, dehydration, drying.
Further, above-mentioned camphor extracting solution is made by following steps：Camphor is taken to shred, 6-8 times of addition is measured clear
Filter residue after filtering, is added the 6-8 times of clear water measured, decocts extraction 50-60min by water boiling and extraction 50-60min, and filtering is closed
And decoction liquor, it is concentrated into the 1/2 of original volume to obtain the final product.
Further, above-mentioned cassia bark extracting solution is made by following steps：It is added in cassia bark compared with cassia bark quality 3-5
Determining alcohol again is 95% ethyl alcohol, is heated to reflux 1-2h, filters to obtain filter residue, filter residue is added in again compared with filter residue quality 3-
5 times of determining alcohol is 95% ethyl alcohol, is heated to reflux 1-2h, and filtering and impurity removing merges filtered fluid, removes ethyl alcohol, is concentrated into substance
Long-pending 1/2 to obtain the final product.
Further, above-mentioned Cortex Eucommiae extracting solution is made by following steps：It is 70% ethyl alcohol to take Cortex Eucommiae volumetric concentration
It is handled in temperature for 24 DEG C of -28 DEG C of extractions, obtains ethanol extract, then ethanol extract is crossed into AB-8 macroporous resin columns, with distillation
Water washing is transparent to efflux, then with volumetric concentration is 3-5 times of column volume of 55%-65% ethanol elutions, obtains ethanol eluate, most
Afterwards Cortex Eucommiae extracting solution is obtained with ethanol eluate recycling ethyl alcohol.
Preferably, above-mentioned surfactant uses sucrose fatty ester, glycerin monostearate or polyoxyethylene
One kind in alcohol acid anhydride monolaurate.
A kind of preparation method of above-mentioned safe and efficient liquid-state feed mould inhibitor, follows the steps below：
(1) raw material is weighed by the weight；
(2) camphor extracting solution, cassia bark extracting solution, Cortex Eucommiae extracting solution are mixed and heated to 40-50 DEG C and stirred evenly, added
Dimethyl fumarate, aminolevulinic acid (ALA), sodium benzoate, caryophyllus oil and citrus dry hide powder are uniformly mixed, and are eventually adding slow-released carrier
With surfactant mixing.
Further, additive amount of the above-mentioned mould inhibitor in feed is controlled in 300-400g/T.
The present invention has following advantageous effect：
(1) Midew preventive for feed of the invention is prepared simple, easy to use, and raw material sources are extensive, of low cost, with dosage
Less, the characteristics of anti-mold effect is good is respectively provided with the effect of mould proof, and this kind of mould inhibitor green for a variety of feeds such as herding, aquatic products
Safe and non-toxic will not cause any harmful effect and harm to raising object, feeding environment and health；
(2) Midew preventive for feed of the invention is with extracting solution and fumaric acid made from camphor, cassia bark, Cortex Eucommiae herbaceous plant
The active ingredients such as dimethyl ester, aminolevulinic acid (ALA), sodium benzoate, caryophyllus oil by reasonably assembling and groping, make it for feed
In various moulds there is good adsorptivity and sterilising, there is green safe nonhazardous, anti-mold effect is good, mould proof timeliness is long
The characteristics of, and the probability that feed deuterogenesis is gone mouldy can be improved；
(3) Midew preventive for feed physicochemical property of the invention is stablized, and shelf-life limit for length is fast using rear diffusion of reagents, palatability
It is good, stimulation will not be generated to animal intestines and stomach, it is safe, moreover it is possible to effectively to prevent the generation of germ pest in feed, improve and raise
Expect quality, the ingredients such as the camphor extracting solution contained in raw material, cassia bark extracting solution, Cortex Eucommiae extracting solution, slow-released carrier can also promote fowl
Dirty swine is long, improves poultry immunity of organisms, improves the physiological status of poultry so that poultry growth and development is fast, delivers for sale morning, carries significantly
The high economic benefit of animal husbandry and culture fishery.
Specific embodiment
The specific embodiment of the present invention is further described with reference to embodiment, following embodiment is only used for more
Technical scheme is clearly demonstrated, and is not intended to limit the protection scope of the present invention and limits the scope of the invention.
Embodiment 1
A kind of safe and efficient liquid-state feed mould inhibitor, weighs following raw material：Camphor extracting solution 30kg, cassia bark extracting solution
30kg, Cortex Eucommiae extracting solution 20kg, dimethyl fumarate 1kg, aminolevulinic acid (ALA) 4kg, sodium benzoate 1kg, caryophyllus oil 3kg, citrus
Dry hide powder 8kg, slow-released carrier 60kg and sucrose-fatty ester surfactant 1kg；
The preparation of slow-released carrier weighs following raw material：Medical stone 20kg, sepiolite 20kg, montmorillonite 2 0kg, white flower deinsectization
Chrysanthemum 3kg, pueraria lobata 3kg, greater celandine 2kg, Chinese wingnut leaf 1kg, luffa vine 1kg, carboxymethyl cellulose 1kg and sodium alginate 1kg；By wheat
Meal stone, sepiolite and montmorillonite are uniformly mixed, and are delivered in calcining furnace, are 580 DEG C of calcining 60min in temperature, are air-cooled to room temperature
It is placed in the hydrogen peroxide solution that concentration is 15% and impregnates 50min, taking-up is washed to neutrality, and drying, ground 120 mesh sieve obtain
Powder；The chopping of chrysanthemum cinesariaefolium, pueraria lobata, greater celandine, Chinese wingnut leaf and luffa vine is uniformly mixed, the clear water for adding in 8 times of amounts decocts
50min to be extracted, after filtering, filter residue is added into 6 times of clear water measured, decocts extraction 40min, filtering merges decoction liquor, concentrates,
It is freeze-dried into powder；Above-mentioned powder, powder are mixed into addition carboxymethyl cellulose and sodium alginate stirs evenly, adds 3
Times amount water ultrasonic wave disperse, after through supercentrifuge high speed centrifugation handle, dehydration, drying.
It is prepared by camphor extracting solution：60kg camphors is taken to shred, add in the clear water boiling and extraction 50min of 6 times of amounts, it, will after filtering
Filter residue adds the clear water of 6 times of amounts, decocts extraction 50min, and filtering merges decoction liquor, is concentrated into the 1/2 of original volume to obtain the final product.
It is prepared by cassia bark extracting solution：60kg cassia barks are taken, add in the ethyl alcohol for being 95% compared with the determining alcohol of 3 times of cassia bark quality,
1h is heated to reflux, filters to obtain filter residue, filter residue is added in the ethyl alcohol for being 95% compared with the determining alcohol of 3 times of filter residue quality again, is added
Heat reflux 1h, filtering and impurity removing merge filtered fluid, remove ethyl alcohol, are concentrated into the 1/2 of original volume to obtain the final product.
It is prepared by Cortex Eucommiae extracting solution：40kg Cortex Eucommiaes are taken, with volumetric concentration be 70% ethyl alcohol in temperature are that 24 DEG C of extractions are handled, are obtained
Ethanol extract, then ethanol extract is crossed into AB-8 macroporous resin columns, it is transparent then dense with volume to be washed with distilled water to efflux
It spends for 55% ethanol elution, 3 times of column volumes, obtains ethanol eluate, finally obtain Cortex Eucommiae extracting solution with ethanol eluate recycling ethyl alcohol.
A kind of preparation method of above-mentioned safe and efficient liquid-state feed mould inhibitor is：First camphor extracting solution, cassia bark are extracted
Liquid, Cortex Eucommiae extracting solution are delivered in electric stirring pot, are heated to 40 DEG C and are stirred evenly, and add dimethyl fumarate, amino fruit
Saccharic acid, sodium benzoate, caryophyllus oil and citrus dry hide powder are uniformly mixed, and are eventually adding slow-released carrier and surfactant stirring 2h,
Speed of agitator is 300r/min, and a kind of system of safe and efficient liquid-state feed mould inhibitor to the present invention is completed in pack after sealing up for safekeeping
It is standby.
Embodiment 2
A kind of safe and efficient liquid-state feed mould inhibitor, weighs following raw material：Camphor extracting solution 35kg, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract
35kg, eucommia ulmoides extracts 25kg, dimethyl fumarate 2kg, aminolevulinic acid (ALA) 5kg, sodium benzoate 1.5kg, caryophyllus oil 4kg, mandarin orange
Tangerine dry hide powder 10kg, slow-released carrier 70kg and polyoxyethylene sorbitan monolaurate surfactant 2kg；
The preparation of slow-released carrier weighs following raw material：Medical stone 25kg, sepiolite 25kg, montmorillonite 2 5kg, white flower deinsectization
Chrysanthemum 4kg, pueraria lobata 4kg, greater celandine 3kg, Chinese wingnut leaf 2kg, luffa vine 2kg, carboxymethyl cellulose 1.5kg and sodium alginate 1.5kg；
Medical stone, sepiolite and montmorillonite are uniformly mixed, are delivered in calcining furnace, is 600 DEG C of calcining 70min in temperature, is air-cooled to
Room temperature, which is placed in the hydrogen peroxide solution that concentration is 15%, impregnates 55min, and taking-up is washed to neutrality, drying, ground 130 mesh
Sieve, obtains powder；The chopping of chrysanthemum cinesariaefolium, pueraria lobata, greater celandine, Chinese wingnut leaf and luffa vine is uniformly mixed, adds in the clear water of 9 times of amounts
Extraction 55min is decocted, after filtering, filter residue is added to the clear water of 7 times of amounts, decocts extraction 45min, filtering merges decoction liquor, dense
Contracting, is freeze-dried into powder；The powder, powder are mixed into addition carboxymethyl cellulose and sodium alginate stirs evenly, then is added
Enter 3 times amount water ultrasonic waves disperse, after through supercentrifuge high speed centrifugation handle, dehydration, drying.
It is prepared by camphor extracting solution：70kg camphors is taken to shred, add in the clear water boiling and extraction 55min of 7 times of amounts, it, will after filtering
Filter residue adds the clear water of 7 times of amounts, decocts extraction 55min, and filtering merges decoction liquor, is concentrated into the 1/2 of original volume to obtain the final product.
It is prepared by cassia bark extracting solution：70kg cassia barks are taken, add in the ethyl alcohol for being 95% compared with the determining alcohol of 4 times of cassia bark quality,
1.5h is heated to reflux, filters to obtain filter residue, filter residue is added in the ethyl alcohol for being 95% compared with the determining alcohol of 4 times of filter residue quality again,
It is heated to reflux 1.5h, filtering and impurity removing merges filtered fluid, removes ethyl alcohol, is concentrated into the 1/2 of original volume to obtain the final product.
It is prepared by Cortex Eucommiae extracting solution：50kg Cortex Eucommiaes are taken, with volumetric concentration be 70% ethyl alcohol in temperature are that 26 DEG C of extractions are handled, are obtained
Ethanol extract, then ethanol extract is crossed into AB-8 macroporous resin columns, it is transparent then dense with volume to be washed with distilled water to efflux
It spends for 60% ethanol elution, 4 times of column volumes, obtains ethanol eluate, finally obtain Cortex Eucommiae extracting solution with ethanol eluate recycling ethyl alcohol.
A kind of preparation method of above-mentioned safe and efficient liquid-state feed mould inhibitor is：First camphor extracting solution, cassia bark are extracted
Liquid, Cortex Eucommiae extracting solution are delivered in electric stirring pot, are heated to 45 DEG C and are stirred evenly, and add dimethyl fumarate, amino fruit
Saccharic acid, sodium benzoate, caryophyllus oil and citrus dry hide powder are uniformly mixed, and are eventually adding slow-released carrier and surfactant stirring
A kind of safe and efficient liquid-state feed mould inhibitor to the present invention is completed in 2.5h, speed of agitator 400r/min, pack after sealing up for safekeeping
Preparation.
Embodiment 3
A kind of safe and efficient liquid-state feed mould inhibitor, weighs following raw material：Camphor extracting solution 40kg, cassia bark extracting solution
40kg, Cortex Eucommiae extracting solution 30kg, dimethyl fumarate 3kg, aminolevulinic acid (ALA) 6kg, sodium benzoate 2kg, caryophyllus oil 5kg, citrus
Dry hide powder 12kg, slow-released carrier 80kg and glycerin monostearate surfactant 3kg；
The preparation of slow-released carrier weighs following raw material：Medical stone 30kg, sepiolite -0kg, montmorillonite 30kg, white flower deinsectization
Chrysanthemum 5kg, pueraria lobata 5kg, greater celandine 4kg, Chinese wingnut leaf 3kg, luffa vine 3kg, carboxymethyl cellulose 2kg and sodium alginate 2kg；By wheat
Meal stone, sepiolite and montmorillonite are uniformly mixed, and are delivered in calcining furnace, are 620 DEG C of calcining 80min in temperature, are air-cooled to room temperature
It is placed in the hydrogen peroxide solution that concentration is 20% and impregnates 60min, taking-up is washed to neutrality, and drying, ground 140 mesh sieve obtain
Powder；The chopping of chrysanthemum cinesariaefolium, pueraria lobata, greater celandine, Chinese wingnut leaf and luffa vine is uniformly mixed, the clear water for adding in 10 times of amounts decocts
60min to be extracted, after filtering, filter residue is added into 8 times of clear water measured, decocts extraction 50min, filtering merges decoction liquor, concentrates,
It is freeze-dried into powder；Above-mentioned powder, powder are mixed into addition carboxymethyl cellulose and sodium alginate stirs evenly, adds 4
Times amount water ultrasonic wave disperse, after through supercentrifuge high speed centrifugation handle, dehydration, drying.
It is prepared by camphor extracting solution：80kg camphors is taken to shred, add in the clear water boiling and extraction 60min of 8 times of amounts, it, will after filtering
Filter residue adds the clear water of 8 times of amounts, decocts extraction 60min, and filtering merges decoction liquor, is concentrated into the 1/2 of original volume to obtain the final product.
It is prepared by cassia bark extracting solution：80kg cassia barks are taken, add in the ethyl alcohol for being 95% compared with the determining alcohol of 5 times of cassia bark quality,
2h is heated to reflux, filters to obtain filter residue, filter residue is added in the ethyl alcohol for being 95% compared with the determining alcohol of 5 times of filter residue quality again, is added
Heat reflux 2h, filtering and impurity removing merge filtered fluid, remove ethyl alcohol, are concentrated into the 1/2 of original volume to obtain the final product.
It is prepared by Cortex Eucommiae extracting solution：60kg Cortex Eucommiaes are taken, with volumetric concentration be 70% ethyl alcohol in temperature are that 28 DEG C of extractions are handled, are obtained
Ethanol extract, then ethanol extract is crossed into AB-8 macroporous resin columns, it is transparent then dense with volume to be washed with distilled water to efflux
It spends for 65% ethanol elution, 5 times of column volumes, obtains ethanol eluate, finally obtain Cortex Eucommiae extracting solution with ethanol eluate recycling ethyl alcohol.
A kind of preparation method of above-mentioned safe and efficient liquid-state feed mould inhibitor is：First camphor extracting solution, cassia bark are extracted
Liquid, Cortex Eucommiae extracting solution are delivered in electric stirring pot, are heated to 50 DEG C and are stirred evenly, and add dimethyl fumarate, amino fruit
Saccharic acid, sodium benzoate, caryophyllus oil and citrus dry hide powder are uniformly mixed, and are eventually adding slow-released carrier and surfactant stirring 3h,
Speed of agitator is 500r/min, and a kind of system of safe and efficient liquid-state feed mould inhibitor to the present invention is completed in pack after sealing up for safekeeping
It is standby.
Additive amount of the mould inhibitor of the present invention in feed is controlled (is per 1T Midew preventive for feed dosages in 300-400g/T
300-400), according to actual demand, aqueous suspension agent is made and is sprayed, wherein, the use of the following table 1 is taken in feed a part species suggestion
Amount；
Table 1
| Fish feed | Chicken class feed | Porcine feed | Duck class feed | Sheep class feed | |
| Dosage (300-400g/T) | 300 | 320 | 400 | 340 | 370 |
It goes mouldy test
Midew preventive for feed made from above-described embodiment 1-3 is respectively applied to fish feed, chicken class feed and porcine to raise
In material, reference is carried out with comparative example (not adding in mould inhibitor), observe and record feed mold situation and raises the growth feelings of object
Condition see the table below shown in 2；
Above-mentioned comparative example includes：Comparative example 1 is applied in fish feed；Comparative example 2 is applied in chicken class feed；Comparative example 3 should
Used in porcine feed.
Table 2
In above-mentioned, rate of going mouldy (%)=feeding quality of going mouldy/feed gross mass × 100%
The foregoing is only a preferred embodiment of the present invention, is not intended to limit the invention, although with reference to foregoing reality
Example is applied the present invention is described in detail, it for those skilled in the art, still can be to foregoing each implementation
Technical solution recorded in example modifies or carries out equivalent substitution to which part technical characteristic.All essences in the present invention
With within principle, any modifications, equivalent replacements and improvements are made should all be included in the protection scope of the present invention god.
Claims (9)
1. a kind of safe and efficient liquid-state feed mould inhibitor, which is characterized in that including following raw material by weight：Camphor extracts
30-40 parts of liquid, 30-40 parts of cassia bark extracting solution, 20-30 parts of Cortex Eucommiae extracting solution, 1-3 parts of dimethyl fumarate, aminolevulinic acid (ALA) 4-6
Part, 1-2 parts of sodium benzoate, 3-5 parts of caryophyllus oil, 8-12 parts of citrus dry hide powder, 60-80 parts of slow-released carrier and surfactant 1-3
Part；
The slow-released carrier is made by following steps：Take the following raw material counted in parts by weight：20-30 parts of medical stone, Hai Pao
20-30 parts of stone, 0-30 parts of montmorillonite 2,3-5 parts of chrysanthemum cinesariaefolium, 3-5 parts of pueraria lobata, 2-4 parts of greater celandine, 1-3 parts of Chinese wingnut leaf, silk
1-2 parts of 1-3 parts of melon vine, 1-2 parts of carboxymethyl cellulose and sodium alginate；Medical stone, sepiolite and montmorillonite are uniformly mixed,
Temperature is 580-620 DEG C of calcining 60-80min, is air-cooled to room temperature and is placed in the hydrogen peroxide solution that concentration is 15-20% and impregnates
50-60min, taking-up are washed to neutrality, and drying, ground 120-140 mesh sieves obtain powder；By chrysanthemum cinesariaefolium, pueraria lobata, bend in vain
Dish, Chinese wingnut leaf and luffa vine chopping are uniformly mixed, and are added in the 8-10 times of clear water boiling and extraction 50-60min measured, after filtering, will be filtered
Slag adds the 6-8 times of clear water measured, and decocts extraction 40-50min, and filtering merges decoction liquor, and concentration is freeze-dried into powder；It will
The powder, powder mixing adds in carboxymethyl cellulose and sodium alginate stirs evenly, and adds the 3-4 times of water ultrasound wavelength-division measured
It dissipates, afterwards high speed centrifugation, dehydration, drying.
2. a kind of safe and efficient liquid-state feed mould inhibitor according to claim 1, which is characterized in that including it is following by weight
The raw material of part meter：35 parts of camphor extracting solution, 35 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, 25 parts of eucommia ulmoides extracts, 2 parts of dimethyl fumarate, amino
2 parts of 5 parts of levulinic acid, 1.5 parts of sodium benzoate, 4 parts of caryophyllus oil, 10 parts of citrus dry hide powder, 70 parts of slow-released carrier and surfactant.
3. a kind of safe and efficient liquid-state feed mould inhibitor according to claim 1, which is characterized in that the slow-released carrier leads to
Following steps are crossed to be made：Take the following raw material counted in parts by weight：25 parts of medical stone, 25 parts of sepiolite, 5 parts of montmorillonite 2, white flower
4 parts of Dalmatian chrysanthemum, 4 parts of pueraria lobata, 3 parts of greater celandine, 2 parts of Chinese wingnut leaf, 2 parts of luffa vine, 1.5 parts of carboxymethyl cellulose and sodium alginate
1.5 part；Medical stone, sepiolite and montmorillonite are uniformly mixed, is 600 DEG C of calcining 70min in temperature, is air-cooled to room temperature and is placed on
Concentration is that 55min is impregnated in 15% hydrogen peroxide solution, and taking-up is washed to neutrality, and drying, ground 130 mesh sieve obtain powder；It will
Chrysanthemum cinesariaefolium, pueraria lobata, greater celandine, Chinese wingnut leaf and luffa vine chopping are uniformly mixed, and add in the clear water boiling and extraction of 9 times of amounts
Filter residue after filtering, is added the clear water of 7 times of amounts by 55min, decocts extraction 45min, and filtering merges decoction liquor, concentrates, freezing
It is dried to powder；The powder, powder are mixed into addition carboxymethyl cellulose and sodium alginate stirs evenly, adds 3 times of amounts
Water ultrasonic wave disperse, high speed centrifugation, dehydration, drying afterwards.
A kind of 4. safe and efficient liquid-state feed mould inhibitor according to claim 1, which is characterized in that the camphor extracting solution
It is made by following steps：Camphor is taken to shred, adds in the 6-8 times of clear water boiling and extraction 50-60min measured, after filtering, by filter residue again
It adds in the 6-8 times of clear water measured, decocts extraction 50-60min, filtering merges decoction liquor, is concentrated into the 1/2 of original volume to obtain the final product.
A kind of 5. safe and efficient liquid-state feed mould inhibitor according to claim 1, which is characterized in that the cassia bark extracting solution
It is made by following steps：The ethyl alcohol for being 95% compared with the determining alcohol of 3-5 times of cassia bark quality is added in cassia bark, is heated to reflux 1-
2h filters to obtain filter residue, and filter residue is added in the ethyl alcohol for being 95% compared with the determining alcohol of 3-5 times of filter residue quality again, is heated to reflux
1-2h, filtering and impurity removing merge filtered fluid, remove ethyl alcohol, are concentrated into the 1/2 of original volume to obtain the final product.
A kind of 6. safe and efficient liquid-state feed mould inhibitor according to claim 1, which is characterized in that the Cortex Eucommiae extracting solution
It is made by following steps：It is that 24 DEG C of -28 DEG C of extractions are handled that take Cortex Eucommiae, which with volumetric concentration be 70% ethyl alcohol in temperature, obtains ethyl alcohol and carries
Liquid is taken, then ethanol extract is crossed into AB-8 macroporous resin columns, it is transparent to be washed with distilled water to efflux, then is with volumetric concentration
3-5 times of column volume of 55%-65% ethanol elutions, obtains ethanol eluate, and finally obtaining Cortex Eucommiae with ethanol eluate recycling ethyl alcohol extracts
Liquid.
A kind of 7. safe and efficient liquid-state feed mould inhibitor according to claim 1, which is characterized in that the surfactant
For one kind in sucrose fatty ester, glycerin monostearate or polyoxyethylene sorbitan monolaurate.
8. a kind of preparation method of safe and efficient liquid-state feed mould inhibitor as described in claim 1-7 any one, feature
It is, comprises the following steps：
(1) raw material is weighed by the weight；
(2) camphor extracting solution, cassia bark extracting solution, Cortex Eucommiae extracting solution are mixed and heated to 40-50 DEG C and stirred evenly, add rich horse
Dimethyl phthalate, aminolevulinic acid (ALA), sodium benzoate, caryophyllus oil and citrus dry hide powder are uniformly mixed, and are eventually adding slow-released carrier and table
Face activating agent mixing.
A kind of 9. application method of safe and efficient liquid-state feed mould inhibitor as defined in claim 1, which is characterized in that institute
Additive amount of the mould inhibitor in feed is stated as 300-400g/T.
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| CN113100189A (en) * | 2021-05-18 | 2021-07-13 | 湖北龙王恨渔具集团有限公司 | Slow-release composite bait and preparation method thereof |
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| Title |
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| 无: "中草药及其提取物在饲料防霉剂中的应用", 《北方牧业》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113100189A (en) * | 2021-05-18 | 2021-07-13 | 湖北龙王恨渔具集团有限公司 | Slow-release composite bait and preparation method thereof |
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