CN108078905A - Anticreep shampoo for men only and its processing method - Google Patents
Anticreep shampoo for men only and its processing method Download PDFInfo
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- CN108078905A CN108078905A CN201810125958.1A CN201810125958A CN108078905A CN 108078905 A CN108078905 A CN 108078905A CN 201810125958 A CN201810125958 A CN 201810125958A CN 108078905 A CN108078905 A CN 108078905A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention discloses a kind of anticreep shampoo for men only and its processing method, the anticreep shampoo for men only includes following compositions：Fleece-flower root root extract, Cacumen Platycladi extract, Herba speranskiae tuberculatae extract, ginger-root extract, cordyceps sinensis (CORDYCEPS SINENSIS) extract, sodium lauroyl sarcosine, EDETATE SODIUM, glycol distearate, guar hydroxypropyltrimonium chloride, cetostearyl alcohol；Panthenol, citric acid etc..The anticreep shampoo for men only of the present invention, component safe without toxic side effect, compatibility science, fleece-flower root root extract, Cacumen Platycladi extract, Herba speranskiae tuberculatae extract, ginger-root extract, the Cordyceps extract contained, energy efficient hardening root of hair inhibits alopecia, adjusts metabolism, promotes kainogenesis long, it is clearly submissive using rear hair, there are anti-dandruff and itching-relieving, biocidal efficacies, long-time service makes hair pitch-black dense.
Description
Technical field
Present invention relates particularly to a kind of Anti-hair loss functional shampoos for men only.
Background technology
Shampoo is also known as shampoo or shampoo, shampoo, is the hair and scalp basic nursing being most widely used
Cosmetic product.Contain Multiple components in shampoo, the comprehensive function of these compositions can play cleaning scalp and hair, moisten drying
Hair makes hair wash rear gloss submissive.Alopecia refers to the phenomenon that epilation.The hair normally to come off be at catagen and
The hair of stand-down.And pathologic alopecia refers to that hair is abnormal or excessive and comes off, long-term pathologic alopecia generates bald tired
It disturbs.Male is the multiple crowd of alopecia, although man's shampoo currently on the market cleans, moistens better function, anticreep
It is poor to send out effect, lacks a kind of Multifunctional washing that can improve rapidly, cure alopecia problem and becomes visible.
The anticreep shampoo for men only of the present invention, rich in a variety of anticreep plant essences, skin conditioning agent, hair conditioning
Agent, detergent, protein, amino acid, mineral element etc..Creative addition fleece-flower root root extract, Cacumen Platycladi extract, thoroughly
Bone grass extract, ginger-root extract, Cordyceps extract and other nutritional ingredients act synergistically, and have cleaning scalp, moisten
Hair, nursing skin of head, the effect eliminating scalp bacterium, inhibit alopecia, promoting natural on-off cycles of hair growth.
The content of the invention
The present invention's provides a kind of anticreep shampoo for men only.To solve the above problems, the present invention uses following skill
Art scheme：
A kind of anticreep shampoo for men only, is made of, the weight percent is to account for raw material A, B, C, D, E group raw material
The percentage of gross weight：A groups：I components of 9-18%, II components of 9-18%, 2-4% sodium lauroyl sarcosines, 0.1-0.2%EDTA bis-
Sodium, 33.26-66.63% water；B groups：1.2-2.4% glycol distearates, 0.5-1.0% melon glue Hydroxyproyl Trimethyls
Ammonium chloride, 0.3-0.6% cetostearyl alcohols；C groups：III components of 5-10%, 0.3-0.6% panthenols, 0.12-0.24% citric acids；D
Group：Fleece-flower root root extract 1.5-3.0%, Cacumen Platycladi extract 1.5-3.0%, Herba speranskiae tuberculatae extract 1.2-2.4%, race carry
Take object 1-2%, Cordyceps extract 0.1-0.2%；E groups：0.5-1.0% essence, IV components of 0.05-0.10%；Described I group
It is (20-30) in mass ratio to be divided into water and laureth sulfuric ester ammonium:The mixture of (70-80)；II component is water and 7
Bay alcohol sulfuric ester ammonium is (20-30) in mass ratio:The mixture of (70-80)；III component is water, cocamidopropyl propyl amide sweet tea
Dish alkali, sodium chloride are (55-65) in mass ratio：(20-30):The mixture of (5-25)；IV component is water and the different thiophene of methyl
Oxazoline ketone is (96-98.5) in mass ratio:The mixture of (1.5-4).
A kind of anticreep shampoo for men only, is made of, the weight percent is to account for raw material A, B, C, D, E group raw material
The percentage of gross weight：A groups：I components of 9-18%, II components of 9-18%, 2-4% sodium lauroyl sarcosines, 0.1-0.2%EDTA bis-
Sodium, 29.26-66.43% water；B groups：1.2-2.4% glycol distearates, 0.5-1.0% melon glue Hydroxyproyl Trimethyls
Ammonium chloride, 0.3-0.6% cetostearyl alcohols；C groups：III components of 5-10%, 0.3-0.6% panthenols, 0.12-0.24% citric acids；D
Group：Fleece-flower root root extract 1.5-3.0%, Cacumen Platycladi extract 1.5-3.0%, Herba speranskiae tuberculatae extract 1.2-2.4%, race carry
Take object 1-2%, Cordyceps extract 0.1-0.2%；E groups：0.5-1.0% essence, IV components of 0.05-0.10%, 0.2-
0.4% bleeding agent；I component is that water and laureth sulfuric ester ammonium are (20-30) in mass ratio:The mixing of (70-80)
Object；II component is that water and 7 bay alcohol sulfuric ester ammoniums are (20-30) in mass ratio:The mixture of (70-80)；Described III group
It is (55-65) in mass ratio to be divided into water, Cocoamidopropyl betaine, sodium chloride：(20-30):The mixture of (5-25)；It is described
IV component is that water and methylisothiazolinone are (96-98.5) in mass ratio:The mixture of (1.5-4).
A kind of anticreep shampoo for men only, is made of, the weight percent is to account for raw material A, B, C, D, E group raw material
The percentage of gross weight：A groups：I components of 9-18%, II components of 9-18%, 2-4% sodium lauroyl sarcosines, 0.1-0.2%EDTA bis-
Sodium, 25.26-66.23% water；B groups：1.2-2.4% glycol distearates, 0.5-1.0% melon glue Hydroxyproyl Trimethyls
Ammonium chloride, 0.3-0.6% cetostearyl alcohols；C groups：III components of 5-10%, 0.3-0.6% panthenols, 0.12-0.24% citric acids；D
Group：Fleece-flower root root extract 1.5-3.0%, Cacumen Platycladi extract 1.5-3.0%, Herba speranskiae tuberculatae extract 1.2-2.4%, race carry
Take object 1-2%, Cordyceps extract 0.1-0.2%；E groups：0.5-1.0% essence, IV components of 0.05-0.10%, 0.2-
0.4% bleeding agent, 0.2-0.4% moisturizer；I component is that water and laureth sulfuric ester ammonium are (20- in mass ratio
30):The mixture of (70-80)；II component is that water and 7 bay alcohol sulfuric ester ammoniums are (20-30) in mass ratio:(70-80)
Mixture；III component is that water, Cocoamidopropyl betaine, sodium chloride are (55-65) in mass ratio：(20-30):
The mixture of (5-25)；IV component is that water and methylisothiazolinone are (96-98.5) in mass ratio:(1.5-4's) is mixed
Close object.
A kind of anticreep shampoo for men only, is made of, the weight percent is to account for raw material A, B, C, D, E group raw material
The percentage of gross weight：A groups：I components of 9-18%, II components of 9-18%, 2-4% sodium lauroyl sarcosines, 0.1-0.2%EDTA bis-
Sodium, 17.26-65.83% water；B groups：1.2-2.4% glycol distearates, 0.5-1.0% melon glue Hydroxyproyl Trimethyls
Ammonium chloride, 0.3-0.6% cetostearyl alcohols；C groups：III components of 5-10%, 0.3-0.6% panthenols, 0.12-0.24% citric acids；D
Group：Fleece-flower root root extract 1.5-3.0%, Cacumen Platycladi extract 1.5-3.0%, Herba speranskiae tuberculatae extract 1.2-2.4%, race carry
Take object 1-2%, Cordyceps extract 0.1-0.2%；E groups：0.5-1.0% essence, IV components of 0.05-0.10%, 0.2-
0.4% bleeding agent, 0.2-0.4% moisturizer, 0.4-0.8% nourishing additive agents；I component is water and laureth sulfuric acid
Ester ammonium is (20-30) in mass ratio:The mixture of (70-80)；II component for water and 7 bay alcohol sulfuric ester ammoniums in mass ratio
For (20-30):The mixture of (70-80)；III component is water, Cocoamidopropyl betaine, sodium chloride are in mass ratio
(55-65)：(20-30):The mixture of (5-25)；IV component is that water and methylisothiazolinone are (96- in mass ratio
98.5):The mixture of (1.5-4)；The nourishing additive agent is yellow meal worm extract and/or corniculate spurgentian herb extract.
Preferably, the nourishing additive agent is that yellow meal worm extract and corniculate spurgentian herb extract are (3-5) in mass ratio:(1-3)
Mixture.
Preferably, the bleeding agent is aminoglucose hydrochloride, dextran sulfate sodium, N-acetylglucosamine are pressed
Mass ratio is (1-5)：(1-5)：The mixture of (1-5).
It is further preferred that the bleeding agent is aminoglucose hydrochloride, dextran sulfate sodium, N- acetylaminos Portugal
Grape sugar is 2 in mass ratio：1：1 mixture.
Preferably, the moisturizer is celestial grass polyoses extract, and the preparation method of the celestial grass polyoses extract is as follows：It will
200-300g celestial grass crushed 30-50 mesh sieves, take 100-120g celestial grass powders, be added to when 45-55 DEG C of dry 10-13 is small
650-800g, temperature be in 98-100 DEG C of boiling water, then with the salt acid for adjusting pH of 1-5mol/L to 4.5-4.8, natural cooling
To 55-70 DEG C, it is 55-70 DEG C, is stirred 45-60 minutes with 50-120 revs/min of rotating speed in temperature, naturally cool to 25-35
DEG C, 0.3-3g zymocyte liquids are added in, is 25-35 DEG C, 15-30 minutes is stirred with 50-120 revs/min of rotating speed in temperature, then
Sealing ferments 2-5 days at 25-35 DEG C, obtains fermentation material, fermentation material is sterilized, the fermentation material after sterilizing is crossed 300-500 mesh
Sieve, filtrate is concentrated by evaporation to 50 DEG C and measures the thick paste that relative density is 1.26-1.28, and it is thick paste matter that quality is added in into thick paste
0.4-0.8 times of ethyl alcohol of amount, when temperature is small for 10-15 DEG C of standing 1-3, then with 3000-10000 revs/min of rotating speed from
The heart collects the precipitation after centrifugation, will be deposited in 40-60 DEG C of dry 6-12 it is small when to get celestial grass polyoses extract；The zymophyte
Liquid is that aspergillus niger bacterium solution and Lactobacillus casei liquid are (1-10) in mass ratio:The mixture of (1-5), the Lactobacillus casei liquid
Preparation method is：By Lactobacillus casei, glucose, water according to mass ratio be 1:(3-7):(20-40) is uniformly mixed, and is in temperature
30-45 DEG C of sealing 6-24h, obtains Lactobacillus casei liquid；The preparation method of the aspergillus niger bacterium solution is：By aspergillus niger, glucose,
Water is 1 according to mass ratio:(4-8):(20-50) is uniformly mixed, and is 35-45 DEG C of sealing 6-24h in temperature, is obtained black-koji mould
Liquid.
It is further preferred that the zymocyte liquid is aspergillus niger bacterium solution and Lactobacillus casei liquid is 4 in mass ratio:1 it is mixed
Object is closed, the preparation method of the Lactobacillus casei liquid is：By Lactobacillus casei, glucose, water according to mass ratio be 1:3:20 is mixed
It closes uniformly, is 30 DEG C of sealing 12h in temperature, obtains Lactobacillus casei liquid；The preparation method of the aspergillus niger bacterium solution is：By black song
Mould, glucose, water are 1 according to mass ratio:4:20 are uniformly mixed, and are 35 DEG C of sealing 12h in temperature, obtain aspergillus niger bacterium solution.
Preferably, the preparation method of the yellow meal worm extract is as follows：Dry yellow meal worm is crushed, crosses 20-50 mesh sieves,
40-60g yellow meal worm powders are taken, are added in 275-300mL ethyl alcohol, when 70-85 DEG C of heating water bath refluxing extraction 6.5-10 is small, mistake
100-200 mesh sieves, it is former filtrate to be concentrated to give volume under the conditions of being 0.04-0.07MPa in 60-75 DEG C of temperature, pressure by filtrate
The concentrate of 0.1-0.3 times of volume, by concentrate when 60-75 DEG C of dry 12-24 is small, then natural cooling, obtains yellow meal worm
Extract.
Preferably, the preparation method of the corniculate spurgentian herb extract is as follows：100-120g flower anchors is small in 45-55 DEG C of dry 8-12
When, 20-50 mesh sieves are smashed it through, 35-45g is taken to spend anchor powder, it is water-soluble to be added to the ethyl alcohol that 400-600g mass fractions are 65-75%
In liquid, when 65-75 DEG C of heating water bath refluxing extraction 4-6 is small, 200-500 mesh sieves are crossed, filtrate is concentrated by evaporation to 50 DEG C of measure
Relative density is the thick paste of 1.27-1.29, and thick paste is dried under reduced pressure, obtains corniculate spurgentian herb extract.
It is further preferred that described be dried under reduced pressure as in the condition that temperature is 40-70 DEG C, vacuum degree is 0.02-0.08MPa
When lower dry 2-8 is small.
The present invention also provides the processing methods of above-mentioned anticreep shampoo for men only, comprise the following steps：(1) quality hundred is pressed
Point than weighing each raw material, by A group raw materials I component, II component, sodium lauroyl sarcosine, EDETATE SODIUM and 30-70% water
It is added in blender, is warming up to 80-85 DEG C, stirred 20-60 minutes at 80-85 DEG C, with 50-500 revs/min of rotating speed；(2)
B group raw materials are added in, continue to stir 20-60 minutes at 80-85 DEG C, with 50-200 revs/min of rotating speed, (3) are cooled to 70-75
DEG C, C group raw materials are added in, are stirred 35-50 minutes at 70-75 DEG C, with 100-300 revs/min of rotating speed；(4) it is cooled to 50-55
DEG C, remaining water in D groups raw material, A group raw materials is added in, at 50-55 DEG C, with 250-500 revs/min of 50-100 points of rotating speed stirring
Clock；(5) 40-45 DEG C is cooled to, adds in E group raw materials, at 40-45 DEG C, with 300-600 revs/min of 50-80 points of rotating speed stirring
Clock；(6) 30-35 DEG C is cooled to, stands 30-60 minutes, tinning obtains anticreep shampoo for men only.
The anticreep shampoo for men only of the present invention, component safe without toxic side effect, compatibility science are carried containing fleece-flower root root
Object, Cacumen Platycladi extract, Herba speranskiae tuberculatae extract, ginger-root extract, Cordyceps extract are taken, it can efficient hardening root of hair, inhibition
Alopecia adjusts metabolism, promotes kainogenesis long, clearly submissive using rear hair, has anti-dandruff and itching-relieving, biocidal efficacies, for a long time
Using making hair pitch-black dense.
On the basis of common knowledge of the art, above-mentioned each optimum condition, can be each preferably to get the present invention in any combination
Embodiment.
Specific embodiment
It is further illustrated the present invention below by the mode of embodiment, but does not therefore limit the present invention to the reality
It applies among a scope.The experimental method of actual conditions is not specified in the following example, according to conventional methods and conditions or according to business
Product specification selects.
In following embodiments, primary raw material and instrument used are as follows：
Laureth sulfuric ester ammonium, English name：AMMONIUM LAURETH SULFATE, No. CAS：32612-48-
9。
Bay alcohol sulfuric ester ammonium, No. CAS：2235-54-3.
Cocoamidopropyl betaine, No. CAS：86438-79-1.
Sodium chloride, No. CAS：7647-14-5.
Sodium lauroyl sarcosine, No. CAS：137-16-6.
EDETATE SODIUM, No. CAS：139-33-3.
Fleece-flower root root extract, main functional component are lecithin, rheum emodin, Rhein and other ingredients.Main function：
Anti-aging effects, the influence to immune system, reducing blood lipid and study of anti-atherogenic effect, myocardium protecting action, hepatoprotective effect,
Neuroprotection, antibacterial action.Fleece-flower root root extract can be by buying or being prepared, and preparation method is according to application
Number for embodiment 1 in 201310313435.7 method.Fleece-flower root root extract used in the present invention extracts from polygonaceae plant
The fleece-flower root (Classification system：Polygonum multiflorum) dried root, withdrawal ratio 10:1,80 mesh of grain size, purchase is certainly
Xi'an Jia Tian bio tech ltd.
Cacumen Platycladi extract has cooling blood and hemostasis, growing and blacking hair and other effects, and Cacumen Platycladi extract can be by buying or making
It is standby to obtain, preparation method according to embodiment 4 in Application No. 201410785394.6 method.Cacumen biotae used in the present invention
Extract extracts from cupressaceae plant arbor-vitae (Classification system：Platycladus orientalis (L.) Franco) branch and
Leaf, withdrawal ratio 10:1,80 mesh of grain size is bought from Tai'an Jia Ye bio tech ltd.
Herba speranskiae tuberculatae extract, lopseed play an important role of clearing heat and detoxicating, activating blood circulation and reducing swelling.It can be by buying or being prepared into
It arrives, the Herba speranskiae tuberculatae extract in the present invention is prepared by the following method to obtain：Take lopseed (Classification system：Phryma
Leptostachya L.subsp.asiatica (Hara) Kitamura) complete stool, when 45 DEG C of dryings 8 are small, it then crushed 50
Mesh sieve obtains deep grass meal, and deep grass meal 100g is taken to be added in 800g water, when 30 DEG C of heat preservations 8 are small, then heats to 75
DEG C, 75 DEG C, it is small with 200 revs/min of rotating speed stirring 1.5 when, cross 100 mesh sieves, filtrate be concentrated by evaporation to 50 DEG C of measure phases
It is the thick paste of 1.27-1.29 to density, by thick paste when drying 12 is small under conditions of temperature is 55 DEG C, vacuum degree is 0.06MPa,
Obtain Herba speranskiae tuberculatae extract.
Glycol distearate, No. CAS：627-83-8.
Ginger-root extract has effects that anticreep, hair tonic, relieving exterior syndrome and dispelling cold.No. CAS：84696-15-1 is bought from this hundred completeization
Learn (Shanghai) Co., Ltd., withdrawal ratio 4:1.
Guar hydroxypropyltrimonium chloride, No. CAS：65497-29-2.
Lemon extract, the production of Guangzhou all sorts of flowers spices limited company, model 6133, food-grade.
Panthenol, i.e. D-pantothenyl aleohol, No. CAS：81-13-0.
Cetostearyl alcohol, No. CAS：67762-27-0.
Citric acid, No. CAS：77-92-9.
Cordyceps extract, main active are cordycepin and adenosine.With strengthen immunity, antitumor, protection
Kidney, anti-oxidant, anti-aging, protection cardiovascular system, it is hypoglycemic the effects that.Cordyceps extract can by purchase or
Be prepared, preparation method according to 201310535298.1 embodiment 3 of Application No. method.The winter worm summer used in the present invention
Careless extract colonizes in Hepialidae with section ergot fungus cordyceps sinensis bacterium Cordycepssinensis (Berk.) Sacc.
The complex of stroma and larva corpse on insect larvae extracts for raw material, withdrawal ratio 10:1, buying from Jin Jin chemistry of finding pleasure in has
Limit company.
Methylisothiazolinone, No. CAS：2682-20-4.
Aminoglucose hydrochloride, No. CAS：66-84-2.
Dextran sulfate sodium, No. CAS：9011-18-1.
N-acetylglucosamine, No. CAS：7512-17-6
Celestial grass, also known as Chinese mesona herb, Classification system：Mesona chinensis Benth. are a kind of important medicine-food two-purposes
Plant resources, in celestial grass ingredient, Flavonoid substances play an important role of inhibit cancer cell growth, reduce blood pressure；It is more
Sugar has enhancing and improves human body immune function effect；Essence is known as the effect of calmness, refreshing and detoxicating profit water；Trace element has
Inhibit free radical formation, the effect of anti-aging, anticancer；Vitamin can adjust and enhance physiological function etc..Used in the present invention
Celestial grass be celestial grass complete stool.
Ethyl alcohol, No. CAS：64-17-5, purity 99.5%.
Lactobacillus casei, Classification system：Lactobacillus casei belong to lactobacillus (Lactobacillus),
It is gram-positive bacteria, is a kind of probiotics.The Lactobacillus casei of the present invention is bought from Shaanxi Sen Fu natural products Co., Ltd,
10,000,000,000 cfu/g of content.
Aspergillus niger, Classification system：Aspergillus niger are distributed widely in grain, plant product all over the world
It is important fermentation industry strain in soil.The aspergillus niger of the present invention is bought from Shandong Changtai bio tech ltd, is contained
Measure 1,000,000,000 cfu/g.
Glucose, No. CAS：14431-43-7.
Yellow meal worm is called bread worm, Classification system：Tenebrio molitor, yellow meal worm contain high protein, it is abundant not
Saturated fatty acid, substantial amounts of amino acid and mineral element.The yellow meal worm water content for the drying that the present invention uses is 6%, and purchase is certainly
New rainbow Science and Technology Co., Ltd. of Beijing.
Flower anchor, Gentianaceae flower anchor belong to flower anchor kind, Classification system：Halenia corniculata (L.) Cornaz, herb enter
Medicine has the effect of clearing heat and promoting diuresis, calm the liver and benefit the lungs.The flower anchor that the present invention uses is flower anchor complete stool.
In following embodiments, used test method and key instrument are as follows：
Hair stretching mechanical property testing：Using brand for DIA-STRON, model MTT175 hair tester into
Row.3g topknots are cleaned, 3min is moistened with 15g anticreep shampoo for men only, is then rinsed well with clear water, combed with comb
Once to remove extra moisture, by hair temperature be 25 DEG C, relative humidity be 50% in the environment of place 24 it is small when.Due to
Three positions in hair longitudinal direction：Root, middle part, the tensile property of taper remove root and taper there are nuance, in remaining
Portion 10cm is tested, and between hair is fixed on two copper sheets of instrument, clamp distance 30mm, tensile speed is
12.5mm/min carries out breaking test, and record breaks work(.20 hairs is taken to be tested, as a result take being averaged for 20 hairs
Value.
Anti-dandruff measure of merit：It is tested using 10 grades of point systems, 0 grade indicates no dandruff, and l-2 grades greyish white for small flakes
Rough scales, 3-4 grades are as low as median size chip, 5-6 grade for the loose big and thin chip being connected of scalp, 7-8 grades are
Big tackness chip, 9-10 grades are certainly to the thicker scales of skin that peel off of yellow with scalp close attachment.Choosing 100 dandruff grades is
7-8 grades of male subject is divided into 10 groups every group 10, and 10 groups of subjects are special using the man of 1-10 of the embodiment of the present invention respectively
With anticreep shampoo, frequency of use, using once, did not used for every 3 days in addition to the anticreep shampoo for men only of the present invention
Other hair washing, hair products, also without the hairs beauty behavior such as have hair dyed, perm during test, after four weeks to anti-dandruff effect into
Row evaluation.Evaluation method：How much carried out with the scurf number adhered on hair in scalp and root of hair more than 4cm according to 10 grades of point systems
Scoring.
It is further illustrated the present invention below by the mode of embodiment, unless otherwise specified, used number is attached most importance to
Measure number.
Embodiment 1
Anticreep shampoo for men only is made of A, B, C, D, E group raw material, and the weight percent is to account for raw material gross weight
Percentage：A groups：9% I component, 9% II component, 2% sodium lauroyl sarcosine, 0.1%EDTA disodiums, 66.63% water；B
Group：1.2% glycol distearate, 0.5% guar hydroxypropyltrimonium chloride, 0.3% cetostearyl alcohol；C groups：
5% III component, 0.3% panthenol, 0.12% citric acid；D groups：Fleece-flower root root extract 1.5%, Cacumen Platycladi extract 1.5%, thoroughly
Bone grass extract 1.2%, ginger-root extract 1%, Cordyceps extract 0.1%；E groups：0.5% essence, 0.05% IV component；
I component is water and laureth sulfuric ester ammonium is 30 in mass ratio:70 mixture；II component is
Water and 7 bay alcohol sulfuric ester ammoniums are 30 in mass ratio:70 mixture；III component for water, Cocoamidopropyl betaine,
Sodium chloride is 65 in mass ratio:30:5 mixture；IV component is that water and methylisothiazolinone are 98.5 in mass ratio:
1.5 mixture.The essence is lemon extract.
The processing method of the anticreep shampoo for men only, which is characterized in that comprise the following steps：(1) quality hundred is pressed
Divide than weighing each raw material, I component, II component, sodium lauroyl sarcosine, EDETATE SODIUM and 50% water in A group raw materials are added
Enter into blender, be warming up to 80 DEG C, stirred 40 minutes at 80 DEG C, with 200 revs/min of rotating speed；(2) B group raw materials are added in, after
Continue and stirred 30 minutes at 80 DEG C, with 200 revs/min of rotating speed, (3) are cooled to 70 DEG C, C group raw materials are added in, at 70 DEG C, with 200
Rev/min rotating speed stir 35 minutes；(4) be cooled to 50 DEG C, add in remaining water in D groups raw material, A group raw materials, 50 DEG C, with
250 revs/min of rotating speed stirs 50 minutes；(5) 40 DEG C are cooled to, adds in E group raw materials, at 40 DEG C, with 300 revs/min of turn
Speed stirring 50 minutes；(6) 30 DEG C are cooled to, stands 30 minutes, tinning obtains anticreep shampoo for men only.
Anti-hair loss measure of merit
Zhang, man, 25 years old, hair loss patient used anticreep shampoo for men only, daily using 1 time, each 10-20 millis
It rises, after a week, within daily alopecia 25, hair quality is soft, and combing is smooth, and color development blacks, and alopecia problem is controlled substantially for continuous use
More, have new hair to grow.
Lee, man, 45 years old, hair loss patient used anticreep shampoo for men only, daily using 1 time, each 15-30 millis
It rises, after a week, alopecia substantially reduces for continuous use, and within 50, the pitch-black bright, nothing of hair dries up, is sallow existing for daily alopecia
As scalp is salubrious.
The anticreep shampoo for men only of the present invention is rich in fleece-flower root root extract, Cacumen Platycladi extract, lopseed extraction
A variety of Chinese herbal medicine extracts, protein, the ammonia such as object, ginger-root extract, cordyceps sinensis (CORDYCEPS SINENSIS) extract
Base acid, minerals, can effectively moisten scalp, eliminate scalp bacterium, hence it is evident that improvement alopecia, hair loss, hair are dried up, white hair phenomenon.
Embodiment 2
A kind of anticreep shampoo for men only, is made of, the weight percent is to account for raw material A, B, C, D, E group raw material
The percentage of gross weight：A groups：9% I component, 9% II component, 2% sodium lauroyl sarcosine, 0.1%EDTA disodiums, 66.43%
Water；B groups：1.2% glycol distearate, 0.5% guar hydroxypropyltrimonium chloride, 0.3% cetostearyl alcohol；C
Group：5% III component, 0.3% panthenol, 0.12% citric acid；D groups：Fleece-flower root root extract 1.5%, Cacumen Platycladi extract
1.5%th, Herba speranskiae tuberculatae extract 1.2%, ginger-root extract 1%, Cordyceps extract 0.1%；E groups：0.5% essence,
0.05% IV component, 0.2% bleeding agent；
I component is water and laureth sulfuric ester ammonium is 30 in mass ratio:70 mixture；II component is
Water and 7 bay alcohol sulfuric ester ammoniums are 30 in mass ratio:70 mixture；III component for water, Cocoamidopropyl betaine,
Sodium chloride is 65 in mass ratio：30:5 mixture；IV component is that water and methylisothiazolinone are 98.5 in mass ratio:
1.5 mixture.The essence is lemon extract.The bleeding agent is aminoglucose hydrochloride, dextran sulfate sodium, N-
Acetylglucosamine is 2 in mass ratio：1：1 mixture.
The processing method of the anticreep shampoo for men only, which is characterized in that comprise the following steps：(1) quality hundred is pressed
Divide than weighing each raw material, I component, II component, sodium lauroyl sarcosine, EDETATE SODIUM and 50% water in A group raw materials are added
Enter into blender, be warming up to 80 DEG C, stirred 40 minutes at 80 DEG C, with 200 revs/min of rotating speed；(2) B group raw materials are added in, after
Continue and stirred 30 minutes at 80 DEG C, with 200 revs/min of rotating speed, (3) are cooled to 70 DEG C, C group raw materials are added in, at 70 DEG C, with 200
Rev/min rotating speed stir 35 minutes；(4) be cooled to 50 DEG C, add in remaining water in D groups raw material, A group raw materials, 50 DEG C, with
250 revs/min of rotating speed stirs 50 minutes；(5) 40 DEG C are cooled to, adds in E group raw materials, at 40 DEG C, with 300 revs/min of turn
Speed stirring 50 minutes；(6) 30 DEG C are cooled to, stands 30 minutes, tinning obtains anticreep shampoo for men only.
Embodiment 3
It is substantially the same manner as Example 2, it differs only in：Bleeding agent described in the present embodiment 3 for aminoglucose hydrochloride,
Dextran sulfate sodium, N-acetylglucosamine are 1 in mass ratio：1：2 mixture.
Embodiment 4
It is substantially the same manner as Example 2, it differs only in：Bleeding agent described in the present embodiment 4 for aminoglucose hydrochloride,
Dextran sulfate sodium, N-acetylglucosamine are 1 in mass ratio：2：1 mixture..
Embodiment 5
A kind of anticreep shampoo for men only, is made of, the weight percent is to account for raw material A, B, C, D, E group raw material
The percentage of gross weight：A groups：9% I component, 9% II component, 2% sodium lauroyl sarcosine, 0.1%EDTA disodiums, 66.23%
Water；B groups：1.2% glycol distearate, 0.5% guar hydroxypropyltrimonium chloride, 0.3% cetostearyl alcohol；C
Group：5% III component, 0.3% panthenol, 0.12% citric acid；D groups：Fleece-flower root root extract 1.5%, Cacumen Platycladi extract
1.5%th, Herba speranskiae tuberculatae extract 1.2%, ginger-root extract 1%, Cordyceps extract 0.1%；E groups：0.5% essence,
0.05% IV component, 0.2% bleeding agent, 0.2% moisturizer；
I component is water and laureth sulfuric ester ammonium is 30 in mass ratio:70 mixture；II component is
Water and 7 bay alcohol sulfuric ester ammoniums are 30 in mass ratio:70 mixture；III component for water, Cocoamidopropyl betaine,
Sodium chloride is 65 in mass ratio：30:5 mixture；IV component is that water and methylisothiazolinone are 98.5 in mass ratio:
1.5 mixture.The essence is lemon extract.
The bleeding agent for aminoglucose hydrochloride, dextran sulfate sodium, N-acetylglucosamine in mass ratio
For 2：1：1 mixture.
The moisturizer is celestial grass polyoses extract, and the preparation method of the celestial grass polyoses extract is as follows：200g is celestial
Grass crushed 30 mesh sieves, take 100g celestial grass powders when 45 DEG C of dryings 10 are small, be added to 650g, in the boiling water that temperature is 100 DEG C,
Then 60 DEG C are naturally cooled to, is 60 DEG C, stirred with 50 revs/min of rotating speed in temperature to 4.5 with the salt acid for adjusting pH of 1mol/L
It mixes 45 minutes, naturally cools to 35 DEG C, add in 1g zymocyte liquids, be 35 DEG C, stir 15 points with 50 revs/min of rotating speed in temperature
Then clock seals, ferment 2 days at 35 DEG C, obtain fermentation material, and fermentation material is warming up to 95 DEG C, and at 95 DEG C keep the temperature 40 minutes into
Row sterilizing, 300 mesh sieves are crossed by the fermentation material after sterilizing, and it is 1.26-1.28 that filtrate, which is concentrated by evaporation, and measures relative density to 50 DEG C
Thick paste, into thick paste add in quality be 0.4 times of thick paste quality ethyl alcohol, temperature for 15 DEG C stand 1 it is small when, then with 5000
Rev/min rotating speed centrifugation, collect centrifugation after precipitation, will be deposited in 40 DEG C of dryings 6 it is small when to get celestial grass polyoses extract；
The zymocyte liquid is aspergillus niger bacterium solution and Lactobacillus casei liquid is 10 in mass ratio:1 mixture, the Lactobacillus casei liquid
Preparation method be：By Lactobacillus casei, glucose, water according to mass ratio be 1:3:20 are uniformly mixed, close for 30 DEG C in temperature
12h is sealed, obtains Lactobacillus casei liquid；The preparation method of the aspergillus niger bacterium solution is：By aspergillus niger, glucose, water according to quality
Than for 1:4:20 are uniformly mixed, and are 35 DEG C of sealing 12h in temperature, obtain aspergillus niger bacterium solution.
The processing method of the anticreep shampoo for men only, which is characterized in that comprise the following steps：(1) quality hundred is pressed
Divide than weighing each raw material, I component, II component, sodium lauroyl sarcosine, EDETATE SODIUM and 50% water in A group raw materials are added
Enter into blender, be warming up to 80 DEG C, stirred 40 minutes at 80 DEG C, with 200 revs/min of rotating speed；(2) B group raw materials are added in, after
Continue and stirred 30 minutes at 80 DEG C, with 200 revs/min of rotating speed, (3) are cooled to 70 DEG C, C group raw materials are added in, at 70 DEG C, with 200
Rev/min rotating speed stir 35 minutes；(4) be cooled to 50 DEG C, add in remaining water in D groups raw material, A group raw materials, 50 DEG C, with
250 revs/min of rotating speed stirs 50 minutes；(5) 40 DEG C are cooled to, adds in E group raw materials, at 40 DEG C, with 300 revs/min of turn
Speed stirring 50 minutes；(6) 30 DEG C are cooled to, stands 30 minutes, tinning obtains anticreep shampoo for men only.
Embodiment 6
It is substantially the same manner as Example 5, it differs only in, the preparation method of celestial grass polyoses extract described in the present embodiment 6 is such as
Under：By 200g celestial grass when 45 DEG C of dryings 10 are small, 30 mesh sieves are crushed, take 100g celestial grass powders, are added to 650g, temperature 100
DEG C boiling water in, then with the salt acid for adjusting pH of 1mol/L to 4.5, naturally cool to 60 DEG C, temperature be 60 DEG C, with 50 turns/
The rotating speed of minute stirs 45 minutes, naturally cools to 35 DEG C, adds in 1g zymocyte liquids, is 35 DEG C, with 50 revs/min in temperature
Rotating speed stirs 15 minutes, then seals, and ferments 2 days at 35 DEG C, obtains fermentation material, fermentation material is warming up to 95 DEG C, and at 95 DEG C
Heat preservation sterilizes for 40 minutes, and the fermentation material after sterilizing is crossed 300 mesh sieves, and filtrate is concentrated by evaporation to 50 DEG C of measure relative densities
For the thick paste of 1.26-1.28, the ethyl alcohol that quality is 0.4 times of thick paste quality is added in into thick paste, it is small for 15 DEG C of standings 1 in temperature
When, then centrifuged with 5000 revs/min of rotating speed, collect the precipitation after centrifugation, will be deposited in 40 DEG C of dryings 6 it is small when to get celestial being
Grass polysaccharide extract；The zymocyte liquid is aspergillus niger bacterium solution and Lactobacillus casei liquid is 4 in mass ratio:1 mixture, it is described
The preparation method of Lactobacillus casei liquid is：By Lactobacillus casei, glucose, water according to mass ratio be 1:3:20 are uniformly mixed,
Temperature is 30 DEG C of sealing 12h, obtains Lactobacillus casei liquid；The preparation method of the aspergillus niger bacterium solution is：By aspergillus niger, grape
Sugar, water are 1 according to mass ratio:4:20 are uniformly mixed, and are 35 DEG C of sealing 12h in temperature, obtain aspergillus niger bacterium solution.
Embodiment 7
It is substantially the same manner as Example 5, it differs only in, the preparation method of celestial grass polyoses extract described in the present embodiment 7 is such as
Under：By 200g celestial grass when 45 DEG C of dryings 10 are small, 30 mesh sieves are crushed, take 100g celestial grass powders, are added to 650g, temperature 100
DEG C boiling water in, then with the salt acid for adjusting pH of 1mol/L to 4.5, naturally cool to 60 DEG C, temperature be 60 DEG C, with 50 turns/
The rotating speed of minute stirs 45 minutes, naturally cools to 35 DEG C, adds in 1g zymocyte liquids, is 35 DEG C, with 50 revs/min in temperature
Rotating speed stirs 15 minutes, then seals, and ferments 2 days at 35 DEG C, obtains fermentation material, fermentation material is warming up to 95 DEG C, and at 95 DEG C
Heat preservation sterilizes for 40 minutes, and the fermentation material after sterilizing is crossed 300 mesh sieves, and filtrate is concentrated by evaporation to 50 DEG C of measure relative densities
For the thick paste of 1.26-1.28, the ethyl alcohol that quality is 0.4 times of thick paste quality is added in into thick paste, it is small for 15 DEG C of standings 1 in temperature
When, then centrifuged with 5000 revs/min of rotating speed, collect the precipitation after centrifugation, will be deposited in 40 DEG C of dryings 6 it is small when to get celestial being
Grass polysaccharide extract；The zymocyte liquid is aspergillus niger bacterium solution and Lactobacillus casei liquid is 2 in mass ratio:1 mixture, it is described
The preparation method of Lactobacillus casei liquid is：By Lactobacillus casei, glucose, water according to mass ratio be 1:3:20 are uniformly mixed,
Temperature is 30 DEG C of sealing 12h, obtains Lactobacillus casei liquid；The preparation method of the aspergillus niger bacterium solution is：By aspergillus niger, grape
Sugar, water are 1 according to mass ratio:4:20 are uniformly mixed, and are 35 DEG C of sealing 12h in temperature, obtain aspergillus niger bacterium solution.
Embodiment 8
Anticreep shampoo for men only is made of A, B, C, D, E group raw material, and the weight percent is to account for raw material gross weight
Percentage：A groups：9% I component, 9% II component, 2% sodium lauroyl sarcosine, 0.1%EDTA disodiums, 65.83% water；B
Group：1.2% glycol distearate, 0.5% guar hydroxypropyltrimonium chloride, 0.3% cetostearyl alcohol；C groups：
5% III component, 0.3% panthenol, 0.12% citric acid；D groups：Fleece-flower root root extract 1.5%, Cacumen Platycladi extract 1.5%, thoroughly
Bone grass extract 1.2%, ginger-root extract 1%, Cordyceps extract 0.1%；E groups：0.5% essence, 0.05% IV component,
0.2% bleeding agent, 0.2% moisturizer, 0.4% nourishing additive agent；
I component is water and laureth sulfuric ester ammonium is 30 in mass ratio:70 mixture；II component is
Water and 7 bay alcohol sulfuric ester ammoniums are 30 in mass ratio:70 mixture；III component for water, Cocoamidopropyl betaine,
Sodium chloride is 65 in mass ratio：30：5 mixture；IV component is that water and methylisothiazolinone are 98.5 in mass ratio:
1.5 mixture.The essence is lemon extract.
The bleeding agent for aminoglucose hydrochloride, dextran sulfate sodium, N-acetylglucosamine in mass ratio
For 2：1：1 mixture.
The moisturizer is celestial grass polyoses extract, and the preparation method of the celestial grass polyoses extract is as follows：200g is celestial
Grass crushed 30 mesh sieves, take 100g celestial grass powders when 45 DEG C of dryings 10 are small, be added to 650g, in the boiling water that temperature is 100 DEG C,
Then 60 DEG C are naturally cooled to, is 60 DEG C, stirred with 50 revs/min of rotating speed in temperature to 4.5 with the salt acid for adjusting pH of 1mol/L
It mixes 45 minutes, naturally cools to 35 DEG C, add in 1g zymocyte liquids, be 35 DEG C, stir 15 points with 50 revs/min of rotating speed in temperature
Then clock seals, ferment 2 days at 35 DEG C, obtain fermentation material, and fermentation material is warming up to 95 DEG C, and at 95 DEG C keep the temperature 40 minutes into
Row sterilizing, 300 mesh sieves are crossed by the fermentation material after sterilizing, and it is 1.26-1.28 that filtrate, which is concentrated by evaporation, and measures relative density to 50 DEG C
Thick paste, into thick paste add in quality be 0.4 times of thick paste quality ethyl alcohol, temperature for 15 DEG C stand 1 it is small when, then with 5000
Rev/min rotating speed centrifugation, collect centrifugation after precipitation, will be deposited in 40 DEG C of dryings 6 it is small when to get celestial grass polyoses extract；
The zymocyte liquid is aspergillus niger bacterium solution and Lactobacillus casei liquid is 4 in mass ratio:1 mixture, the Lactobacillus casei liquid
Preparation method be：By Lactobacillus casei, glucose, water according to mass ratio be 1:3:20 are uniformly mixed, close for 30 DEG C in temperature
12h is sealed, obtains Lactobacillus casei liquid；The preparation method of the aspergillus niger bacterium solution is：By aspergillus niger, glucose, water according to quality
Than for 1:4:20 are uniformly mixed, and are 35 DEG C of sealing 12h in temperature, obtain aspergillus niger bacterium solution.
The nourishing additive agent is yellow meal worm extract.The preparation method of the yellow meal worm extract is as follows：It will be dry
Yellow meal worm crushes, and crosses 50 mesh sieves, takes 40g yellow meal worm powders, adds in 275mL ethyl alcohol, small in 70 DEG C of heating water bath refluxing extractions 6.5
When, 100 mesh sieves are crossed, it is former filtrate volume 0.2 that volume is concentrated to give under the conditions of being 0.06MPa in temperature 60 C, pressure by filtrate
Concentrate again, by concentrate when 60 DEG C of dryings 12 are small, then natural cooling, obtains yellow meal worm extract.
The processing method of the anticreep shampoo for men only, which is characterized in that comprise the following steps：(1) quality hundred is pressed
Divide than weighing each raw material, I component, II component, sodium lauroyl sarcosine, EDETATE SODIUM and 50% water in A group raw materials are added
Enter into blender, be warming up to 80 DEG C, stirred 40 minutes at 80 DEG C, with 200 revs/min of rotating speed；(2) B group raw materials are added in, after
Continue and stirred 30 minutes at 80 DEG C, with 200 revs/min of rotating speed, (3) are cooled to 70 DEG C, C group raw materials are added in, at 70 DEG C, with 200
Rev/min rotating speed stir 35 minutes；(4) be cooled to 50 DEG C, add in remaining water in D groups raw material, A group raw materials, 50 DEG C, with
250 revs/min of rotating speed stirs 50 minutes；(5) 40 DEG C are cooled to, adds in E group raw materials, at 40 DEG C, with 300 revs/min of turn
Speed stirring 50 minutes；(6) 30 DEG C are cooled to, stands 30 minutes, tinning obtains anticreep shampoo for men only.
Embodiment 9
It is substantially the same manner as Example 8, it differs only in, nourishing additive agent described in the present embodiment 9 is corniculate spurgentian herb extract.It is described
The preparation method of corniculate spurgentian herb extract is as follows：By 100g flower anchors when 45 DEG C of dryings 8 are small, 50 mesh sieves are smashed it through, 35g is taken to spend anchor
Powder is added in the ethanol water that 400g mass fractions are 70%, when 65 DEG C of heating water bath refluxing extractions 4 are small, crosses 200 mesh
Filtrate is concentrated by evaporation to 50 DEG C and measures the thick paste that relative density is 1.27, thick paste is dried under reduced pressure by sieve, obtains spending anchor extraction
Object, under conditions of described to be dried under reduced pressure be 50 DEG C in temperature, vacuum degree is 0.06MPa it is dry 6 it is small when.
Embodiment 10
It is substantially the same manner as Example 8, differ only in, nourishing additive agent described in the present embodiment 10 for yellow meal worm extract and
Corniculate spurgentian herb extract is 3 in mass ratio:1 mixture.The preparation method of the yellow meal worm extract is as follows：By dry yellow meal worm
It crushes, crosses 50 mesh sieves, take 40g yellow meal worm powders, add in 275mL ethyl alcohol, when 70 DEG C of heating water bath refluxing extractions 6.5 are small, mistake
100 mesh sieves, it is the dense of former 0.2 times of filtrate volume that volume is concentrated to give under the conditions of being 0.06MPa in temperature 60 C, pressure by filtrate
Contracting liquid, by concentrate when 60 DEG C of dryings 12 are small, then natural cooling, obtains yellow meal worm extract.The corniculate spurgentian herb extract
Preparation method is as follows：By 100g flower anchors when 45 DEG C of dryings 8 are small, 50 mesh sieves are smashed it through, 35g is taken to spend anchor powder, is added to 400g
Mass fraction is in 70% ethanol water, when 65 DEG C of heating water bath refluxing extractions 4 are small, cross 200 mesh sieves, filtrate is evaporated
It is concentrated into 50 DEG C and measures the thick paste that relative density is 1.27, thick paste is dried under reduced pressure, obtains corniculate spurgentian herb extract, it is described to be dried under reduced pressure
For be 50 DEG C in temperature, under conditions of vacuum degree is 0.06MPa it is dry 6 it is small when.
Hair stretching mechanical property testing
To present invention anticreep shampoo for men only is used to carry out hair stretching mechanical property testing, concrete outcome is shown in Table 1.
Table 1：Hair stretching mechanical property testing result table
| Break work(/ 10-2J | |
| Embodiment 2 | 2.1 |
| Embodiment 3 | 1.9 |
| Embodiment 4 | 1.8 |
| Embodiment 5 | 2.2 |
| Embodiment 6 | 2.5 |
| Embodiment 7 | 2.1 |
| Embodiment 8 | 2.8 |
| Embodiment 9 | 2.9 |
| Embodiment 10 | 3.4 |
Contain bleeding agent in the shampoo of embodiment 2-4, bleeding agent can promote expansion of the nutriment on hair fiber surface
It dissipates, nutriment is preferably absorbed by hair, the elasticity raising of hair, the enhancing of stretch-proof fracture property.Embodiment 5-7 is further
Celestial grass polyoses extract moisturizer is with the addition of in shampoo, celestial grass polyoses extract energy elongated insertion part shampoo point reduces hair and does
Withered fracture.Yellow meal worm extract that the shampoo of embodiment 8-10 contains, corniculate spurgentian herb extract are as nourishing additive agent, rich in fat
Acid, amino acid, flavone compound, the break resistance of hair further improve.
Anti-dandruff measure of merit
To present invention anticreep shampoo for men only is used to carry out anti-dandruff functional test, concrete outcome is shown in Table 2.
Table 2：Anti-dandruff functional test results table
| Anti-dandruff grade | |
| Embodiment 2 | 4 grades |
| Embodiment 6 | 3 grades |
| Embodiment 8 | 2 grades |
| Embodiment 9 | 2 grades |
| Embodiment 10 | 0 grade |
Scalp surface bacterium amount reproduction, Microflora is unbalance be generate dandruff one of the major reasons, the present invention man
Scholar's Special anti-loosening shampoo contains antimicrobial component, inhibits the growth and breeding of scalp surface bacterium, and long-time service, which has, significantly goes
Consider effect to be worth doing.
The preferred embodiment of the present invention described in detail above.It should be appreciated that those of ordinary skill in the art without
Creative work is needed according to the present invention can to conceive and makes many modifications and variations.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical solution, all should be in the protection domain being defined in the patent claims.
Claims (10)
1. a kind of anticreep shampoo for men only, which is characterized in that be made of A, B, C, D, E group raw material, the weight percent
It is the percentage for accounting for raw material gross weight：A groups：I components of 9-18%, II components of 9-18%, 2-4% sodium lauroyl sarcosines, 0.1-
0.2%EDTA disodiums, 33.26-66.63% water；B groups：1.2-2.4% glycol distearates, 0.5-1.0% melon glue hydroxyls
Hydroxypropyltrimonium chloride, 0.3-0.6% cetostearyl alcohols；C groups：III components of 5-10%, 0.3-0.6% panthenols, 0.12-
0.24% citric acid；D groups：Fleece-flower root root extract 1.5-3.0%, Cacumen Platycladi extract 1.5-3.0%, Herba speranskiae tuberculatae extract
1.2-2.4%, ginger-root extract 1-2%, Cordyceps extract 0.1-0.2%；E groups：0.5-1.0% essence, 0.05-
0.10% IV component；
I component is that water and laureth sulfuric ester ammonium are (20-30) in mass ratio:The mixture of (70-80)；Described II
Component is that water and 7 bay alcohol sulfuric ester ammoniums are (20-30) in mass ratio:The mixture of (70-80)；III component is water, coconut palm
Oleamide propyl betaine, sodium chloride are (55-65) in mass ratio：(20-30):The mixture of (5-25)；IV component is
Water and methylisothiazolinone are (96-98.5) in mass ratio:The mixture of (1.5-4).
2. a kind of anticreep shampoo for men only, which is characterized in that be made of A, B, C, D, E group raw material, the weight percent
It is the percentage for accounting for raw material gross weight：A groups：I components of 9-18%, II components of 9-18%, 2-4% sodium lauroyl sarcosines, 0.1-
0.2%EDTA disodiums, 29.26-66.43% water；B groups：1.2-2.4% glycol distearates, 0.5-1.0% melon glue hydroxyls
Hydroxypropyltrimonium chloride, 0.3-0.6% cetostearyl alcohols；C groups：III components of 5-10%, 0.3-0.6% panthenols, 0.12-
0.24% citric acid；D groups：Fleece-flower root root extract 1.5-3.0%, Cacumen Platycladi extract 1.5-3.0%, Herba speranskiae tuberculatae extract
1.2-2.4%, ginger-root extract 1-2%, Cordyceps extract 0.1-0.2%；E groups：0.5-1.0% essence, 0.05-
0.10% IV component, 0.2-0.4% bleeding agents；
I component is that water and laureth sulfuric ester ammonium are (20-30) in mass ratio:The mixture of (70-80)；Described II
Component is that water and 7 bay alcohol sulfuric ester ammoniums are (20-30) in mass ratio:The mixture of (70-80)；III component is water, coconut palm
Oleamide propyl betaine, sodium chloride are (55-65) in mass ratio：(20-30):The mixture of (5-25)；IV component is
Water and methylisothiazolinone are (96-98.5) in mass ratio:The mixture of (1.5-4).
3. a kind of anticreep shampoo for men only, which is characterized in that be made of A, B, C, D, E group raw material, the weight percent
It is the percentage for accounting for raw material gross weight：A groups：I components of 9-18%, II components of 9-18%, 2-4% sodium lauroyl sarcosines, 0.1-
0.2%EDTA disodiums, 25.26-66.23% water；B groups：1.2-2.4% glycol distearates, 0.5-1.0% melon glue hydroxyls
Hydroxypropyltrimonium chloride, 0.3-0.6% cetostearyl alcohols；C groups：III components of 5-10%, 0.3-0.6% panthenols, 0.12-
0.24% citric acid；D groups：Fleece-flower root root extract 1.5-3.0%, Cacumen Platycladi extract 1.5-3.0%, Herba speranskiae tuberculatae extract
1.2-2.4%, ginger-root extract 1-2%, Cordyceps extract 0.1-0.2%；E groups：0.5-1.0% essence, 0.05-
0.10% IV component, 0.2-0.4% bleeding agents, 0.2-0.4% moisturizer；
I component is that water and laureth sulfuric ester ammonium are (20-30) in mass ratio:The mixture of (70-80)；Described II
Component is that water and 7 bay alcohol sulfuric ester ammoniums are (20-30) in mass ratio:The mixture of (70-80)；III component is water, coconut palm
Oleamide propyl betaine, sodium chloride are (55-65) in mass ratio：(20-30):The mixture of (5-25)；IV component is
Water and methylisothiazolinone are (96-98.5) in mass ratio:The mixture of (1.5-4).
4. a kind of anticreep shampoo for men only, which is characterized in that be made of A, B, C, D, E group raw material, the weight percent
It is the percentage for accounting for raw material gross weight：A groups：I components of 9-18%, II components of 9-18%, 2-4% sodium lauroyl sarcosines, 0.1-
0.2%EDTA disodiums, 17.26-65.83% water；B groups：1.2-2.4% glycol distearates, 0.5-1.0% melon glue hydroxyls
Hydroxypropyltrimonium chloride, 0.3-0.6% cetostearyl alcohols；C groups：III components of 5-10%, 0.3-0.6% panthenols, 0.12-
0.24% citric acid；D groups：Fleece-flower root root extract 1.5-3.0%, Cacumen Platycladi extract 1.5-3.0%, Herba speranskiae tuberculatae extract
1.2-2.4%, ginger-root extract 1-2%, Cordyceps extract 0.1-0.2%；E groups：0.5-1.0% essence, 0.05-
0.10% IV component, 0.2-0.4% bleeding agents, 0.2-0.4% moisturizer, 0.4-0.8% nourishing additive agents；
I component is that water and laureth sulfuric ester ammonium are (20-30) in mass ratio:The mixture of (70-80)；Described II
Component is that water and 7 bay alcohol sulfuric ester ammoniums are (20-30) in mass ratio:The mixture of (70-80)；III component is water, coconut palm
Oleamide propyl betaine, sodium chloride are (55-65) in mass ratio：(20-30):The mixture of (5-25)；IV component is
Water and methylisothiazolinone are (96-98.5) in mass ratio:The mixture of (1.5-4)；The nourishing additive agent is yellow meal worm
Extract and/or corniculate spurgentian herb extract.
5. the anticreep shampoo for men only according to any one of claim 2-4, which is characterized in that the bleeding agent is
Aminoglucose hydrochloride, dextran sulfate sodium, N-acetylglucosamine are (1-5) in mass ratio：(1-5)：(1-5's)
Mixture.
6. the anticreep shampoo for men only according to claim 3 or 4, which is characterized in that the moisturizer is more for celestial grass
Sugar extract, the preparation method of the celestial grass polyoses extract are as follows：200-300g celestial grass is small in 45-55 DEG C of dry 10-13
When, 30-50 mesh sieves are crushed, take 100-120g celestial grass powders, are added to 650-800g, in the boiling water that temperature is 98-100 DEG C, so
55-70 DEG C is naturally cooled to, is 55-70 DEG C, with 50-120 in temperature to 4.5-4.8 with the salt acid for adjusting pH of 1-5mol/L afterwards
Rev/min rotating speed stir 45-60 minute, naturally cool to 25-35 DEG C, add in 0.3-3g zymocyte liquids, be 25-35 in temperature
DEG C, stirred 15-30 minute with 50-120 revs/min of rotating speed, then seal, in 25-35 DEG C of fermentation 2-5 days, obtain fermentation material,
Fermentation material is sterilized, the fermentation material after sterilizing is crossed into 300-500 mesh sieves, by filtrate be concentrated by evaporation to 50 DEG C measure relative densities be
The thick paste of 1.26-1.28 adds in the ethyl alcohol that quality is 0.4-0.8 times of thick paste quality into thick paste, is 10-15 DEG C of standing in temperature
It when 1-3 is small, is then centrifuged with 3000-10000 revs/min of rotating speed, collects the precipitation after centrifugation, 40-60 DEG C will be deposited in and done
To get celestial grass polyoses extract when dry 6-12 is small；The zymocyte liquid for aspergillus niger bacterium solution and Lactobacillus casei liquid in mass ratio
For (1-10):The mixture of (1-5), the preparation method of the Lactobacillus casei liquid are：Lactobacillus casei, glucose, water are pressed
It is 1 according to mass ratio:(3-7):(20-40) is uniformly mixed, and is 30-45 DEG C of sealing 6-24h in temperature, is obtained Lactobacillus casei liquid；
The preparation method of the aspergillus niger bacterium solution is：By aspergillus niger, glucose, water according to mass ratio be 1:(4-8):(20-50) is mixed
Uniformly, it is 35-45 DEG C of sealing 6-24h in temperature, obtains aspergillus niger bacterium solution.
7. anticreep shampoo for men only according to claim 4, which is characterized in that the preparation of the yellow meal worm extract
Method is as follows：Dry yellow meal worm is crushed, crosses 20-50 mesh sieves, takes 40-60g yellow meal worm powders, is added in 275-300mL ethyl alcohol,
When 70-85 DEG C of heating water bath refluxing extraction 6.5-10 is small, 100-200 mesh sieves are crossed, are in 60-75 DEG C of temperature, pressure by filtrate
The concentrate that volume is former 0.1-0.3 times of filtrate volume is concentrated to give under the conditions of 0.04-0.07MPa, by concentrate at 60-75 DEG C
When drying 12-24 is small, then natural cooling, obtains yellow meal worm extract.
8. anticreep shampoo for men only according to claim 4, which is characterized in that the preparation side of the corniculate spurgentian herb extract
Method is as follows：By 100-120g flower anchors when 45-55 DEG C of dry 8-12 is small, 20-50 mesh sieves are smashed it through, take 35-45g flower anchor powder,
It is added in the ethanol water that 400-600g mass fractions are 65-75%, it is small in 65-75 DEG C of heating water bath refluxing extraction 4-6
When, 200-500 mesh sieves are crossed, filtrate is concentrated by evaporation to 50 DEG C and measures the thick paste that relative density is 1.27-1.29, thick paste is depressurized
It is dry, obtain corniculate spurgentian herb extract.
9. anticreep shampoo for men only according to claim 8, which is characterized in that it is described be dried under reduced pressure be in temperature
40-70 DEG C, vacuum degree is when dry 2-8 is small under conditions of 0.02-0.08MPa.
10. the processing method of anticreep shampoo for men only according to any one of claim 1-4, which is characterized in that bag
Include following steps：(1) weigh each raw material by mass percentage, by A group raw materials I component, II component, Hamposyl L
The water of sodium, EDETATE SODIUM and 30-70% is added in blender, is warming up to 80-85 DEG C, at 80-85 DEG C, with 50-500 revs/min
The rotating speed of clock stirs 20-60 minutes；(2) B group raw materials are added in, continue to stir at 80-85 DEG C, with 50-200 revs/min of rotating speed
20-60 minutes, (3) were cooled to 70-75 DEG C, added in C group raw materials, were stirred at 70-75 DEG C, with 100-300 revs/min of rotating speed
35-50 minutes；(4) 50-55 DEG C is cooled to, remaining water in D groups raw material, A group raw materials is added in, at 50-55 DEG C, with 250-500
Rev/min rotating speed stir 50-100 minutes；(5) 40-45 DEG C is cooled to, E group raw materials are added in, at 40-45 DEG C, with 300-600
Rev/min rotating speed stir 50-80 minutes；(6) 30-35 DEG C is cooled to, stands 30-60 minutes, tinning obtains for men only anti-
De- shampoo.
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| CN114376957A (en) * | 2022-01-13 | 2022-04-22 | 广东星芮生物科技有限公司 | Scalp-maintaining, tough and anti-hair-loss double-repairing shampoo and preparation method thereof |
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| CN114376957A (en) * | 2022-01-13 | 2022-04-22 | 广东星芮生物科技有限公司 | Scalp-maintaining, tough and anti-hair-loss double-repairing shampoo and preparation method thereof |
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