CN104970989A - Natural hair dye composition - Google Patents

Natural hair dye composition Download PDF

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CN104970989A
CN104970989A CN201510430921.6A CN201510430921A CN104970989A CN 104970989 A CN104970989 A CN 104970989A CN 201510430921 A CN201510430921 A CN 201510430921A CN 104970989 A CN104970989 A CN 104970989A
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hair
agent
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刘万顺
韩宝芹
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Qingdao healthy marine bio Pharmaceutical Co Ltd
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Qingdao Huishenghuizhong Biotechnology Co Ltd
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Abstract

The invention relates to a natural hair dye composition. The natural hair dye composition is composed of two parts, a first part is solution prepared from the following components in weight proportion: 0.5-20g of a reducing agent, 0.1-8g of antioxidant, 0.1-10g of a nutrition penetrant, 0.1-10g of a moisturizer, 0.1-5g of a surface active agent, 0.5-20g of a colouring agent and 10-200ml of water, wherein a pH regulator is used for regulating pH to be 7.5-10; a second part is a solution prepared from the following components in weight proportion: 0.5-20g of dye mordant, 0.1-10g of a nutrition penetrating agent, 0.1-10g of a moisturizer, 0.1-5g of a surface active agent and 10-200ml water. The natural hair dye composition is applicable to dyeing of white hair to obtain black hair, no anaphylactic reaction is carried out, no toxic or side effect is produced, the nutrition penetrating agent can permeate quickly and is absorbed by skin, the effect is taken quickly, the hair-blacking and hair-nourishing effect is good, and the natural hair dye composition is simple and convenient.

Description

A kind of natural hair dye compositions
Technical field
The present invention relates to a kind of hair dye, particularly relate to a kind of natural hair dye compositions.
Background technology
The hair dye major part that market is sold is containing p-phenylenediamine (PPD) and analog thereof.Conventional black hair dye is with p-phenylenediamine (PPD) (PPD) for main component, and the colored tint applied in recent years is also all formed by the derivant of PPD and other chemical composition different ratio.PPD itself there is very strong sensitization (sensitization rate can up to 10%) and can with other many kinds of substance generation cross allergies.PPD also The book of Changes skin absorbs, and causes gastrointestinal tract, nervous system damage, renal failure, distortion, carcinogenic and immune system damage (Jin Hongxi, 2005).Life stress, the operating pressure of current people are all very large, and the crowd of poliosis is increasing, more and more rejuvenation, and the demand for hair dye gets more and more.Along with the raising of people's living standard, health perception strengthens gradually, the hair dye of the natural component of urgent needs Nantural non-toxic side effect.Therefore, prepare the nontoxic natural botanical hair dye without allergy and become current study hotspot.
Hair color is the same with skin, depend on that melanin generates, the melanocyte synthesis melanocyte in ball top portion, is transported to the keratinocyte of surrounding, in cortex of hair the kind of melanin granule and quantity determine the color of hair, hair can have yellow, brown, red or black, white etc.
The traditional Chinese medical science thinks kidney storing essence, and smart hemopoietic, illustrates the generation of blood, originally come from congenital essence, changes hemopoietic liquid with nutrition hair.The vigour root of people, in kidney, is by the life of essence in kidney instituteization.Vigour is the motive power of human life transporting, can excite and promote the growth of hair.Human body kidney essense is sufficient, and hair is then grown normally, shows as dense, bright, soft and moist; Otherwise it is then rare, withered, not damp.The physiological action of kidney to hair is as follows: the first, kidney essense hemopoietic liquid, nutrition hair; The second, the raw vigour of kidney essenseization, excites and impels hair growth; 3rd, kidney essense by governor vessel and through gas effect hair of supplementing nutrition.Governor vessel separates genus kidney from ridge.Therefore the source of nutrition of hair is in QI and blood, its life then root in kidney.Therefore, the specific Chinese medicine of compatibility in the hair dye of routine, trophocyte, shines the vigor of cell itself, thus makes hair growth, carries out " the kidney invigorating " cell, makes hair blackening.
The present invention relates to natural hair dye compositions.Reducing agent cysteine, cysteine hydrochloride or acetylcysteine in hair coloring preparation composition, can open the disulfide bond in hair keratin, the scale of hair of loosening, be conducive to the infiltration of mordant and stain.The amino monosaccharide of nutrient permeation agent in hair coloring preparation composition or amino-oligosacchride, be through the micromolecule amino sugar of experiment screening, in molecular structure, there is amino structure, it is the constituent of human body glycosaminoglycans, these amino monosaccharide or amino-oligosacchride easily penetrate into hair inside, the hydrogen bond of hair can be cut off, hair scale is opened further, the infiltration of further promotion mordant and stain, there is the effect increasing coloring effect and improve firm coloration degree, above-mentioned amino monosaccharide and amino-oligosacchride simultaneously, as the constituent of human body glycosaminoglycans, absorb easily through skin and hair, nutrition skin of head, make hair more healthy.The present invention is also preferred part natural product is as nutrient permeation agent.Stain in hair coloring preparation composition is gallic acid, metagallic acid, or the natural chromogenic agent of other plant origin, and these stains are natural components, to human non-toxic's side effect.Wetting agent in hair coloring preparation composition is conducive to increasing the brightness of hair and moist degree.Mordant in hair coloring preparation composition is bivalent metal ion, preferred ferrous ion (Fe 2+), be combined into indigote with stain.Surfactant in hair coloring preparation composition, acid-base modifier are all materials that cosmetic field is conventional.
Main component in hair coloring preparation composition of the present invention is all natural components, to human non-toxic's side effect, uses not irritated.Compare with other natural hair dye, containing the amino monosaccharide of nutrient permeation agent or amino-oligosacchride in hair coloring preparation composition of the present invention, these amino monosaccharide or amino-oligosacchride easily penetrate into hair inside, the hydrogen bond of hair can be cut off, hair scale is opened further, the infiltration of further promotion mordant and stain, has the effect increasing coloring effect and improve firm coloration degree.Above-mentioned amino monosaccharide and amino-oligosacchride simultaneously, as the constituent of human body glycosaminoglycans, absorb easily through skin and hair, nutrition skin of head, is beneficial to hair growth promoting and black hair, makes hair more healthy.Compare with other natural hair dye, hair coloring preparation composition of the present invention, also containing wetting agent, is conducive to increasing the brightness of hair and moist degree.Therefore, natural hair dye compositions of the present invention hair dyeing fast colours, not easily decolours, simultaneously to human non-toxic's side effect, not irritated, simultaneously also nourishing hair and scalp, and moisturizing, hair is more healthy.
Summary of the invention
The object of this invention is to provide a kind of natural hair dye compositions, to make up the above-mentioned deficiency of prior art.
A kind of natural hair dye compositions, is characterized in that being made up of 2 parts:
Part 1 becomes solution by following proportions: the reducing agent of 0.5 gram ~ 20 grams, the antioxidant of 0.1 gram ~ 8 grams, the nutrient permeation agent of 0.1 gram ~ 10 grams, the wetting agent of 0.1 gram ~ 10 grams, the surfactant of 0.1 gram ~ 5 grams, the stain of 0.5 gram ~ 20 grams, 10-200ml water, acid-base modifier regulates pH7.5 ~ 10;
Part 2 becomes solution by following proportions: the mordant of 0.5 gram ~ 20 grams, the nutrient permeation agent of 0.1 gram ~ 10 grams, the wetting agent of 0.1 gram ~ 10 grams, the surfactant of 0.1 gram ~ 5 grams, 10-200ml water;
Described reducing agent is one or both in cysteine, cysteine hydrochloride, acetylcysteine; Described antioxidant is sodium sulfite, ascorbic acid or sodium ascorbate;
Described nutrient permeation agent is carboxymethyl chitosan, carboxymethyl chitin, hydroxyethyl chitosan, ethoxyl chitin, succinyl-chitosan, carboxymethyl chitosan oligosaccharide, glucosamine hydrochloride, 2-Acetamido-2-deoxy-D-glucose, chitin oligosaccharide (chitinous oligomers), oligochitosan, rhamnetin, Quercetin, total flavone in Sanguis Draconis, astragalus polysaccharides, ginseng polysaccharide, berberine, phellodendrine, glossy privet fruit total saponin;
Described wetting agent is trehalose, glycerol, or other Moisturizing Agent Used in Cosmetic;
Described surfactant is polyoxyethylene lauryl ether, polysorbate, other surfactant used for cosmetic;
Described stain is gallic acid, metagallic acid, or the natural chromogenic agent of other source implant;
Described acid-base modifier is NaOH, Na 2cO 3, triethanolamine or other acid-base modifier used for cosmetic;
Described mordant is ferrous sulfate or zinc chloride.
Main component in hair coloring preparation composition of the present invention is all natural components, to human non-toxic's side effect, uses not irritated; The nutrient permeation agent wherein contained has the effect increasing coloring effect and improve firm coloration degree, and absorb easily through skin and hair, nutrition skin of head, is beneficial to hair growth promoting and black hair, makes hair more healthy; The wetting agent wherein contained, is conducive to increasing the brightness of hair and moist degree.Therefore, natural hair dye compositions of the present invention hair dyeing fast colours, not easily decolours, simultaneously to human non-toxic's side effect, not irritated, simultaneously also nourishing hair and scalp, and moisturizing, hair is more healthy.
Nutrient permeation agent is for the facilitation of Growth of Cells:
The present invention have studied nutrient permeation agent carboxymethyl chitosan, carboxymethyl chitin, hydroxyethyl chitosan, ethoxyl chitin, succinyl-chitosan, carboxymethyl chitosan oligosaccharide, glucosamine hydrochloride, 2-Acetamido-2-deoxy-D-glucose, chitin oligosaccharide (chitinous oligomers), oligochitosan, and rhamnetin, Quercetin, total flavone in Sanguis Draconis, astragalus polysaccharides, ginseng polysaccharide, berberine, phellodendrine, glossy privet fruit total saponin, to the growth of application on human skin epidermal keratinocytes (HaCaT) and normal human melanocytes (NHM), there is significant facilitation.
External use serum-free medium (Invitrogen) cultivates application on human skin epidermal keratinocytes (HaCaT), and cell covers with to monolayer, uses 0.05% trypsinization, makes single cell suspension, and adjustment cell concentration is 5.0 × 10 4/ ml, is inoculated in 96 porocyte culture plates, and every hole adds 100 μ l cell suspension, after cultivating 24h, changes a serum-free medium in cell culture incubator, continues to cultivate 24h.Afterwards by following nutrient permeation agent grouping, change the culture fluid containing Different Nutrition penetrating agent into, if blank group, cultivate 48h, mtt assay measures each group of light absorption in microplate reader 492nm place, calculates cell proliferation rate.
External use M2 culture medium culturing normal human melanocytes (NHM), cell covers with to monolayer, uses 0.05% trypsinization, makes single cell suspension, and adjustment cell concentration is 5.0 × 10 4/ ml, is inoculated in 96 porocyte culture plates, and every hole adds 100 μ l cell suspension, after cultivating 24h, changes a culture fluid in cell culture incubator, continues to cultivate 24h.Afterwards by following nutrient permeation agent grouping, change the culture fluid containing Different Nutrition penetrating agent into, if blank group, cultivate 48h, mtt assay measures each group of light absorption in microplate reader 492nm place, calculates cell proliferation rate.
Nutrient permeation agent is divided into groups:
Blank group: do not add nutrient permeation agent composition
Nutrient permeation agent 1 group: carboxymethyl chitosan 50 μ g/ml,
Nutrient permeation agent 2 groups: carboxymethyl chitin 50 μ g/ml,
Nutrient permeation agent 3 groups: 2-Acetamido-2-deoxy-D-glucose 50 μ g/ml,
Nutrient permeation agent 4 groups: hydroxyethyl chitosan 20 μ g/ml+ carboxymethyl chitosan oligosaccharide 30 μ g/ml,
Nutrient permeation agent 5 groups: glucosamine hydrochloride 10 μ g/ml+ oligochitosan 30 μ g/ml,
Nutrient permeation agent 6 groups: hydroxypropyl chitosan 10 μ g/ml+ succinyl-chitosan 30 μ g/ml,
Nutrient permeation agent 7 groups: carboxymethyl chitin 20 μ g/ml+ chitinous oligomers 30 μ g/ml,
Nutrient permeation agent 8 groups: astragalus polysaccharides 10 μ g/ml+ total flavone in Sanguis Draconis 10 μ g/ml,
Nutrient permeation agent 9 groups: ginseng polysaccharide 10 μ g/ml+ rhamnetin 10 μ g/ml,
Nutrient permeation agent 10 groups: astragalus polysaccharides 10 μ g/ml+ Quercetin 10 μ g/ml,
Nutrient permeation agent 11 groups: astragalus polysaccharides 10 μ g/ml,
Nutrient permeation agent 12 groups: ginseng polysaccharide 10 μ g/ml,
Nutrient permeation agent 13 groups: rhamnetin 10 μ g/ml,
Nutrient permeation agent 14 groups: Quercetin 10 μ g/ml,
Nutrient permeation agent 15 groups: total flavone in Sanguis Draconis 10 μ g/ml,
Nutrient permeation agent 16 groups: berberine 10 μ g/ml,
Nutrient permeation agent 17 groups: phellodendrine 10 μ g/ml,
Nutrient permeation agent 18 groups: glossy privet fruit total saponin 10 μ g/ml.
Cell proliferation rate result after 48h is as follows:
Above-mentioned experimental result shows nutrient permeation agent carboxymethyl chitosan, carboxymethyl chitin, hydroxyethyl chitosan, ethoxyl chitin, succinyl-chitosan, carboxymethyl chitosan oligosaccharide, glucosamine hydrochloride, 2-Acetamido-2-deoxy-D-glucose, chitin oligosaccharide (chitinous oligomers), oligochitosan, and rhamnetin, Quercetin, total flavone in Sanguis Draconis, astragalus polysaccharides, ginseng polysaccharide, berberine, phellodendrine, glossy privet fruit total saponin, to the growth of application on human skin epidermal keratinocytes (HaCaT) and normal human melanocytes (NHM) and propagation, there is significant facilitation.
Preparation is containing the hair nourishing composition of nutrient permeation agent:
Hair nourishing composition 1 containing nutrient permeation agent: take reducing agent cysteine 0.5g, is placed in clean beaker, adds 50ml distilled water and dissolves, add antioxidants ascorbic acid 0.1g, add nutrient permeation agent 0.1g glucosamine hydrochloride, add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, add acid-base modifier NaOH in right amount, regulate pH to 9.5, solution in beaker is poured in plastic bottle, cover tightly, sealing, obtains hair nourishing composition 1.
Hair nourishing composition 2 containing nutrient permeation agent: take reducing agent cysteine hydrochloride 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid 0.1g, add nutrient permeation agent 0.2g (0.1g oligochitosan+0.1g hydroxyethyl chitosan), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, add acid-base modifier NaOH in right amount, regulate pH to 9.5, solution in beaker is poured in plastic bottle, cover tightly, sealing, obtains hair nourishing composition 2.
Hair nourishing composition 3 containing nutrient permeation agent: take reducing agent acetylcysteine 1.5g, is placed in clean beaker, adds 50ml distilled water and dissolves, add antioxidants ascorbic acid 0.1g, add nutrient permeation agent astragalus polysaccharides 0.1g, add wetting agent glycerol 1.0g, add surfactant Polysorbate 0.1g, after stirring and dissolving, add acid-base modifier NaOH in right amount, regulate pH to 9.0, solution in beaker is poured in plastic bottle, cover tightly, sealing, obtains hair nourishing composition 3.
Hair nourishing composition 4 containing nutrient permeation agent: take reducing agent Cys2 .0g, cysteine hydrochloride 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidant sodium sulfite 3.0g, add nutrient permeation agent 0.1g (ginseng polysaccharide 0.05g+ rhamnetin 0.05g), add wetting agent trehalose 2.0g, add surfactant Polysorbate 0.1g, after stirring and dissolving, add acid-base modifier NaOH appropriate, regulate pH to 8.5, the solution in beaker is poured in plastic bottle, covers tightly, sealing, obtains hair nourishing composition 4.
Hair nourishing composition 5 containing nutrient permeation agent: take reducing agent cysteine 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid 0.1g, add nutrient permeation agent 0.15g (total flavone in Sanguis Draconis 0.05g+ Quercetin 0.1g), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, add acid-base modifier NaOH in right amount, regulate pH to 8.0, solution in beaker is poured in plastic bottle, cover tightly, sealing, obtains hair nourishing composition 5.
Hair nourishing composition 6 containing nutrient permeation agent: take reducing agent cysteine 1.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid sodium 0.1g, add nutrient permeation agent 0.55g (carboxymethyl chitosan 0.5g+ berberine 0.05g), add wetting agent trehalose 0.5g, add surfactant polyoxyethylene lauryl ether 0.2g, after stirring and dissolving, add acid-base modifier triethanolamine in right amount, regulate pH to 7.5, solution in beaker is poured in plastic bottle, cover tightly, sealing, obtains hair nourishing composition 6.
Hair nourishing composition 7 containing nutrient permeation agent: take reducing agent cysteine 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid 0.1g, add nutrient permeation agent 0.1g (phellodendrine 0.02g+ Quercetin 0.06g+ glossy privet fruit total saponin 0.02g), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, add acid-base modifier NaOH in right amount, regulate pH to 9.5, solution in beaker is poured in plastic bottle, cover tightly, sealing, obtains hair nourishing composition 7.
70 poliosis experimenters, 30 examples in 2 years poliosis time, 30 examples of 2 ~ 4 years, 10 examples of more than 4 years.70 poliosis experimenters are divided into 7 groups at random, often organize 10, often organize poliosis experimenter correspondence and use the above-mentioned hair nourishing composition a kind containing nutrient permeation agent, hair nourishing composition within every two days, is used to smear root of hair and scalp 1 time, each 30min, afterwash hair, long run test 30 days, observes the improvement of above-mentioned hair nourishing composition 1 ~ 7 pair of poliosis containing nutrient permeation agent and control effects and the zest to scalp.Effect standard is divided into: effectively, blackening hair more than 20%, and poliosis is controlled; Invalid, poliosis does not substantially improve and alleviates.Result of the test is as following table:
Hair nourishing composition is to the improvement of poliosis and control effects and the irritation test result to scalp
Effectively Invalid Nonirritant Irritant
Containing the hair nourishing composition 1 of nutrient permeation agent 9 1 10 0
Containing the hair nourishing composition 2 of nutrient permeation agent 9 1 10 0
Containing the hair nourishing composition 3 of nutrient permeation agent 8 2 10 0
Containing the hair nourishing composition 4 of nutrient permeation agent 8 2 10 0
Containing the hair nourishing composition 5 of nutrient permeation agent 9 1 10 0
Containing the hair nourishing composition 6 of nutrient permeation agent 7 3 10 0
Containing the hair nourishing composition 7 of nutrient permeation agent 9 1 10 0
Above-mentioned result of the test shows, the hair nourishing composition containing nutrient permeation agent of the present invention is applicable to hair and the scalp of poliosis crowd, without anaphylaxis, have no stimulation, hair nourishing composition can infiltrate rapidly root of hair makes skin absorb, and hair blackening is effective, instant effect, simple and easy to do.
According to above-mentioned result of the test, invention has been the preparation of natural hair dye.Natural hair dye of the present invention is the compositions comprising part 1 and part 2, part 1 is made up of reducing agent, antioxidant, nutrient permeation agent, wetting agent, surfactant, stain, acid-base modifier and water, part 2 is made up of mordant, nutrient permeation agent, wetting agent, surfactant and water, is specifically implemented as follows.
Detailed description of the invention
The preparation of embodiment 1 hair coloring preparation composition:
Part 1: take reducing agent cysteine hydrochloride 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid 0.1g, add nutrient permeation agent 0.1g acetylglucosamine, add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, add stain gallic acid 0.5g, after stirring and dissolving, add acid-base modifier NaOH appropriate, regulate pH to 9.5, the solution in beaker is poured in plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 1.
Part 2: take mordant ferrous sulfate 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add nutrient permeation agent 0.1g glucosamine hydrochloride, add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, the solution in beaker is poured in another plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 2.
The preparation of embodiment 2 hair coloring preparation composition:
Part 1: take reducing agent acetylcysteine 5.0g, cysteine hydrochloride 2.5g, be placed in clean beaker, add 50ml distilled water and dissolve, add antioxidant sodium sulfite 3.0g, add nutrient permeation agent 4g glucosamine hydrochloride, add wetting agent glycerol 5.0g, add surfactant polyoxyethylene lauryl ether 1.5g, add stain metagallic acid 7.5g, after stirring and dissolving, add acid-base modifier Na 2cO 3, regulate pH to 7.5, pour in plastic bottle, cover tightly the solution in beaker, sealing, obtains hair coloring preparation composition part 1.
Part 2: take mordant zinc chloride 7.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add nutrient permeation agent 4g glucosamine hydrochloride, add wetting agent glycerol 2.0g, add surfactant polyoxyethylene lauryl ether 1.5g, after stirring and dissolving, the solution in beaker is poured in another plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 2.
The preparation of embodiment 3 hair coloring preparation composition:
Part 1: take reducing agent cysteine hydrochloride 4.0g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid sodium 2.0g, add nutrient permeation agent 2g (1g chitin oligosaccharide+1g hydroxyethyl chitosan), add wetting agent glycerol 3.0g, add surfactant moon polysorbate 1.0g, add stain gallic acid 4g, add acid-base modifier triethanolamine, regulate pH to 9, solution in beaker is poured in plastic bottle, cover tightly, sealing, obtains hair coloring preparation composition part 1.
Part 2: take mordant ferrous sulfate 2.0g, be placed in clean beaker, add 50ml distilled water to dissolve, add nutrient permeation agent 2g (1g chitin oligosaccharide+1g hydroxyethyl chitosan), add wetting agent glycerol 2.0g, add surfactant polyoxyethylene lauryl ether 1.0g, after stirring and dissolving, the solution in beaker is poured in another plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 2.
The preparation of embodiment 4 hair coloring preparation composition:
Part 1: take reducing agent cysteine 1.5g, is placed in clean beaker, adds 50ml distilled water and dissolves, add antioxidants ascorbic acid 0.5g, add nutrient permeation agent astragalus polysaccharides 0.2g, add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, add stain gallic acid 0.5g, after stirring and dissolving, add acid-base modifier NaOH appropriate, regulate pH to 9.0, the solution in beaker is poured in plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 1.
Part 2: take mordant ferrous sulfate 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add nutrient permeation agent astragalus polysaccharides 0.2g, add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, the solution in beaker is poured in another plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 2.
The preparation of embodiment 5 hair coloring preparation composition:
Part 1: take reducing agent Cys2 .5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidant sodium sulfite 3.0g, add nutrient permeation agent 1.0g (0.5g ginseng polysaccharide+0.5g rhamnetin), add wetting agent trehalose 2.0g, add surfactant Polysorbate 0.5g, add stain gallic acid 2.5g, after stirring and dissolving, add acid-base modifier triethanolamine appropriate, regulate pH to 8.5, the solution in beaker is poured in plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 1.
Part 2: take mordant ferrous sulfate 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add nutrient permeation agent 1.0g (0.5g ginseng polysaccharide+0.5g rhamnetin), add wetting agent trehalose 2.0g, add surfactant Polysorbate 0.1g, after stirring and dissolving, the solution in beaker is poured in another plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 2.
The preparation of embodiment 6 hair coloring preparation composition:
Part 1: take reducing agent cysteine hydrochloride 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid 0.1g, add nutrient permeation agent 0.15g (total flavone in Sanguis Draconis 0.05g+ Quercetin 0.1g), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, add stain gallic acid 0.5g, after stirring and dissolving, add acid-base modifier NaOH appropriate, regulate pH to 10, the solution in beaker is poured in plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 1.
Part 2: take mordant ferrous sulfate 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add nutrient permeation agent 0.15g (total flavone in Sanguis Draconis 0.05g+ Quercetin 0.1g), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, the solution in beaker is poured in another plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 2.
The preparation of embodiment 7 hair coloring preparation composition:
Part 1: take reducing agent cysteine 1.0g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid 0.1g, add nutrient permeation agent 0.5g (0.2g astragalus polysaccharides+0.2g total flavone in Sanguis Draconis+0.1g phellodendrine), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, add stain gallic acid 0.5g, after stirring and dissolving, add acid-base modifier NaOH appropriate, regulate pH to 9.5, the solution in beaker is poured in plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 1.
Part 2: take mordant ferrous sulfate 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add nutrient permeation agent 0.5g (0.2g astragalus polysaccharides+0.2g total flavone in Sanguis Draconis+0.1g phellodendrine), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, the solution in beaker is poured in another plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 2.
The preparation of embodiment 8 hair coloring preparation composition:
Part 1: take reducing agent cysteine 5.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid 2.5g, add nutrient permeation agent 1.0g (0.5g ginseng polysaccharide+0.5g berberine), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, add stain gallic acid 0.5g, after stirring and dissolving, add acid-base modifier Na 2cO 3in right amount, regulate pH to 8.5, pour in plastic bottle, cover tightly the solution in beaker, sealing, obtains hair coloring preparation composition part 1.
Part 2: take mordant ferrous sulfate 0.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add nutrient permeation agent 1.0g (0.5g ginseng polysaccharide+0.5g berberine), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, the solution in beaker is poured in another plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 2.
The preparation of embodiment 9 hair coloring preparation composition:
Part 1: take reducing agent cysteine 7.5g, be placed in clean beaker, add 50ml distilled water to dissolve, add antioxidants ascorbic acid 3.0g, add nutrient permeation agent 1.5g (0.5g astragalus polysaccharides+0.5g Quercetin+0.5g glossy privet fruit total saponin), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, add stain gallic acid 5.0g, after stirring and dissolving, add acid-base modifier Na 2cO 3in right amount, regulate pH to 9.5, pour in plastic bottle, cover tightly the solution in beaker, sealing, obtains hair coloring preparation composition part 1.
Part 2: take mordant ferrous sulfate 5.0g, be placed in clean beaker, add 50ml distilled water to dissolve, add nutrient permeation agent 1.5g (0.5g astragalus polysaccharides+0.5g Quercetin+0.5g glossy privet fruit total saponin), add wetting agent trehalose 0.1g, add surfactant Polysorbate 0.1g, after stirring and dissolving, the solution in beaker is poured in another plastic bottle, covers tightly, sealing, obtains hair coloring preparation composition part 2.
In above-described embodiment 1 ~ 9, natural hair dye compositions of the present invention is made up of 2 parts, part 1 and part 2.
Part 1 becomes solution by following proportions: the reducing agent of 0.5 gram ~ 20 grams, the antioxidant of 0.1 gram ~ 8 grams, the nutrient permeation agent of 0.1 gram ~ 10 grams, the wetting agent of 0.1 gram ~ 10 grams, the surfactant of 0.1 gram ~ 5 grams, the stain of 0.5 gram ~ 20 grams, 100ml water, acid-base modifier regulates pH7.5 ~ 10;
Part 2 becomes solution by following proportions: the mordant of 0.5 gram ~ 20 grams, the nutrient permeation agent of 0.1 gram ~ 10 grams, the wetting agent of 0.1 gram ~ 10 grams, the surfactant of 0.1 gram ~ 5 grams, 100ml water;
Described reducing agent is one or both in cysteine, cysteine hydrochloride, acetylcysteine; Described antioxidant is sodium sulfite, ascorbic acid or sodium ascorbate;
Described nutrient permeation agent is carboxymethyl chitosan, carboxymethyl chitin, hydroxyethyl chitosan, ethoxyl chitin, succinyl-chitosan, carboxymethyl chitosan oligosaccharide, glucosamine hydrochloride, 2-Acetamido-2-deoxy-D-glucose, chitin oligosaccharide (chitinous oligomers), oligochitosan, rhamnetin, Quercetin, total flavone in Sanguis Draconis, astragalus polysaccharides, ginseng polysaccharide, berberine, phellodendrine, glossy privet fruit total saponin;
Described wetting agent is trehalose, glycerol, or other Moisturizing Agent Used in Cosmetic;
Described surfactant is polyoxyethylene lauryl ether, polysorbate, other surfactant used for cosmetic;
Described stain is gallic acid, metagallic acid, or the natural chromogenic agent of other source implant;
Described acid-base modifier is NaOH, Na 2cO 3, triethanolamine or other acid-base modifier used for cosmetic;
Described mordant is ferrous sulfate or zinc chloride.
Part 1 in hair coloring preparation composition of the present invention and part 2 all can be now with the current.
When using hair coloring preparation composition of the present invention to have hair dyed, first the part 1 of hair coloring preparation composition is evenly coated on hair, places after 5 ~ 60 minutes, after washing hair, remove unnecessary hair dye; Again part 2 is evenly coated on hair, places 5 ~ 30 minutes, after washing hair, remove unnecessary hair dye, desirable Color can be obtained.
Heat in hair dye, coloring effect is better.
Main component in hair coloring preparation composition of the present invention is all natural components, to human non-toxic's side effect, uses not irritated; The nutrient permeation agent wherein contained has the effect increasing coloring effect and improve firm coloration degree, and absorb easily through skin and hair, nutrition skin of head, is beneficial to hair growth promoting and black hair, makes hair more healthy; The wetting agent wherein contained, is conducive to increasing the brightness of hair and moist degree.Therefore, natural hair dye compositions of the present invention hair dyeing fast colours, not easily decolours, simultaneously to human non-toxic's side effect, not irritated, simultaneously also nourishing hair and scalp, and moisturizing, hair is more healthy.

Claims (1)

1. a natural hair dye compositions, is characterized in that being made up of 2 parts:
Part 1 becomes solution by following proportions: the reducing agent of 0.5 gram ~ 20 grams, the antioxidant of 0.1 gram ~ 8 grams, the nutrient permeation agent of 0.1 gram ~ 10 grams, the wetting agent of 0.1 gram ~ 10 grams, the surfactant of 0.1 gram ~ 5 grams, the stain of 0.5 gram ~ 20 grams, 10-200ml water, acid-base modifier regulates pH7.5 ~ 10;
Part 2 becomes solution by following proportions: the mordant of 0.5 gram ~ 20 grams, the nutrient permeation agent of 0.1 gram ~ 10 grams, the wetting agent of 0.1 gram ~ 10 grams, the surfactant of 0.1 gram ~ 5 grams, 10-200ml water;
Described reducing agent is one or both in cysteine, cysteine hydrochloride, acetylcysteine; Described antioxidant is sodium sulfite, ascorbic acid or sodium ascorbate;
Described nutrient permeation agent is carboxymethyl chitosan, carboxymethyl chitin, hydroxyethyl chitosan, ethoxyl chitin, succinyl-chitosan, carboxymethyl chitosan oligosaccharide, glucosamine hydrochloride, 2-Acetamido-2-deoxy-D-glucose, chitin oligosaccharide (chitinous oligomers), oligochitosan, rhamnetin, Quercetin, total flavone in Sanguis Draconis, astragalus polysaccharides, ginseng polysaccharide, berberine, phellodendrine, glossy privet fruit total saponin;
Described wetting agent is trehalose, glycerol, or other Moisturizing Agent Used in Cosmetic;
Described surfactant is polyoxyethylene lauryl ether, polysorbate, other surfactant used for cosmetic;
Described stain is gallic acid, metagallic acid, or the natural chromogenic agent of other source implant;
Described acid-base modifier is NaOH, Na 2cO 3, triethanolamine or other acid-base modifier used for cosmetic;
Described mordant is ferrous sulfate or zinc chloride.
CN201510430921.6A 2015-07-21 2015-07-21 Natural hair dye composition Pending CN104970989A (en)

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CN105596228A (en) * 2015-12-28 2016-05-25 肇庆迪彩日化科技有限公司 Oxidized type dyeing composition
CN108078905A (en) * 2018-02-08 2018-05-29 陕西莹润生物医药科技有限公司 Anticreep shampoo for men only and its processing method
AU2021240202A1 (en) * 2021-07-08 2023-02-02 Korea Advanced Institute Of Science And Technology A composition for developing hair color comprising polyphenol

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105596228A (en) * 2015-12-28 2016-05-25 肇庆迪彩日化科技有限公司 Oxidized type dyeing composition
CN105596228B (en) * 2015-12-28 2018-11-02 肇庆迪彩日化科技有限公司 A kind of oxidized form colouring compositions
CN108078905A (en) * 2018-02-08 2018-05-29 陕西莹润生物医药科技有限公司 Anticreep shampoo for men only and its processing method
CN108078905B (en) * 2018-02-08 2019-12-13 西安蓝风生物科技有限公司 special anti-hair-loss shampoo for men and processing method thereof
AU2021240202A1 (en) * 2021-07-08 2023-02-02 Korea Advanced Institute Of Science And Technology A composition for developing hair color comprising polyphenol
AU2021240202B2 (en) * 2021-07-08 2023-07-06 Korea Advanced Institute Of Science And Technology A composition for developing hair color comprising polyphenol

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