CN107988589B - 一种纳米金属复合物及其制备方法 - Google Patents
一种纳米金属复合物及其制备方法 Download PDFInfo
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- CN107988589B CN107988589B CN201711183376.0A CN201711183376A CN107988589B CN 107988589 B CN107988589 B CN 107988589B CN 201711183376 A CN201711183376 A CN 201711183376A CN 107988589 B CN107988589 B CN 107988589B
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- base material
- nano
- coupling agent
- silane coupling
- nano metal
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- 150000002736 metal compounds Chemical class 0.000 title abstract description 28
- 238000002360 preparation method Methods 0.000 title abstract description 17
- 239000000463 material Substances 0.000 claims abstract description 52
- 239000002184 metal Substances 0.000 claims abstract description 47
- 229910052751 metal Inorganic materials 0.000 claims abstract description 47
- 239000006087 Silane Coupling Agent Substances 0.000 claims abstract description 38
- 229920000642 polymer Polymers 0.000 claims abstract description 33
- 239000000758 substrate Substances 0.000 claims abstract description 25
- 239000002905 metal composite material Substances 0.000 claims abstract description 22
- 239000000178 monomer Substances 0.000 claims abstract description 22
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims abstract description 22
- 238000000034 method Methods 0.000 claims abstract description 21
- 229920002554 vinyl polymer Polymers 0.000 claims abstract description 21
- 238000005342 ion exchange Methods 0.000 claims abstract description 19
- 238000010526 radical polymerization reaction Methods 0.000 claims abstract description 18
- 238000007747 plating Methods 0.000 claims abstract description 13
- 239000003999 initiator Substances 0.000 claims abstract description 12
- 230000008021 deposition Effects 0.000 claims abstract description 11
- 230000004048 modification Effects 0.000 claims abstract description 8
- 238000012986 modification Methods 0.000 claims abstract description 8
- 238000006116 polymerization reaction Methods 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 4
- 150000003254 radicals Chemical class 0.000 claims abstract description 4
- 229920002379 silicone rubber Polymers 0.000 claims description 35
- 239000000243 solution Substances 0.000 claims description 33
- 238000006243 chemical reaction Methods 0.000 claims description 12
- 239000010931 gold Substances 0.000 claims description 12
- 229910052737 gold Inorganic materials 0.000 claims description 12
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 10
- 150000002500 ions Chemical class 0.000 claims description 9
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims description 8
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 claims description 4
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-M acrylate group Chemical group C(C=C)(=O)[O-] NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 4
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims description 4
- NKSJNEHGWDZZQF-UHFFFAOYSA-N ethenyl(trimethoxy)silane Chemical group CO[Si](OC)(OC)C=C NKSJNEHGWDZZQF-UHFFFAOYSA-N 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 claims description 3
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 claims description 3
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- -1 maleic anhydride ester Chemical class 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- 238000010306 acid treatment Methods 0.000 claims description 2
- 238000009832 plasma treatment Methods 0.000 claims description 2
- 101150003085 Pdcl gene Proteins 0.000 claims 2
- 239000002245 particle Substances 0.000 claims 1
- 230000035484 reaction time Effects 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 abstract description 9
- 230000009257 reactivity Effects 0.000 abstract 1
- 239000002585 base Substances 0.000 description 27
- 239000002923 metal particle Substances 0.000 description 13
- 238000000151 deposition Methods 0.000 description 12
- 239000004945 silicone rubber Substances 0.000 description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 8
- 230000003197 catalytic effect Effects 0.000 description 8
- 238000004140 cleaning Methods 0.000 description 8
- 238000005406 washing Methods 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000008367 deionised water Substances 0.000 description 7
- 229910021641 deionized water Inorganic materials 0.000 description 7
- 230000009471 action Effects 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- 238000001035 drying Methods 0.000 description 4
- 238000004506 ultrasonic cleaning Methods 0.000 description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 239000002105 nanoparticle Substances 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 2
- 238000001000 micrograph Methods 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 238000001069 Raman spectroscopy Methods 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- OFLYIWITHZJFLS-UHFFFAOYSA-N [Si].[Au] Chemical compound [Si].[Au] OFLYIWITHZJFLS-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000005389 magnetism Effects 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 238000006011 modification reaction Methods 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000007348 radical reaction Methods 0.000 description 1
- 238000001878 scanning electron micrograph Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/18—Pretreatment of the material to be coated
- C23C18/20—Pretreatment of the material to be coated of organic surfaces, e.g. resins
- C23C18/2006—Pretreatment of the material to be coated of organic surfaces, e.g. resins by other methods than those of C23C18/22 - C23C18/30
- C23C18/2046—Pretreatment of the material to be coated of organic surfaces, e.g. resins by other methods than those of C23C18/22 - C23C18/30 by chemical pretreatment
- C23C18/2053—Pretreatment of the material to be coated of organic surfaces, e.g. resins by other methods than those of C23C18/22 - C23C18/30 by chemical pretreatment only one step pretreatment
- C23C18/2066—Use of organic or inorganic compounds other than metals, e.g. activation, sensitisation with polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F283/00—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G
- C08F283/12—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G on to polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/36—After-treatment
- C08J9/40—Impregnation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/36—After-treatment
- C08J9/40—Impregnation
- C08J9/405—Impregnation with polymerisable compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2383/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
- C08J2383/04—Polysiloxanes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemically Coating (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
Abstract
Description
Claims (7)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711183376.0A CN107988589B (zh) | 2017-11-23 | 2017-11-23 | 一种纳米金属复合物及其制备方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711183376.0A CN107988589B (zh) | 2017-11-23 | 2017-11-23 | 一种纳米金属复合物及其制备方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107988589A CN107988589A (zh) | 2018-05-04 |
| CN107988589B true CN107988589B (zh) | 2019-12-17 |
Family
ID=62032139
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711183376.0A Active CN107988589B (zh) | 2017-11-23 | 2017-11-23 | 一种纳米金属复合物及其制备方法 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107988589B (zh) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108727937B (zh) * | 2018-05-22 | 2020-01-14 | 浙江大学 | 一种高强防污减阻水凝胶软涂层的制备方法及应用 |
| CN109364994A (zh) * | 2018-09-10 | 2019-02-22 | 深圳大学 | 负载型光催化剂及其应用 |
| CN111501029A (zh) * | 2020-04-21 | 2020-08-07 | 华东理工大学 | 带有图案化金属层的硅基材的制造方法 |
| CN112048097B (zh) * | 2020-08-24 | 2021-10-22 | 华南农业大学 | 一种具有催化功能的金属负载多孔聚合物泡沫及其制备方法和应用 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101381437B (zh) * | 2008-10-15 | 2011-05-11 | 华南理工大学 | 一种具有壳-核结构的高选择性吸湿剂的制备方法 |
| CN102168260B (zh) * | 2011-04-07 | 2012-09-05 | 西安交通大学 | 钯电极型离子聚合物-金属复合材料的制备工艺 |
| CN107303483A (zh) * | 2016-04-25 | 2017-10-31 | 武汉理工大学 | 多重有机修饰磁性复合物及其制备方法和在废水处理中的应用 |
| CN106282979B (zh) * | 2016-09-18 | 2019-12-27 | 遂宁迪印科技有限公司 | 一种有机聚合物基材的表面修饰方法 |
| CN106758173B (zh) * | 2016-11-25 | 2019-03-12 | 深圳大学 | 一种金属修饰的碳纤维及其制备方法 |
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2017
- 2017-11-23 CN CN201711183376.0A patent/CN107988589B/zh active Active
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| Publication number | Publication date |
|---|---|
| CN107988589A (zh) | 2018-05-04 |
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Application publication date: 20180504 Assignee: Shenzhen Sunny Advertising Logo Co.,Ltd. Assignor: SHENZHEN University Contract record no.: X2022980024786 Denomination of invention: A nano metal composite and its preparation method Granted publication date: 20191217 License type: Common License Record date: 20221206 Application publication date: 20180504 Assignee: Shuangyu Logo Design (Shenzhen) Co.,Ltd. Assignor: SHENZHEN University Contract record no.: X2022980024843 Denomination of invention: A nano metal composite and its preparation method Granted publication date: 20191217 License type: Common License Record date: 20221206 Application publication date: 20180504 Assignee: Shenzhen Maiwo Innovation Technology Co.,Ltd. Assignor: SHENZHEN University Contract record no.: X2022980024758 Denomination of invention: A nano metal composite and its preparation method Granted publication date: 20191217 License type: Common License Record date: 20221207 Application publication date: 20180504 Assignee: Shenzhen Orange Product Logo Design Engineering Co.,Ltd. Assignor: SHENZHEN University Contract record no.: X2022980024781 Denomination of invention: A nano metal composite and its preparation method Granted publication date: 20191217 License type: Common License Record date: 20221206 Application publication date: 20180504 Assignee: Shenzhen Huahong Testing Technology Co.,Ltd. Assignor: SHENZHEN University Contract record no.: X2022980024778 Denomination of invention: A nano metal composite and its preparation method Granted publication date: 20191217 License type: Common License Record date: 20221206 Application publication date: 20180504 Assignee: Shenzhen Bangqi Technology Co.,Ltd. Assignor: SHENZHEN University Contract record no.: X2022980024743 Denomination of invention: A nano metal composite and its preparation method Granted publication date: 20191217 License type: Common License Record date: 20221207 |
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Application publication date: 20180504 Assignee: Shenzhen Standard Technical Service Co.,Ltd. Assignor: SHENZHEN University Contract record no.: X2022980025053 Denomination of invention: A nano metal composite and its preparation method Granted publication date: 20191217 License type: Common License Record date: 20221208 Application publication date: 20180504 Assignee: Ruian Design (Shenzhen) Co.,Ltd. Assignor: SHENZHEN University Contract record no.: X2022980025029 Denomination of invention: A nano metal composite and its preparation method Granted publication date: 20191217 License type: Common License Record date: 20221208 Application publication date: 20180504 Assignee: Shenzhen Pitch Technology Co.,Ltd. Assignor: SHENZHEN University Contract record no.: X2022980026677 Denomination of invention: A nano metal composite and its preparation method Granted publication date: 20191217 License type: Common License Record date: 20221210 |
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