CN107982167A - Clearly not de- adornment element face is white for a kind of low oil content - Google Patents
Clearly not de- adornment element face is white for a kind of low oil content Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/892—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a hydroxy group, e.g. dimethiconol
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
Do not take off the plain face frost of adornment clearly the invention discloses a kind of low oil content, which includes oiliness emollient, polyalcohol moisturizer, skin conditioning agent, polymeric rheology conditioning agent, titanium dioxide class covering agent, synergist, preservative and essence.Oil content is low compared with prior art for plain face frost prepared by the present invention, has contained little or no emulsifying agent；It is strong that adornment ability is held with good water resistant film forming, it is not easy to de- adornment；And there is good stability, be adapted to produce in enormous quantities.
Description
Technical field
The invention belongs to cosmetic field, the present invention relates to a kind of low oil content clearly the formula of the plain face frost of not de- adornment and
Its production method.
Background technology
The appearance of BB frosts and foundation cream, is an innovation of cosmetic industry.BB frost foundation emulsion collection skin cares, color make-up in one,
It is easy to use, it is once fashionable for a time.But such usual quality of product is thick and heavy, silty quasi-grease constituents content is high, easily stifled
Fill in pore, cutaneous malignancies.
Plain face frost is the category newly risen in recent years, belongs to face cream but has than common face cream and significantly highlights whitening
Effect, wherein main component can be used as physical sunscreen agent, such as Chinese patent CN201611114201.X to disclose a kind of treasure
Pearl element face frost and preparation method thereof, the element face frost are by isononyl isononanoate, four ester of pentaerythrite, boron nitride, pearl powder, emulsification
Agent, thickener, glycerine, starch ocentyl succinic aluminium, bismoclite, extracting solution, pearl extracting solution, Iceland's lichens carry in one's early teens
Thing, nutgrass flatsedge extract, hydroxy-proline ester silanol, preservative and deionized water is taken to be made.In the plain face frost formula of the invention,
Pearl powder, pearl extracting solution, Katsumadai seed extract and Iceland's lichens extract these types active ingredient are each playing effect
Meanwhile and play complementary and synergistic effect in terms of conditioning skin, bright color.The preparation of the invention pearl essence face frost
Technique matches somebody with somebody method using cold, economical, environmentally friendly, easy to operate.But formula is still traditional oil packed water formulation body described in the patent
System, oil content is higher, and skin sense sticks greasy partially.
And for example, Chinese patent CN201610778719.7 discloses a kind of water resistant and exempts from plain face frost and preparation method thereof of removing ornaments and formal dress,
The element face frost is made of grease, emulsifying agent, rheology control agent, moisturizer, titanium dioxide, active ingredient and its deionized water.Should
Its water-resistance is good compared with prior art for the prepared plain face frost of invention, holds adornment time length, naturally screening flaw whitening, institute in the present invention
With the appropriate collocation of grease and powder, improve and powder is floated after market product is used, easily rub the phenomenon of mud with the hands.But the invention formula
Still the problems such as containing substantial amounts of lanolin and Dormant oils, easily blocking pore, trigger acne.
For another example, Chinese patent CN201510274113.5 discloses the plain face frost and its system of a kind of essence lotion containing high concentration
Preparation Method, element face frost include following component (weight percentage)：Essence lotion 10.0%-30.0%, foundation emulsion
70.0%-90.0%；Wherein, its formula of the essence lotion includes butanediol, polyglutamic acid, trehalose, sodium acrylate/propylene
Acyl dimethyltaurine sodium copolymer, isohexadecane, Polyoxyethylene Sorbitan Monooleate, cyclopenta siloxanes (and) dimethyl silicone polymer
Alcohol, wing seed Moringa seed extract etc.；Its formula of the foundation emulsion includes physics whitening agent, colouring agent, cyclopenta siloxanes (and)
Trimethyl silicane alkoxy esters of silicon acis, sorbitan sesquioleate, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymerics
Thing, Magnesiumaluminumsilicate, xanthans, propane diols etc..The patent water content is high, but still with the low HLB such as sorbitan sesquioleate
The surfactant of value is primary emulsion, which is water-in-oil emulsifier, and clearly degree is still inadequate for system.
So preparing one kind has extraordinary whitening covering power, and skin sense is clearly not glutinous greasy, and with fine
The plain face frost of stability is always the target that those skilled in the art pursue.
The content of the invention
The present invention is in order to make up prior art deficiency, there is provided a kind of low oil content clearly the plain face frost formula of not de- adornment and its
Production method.The formula that this patent provides, oil content is low, has contained little or no emulsifying agent, skin sense is salubrious, while holds adornment
Ability is strong, it is not easy to which de- adornment, moisture-retaining capacity is strong, and has good stability, is very suitable for light make-up crowd and uses.
In order to solve the above technical problems, the present invention adopts the following technical scheme that realization：
On the one hand, the present invention provides a kind of low oil content, clearly not de- adornment element face is white, it is characterised in that：Including：Oiliness
Emollient, polyalcohol moisturizer, skin conditioning agent, polymeric rheology conditioning agent, titanium dioxide class covering agent, preservative and essence.
Further, clearly not de- adornment element face frost further includes synergist to the low oil content：The synergist is selected from
One or more in caffeic acid, papain and vanillic aldehyde.
Preferably, the synergist is selected from the one or more of caffeic acid and papain.
It is highly preferred that the synergist is caffeic acid.
For above-mentioned low oil content clearly in not de- adornment element face frost, the oiliness emollient can be selected from vegetable oil, artificial oil
One or more in fat, silicone oil quasi-grease and induction biosynthesis wax.
Wherein, the Synthetic Oil can be selected from C12-15 alcohol benzoic ethers, myristyl alcohol myristinate, three hydroxyl first
Three isostearate of base propane, pentaerythritol tetraoctyl stearate, caprylic/capric triglyceride, Parleam, palmitic acid
Ethylhexyl, two octanoic acids of butanediol/dicaprate, lauric alcohol-caprylate/decylate, propylene/dicaprate,
One kind in cetanol ethylhexoate, neopentyl glycol dicaprylate/dicaprate, isononyl isononanoate and isopropyl palmitate
It is or several.
Preferably, the Synthetic Oil is salubrious inirritative grease, as isononyl isononanoate, the octanoic acid of butanediol two/
One in dicaprate, lauric alcohol-caprylate/decylate, cetanol ethylhexoate and propylene/dicaprate
Kind is several.
Wherein, the silicone oil quasi-grease can be selected from dimethyl silicone polymer, cyclomethicone, poly dimethyl
One or more in silica alkanol, alkyl dimethicone and silicone elastomer.
Preferably, the silicone oil quasi-grease is less than the dimethyl silicone polymer and ring poly dimethyl silicon of 10cst for viscosity
One or more in oxygen alkane.
It is further preferred that above-mentioned silicone oil quasi-grease can be selected from ring five dimethyl silicone polymer, six poly dimethyl silicon of ring
One or more in oxygen alkane and dimethiconol.
Above-mentioned low oil content is clearly in not de- adornment element face frost, the polyalcohol moisturizer can be selected from glycerine, propane diols,
One or more in 1,3 propane diols, butanediol, dipropylene glycol, D-sorbite and Natrulon H-10.
Preferably, the polyalcohol moisturizer is selected from the one or more in 1,3 propane diols, glycerine and Natrulon H-10.
For above-mentioned low oil content clearly in not de- adornment element face frost, the skin conditioning agent can be selected from allantoin, panthenol, sea
One or more in algae sugar, glycine betaine, glycosphingolipids, phytosterin ester and beta glucan.
Above-mentioned skin conditioning agent act as moisturizing, whitening, crease-resistant, anti-inflammatory are releived, anti-oxidant and except acne etc..
Above-mentioned low oil content is clearly in not de- adornment element face frost, the polymeric rheology conditioning agent can be selected from carbomer,
Carbomer sodium, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, acrylic acid (ester) analog copolymer, polypropylene
Sour sodium, polyacrylate cross-linked polymer -6, ammonium acryloyl taurate/VP copolymer, Sodium Polyacrylate graft starch,
Polypropylene acyl group dimethyltaurine sodium, hydrolysis Scleroglucan, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymerization
Thing, sodium acrylate/sodium acryloyldimethyl taurate copolymers, Sodium Polyacrylate powder, Sodium Polyacrylate/C18-21 alkane/ten
The mixtures of three alkanol polyethers -6, sodium acrylate/sodium acryloyldimethyl taurate copolymers, isohexadecane/polysorbate -
One or more in the mixture and hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers of 80/ water.
Wherein, the macromolecule described in above-mentioned polymeric rheology conditioning agent can be single pulverulence, can also divide
It is dispersed in liquid fat and a small amount of emulsifying agent and uses.
Above-mentioned low oil content is clearly in not de- adornment element face frost, the titanium dioxide class covering agent for titanium dioxide slurry and/or
Titanium dioxide powder.
Preferably, the titanium dioxide class covering agent is the titanium dioxide and surface fluorination of triethoxy octyl group siloxane treated
One or more in the titanium dioxide slurry of processing.
It is further preferred that above-mentioned titanium dioxide class covering agent is the titanium dioxide slurry of surface fluorination processing.
For above-mentioned low oil content clearly in not de- adornment element face frost, the preservative is usually used in cosmetic field appoints
What preservative, be selected from methyl hydroxybenzoate, Nipasol, Phenoxyethanol, 1,2- hexylene glycols, Sensiva SC50, Chlorphenesin,
One or more in DMDM hydantoin and iodine propilolic alcohol butyl mephenesin Carbamate.
Clearly in not de- adornment element face frost, the essence can be that cosmetic field is usually used appoints above-mentioned low oil content
What essence, such as liquid essence, its odor type can be flowers and fruits composite fragrant.
In some embodiments, use of the above-mentioned raw materials in low oil content provided by the invention clearly not de- adornment element face frost
Measure and be：In parts by weight：0.0001-50 parts of oiliness emollient, 0.0001-50 parts of polyalcohol moisturizer, skin conditioning agent
0.0001-10 parts, 0.0001-10 parts of polymeric rheology conditioning agent, 0.0001-20 parts of titanium dioxide class covering agent, preservative
0.0001-10 parts, 0.001-1 parts of essence, 0.001-5 parts of synergist.
In some preferred embodiments, clearly not de- adornment element face is white in low oil content provided by the invention for above-mentioned raw materials
In dosage be：In parts by weight：0.1-40 parts of oiliness emollient, 0.1-40 parts of polyalcohol moisturizer, skin conditioning agent
0.1-9 parts, 0.1-9 parts of polymeric rheology conditioning agent, 0.1-15 parts of titanium dioxide class covering agent, 0.1-9 parts of preservative, essence 0.1-
0.9 part, 0.01-4 parts of synergist.
It is highly preferred that dosage of the above-mentioned raw materials in low oil content provided by the invention clearly not de- adornment element face frost is：Press
According to parts by weight meter：1-30 parts of oiliness emollient, 1-30 parts of polyalcohol moisturizer, 1-5 parts of skin conditioning agent, polymeric rheology are adjusted
1-5 parts of agent, 1-10 parts of titanium dioxide class covering agent, 1-5 parts of preservative, 0.3-0.6 parts of essence, 0.1-3 parts of synergist.
It is further preferred that dosage of the above-mentioned raw materials in low oil content provided by the invention clearly not de- adornment element face frost
For：In parts by weight：10-20 parts of oiliness emollient, 10-20 parts of polyalcohol moisturizer, 3-4 parts of skin conditioning agent, macromolecule
3-4 parts of rheology control agent, 4-6 parts of titanium dioxide class covering agent, 4-5 parts of preservative, 0.4-0.5 parts of essence, 0.1-1 parts of synergist.
Compared with prior art, the present invention the present invention has following advantage：
(1) plain face frost oil content provided by the invention is low, has contained little or no emulsifying agent；
(2) plain face frost skin sense provided by the invention is salubrious, while it is strong to hold adornment ability, it is not easy to which de- adornment, moisture-retaining capacity is strong, non-
Often it is adapted to light make-up crowd to use.
(3) plain face frost skin sense provided by the invention clearly has good stability, is adapted to produce in enormous quantities.
Embodiment
Beneficial effects of the present invention are further described by following embodiments, embodiment is only used for the purpose of illustration, no
Limit the scope of the invention, while the obvious change and modification that those of ordinary skill in the art are made according to the present invention
Comprising within the scope of the present invention, following component is calculated in parts by weight in addition to especially indicating.
The DC 1403 being previously mentioned in following embodiments is six dimethyl silicone polymer of ring and and dimethiconol
Compound, purchased from Dow corning company, trade name DC 1403；Sepinov EMT 10 are hydroxy-ethyl acrylate and propylene
The copolymer of acyl dimethyltaurine sodium, purchased from match BIC Corp of SEPPIC France；COSMEDIA SP are Sodium Polyacrylate, purchase
From BASF BASF AG；SIMULGELEG is the copolymer of sodium acrylate and sodium acryloyldimethyl taurate, is purchased from
Match BIC Corp of SEPPIC France；G57 is Sodium Polyacrylate, C18-21 alkane, the mixture of trideceth -6, is purchased from
Xian Ting companies of SETHIC France；VanCarePhytomide is phytosterin ester, purchased from Dutch Fan Ai morals company；Mikrokill
Cos is Phenoxyethanol, pungent glycol, the mixture of Chlorphenesin, is a kind of preservative of compound highly effective, purchased from LONZA, Switzerland dragon
Sha companies；Pre-Emul 6225 is a kind of titanium dioxide of surface fluorination processing, purchased from joint micro mist company.
A kind of 1 low oil content of embodiment does not take off adornment element face frost and preparation method thereof clearly
Formula：
Preparation method：
(1) A1 phase raw materials are uniformly mixed, obtain lotion A；B phase raw materials are uniformly mixed, 80 DEG C or so is heated to, obtains
Lotion B；
(2) the lotion A and lotion B that are obtained in step (1) are uniformly mixed, then sequentially add A2 and A3 phase raw materials, mixed
Close uniform, acquisition lotion C；
(3) the lotion C that step (2) obtains is emulsified, then adds C phase raw materials, be uniformly mixed to grainless state,
Obtain lotion D；Then D phases raw material adds in lotion D after mixing, adds synergist caffeic acid, is uniformly mixed to no particle,
Obtain lotion E；
(4) the lotion E obtained in step (3) will be carried out being cooled to 35 DEG C in step (3), up to required product.
A kind of 2 low oil content of embodiment does not take off adornment element face frost and preparation method thereof clearly
Formula：
Preparation method：In addition to raw material, remaining is the same as embodiment 1.
A kind of 3 low oil content of embodiment does not take off adornment element face frost and preparation method thereof clearly
Formula：
Preparation method：In addition to raw material, remaining is the same as embodiment 1.
A kind of 4 low oil content of embodiment does not take off adornment element face frost and preparation method thereof clearly
Formula：
Preparation method：In addition to raw material, remaining is the same as embodiment 1.
A kind of 1 low oil content of comparative example does not take off adornment element face frost and preparation method thereof clearly
Formula：The content of macromolecule unsteady flow conditioning agent is improved 10% on the basis of embodiment 1, i.e. Sepinov EMT
10 2 parts, 3 parts of COSMEDIA SP, 8.7 parts of SIMULGEL EG, 1 part of G57；The content of water is reduced into 10%, i.e. water at the same time
For 37.53 parts, remaining content is the same as embodiment 1.
Preparation method：In addition to raw material, remaining is the same as embodiment 1.
A kind of 2 low oil content of comparative example does not take off adornment element face frost and preparation method thereof clearly
Formula：The content of polynary moisturizer and oiliness emollient is improved into 20%, i.e., 1,3- altogether on the basis of embodiment 1
10 parts of propane diols, 15 parts of glycerine, 15 parts of Natrulon H-10,1.4 parts of 1,2- hexylene glycols, 3 parts of cetanol ethylhexoate, cocounut oil
Alcohol -3 parts of caprylate/decylate, while the content of water is reduced by 20%, i.e. water is 27.53 parts, remaining content is the same as embodiment 1.
Preparation method：In addition to raw material, remaining is the same as embodiment 1.
A kind of 3 low oil content of comparative example does not take off adornment element face frost and preparation method thereof clearly
Formula：In addition to without caffeic acid, other are same as Example 1.
Preparation method：In addition to raw material, remaining is the same as embodiment 1.
Comparative example 4 exempts from plain face frost of removing ornaments and formal dress for a kind of water resistant disclosed in Chinese patent application CN201610778719.7.
Comparative example 5 is a kind of element of essence lotion containing high concentration disclosed in Chinese patent application CN201510274113.5
Yan Shuan.
A kind of pearl essence face frost disclosed in Chinese patent CN201611114201.X of comparative example 6.
Comparative example 7 is the commercially available beautiful plus fragrant plain face frost of low oil.
Contrast test
1st, water resistant film forming is tested
Operating method：A. first skin is dyed with ink；B. sample to be tested is coated in dyeing part；C. used in test position
SLES solution washes away inks；D. the shade of test position is observed, shade is beaten by 8 skilled researchers
Point, for measure stability to experiment skin carried out 8 it is small when Detection of Stability, surveyed respectively in 0h, 1h, 3h, 5h and 8h
Examination, is 0 point without color, color it is the same with before not rinsing for 10 points, calculating average.Test result see the table below 1.
1 water resistant film forming contrast test result of table
From upper table result, element face frost produced by the invention, has good water resistant effect, is scored by embodiment 1-4
As a result as can be seen that water resistant film forming appraisal result still more than 8.5 points, averagely comment by 8 interior water resistant film formings when small after when 8 is small
Divide more than 9.2 points, that is to say, that element face frost produced by the invention still has good water resistant effect after smearing one day, can
Ensure that a whole day does not take off adornment, and water resistant ability has almost no change after coating one hour, illustrate that this product stability is fine, tool
There is the effect of not de- adornment for a long time；Comparative example 1, is that containing for water and macromolecule unsteady flow conditioning agent is adjusted on the basis of embodiment 1
Amount, comparative example 2, it is being that water and polynary moisturizer and the content of oiliness emollient are adjusted on the basis of embodiment 1 to be, from scoring
As a result it can be seen that adjusting water and macromolecule unsteady flow conditioning agent and making this hair with the content of polynary moisturizer and oiliness emollient
The water resistant effect of the plain face frost of open-birth production has reduction by a small margin, but still has preferable water resistant film forming；And in comparative example 3 not
Containing caffeic acid, increasing its water resistant film-formation result with the time substantially reduces, 8 it is small when after water-resistance almost disappear, comparative example 4-
7, white for the white and commercially available common plain face of disclosed plain face, its water resistant film forming duration is equally very short, 8 it is small when after water-resistance it is several
It is wholly absent.
2. skin oil content is tested
The present invention provides a kind of low oil content clearly not de- adornment element face frost, when being applied to face or other positions of human body, energy
Feel salubrious not glutinous greasy sensation, be adapted to long-time service.A kind of test appraisal procedure of subsidiary offer of the invention is as follows.
Test philosophy：
Measured using SEBUMETER methods, it is to be based on photometer principle, utilizes a kind of special delustring glue of 0.1 millimeters thick
After the grease absorbed on human skin, a kind of translucent adhesive tape will be become, its light transmission capacity will change, and absorb
Grease it is more, light transmission capacity will be bigger, so as to measure the content of skin oil.This method biggest advantage is test probe
It is small, it is easy to use, any position of skin can be tested.This is a kind of indirect method of measurement of grease glandular secretion thing, as a result may be used
With for distinguishing different skin types, make to understand exactly the grease change as caused by inside and outside reason becomes can
Energy.
Operating procedure：
Choose the tested volunteer 15 of 20~35 years old women, wherein more than 30 years old 3,20~30 years old 12.Choose face
Symmetrical two regions, respectively as control group and the test zone of experimental group, in the environment of constant temperature and humidity, test skin oil
Divide content.Experimental group uses contrast using the high plain face frost of the salubrious stability of low oil content prepared by embodiment 1-4, control group
Plain face frost prepared by example, the two does same test under the same conditions.
Skin of face is cleaned, after subject sits quietly 30 minutes in constant-temperature constant-humidity environment (25 DEG C of temperature, humidity 60%), is pressed
According to test group and control group subregion, recipient site blank value is carried out using skinanalysis apparatus (German CK, CutometerMPA580)
Measurement.The corresponding position respectively at face measure blank value smears the embodiment 1-4 of equivalent again and comparative example prepares plain face frost,
1 it is small when after, test and record the oil content in two regions, at interval of 2 it is small when test 1 time, test period for 8 it is small when.Skin
The result of oil content represented by the oil measured value (OilMeasurementValue, OMV) of setting, its scope 0~
Between 350.Each test data is subtracted into the change that its blank value is period OMV, then divided by blank value draw OMV's
Growth rate.
Skin oil content Growth Rate Calculation formula is：
Skin oil content growth rate %=(OMVt-OMV0)/OMV0× 100%
OMV0--- skin OMV before smearing；OMVt--- t period skins OMV test results see the table below 2 after smearing.
2 skin oil content of table is tested
By 2 data of upper table it is known that product produced by the invention is the low salubrious product of oil, and energy long-time oil-control,
It can be seen from embodiment 1-4 appraisal results 8 it is small when inner skin oil content average growth rate there was only 10% or so, that is to say, that
Element face frost produced by the invention is still very salubrious after smearing one day, it is ensured that skin a whole day, low oil was salubrious, illustrated this product
Stability is fine, has the effect of long-time oil resistant；Comparative example 1, is that water and macromolecule unsteady flow are adjusted on the basis of embodiment 1
The content of conditioning agent, comparative example 2, it is being that water and polynary moisturizer and oiliness emollient are adjusted on the basis of embodiment 1 to be
Content, can be seen that from skin oil content average growth rate result adjust water and macromolecule unsteady flow conditioning agent and with polynary moisturizing
The content of agent and oiliness emollient makes the oil resistant effect of plain face frost produced by the invention decrease, but this product still has preferably
Grease resistance；And caffeic acid is free of in comparative example 3, with the time increase its oil resistant positive effect reduction, 8 it is small when inner skin oil content
Average growth rate is 69.3%, comparative example 4-7, for the white and commercially available common plain face frost of disclosed plain face, its grease resistance duration
It is equally very short, 8 it is small when inner skin oil content average growth rate be 65%.There is above-mentioned testing result to understand, element produced by the invention
Yan Shuan can ensure skin refreshing non-greasy when in use, be well suited for usually changing light make-up crowd's use.
3. product stability is tested
Operating method：Low oil content produced by the invention clearly not de- adornment element face frost is taken, is placed in constant temperature and humidity ring
18 months in border (25 DEG C of temperature, humidity 60%), it was detected at 1 month, 3 months, 6 months, 12 months and 18 months respectively
Precipitation situation is layered, layering precipitation situation is divided into 4 grades：0 grade is without precipitation delamination, and 1 grade is slightly to be layered precipitation situation, 2
Level is obvious layering precipitation situation, and 3 grades separate out delamination to be serious."-" is represented and up to the present not obtained also in form
Corresponding test result.
3 product stability of table is tested
From 3 data of upper table, product produced by the invention is the high product of the low salubrious stability of oil, to product stability
Test, from embodiment 1-4, which only there is slight layering after placing 12 months, and comparative example 4-7 is being placed 6 months
When just there is obvious layering, understand that plain face frost produced by the invention has fine stability by contrast test, it is suitable
Produce in enormous quantities.
Claims (10)
1. clearly not de- adornment element face is white for a kind of low oil content, it is characterised in that：Including：Oiliness emollient,
Polyalcohol moisturizer, skin conditioning agent, polymeric rheology conditioning agent, titanium dioxide class covering agent, preservative and essence.
2. clearly not de- adornment element face is white for low oil content according to claim 1, it is characterised in that：Synergist is further included, institute
One or more of the synergist stated in caffeic acid, papain and vanillic aldehyde.
3. clearly not de- adornment element face is white for low oil content according to claim 1, it is characterised in that：The oiliness emollient
Can be selected from the one or more in vegetable oil, Synthetic Oil, silicone oil quasi-grease and induction biosynthesis wax.
4. clearly not de- adornment element face is white for low oil content according to claim 1, it is characterised in that：The polyalcohol moisturizing
Agent can be selected from glycerine, propane diols, 1,3 propane diols, butanediol, dipropylene glycol, D-sorbite and one kind in Natrulon H-10 or
It is several.
5. clearly not de- adornment element face is white for low oil content according to claim 1, it is characterised in that：The skin conditioning agent
Can be selected from one kind in allantoin, panthenol, trehalose, glycine betaine, glycosphingolipids, phytosterin ester and beta glucan or several
Kind.
6. clearly not de- adornment element face is white for low oil content according to claim 1, it is characterised in that：The polymeric rheology
Conditioning agent can be selected from carbomer, carbomer sodium, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, propylene
Sour (ester) analog copolymer, Sodium Polyacrylate, polyacrylate cross-linked polymer -6, ammonium acryloyldime-thyltaurate/VP copolymerization
Thing, Sodium Polyacrylate graft starch, polypropylene acyl group dimethyltaurine sodium, hydrolysis Scleroglucan, hydroxy-ethyl acrylate/propylene
It is acyl dimethyltaurine sodium copolymer, sodium acrylate/sodium acryloyldimethyl taurate copolymers, Sodium Polyacrylate powder, poly-
The mixture of sodium acrylate/C18-21 alkane/trideceth -6, sodium acrylate/sodium acryloyldimethyl taurate copolymers,
In the mixture and hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers of isohexadecane/Polyoxyethylene Sorbitan Monooleate/water
One or more.
7. clearly not de- adornment element face is white for low oil content according to claim 1, it is characterised in that：The titanium dioxide class hides
Lid agent is titanium dioxide slurry and/or titanium dioxide powder.
8. clearly not de- adornment element face is white for low oil content according to claim 1, it is characterised in that：The preservative is selected from
Methyl hydroxybenzoate, Nipasol, Phenoxyethanol, 1,2- hexylene glycols, Sensiva SC50, Chlorphenesin, DMDM hydantoin and iodine
One or more in propilolic alcohol butyl mephenesin Carbamate.
9. clearly not de- adornment element face is white for low oil content according to claim 2, it is characterised in that：The plain face frost bag
Include：In parts by weight：0.0001-50 parts of oiliness emollient, 0.0001-50 parts of polyalcohol moisturizer, skin conditioning agent
0.0001-10 parts, 0.0001-10 parts of polymeric rheology conditioning agent, 0.0001-20 parts of titanium dioxide class covering agent, preservative
0.001-5 parts of 0.0001-10 parts, 0.001-1 parts of essence and synergist.
10. clearly not de- adornment element face is white for low oil content according to claim 9, it is characterised in that：The plain face frost bag
Include：In parts by weight：0.1-40 parts of oiliness emollient, 0.1-40 parts of polyalcohol moisturizer, 0.1-9 parts of skin conditioning agent,
0.1-9 parts of polymeric rheology conditioning agent, 0.1-15 parts of titanium dioxide class covering agent, 0.1-9 parts of preservative, 0.1-0.9 parts of essence and
0.01-4 parts of synergist.
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| CN109498477A (en) * | 2018-12-27 | 2019-03-22 | 上海宜侬生物科技有限公司 | A kind of oil-in-water foundation liquid and preparation method thereof with water resistant sweat resistance |
| CN110448511A (en) * | 2019-09-06 | 2019-11-15 | 广州留今科学研究有限公司 | The skin conditioning agent of a kind of anticreep adornment and anti-blue light, plain face frost and preparation method thereof |
| CN111662639A (en) * | 2020-07-03 | 2020-09-15 | 浙江工业大学 | Novel film forming material and preparation method thereof |
| CN112516054A (en) * | 2020-12-30 | 2021-03-19 | 福建臻昕美生物科技有限公司 | Tea polyphenol protein cream for repairing, moisturizing and strengthening skin and production process thereof |
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| CN109498477A (en) * | 2018-12-27 | 2019-03-22 | 上海宜侬生物科技有限公司 | A kind of oil-in-water foundation liquid and preparation method thereof with water resistant sweat resistance |
| CN113645945A (en) * | 2019-03-29 | 2021-11-12 | 罗盖特公司 | Make-up cream for imparting long-lasting makeup |
| CN110448511A (en) * | 2019-09-06 | 2019-11-15 | 广州留今科学研究有限公司 | The skin conditioning agent of a kind of anticreep adornment and anti-blue light, plain face frost and preparation method thereof |
| CN110448511B (en) * | 2019-09-06 | 2022-09-02 | 广州一一生物技术有限公司 | Anti-makeup and anti-blue-light skin conditioner, skin cream and preparation method thereof |
| CN111662639A (en) * | 2020-07-03 | 2020-09-15 | 浙江工业大学 | Novel film forming material and preparation method thereof |
| CN111662639B (en) * | 2020-07-03 | 2021-10-01 | 浙江工业大学 | Film forming material and preparation method thereof |
| CN112516054A (en) * | 2020-12-30 | 2021-03-19 | 福建臻昕美生物科技有限公司 | Tea polyphenol protein cream for repairing, moisturizing and strengthening skin and production process thereof |
| CN113940905A (en) * | 2021-06-25 | 2022-01-18 | 太和康美(北京)中医研究院有限公司 | Face-beautifying cream and preparation method thereof |
| CN113940905B (en) * | 2021-06-25 | 2022-06-17 | 太和康美(北京)中医研究院有限公司 | Face-beautifying cream and preparation method thereof |
| CN114668688A (en) * | 2022-03-23 | 2022-06-28 | 广州市白云区大荣精细化工有限公司 | Waterproof face beautifying cream and preparation method thereof |
| CN117243834A (en) * | 2023-10-09 | 2023-12-19 | 广州百孚润化工有限公司 | Oil-control acne-removing composition with high octanoyl glycine content, and preparation method and application thereof |
| CN117243834B (en) * | 2023-10-09 | 2024-04-26 | 广州百孚润化工有限公司 | Oil-control acne-removing composition with high octanoyl glycine content, and preparation method and application thereof |
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