Summary of the invention
Goal of the invention: the present invention will provide a kind of titanium dioxide cold cream and preparation method thereof, to address the above problem.
Technical scheme: a kind of titanium dioxide cold cream, in parts by weight, component is as follows: glycerol 6-12 part; Stearic acid 2-5 part; Hyaluronic acid 1-5 part; Octadecanol or hexadecanol 3-5 part; Emulsifying agent 10-15 part; Wetting agent 5-12 part; Margarita powder 3-5 part; Titanium dioxide 1-3 part; Zinc oxide 0.5-1.5 part; Essence 0.2-0.5 part; Triethanolamine 0.1-0.5 part; Acetylated lanolin 0.2-1.0 part; Glycerol 3-5 part; Deionized water 10-15 part; Plant SOD 3-6 part;
Described wetting agent is at least a in trehalose, α-mannan, dimethicone or the lecithin; Described emulsifying agent is at least a in glyceryl monostearate, alkyl polyglucoside, hydrolecithin and the Polyethylene Glycol; Described essence is cephrol, vanillin, coumarin or ionoionone.
As preferred embodiment, in parts by weight, described component is: glycerol 8-10 part; Stearic acid 3-4 part; Hyaluronic acid 2-4 part; Octadecanol or hexadecanol 3-5 part; Hydrolecithin 10-12 part; Trehalose 8-10 part; Margarita powder 3-5 part; Titanium dioxide 2-3 part; Zinc oxide 1-1.5 part; Vanillin 0.2-0.4 part; Triethanolamine 0.2-0.4 part; Acetylated lanolin 0.2-0.6 part; Glycerol 3-5 part; Deionized water 10-15 part; Plant SOD 3-6 part.
The particle diameter of described titanium dioxide is the Rutile type titanium dioxide of 30-50 nanometer.
The present invention further provides the preparation method of above-mentioned titanium dioxide cold cream, comprised the steps:
S1, glycerol, stearic acid, octadecanol or hexadecanol, titanium dioxide, hyaluronic acid, zinc oxide and glycerol are mixed, make its mix homogeneously with the stirring of thermostatic electromagnetic agitator, mixing speed is 1200-1500r/min, temperature is 60-70 ℃, stirred 5-10 minute, after stirring is finished, place 45-55 ℃ of lower constant temperature to preserve;
S2, triethanolamine, acetylated lanolin, Margarita powder and deionized water are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 800-1000r/min, and temperature is 55-65 ℃, stirs 10-20 minute;
S3, reduce temperature to 45-50 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 500-600r/min, continues to stir, and adds emulsifying agent and wetting agent, stirs 5-8 minute; Improve rotating speed to 1000-1200r/min, add essence, stirred 5-10 minute, reduce temperature to 4-10 ℃, add plant SOD, stirred 1-5 minute, rotating speed is 200-260r/min; The check encapsulation.
As preferred embodiment, above-mentioned S3 step further is:
S31, reduce temperature to 45-50 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 500-600r/min, continues to stir, and adds emulsifying agent and part lecithin, stirs 5-8 minute; Improve rotating speed to 1000-1200r/min, add essence, stirred 5-10 minute, reduce temperature to 4-10 ℃;
S32, in another container, remaining lecithin is mixed with plant SOD, stirred 3-10 minute at 3-8 ℃ of lower constant temperature, lecithin and plant SOD mixture are joined in the mixture of step S31 acquisition, stirred 1-5 minute, rotating speed is 200-260r/min; The check encapsulation.
Beneficial effect: titanium dioxide cold cream of the present invention does not have greasy feeling, has the function of maintaining skin, and through use after a while, it is fine and smooth that skin can become; Refrigerant sense is arranged, be particularly suitable for using summer, the relative amount of oils and fats is low, can not allow user cause long pox owing to the obstruction fine hair hole is blocked; Cold cream of the present invention can prolong the high activity time of SOD, and the cycle of partly declining is long, even at normal temperatures, also can use 5-10 days more.
The specific embodiment
Embodiment 1
A kind of titanium dioxide cold cream, in parts by weight, component is as follows: 8 parts of glycerol; 3 parts of stearic acid; 3.5 parts of hyaluronic acids; 3.6 parts of octadecanol or hexadecanol; 11 parts of emulsifying agents; 9 parts of wetting agents; 3.6 parts of Margarita powder; 2.5 parts of titanium dioxides; 1.2 parts of zinc oxide; 0.3 part in essence; 0.3 part of triethanolamine; 0.3 part of acetylated lanolin; 3.6 parts of glycerol; 11 parts of deionized waters; 4 parts of plant SOD; Described wetting agent be trehalose and α-mannan, weight ratio is the mixture of 1:2; Described emulsifying agent is the equimolar amounts mixture of glyceryl monostearate, hydrolecithin and Polyethylene Glycol; Described essence is ionoionone; The particle diameter of described titanium dioxide is the Rutile type titanium dioxide of 30-50 nanometer.
The preparation method of above-mentioned titanium dioxide cold cream comprises the steps:
S1, glycerol, stearic acid, octadecanol or hexadecanol, titanium dioxide, hyaluronic acid, zinc oxide and glycerol are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1300r/min, temperature is 62 ℃, stirred 6 minutes, and after stirring is finished, placed 45 ℃ of lower constant temperature to preserve;
S2, triethanolamine, acetylated lanolin, Margarita powder and deionized water are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 950r/min, and temperature is 60 ℃, stirs 12 minutes;
S3, reduce temperature to 48 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 540r/min, continues to stir, and adds emulsifying agent and wetting agent, stirs 6 minutes; Improve rotating speed to 1100r/min, add essence, stirred 7 minutes, reduce temperature to 6 ℃, adding plant SOD stirred 3 minutes, and rotating speed is 250r/min; The check encapsulation.
Embodiment 2
A kind of titanium dioxide cold cream, in parts by weight, component is as follows: 9 parts of glycerol; 4 parts of stearic acid; 4 parts of hyaluronic acids; 4 parts of octadecanol or hexadecanol; 13 parts of emulsifying agents; 10 parts of wetting agents; 4 parts of Margarita powder; 2 parts of titanium dioxides; 1 part of zinc oxide; 0.2 part in essence; 0.4 part of triethanolamine; 0.6 part of acetylated lanolin; 3.2 parts of glycerol; 13 parts of deionized waters; 5 parts of plant SOD;
Described wetting agent is the homogenous quantities mixture of trehalose and lecithin; Described emulsifying agent is Polyethylene Glycol; Described essence is coumarin; The particle diameter of described titanium dioxide is the Rutile type titanium dioxide of 30-50 nanometer.
The preparation method of above-mentioned titanium dioxide cold cream comprises the steps:
S1, glycerol, stearic acid, octadecanol or hexadecanol, titanium dioxide, hyaluronic acid, zinc oxide and glycerol are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1200r/min, temperature is 65 ℃, stirred 8 minutes, and after stirring is finished, placed 50 ℃ of lower constant temperature to preserve;
S2, triethanolamine, acetylated lanolin, Margarita powder and deionized water are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 800r/min, and temperature is 55 ℃, stirs 16 minutes;
S3, reduce temperature to 50 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 560r/min, continues to stir, and adds emulsifying agent and wetting agent, stirs 7 minutes; Improve rotating speed to 1150r/min, add essence, stirred 9 minutes, reduce temperature to 8 ℃, adding plant SOD stirred 5 minutes, and rotating speed is 260r/min; The check encapsulation.
Embodiment 3
A kind of titanium dioxide cold cream, in parts by weight, component is as follows: 11 parts of glycerol; 4.5 parts of stearic acid; 1 part of hyaluronic acid; 3 parts of octadecanol or hexadecanol; 10 parts of emulsifying agents; 5 parts of wetting agents; 3 parts of Margarita powder; 2.8 parts of titanium dioxides; 0.5 part of zinc oxide; 0.25 part in essence; 0.2 part of triethanolamine; 0.2 part of acetylated lanolin; 3 parts of glycerol; 10 parts of deionized waters; Plant SOD3 part;
Described wetting agent is that the weight ratio of trehalose, α-mannan and lecithin is the mixture of 1:1:1; Described emulsifying agent is glyceryl monostearate; Described essence is cephrol; The particle diameter of described titanium dioxide is the Rutile type titanium dioxide of 30-50 nanometer.
The preparation method of above-mentioned titanium dioxide cold cream comprises the steps:
S1, glycerol, stearic acid, octadecanol or hexadecanol, titanium dioxide, hyaluronic acid, zinc oxide and glycerol are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1400r/min, temperature is 68 ℃, stirred 10 minutes, and after stirring is finished, placed 55 ℃ of lower constant temperature to preserve;
S2, triethanolamine, acetylated lanolin, Margarita powder and deionized water are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 850r/min, and temperature is 58 ℃, stirs 20 minutes;
S3, reduce temperature to 45 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 500r/min, continues to stir, and adds emulsifying agent and wetting agent, stirs 5 minutes; Improve rotating speed to 1200r/min, add essence, stirred 5 minutes, reduce temperature to 10 ℃, adding plant SOD stirred 2 minutes, and rotating speed is 200r/min; The check encapsulation.
Embodiment 4
A kind of titanium dioxide cold cream, in parts by weight, component is as follows: 10 parts of glycerol; 3.5 parts of stearic acid; 3.5 parts of hyaluronic acids; 3.6 parts of octadecanol or hexadecanol; 11 parts of emulsifying agents; 9 parts of wetting agents; 3.6 parts of Margarita powder; 2.5 parts of titanium dioxides; 1.2 parts of zinc oxide; 0.3 part in essence; 0.3 part of triethanolamine; 0.3 part of acetylated lanolin; 3.6 parts of glycerol; 11 parts of deionized waters; 4 parts of plant SOD;
Described wetting agent is dimethicone; Described emulsifying agent is alkyl polyglucoside; Described essence is cephrol; The particle diameter of described titanium dioxide is the Rutile type titanium dioxide of 30-50 nanometer.
The preparation method of above-mentioned titanium dioxide cold cream comprises the steps:
S1, glycerol, stearic acid, octadecanol or hexadecanol, titanium dioxide, hyaluronic acid, zinc oxide and glycerol are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1500r/min, temperature is 70 ℃, stirred 5 minutes, and after stirring is finished, placed 52 ℃ of lower constant temperature to preserve;
S2, triethanolamine, acetylated lanolin, Margarita powder and deionized water are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1000r/min, and temperature is 65 ℃, stirs 10 minutes;
S3, reduce temperature to 46 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 590r/min, continues to stir, and adds emulsifying agent and wetting agent, stirs 8 minutes; Improve rotating speed to 1000r/min, add essence, stirred 10 minutes, reduce temperature to 4 ℃, adding plant SOD stirred 4 minutes, and rotating speed is 220r/min; The check encapsulation.
Embodiment 5
A kind of titanium dioxide cold cream, in parts by weight, component is as follows: 8 parts of glycerol; 4 parts of stearic acid; 4 parts of hyaluronic acids; 4 parts of octadecanol or hexadecanol; 11 parts of emulsifying agents; 9 parts of wetting agents; 3.6 parts of Margarita powder; 2.5 parts of titanium dioxides; 1.2 parts of zinc oxide; 0.3 part in essence; 0.4 part of triethanolamine; 0.4 part of acetylated lanolin; 3.6 parts of glycerol; 11 parts of deionized waters; Plant SOD4 part;
Described wetting agent is that the weight ratio of trehalose and lecithin is the mixture of 1:1; Described emulsifying agent is hydrolecithin; Described essence is coumarin, and the particle diameter of described titanium dioxide is the Rutile type titanium dioxide of 30-50 nanometer.
The preparation method of above-mentioned titanium dioxide cold cream comprises the steps:
S1, glycerol, stearic acid, octadecanol or hexadecanol, titanium dioxide, hyaluronic acid, zinc oxide and glycerol are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1300r/min, temperature is 64 ℃, stirred 5 minutes, and after stirring is finished, placed 50 ℃ of lower constant temperature to preserve;
S2, triethanolamine, acetylated lanolin, Margarita powder and deionized water are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 850r/min, and temperature is 60 ℃, stirs 14 minutes;
S31, reduce temperature to 45 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 530r/min, continues to stir, and adds emulsifying agent, trehalose and part lecithin, stirs 6 minutes; Improve rotating speed to 1150r/min, add essence, stirred 8 minutes, reduction temperature to 5 ℃;
S32, in another container, remaining lecithin is mixed with plant SOD, stirred 5 minutes at 4 ℃ of lower constant temperature, lecithin and plant SOD mixture are joined in the mixture of step S31 acquisition, stirred 3 minutes, rotating speed is 240r/min; The check encapsulation.
Embodiment 6
A kind of titanium dioxide cold cream, in parts by weight, component is as follows: 10 parts of glycerol; 3 parts of stearic acid; 3 parts of hyaluronic acids; 3.6 parts of octadecanol or hexadecanol; 12 parts of emulsifying agents; 10 parts of wetting agents; 3.2 parts of Margarita powder; 2 parts of titanium dioxides; 1 part of zinc oxide; 0.4 part in essence; 0.45 part of triethanolamine; 0.6 part of acetylated lanolin; 3.2 parts of glycerol; 12 parts of deionized waters; 4.5 parts of plant SOD;
Described wetting agent is that the weight ratio in trehalose, α-mannan, dimethicone and the lecithin is the mixture of 1:1:1:1; Described emulsifying agent is that the weight ratio in glyceryl monostearate, alkyl polyglucoside, hydrolecithin and the Polyethylene Glycol is the mixture of 1:1:1:1; Described essence is cephrol.
The preparation method of above-mentioned titanium dioxide cold cream comprises the steps:
S1, glycerol, stearic acid, octadecanol or hexadecanol, titanium dioxide, hyaluronic acid, zinc oxide and glycerol are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1400r/min, temperature is 66 ℃, stirred 8 minutes, and after stirring is finished, placed 53 ℃ of lower constant temperature to preserve;
S2, triethanolamine, acetylated lanolin, Margarita powder and deionized water are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 900r/min, and temperature is 63 ℃, stirs 18 minutes;
S31, reduce temperature to 48 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 580r/min, continues to stir, and adds emulsifying agent, trehalose, α-mannan and dimethicone, stirs 8 minutes; Improve rotating speed to 1200r/min, add essence, stirred 10 minutes, reduction temperature to 8 ℃;
S32, in another container, lecithin is mixed with plant SOD, stirred 8 minutes at 5 ℃ of lower constant temperature, lecithin and plant SOD mixture are joined in the mixture of step S31 acquisition, stirred 5 minutes, rotating speed is 260r/min; The check encapsulation.
Embodiment 7
A kind of titanium dioxide cold cream, in parts by weight, component is as follows: 6 parts of glycerol; 2 parts of stearic acid; 2 parts of hyaluronic acids; 4.5 parts of octadecanol or hexadecanol; 14 parts of emulsifying agents; 7 parts of wetting agents; 4.5 parts of Margarita powder; 1 part of titanium dioxide; 0.8 part of zinc oxide; 0.4 part in essence; 0.5 part of triethanolamine; 0.8 part of acetylated lanolin; 4 parts of glycerol; 13 parts of deionized waters; 6 parts of plant SOD;
Described wetting agent is lecithin; Described emulsifying agent is at least a in glyceryl monostearate, alkyl polyglucoside, hydrolecithin and the Polyethylene Glycol; Described essence is cephrol, vanillin, coumarin or ionoionone.
The preparation method of above-mentioned titanium dioxide cold cream comprises the steps:
S1, glycerol, stearic acid, octadecanol or hexadecanol, titanium dioxide, hyaluronic acid, zinc oxide and glycerol are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1200r/min, temperature is 70 ℃, stirred 10 minutes, and after stirring is finished, placed 55 ℃ of lower constant temperature to preserve;
S2, triethanolamine, acetylated lanolin, Margarita powder and deionized water are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1000r/min, and temperature is 65 ℃, stirs 20 minutes;
S31, reduce temperature to 50 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 600r/min, continues to stir, and adds emulsifying agent and part lecithin, stirs 7 minutes; Improve rotating speed to 1050r/min, add essence, stirred 6 minutes, reduction temperature to 4 ℃;
S32, in another container, remaining lecithin is mixed with plant SOD, stirred 10 minutes at 4.5 ℃ of lower constant temperature, lecithin and plant SOD mixture are joined in the mixture of step S31 acquisition, stirred 1 minute, rotating speed is 200r/min; The check encapsulation.
Embodiment 8
A kind of titanium dioxide cold cream, in parts by weight, component is as follows: 12 parts of glycerol; 5 parts of stearic acid; 5 parts of hyaluronic acids; 3 parts of octadecanol or hexadecanol; 10 parts of emulsifying agents; 12 parts of wetting agents; 5 parts of Margarita powder; 3 parts of titanium dioxides; 1.3 parts of zinc oxide; 0.5 part in essence; 0.3 part of triethanolamine; 1 part of acetylated lanolin; 4.5 parts of glycerol; 12 parts of deionized waters; 6 parts of plant SOD;
Described wetting agent is lecithin; Described emulsifying agent is glyceryl monostearate; Described essence is vanillin.
The preparation method of above-mentioned titanium dioxide cold cream comprises the steps:
S1, glycerol, stearic acid, octadecanol or hexadecanol, titanium dioxide, hyaluronic acid, zinc oxide and glycerol are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 1500r/min, temperature is 60 ℃, stirred 6 minutes, and after stirring is finished, placed 45 ℃ of lower constant temperature to preserve;
S2, triethanolamine, acetylated lanolin, Margarita powder and deionized water are mixed, making its mix homogeneously, mixing speed with the stirring of thermostatic electromagnetic agitator is 800r/min, and temperature is 55 ℃, stirs 10 minutes;
S31, reduce temperature to 46 ℃, the mixture that step 1 is obtained joins among the mixture that step 2 obtains, and reduces rotating speed to 500r/min, continues to stir, and adds emulsifying agent and part lecithin, stirs 5 minutes; Improve rotating speed to 1000r/min, add essence, stirred 5 minutes, reduction temperature to 7 ℃;
S32, in another container, remaining lecithin is mixed with plant SOD, stirred 3 minutes at 3 ℃ of lower constant temperature, lecithin and plant SOD mixture are joined in the mixture of step S31 acquisition, stirred 2 minutes, rotating speed is 250r/min; The check encapsulation.In this embodiment, plant SOD is surrounded by the liposome that lecithin forms first, and SOD is not easy inactivation more, and the cycle of partly declining is longer.