CN107981104A - The preparation method of the environmentally friendly prawn feed of water quality can be improved - Google Patents
The preparation method of the environmentally friendly prawn feed of water quality can be improved Download PDFInfo
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- A—HUMAN NECESSITIES
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- A23K10/22—Animal feeding-stuffs from material of animal origin from fish
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- A23K10/00—Animal feeding-stuffs
- A23K10/20—Animal feeding-stuffs from material of animal origin
- A23K10/26—Animal feeding-stuffs from material of animal origin from waste material, e.g. feathers, bones or skin
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Abstract
The present invention provides a kind of preparation method for the environmentally friendly prawn feed for improving water quality, comprise the following steps：S1, by clam shell crush be placed on phosphoric acid solution immersion；Then clam shell is placed in sodium carbonate liquor and soaked, mixed after dry with far-infared ceramic powder, be calcined, obtain modified clam shell powder；S2, crush radix astragali, Angelica sinensis, the membrane of a chicken's gizzard, rhizoma anemarrhenae, blackberry lily, giant knotweed, Phytolacca acinosa mixed grinding, is subsequently placed in ethanol solution and flows back, collects filtrate and filter residue；S3, ferment after mixing corn flour, fish meal, rapeseed dregs, dregs of beans, silkworm chrysalis, filter residue, fermentation medium, obtains the first fermentate；Then after the first fermentate mix with modified clam shell powder, then ferment, filter, dry the second fermentate at temperature is 60~70 DEG C；S4, the second fermentate of mixing, multi-vitamins, filtrate, are granulated, drying.The feed of the present invention can improve water quality using clam shell powder as raw material and after passing it through phosphoric acid, sodium carbonate and calcination processing.
Description
Technical field
The present invention relates to prawn feed technical field, and in particular to a kind of preparation for the environmentally friendly prawn feed for improving water quality
Method.
Background technology
Prawn is full of nutrition, and unique flavor, is favored by market, is the important aquaculture object in China.With cultivation
Area and production scale constantly expand, and high-density breeding, launch excessive bait and drug abuse, bring such as breeding environment evil
The problems such as change, pest and disease damage is serious, and water quality seriously pollutes, deterioration in quality.It is but highly dense from the point of view of the development trend of aquaculture
Degree, efficient, ecologic breeding are the directions of shrimp culture industry from now on.How reasonable preparation feed, improve its utilization rate, reduce feed
Amount, at the same efficiently, quickly handle aquaculture wastewater, reach requirement of the aquaculture to water quality, reduce pest and disease damage, into
For high density, efficient, ecologic breeding industry large-scale development key.Existing prawn feed, input amount is big, is not absorbed by prawn
Or a large amount of the problem of remaining in water, making Water Eutrophication cause prawn quality, yield to decline.Prawn feed does not have at present
The effect of for killing pests and suppressing bacteria and water quality can be improved.
The content of the invention
It is an object of the invention to solve at least the above, and provide the advantages of at least will be described later.
It is an object of the present invention to provide a kind of preparation method for the environmentally friendly prawn feed for improving water quality, its by with
Clam shell powder can improve water quality for raw material and after passing it through phosphoric acid, sodium carbonate and calcination processing.
In order to realize object of the present invention and further advantage, there is provided a kind of environmentally friendly prawn feed for improving water quality
Preparation method, comprise the following steps：
S1, after the clam shell that parts by weight are 30~40 parts is crushed, it is dense to be subsequently placed in the quality that parts by weight are 50~60 parts
Spend in the phosphoric acid solution for 10~15% in temperature be at 30~50 DEG C immersion 2~3h, take out, clean；Then after cleaning
Clam shell is placed in 20~30min of immersion in the sodium carbonate liquor that the mass concentration that parts by weight are 20~30 parts is 5~8%, takes out,
After cleaning, drying with parts by weight be 0.5~1 part far-infared ceramic powder after mixing, calcination, obtain modified clam shell powder；
S2, the radix astragali by parts by weight are 3~6 parts, 2~5 parts of Angelica sinensis, 3~5 parts of the membrane of a chicken's gizzard, 2~5 parts of rhizoma anemarrhenae, 3~5
The blackberry lily, 3~5 parts of giant knotweed, 3~5 parts of Phytolacca acinosa mixed grinding of part crush, and are subsequently placed in the quality that parts by weight are 80~90 parts
Flow back 10~15h in the ethanol solution that fraction is 70~80%, collects filtrate and filter residue；
S3, the corn flour by parts by weight are 20~30 parts, 15~20 parts of fish meal, 15~20 parts of rapeseed dregs, 15~20
It is 50~60 DEG C that the dregs of beans, 10~15 parts of silkworm chrysalis, the filter residue in S2,10~20 parts of fermentation medium of part, which are mixed after temperature,
10~15d of lower fermentation, obtains the first fermentate；Then by the first fermentate and modified clam shell powder in mass ratio 3~5:1 mixing
Afterwards, then in temperature be the 2~3d that ferments at 60~70 DEG C, filtering, dry the second fermentate；
S4, be 100 in mass ratio:0.1~0.2:Filtrate in 5~10 the second fermentates of mixing, multi-vitamins, S1, stirs
Mix uniformly, be granulated, drying, to obtain the final product；
Wherein, the preparation method of fermentation medium is：By molasses of the parts by weight for 0.3~0.5 part, 1~2 part of sulfuric acid Asia
Iron, 3~4 parts of zinc sulfate, 3~5 parts of manganese sulfate, 0.1~0.5 part of photosynthetic bacteria, 10~15 parts of water are mixed after light
2~3d of anaerobic fermentation according under the conditions of, then adds saccharomycete, 0.1~0.2 part of unwrapping wire that parts by weight are 0.05~0.1 part
Bacterium, 0.1~0.2 part of 3~5d of EM bacterium aerobic fermentations to obtain the final product.
Preferably, the preparation method of the environmentally friendly prawn feed for improving water quality, further includes in S4 and is by quality
5~10% phagostimulant of the second fermentate quality is mixed with filtrate in the second fermentate, multi-vitamins, S1；It is wherein described
The preparation of phagostimulant comprises the following steps：
Step 1: by illiciumverum that parts by weight are 1~2 part, 2~3 parts of vomiting nut, 1~2 part of onion, 2~3 parts big
Garlic, 1~2 part of hawthorn, 2~3 parts of peppermint are added after crushing in the water that parts by weight are 30~40 parts, stirring, and add weight
Part is 0.1~0.5 part of 1~2h of complex enzyme zymohydrolysis, and enzyme deactivation, obtains slurry；Wherein, it is 1 that complex enzyme, which includes mass ratio,:2~3:1
~2:1~2:2~3 lywallzyme, pectase, cellulase, protease and lipase；
Step 2: it is 5~10 parts of maize flour, 5~10 parts of shrimp shell, 2~5 parts of Pizza grass mixed grinding by parts by weight
Cuttlefish powder that Cheng Fenhou and parts by weight are 10~15 parts, 8~10 parts of albumen powder, 0.1~0.5 part of carvacrol, 5~10 parts
Slurry mixes, and is granulated, up to phagostimulant.
Preferably, the preparation method of the environmentally friendly prawn feed for improving water quality, in S1 calcination include prior to temperature
Spend to be calcined 1~2h at 300~350 DEG C；Then using heating rate as 6~8 DEG C/min be warming up to 550~600 DEG C and keep 1~
1.5h, then be cooled to 350~400 DEG C with 8~10 DEG C/min rate of temperature fall and keep 30~40min, then again with heating rate
700~750 DEG C are warming up to for 10~12 DEG C/min and keeps 0.5~1h, are subsequently cooled to room temperature, are obtained modified clam shell powder.
Preferably, the preparation method of the environmentally friendly prawn feed for improving water quality, radix astragali in S2, Angelica sinensis, in chicken
After gold, rhizoma anemarrhenae, blackberry lily, giant knotweed, Phytolacca acinosa mixed grinding crush, it is in temperature in the soda water that addition parts by weight are 120~150 parts
20~30min is soaked at 25~30 DEG C, separating mixture, then adds the matter that parts by weight are 120~150 parts into mixture again
Amount concentration be 2~4% acetum in temperature be at 30~35 DEG C immersion 0.5~1h；Then it is mixed after acetic acid is soaked
Compound adds parts by weight and is 20~30 parts, 1~2h is soaked in the water that temperature is 95~100 DEG C, is then protected at -20~-25 DEG C
10~12h is held, most adds in ethanol solution and flows back after 20~30min of holding at 25~30 DEG C.
Preferably, the preparation method of the environmentally friendly prawn feed for improving water quality, 10~15d processes of fermenting in S3
In, every 2~3d turnings are once.
Preferably, the preparation method of the environmentally friendly prawn feed for improving water quality, obtains the first fermentate in S3
Afterwards and 10~20min of irradiation under the infrared lamp that power is 500~1000W is placed on, then carries out second of fermentation.
The present invention includes at least following beneficial effect：
1st, the preparation method of the environmentally friendly prawn feed for improving water quality of the invention, uses after clam shell is crushed and first phosphoric acid
Solution soaks and then with after soaking in sodium carbonate solution, and can obtain after repeatedly segmentation calcination poroid being evenly distributed, being fine and close
Porous material so that Nutrient distribution in feed is slowly discharged in hole, extends the term of validity of feed, at the same time
Cavernous clam shell powder can be with the heavy metal in adsorbed water body, plankton, existing inorganic in a variety of manners and have
Machine nitrogen, to reach the effect of water purification；Far-infared ceramic powder is added in feed at the same time, the far-infared ceramic powder of addition is in clam
Promote porous formation in shell calcination, and make hole fine and close, while far-infared ceramic powder can kill bacterium in water, accelerate hydrone
Movement increase oxygen in water, improves water quality.
2nd, the preparation method of the environmentally friendly prawn feed for improving water quality of the invention, by radix astragali, Angelica sinensis, the membrane of a chicken's gizzard, rhizoma anemarrhenae,
Extracted after blackberry lily, part giant knotweed, Phytolacca acinosa these raw materials crushing and with ethanol, and after follow-up fermentation so that feed can improve
The resistance of prawn, reduces incidence.
3rd, the preparation method of the environmentally friendly prawn feed for improving water quality of the invention, by radix astragali, Angelica sinensis, the membrane of a chicken's gizzard, rhizoma anemarrhenae,
After blackberry lily, giant knotweed, Phytolacca acinosa crush, the softening of the cell wall of raw material is first soaked and then can made with acetum with soda water, then will
It is immersion, 10~12h of holding at -20~-25 DEG C in 95~100 DEG C of water with temperature, after raw material contacts hot water, cell
Wall can expand, and have an effect that part cell reaches broken wall again, and the body of the liquid water of the more same quality of volume after water freezing
Product increase, moisture build-up ice in the short time trichite life volumetric expansion while, also quickly can fully burst plant medicinal material
Cell membrane, reaches more effective shell-broken effect, so as to fully discharge the active ingredient of each raw material, substantially increases drug effect.
4th, the preparation method of the environmentally friendly prawn feed for improving water quality of the invention, also contains in fermentation medium of the invention
There are ferrous sulfate, zinc sulfate, manganese sulfate to provide mineral nutrient element for prawn；In fermentation medium also containing photosynthetic bacteria,
Actinomyces, EM bacterium its organic matter degradations such as the nitrate in water body, nitrite, ammonia nitrogen can be converted into can by prawn absorb
Material, and water body dissolved oxygen amount can be increased, following for quickening polluted-water material is bad, maintains Ecology balance.
5th, the preparation method of the environmentally friendly prawn feed for improving water quality of the invention, also contains phagostimulant, in phagostimulant
Garlic contains allicin not only with good attractant effect also with bactericidal effect；Illiciumverum, hawthorn, peppermint have special fragrance
The appetite of prawn can be increased；, can be big containing substantial amounts of amino acid and nucleotide is largely contained in shrimp shell, cuttlefish powder, albumen powder
It is big to stimulate the smell of prawn, the sense of taste it is gathered around feed, accelerate to ingest, improve feed intake.
Further advantage, target and the feature of the present invention embodies part by following explanation, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to specification
Word can be implemented according to this.
It should be noted that experimental method described in following embodiments, is conventional method unless otherwise specified, institute
Reagent and material are stated, unless otherwise specified, is commercially obtained.
Embodiment 1
A kind of preparation method for the environmentally friendly prawn feed for improving water quality, comprises the following steps：
S1, by parts by weight be 30 parts clam shell crush after, it is 10% to be subsequently placed in the mass concentration that parts by weight are 50 parts
Phosphoric acid solution in temperature be 30 DEG C at soak 2h, take out, clean；Then the clam shell after cleaning is placed in parts by weight as 20
Part mass concentration be to soak 20min in 5% sodium carbonate liquor, take out, with parts by weight be 0.5 part remote after cleaning, drying
After mixing, calcination, obtains modified clam shell powder to infrared ceramic powder；
S2, the radix astragali by parts by weight are 3 parts, 2 parts of Angelica sinensis, 3 parts of the membrane of a chicken's gizzard, 2 parts of rhizoma anemarrhenae, 3 parts of blackberry lily, 3 parts
Giant knotweed, 3 parts of Phytolacca acinosa mixed grinding crush, and are subsequently placed in the ethanol solution that the mass fraction that parts by weight are 80 parts is 70% and return
10h is flowed, collects filtrate and filter residue；
S3, the corn flour by parts by weight are 20 parts, 15 parts of fish meal, 15 parts of rapeseed dregs, 15 parts of dregs of beans, 10 parts of silkworm
It is the 10d that ferments at 50 DEG C that filter residue, 10 parts of fermentation medium in pupa, S2, which are mixed after temperature, obtains the first fermentate；Then will
First fermentate and modified clam shell powder in mass ratio 3:After 1 mixing, it is then the 2d that ferments at 60 DEG C in temperature, filters, is dry
Obtain the second fermentate；
S4, be 100 in mass ratio:0.1:Filtrate in 8 the second fermentates of mixing, multi-vitamins, S1, stirs evenly, makes
Grain, drying, to obtain the final product；
Wherein, the preparation method of fermentation medium is：By molasses that parts by weight are 0.3 part, 1 part of ferrous sulfate, 3 parts
Zinc sulfate, 3 parts of manganese sulfate, 0.1 part of photosynthetic bacteria, the mixing of 10 parts of water are after anaerobic fermentation 2d under illumination condition, then
Add parts by weight be 0.05 part saccharomycete, 0.1 part of actinomyces, 0.1 part of EM bacterium aerobic fermentations 3d to obtain the final product.
The preparation method of the environmentally friendly prawn feed for improving water quality, it is the second fermentate to further include quality in S4
5% phagostimulant of quality is mixed with filtrate in the second fermentate, multi-vitamins, S1；The preparation bag of wherein described phagostimulant
Include following steps：
Step 1: by parts by weight be 1 part illiciumverum, 2 parts of vomiting nut, 1 part of onion, 2 parts of garlic, 1 part of hawthorn,
2 parts of peppermint is added after crushing in the water that parts by weight are 30 parts, stirring, and adds the complex enzyme zymohydrolysis 1h that parts by weight are 0.1 part,
Enzyme deactivation, obtains slurry；Wherein, it is 1 that complex enzyme, which includes mass ratio,:2:1:1:2 lywallzyme, pectase, cellulase, protease
And lipase；
Step 2: by parts by weight be 5 parts maize flour, 5 parts of shrimp shell, 2 parts of Pizza grass mixed grinding Cheng Fenhou with again
The cuttlefish powder, 8 parts of albumen powder, 0.1 part of carvacrol, the mixing of 5 parts of slurry that part is 10 parts are measured, is granulated, up to phagostimulant.
The preparation method of the environmentally friendly prawn feed for improving water quality, it is 300 DEG C that calcination, which is included prior to temperature, in S1
Lower calcination 1h；Then 550 DEG C are warming up to as 6 DEG C/min using heating rate and keep 1h, then be cooled to 8 DEG C/min rate of temperature fall
350 DEG C and 30min is kept, be then warming up to 700 DEG C as 10 DEG C/min using heating rate again and keep 0.5h, be subsequently cooled to room
Temperature, obtains modified clam shell powder.
The preparation method of the environmentally friendly prawn feed for improving water quality, radix astragali in S2, Angelica sinensis, the membrane of a chicken's gizzard, rhizoma anemarrhenae, penetrate
After dry, giant knotweed, Phytolacca acinosa mixed grinding crush, it is to be soaked at 25 DEG C to add in the soda water that parts by weight are 120 parts in temperature
20min, separating mixture, then again into mixture add parts by weight be 120 parts mass concentration be 2% acetum in
It is to soak 0.5h at 30 DEG C in temperature；Then the mixture addition parts by weight after acetic acid is soaked are 20 parts, temperature is 95 DEG C
1h is soaked in water, 10h is then kept at -20 DEG C, most adds in ethanol solution and flows back after holding 20min at 25 DEG C.
The preparation method of the environmentally friendly prawn feed for improving water quality, during the 10d that ferments in S3, per 2d turnings one
It is secondary.
The preparation method of the environmentally friendly prawn feed for improving water quality, obtains in S3 after the first fermentate and is put
It is to irradiate 10min under the infrared lamp of 500W in power, then carries out second of fermentation.
Embodiment 2
A kind of preparation method for the environmentally friendly prawn feed for improving water quality, comprises the following steps：
S1, by parts by weight be 35 parts clam shell crush after, it is 13% to be subsequently placed in the mass concentration that parts by weight are 55 parts
Phosphoric acid solution in temperature be 40 DEG C at soak 3h, take out, clean；Then the clam shell after cleaning is placed in parts by weight as 25
Part mass concentration be to soak 25min in 6% sodium carbonate liquor, take out, with parts by weight be 0.8 part remote after cleaning, drying
After mixing, calcination, obtains modified clam shell powder to infrared ceramic powder；
S2, the radix astragali by parts by weight are 5 parts, 4 parts of Angelica sinensis, 4 parts of the membrane of a chicken's gizzard, 3 parts of rhizoma anemarrhenae, 4 parts of blackberry lily, 4 parts
Giant knotweed, 4 parts of Phytolacca acinosa mixed grinding crush, and are subsequently placed in the ethanol solution that the mass fraction that parts by weight are 85 parts is 75% and return
13h is flowed, collects filtrate and filter residue；
S3, the corn flour by parts by weight are 25 parts, 18 parts of fish meal, 18 parts of rapeseed dregs, 18 parts of dregs of beans, 13 parts of silkworm
It is the 13d that ferments at 55 DEG C that filter residue, 15 parts of fermentation medium in pupa, S2, which are mixed after temperature, obtains the first fermentate；Then will
First fermentate and modified clam shell powder in mass ratio 4:After 1 mixing, it is then the 3d that ferments at 65 DEG C in temperature, filters, is dry
Obtain the second fermentate；
S4, be 100 in mass ratio:0.2:Filtrate in 8 the second fermentates of mixing, multi-vitamins, S1, stirs evenly, makes
Grain, drying, to obtain the final product；
Wherein, the preparation method of fermentation medium is：By molasses that parts by weight are 0.4 part, 2 parts of ferrous sulfate, 4 parts
Zinc sulfate, 4 parts of manganese sulfate, 0.3 part of photosynthetic bacteria, the mixing of 13 parts of water are after anaerobic fermentation 3d under illumination condition, then
Add parts by weight be 0.08 part saccharomycete, 0.2 part of actinomyces, 0.2 part of EM bacterium aerobic fermentations 5d to obtain the final product.
The preparation method of the environmentally friendly prawn feed for improving water quality, it is the second fermentate to further include quality in S4
8% phagostimulant of quality is mixed with filtrate in the second fermentate, multi-vitamins, S1；The preparation bag of wherein described phagostimulant
Include following steps：
Step 1: by parts by weight be 2 parts illiciumverum, 3 parts of vomiting nut, 2 parts of onion, 3 parts of garlic, 2 parts of hawthorn,
3 parts of peppermint is added after crushing in the water that parts by weight are 35 parts, stirring, and adds the complex enzyme zymohydrolysis 2h that parts by weight are 0.3 part,
Enzyme deactivation, obtains slurry；Wherein, it is 1 that complex enzyme, which includes mass ratio,:3:1:1:3 lywallzyme, pectase, cellulase, protease
And lipase；
Step 2: by parts by weight be 8 parts maize flour, 8 parts of shrimp shell, 3 parts of Pizza grass mixed grinding Cheng Fenhou with again
The cuttlefish powder, 9 parts of albumen powder, 0.3 part of carvacrol, the mixing of 8 parts of slurry that part is 12 parts are measured, is granulated, up to phagostimulant.
The preparation method of the environmentally friendly prawn feed for improving water quality, it is 330 DEG C that calcination, which is included prior to temperature, in S1
Lower calcination 2h；Then 580 DEG C are warming up to as 7 DEG C/min using heating rate and keep 1.5h, then cooled down with 9 DEG C/min rate of temperature fall
To 380 DEG C and 35min is kept, then 730 DEG C is warming up to as 11 DEG C/min using heating rate again and keeps 0.8h, be subsequently cooled to
Room temperature, obtains modified clam shell powder.
The preparation method of the environmentally friendly prawn feed for improving water quality, radix astragali in S2, Angelica sinensis, the membrane of a chicken's gizzard, rhizoma anemarrhenae, penetrate
After dry, giant knotweed, Phytolacca acinosa mixed grinding crush, it is to be soaked at 28 DEG C to add in the soda water that parts by weight are 130 parts in temperature
25min, separating mixture, then again into mixture add parts by weight be 130 parts mass concentration be 3% acetum in
It is to soak 0.8h at 33 DEG C in temperature；Then the mixture addition parts by weight after acetic acid is soaked are 25 parts, temperature is 98 DEG C
2h is soaked in water, 11h is then kept at -23 DEG C, most adds in ethanol solution and flows back after holding 25min at 28 DEG C.
The preparation method of the environmentally friendly prawn feed for improving water quality, during the 13d that ferments in S3, per 3d turnings one
It is secondary.
The preparation method of the environmentally friendly prawn feed for improving water quality, obtains in S3 after the first fermentate and is put
It is to irradiate 15min under the infrared lamp of 800W in power, then carries out second of fermentation.
Embodiment 3
A kind of preparation method for the environmentally friendly prawn feed for improving water quality, comprises the following steps：
S1, by parts by weight be 40 parts clam shell crush after, it is 15% to be subsequently placed in the mass concentration that parts by weight are 60 parts
Phosphoric acid solution in temperature be 50 DEG C at soak 3h, take out, clean；Then the clam shell after cleaning is placed in parts by weight as 30
Part mass concentration be to soak 30min in 8% sodium carbonate liquor, take out, with parts by weight be 1 part remote red after cleaning, drying
After mixing, calcination, obtains modified clam shell powder to outer ceramic powder；
S2, the radix astragali by parts by weight are 6 parts, 5 parts of Angelica sinensis, 5 parts of the membrane of a chicken's gizzard, 5 parts of rhizoma anemarrhenae, 5 parts of blackberry lily, 5 parts
Giant knotweed, 5 parts of Phytolacca acinosa mixed grinding crush, and are subsequently placed in the ethanol solution that the mass fraction that parts by weight are 90 parts is 80% and return
15h is flowed, collects filtrate and filter residue；
S3, the corn flour by parts by weight are 30 parts, 20 parts of fish meal, 20 parts of rapeseed dregs, 20 parts of dregs of beans, 15 parts of silkworm
It is the 15d that ferments at 60 DEG C that filter residue, 20 parts of fermentation medium in pupa, S2, which are mixed after temperature, obtains the first fermentate；Then will
First fermentate and modified clam shell powder in mass ratio 5:After 1 mixing, it is then the 3d that ferments at 70 DEG C in temperature, filters, is dry
Obtain the second fermentate；
S4, be 100 in mass ratio:0.2:Filtrate in 10 the second fermentates of mixing, multi-vitamins, S1, stirs evenly, makes
Grain, drying, to obtain the final product；
Wherein, the preparation method of fermentation medium is：By molasses that parts by weight are 0.5 part, 2 parts of ferrous sulfate, 4 parts
Zinc sulfate, 5 parts of manganese sulfate, 0.5 part of photosynthetic bacteria, the mixing of 15 parts of water are after anaerobic fermentation 3d under illumination condition, then
Add parts by weight be 0.1 part saccharomycete, 0.2 part of actinomyces, 0.2 part of EM bacterium aerobic fermentations 5d to obtain the final product.
The preparation method of the environmentally friendly prawn feed for improving water quality, it is the second fermentate to further include quality in S4
10% phagostimulant of quality is mixed with filtrate in the second fermentate, multi-vitamins, S1；The preparation bag of wherein described phagostimulant
Include following steps：
Step 1: by parts by weight be 2 parts illiciumverum, 3 parts of vomiting nut, 2 parts of onion, 3 parts of garlic, 2 parts of hawthorn,
3 parts of peppermint is added after crushing in the water that parts by weight are 40 parts, stirring, and adds the complex enzyme zymohydrolysis 2h that parts by weight are 0.5 part,
Enzyme deactivation, obtains slurry；Wherein, it is 1 that complex enzyme, which includes mass ratio,:3:2:2:3 lywallzyme, pectase, cellulase, protease
And lipase；
Step 2: by parts by weight be 10 parts maize flour, 10 parts of shrimp shell, 5 parts of Pizza grass mixed grinding Cheng Fenhou with
Parts by weight are 15 parts of cuttlefish powder, 10 parts of albumen powder, 0.5 part of carvacrol, 10 parts of slurry mix, and are granulated, up to food calling
Agent.
The preparation method of the environmentally friendly prawn feed for improving water quality, it is 350 DEG C that calcination, which is included prior to temperature, in S1
Lower calcination 2h；Then 600 DEG C are warming up to as 8 DEG C/min using heating rate and keep 1.5h, then dropped with 10 DEG C/min rate of temperature fall
Temperature is to 400 DEG C and keeps 40min, is then warming up to 750 DEG C as 12 DEG C/min using heating rate again and keeps 1h, is subsequently cooled to
Room temperature, obtains modified clam shell powder.
The preparation method of the environmentally friendly prawn feed for improving water quality, radix astragali in S2, Angelica sinensis, the membrane of a chicken's gizzard, rhizoma anemarrhenae, penetrate
After dry, giant knotweed, Phytolacca acinosa mixed grinding crush, it is to be soaked at 30 DEG C to add in the soda water that parts by weight are 150 parts in temperature
30min, separating mixture, then again into mixture add parts by weight be 150 parts mass concentration be 4% acetum in
It is to soak 1h at 35 DEG C in temperature；Then the mixture addition parts by weight after acetic acid is soaked are 30 parts, the water that temperature is 100 DEG C
Middle immersion 2h, then keeps 12h at -25 DEG C, most adds in ethanol solution and flows back after holding 30min at 30 DEG C.
The preparation method of the environmentally friendly prawn feed for improving water quality, during the 15d that ferments in S3, per 3d turnings one
It is secondary.
The preparation method of the environmentally friendly prawn feed for improving water quality, obtains in S3 after the first fermentate and is put
It is to irradiate 20min under the infrared lamp of 1000W in power, then carries out second of fermentation.
Prawn feed prepared by embodiment 1 and Wudi Rui Xing bio tech ltd production prawn feed as pair
According to group, cultivation comparison is carried out under the same conditions, and the index for cultivating raw water is：DO is 4.2mg/L, COD 17.3mg/
L, TN 1.38mg/L, TP 0.083mg/L, measure front and rear change of water quality in breeding process, the results are shown in Table 1；
Prawn feed prepared by embodiment 1~3 and the prawn feed of Wudi Rui Xing bio tech ltd production are made
For control group, 1000 tail south prawns (average weight is 0.33g ± 0.04g) are launched under the same conditions, experimental group is fed respectively
The feed of embodiment 1~3, control group feed the prawn feed of Wudi Rui Xing bio tech ltd production.Supported by 60 days
Grow, measure the prawn average growth rate of each group survival respectively, the results are shown in Table 2 for rate for morbidity (fin rot, soft-shell disease).
The feed of embodiment 1 is in cultured prawn breeding process as can be seen from Table 1, and DO increases, COD, TN, TP are equal
Decline, water quality reaches cultivation water quality standard.Control group feed cultured prawn, although indices also superior to raw water, embodiment 1
Feed in the incrementss for cultivating early period and later stage DO in contrast, be all higher than the incrementss of control group, the slippage of COD, TN, TP
The slippage of control group is all higher than, therefore the feed purifying water effect of the present invention is substantially better than control feed.
Feed of the invention is cultivating in cultured prawn breeding process in the feed of the present invention as can be seen from Table 2
During fin rot, the incidence of soft-shell disease be respectively less than the incidence of control group, and rate of body weight gain is more than control group, illustrates the present invention
Feed have effects that promote prawn growth and reduce incidence.
Table 1 cultivates front and rear change of water quality
The incidence and yield of 2 different feeds cultured prawn of table
| Index | Fin rot (%) | Soft-shell disease (%) | Average growth rate (%) |
| Embodiment 1 | 0.9 | 0.7 | 2198.36 |
| Embodiment 2 | 0.8 | 0.6 | 2281.53 |
| Embodiment 3 | 0.7 | 0.6 | 2281.53 |
| Control group | 1.5 | 1.8 | 1881.53 |
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Realize other modification, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited
In specific details.
Claims (6)
1. a kind of preparation method for the environmentally friendly prawn feed for improving water quality, it is characterised in that comprise the following steps：
S1, by parts by weight be 30~40 parts clam shell crush after, being subsequently placed in the mass concentration that parts by weight are 50~60 parts is
2~3h is soaked at temperature is 30~50 DEG C in 10~15% phosphoric acid solution, is taken out, is cleaned；Then by the clam after cleaning
Shell is placed in 20~30min of immersion in the sodium carbonate liquor that the mass concentration that parts by weight are 20~30 parts is 5~8%, takes out, washes
Only, after dry with far-infared ceramic powder that parts by weight are 0.5~1 part after mixing, calcination, obtains modified clam shell powder；
S2, the radix astragali by parts by weight are 3~6 parts, 2~5 parts of Angelica sinensis, 3~5 parts of the membrane of a chicken's gizzard, 2~5 parts of rhizoma anemarrhenae, 3~5 parts
Blackberry lily, 3~5 parts of giant knotweed, 3~5 parts of Phytolacca acinosa mixed grinding crush, and are subsequently placed in the mass fraction that parts by weight are 80~90 parts
For the 10~15h that flows back in 70~80% ethanol solution, filtrate and filter residue are collected；
S3, the corn flour by parts by weight are 20~30 parts, 15~20 parts of fish meal, 15~20 parts of rapeseed dregs, 15~20 parts
Dregs of beans, 10~15 parts of silkworm chrysalis, the filter residue in S2, the mixing of 10~20 parts of fermentation medium are issued after temperature for 50~60 DEG C
10~15d of ferment, obtains the first fermentate；Then by the first fermentate and modified clam shell powder in mass ratio 3~5:After 1 mixing, so
After temperature be the 2~3d that ferments at 60~70 DEG C, filtering, dry the second fermentate；
S4, be 100 in mass ratio:0.1~0.2:Filtrate in 5~10 the second fermentates of mixing, multi-vitamins, S1, stirring are equal
It is even, it is granulated, drying, to obtain the final product；
Wherein, the preparation method of fermentation medium is：It is 0.3~0.5 part of molasses, 1~2 part of ferrous sulfate, 3 by parts by weight
~4 parts of zinc sulfate, 3~5 parts of manganese sulfate, 0.1~0.5 part of photosynthetic bacteria, 10~15 parts of water are mixed after illumination bar
2~3d of anaerobic fermentation under part, then add parts by weight be 0.05~0.1 part saccharomycete, 0.1~0.2 part of actinomyces,
0.1~0.2 part of 3~5d of EM bacterium aerobic fermentations to obtain the final product.
2. the preparation method of the environmentally friendly prawn feed of water quality can be improved as claimed in claim 1, it is characterised in that also wrapped in S4
Include and mix quality with filtrate in the second fermentate, multi-vitamins, S1 for 5~10% phagostimulant of the second fermentate quality
Close；The preparation of wherein described phagostimulant comprises the following steps：
Step 1: it is 1~2 part of illiciumverum, 2~3 parts of vomiting nut, 1~2 part of onion, 2~3 parts of garlic, 1 by parts by weight
~2 parts of hawthorn, 2~3 parts of peppermint are added after crushing in the water that parts by weight are 30~40 parts, stirring, and are added parts by weight and be
0.1~0.5 part of 1~2h of complex enzyme zymohydrolysis, enzyme deactivation, obtains slurry；Wherein, it is 1 that complex enzyme, which includes mass ratio,:2~3:1~2:
1~2:2~3 lywallzyme, pectase, cellulase, protease and lipase；
Step 2: by maize flour that parts by weight are 5~10 parts, 5~10 parts of shrimp shell, 2~5 parts of Pizza grass mixed grinding into powder
It is afterwards 10~15 parts of cuttlefish powder, 8~10 parts of albumen powder, 0.1~0.5 part of carvacrol, 5~10 parts of slurry with parts by weight
Mixing, is granulated, up to phagostimulant.
3. the preparation method of the environmentally friendly prawn feed of water quality can be improved as claimed in claim 1, it is characterised in that be calcined in S1
Including being that 1~2h is calcined at 300~350 DEG C prior to temperature；Then 550~600 are warming up to by 6~8 DEG C/min of heating rate
DEG C and keep 1~1.5h, then with 8~10 DEG C/min rate of temperature fall be cooled to 350~400 DEG C and keep 30~40min, Ran Houzai
700~750 DEG C are warming up to as 10~12 DEG C/min using heating rate and keep 0.5~1h, be subsequently cooled to room temperature, must be modified text
Concha Meretricis Seu Cyclinae powder.
4. the preparation method of the environmentally friendly prawn feed of water quality can be improved as claimed in claim 1, it is characterised in that yellow in S2
After stilbene, Angelica sinensis, the membrane of a chicken's gizzard, rhizoma anemarrhenae, blackberry lily, giant knotweed, Phytolacca acinosa mixed grinding crush, the soda that parts by weight are 120~150 parts is added
20~30min is soaked in water at temperature is 25~30 DEG C, separating mixture, parts by weight are then added into mixture again is
In the acetum that 120~150 parts of mass concentration is 2~4% in temperature be at 30~35 DEG C immersion 0.5~1h；Then will
Acetic acid immersion after mixture add parts by weight be 20~30 parts, in the water that temperature is 95~100 DEG C soak 1~2h, then in-
10~12h is kept at 20~-25 DEG C, most adds in ethanol solution and flows back after 20~30min of holding at 25~30 DEG C.
5. the preparation method of the environmentally friendly prawn feed of water quality can be improved as claimed in claim 1, it is characterised in that ferment in S3
During 10~15d, every 2~3d turnings are once.
6. the preparation method of the environmentally friendly prawn feed of water quality can be improved as claimed in claim 1, it is characterised in that obtained in S3
After first fermentate and 10~20min of irradiation under the infrared lamp that power is 500~1000W is placed on, then carries out second of hair
Ferment.
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6214993A (en) * | 1985-07-10 | 1987-01-23 | Nissho:Kk | Preservative for drinking water |
| CN101664116A (en) * | 2008-09-04 | 2010-03-10 | 李活 | Method for preparing multifunctional shrimp feed additive by using oyster shell powder and gracilaria powder as carriers |
| CN101715742A (en) * | 2009-11-16 | 2010-06-02 | 大连金砣水产食品有限公司 | Holothurian cultivation pond water quality modifier and preparation method thereof |
| CN105053002A (en) * | 2015-08-07 | 2015-11-18 | 梁友 | Shell powder, preparation method thereof, modification method thereof and application thereof |
| CN105284883A (en) * | 2015-09-15 | 2016-02-03 | 青岛大学 | Buffer system oyster shell pesticide residue-removal antibacterial material and preparation method and use method thereof |
| CN106278769A (en) * | 2016-08-31 | 2017-01-04 | 恒茂实业集团有限公司 | A kind of aquaculture nutrition slow-release agent and preparation method thereof |
| CN107028027A (en) * | 2017-05-08 | 2017-08-11 | 浦江海璞食品科技有限公司 | The preparation method of culture of Penaeus vannamei feed |
-
2017
- 2017-12-04 CN CN201711282770.XA patent/CN107981104A/en not_active Withdrawn
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6214993A (en) * | 1985-07-10 | 1987-01-23 | Nissho:Kk | Preservative for drinking water |
| CN101664116A (en) * | 2008-09-04 | 2010-03-10 | 李活 | Method for preparing multifunctional shrimp feed additive by using oyster shell powder and gracilaria powder as carriers |
| CN101715742A (en) * | 2009-11-16 | 2010-06-02 | 大连金砣水产食品有限公司 | Holothurian cultivation pond water quality modifier and preparation method thereof |
| CN105053002A (en) * | 2015-08-07 | 2015-11-18 | 梁友 | Shell powder, preparation method thereof, modification method thereof and application thereof |
| CN105284883A (en) * | 2015-09-15 | 2016-02-03 | 青岛大学 | Buffer system oyster shell pesticide residue-removal antibacterial material and preparation method and use method thereof |
| CN106278769A (en) * | 2016-08-31 | 2017-01-04 | 恒茂实业集团有限公司 | A kind of aquaculture nutrition slow-release agent and preparation method thereof |
| CN107028027A (en) * | 2017-05-08 | 2017-08-11 | 浦江海璞食品科技有限公司 | The preparation method of culture of Penaeus vannamei feed |
Non-Patent Citations (1)
| Title |
|---|
| 曲远方: "《现代陶瓷材料及技术》", 31 May 2008, 华东理工大学出版社 * |
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