CN107881781A - 一种刺绣用透气整理剂的制备方法 - Google Patents

一种刺绣用透气整理剂的制备方法 Download PDF

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CN107881781A
CN107881781A CN201711238694.2A CN201711238694A CN107881781A CN 107881781 A CN107881781 A CN 107881781A CN 201711238694 A CN201711238694 A CN 201711238694A CN 107881781 A CN107881781 A CN 107881781A
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王学珍
王丽佳
王月忠
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Suzhou Embroidery Art World Embroidery Technology Co Ltd
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Abstract

本申请公开了一种刺绣用透气整理剂的制备方法，称取水、二硝基苯酚、活性剂、二元酸、羧甲基纤维素、聚乙二醇双硬脂酸酯、六水硫酸镁、乙基纤维素、海藻酸钠、双草酸酯和乙二醇；制备方法简单，透气性能好，防霉效果好，抗拉强度3‑5MPa，抗潮气性优良；工艺简单，光泽度高，附着力1级，耐腐蚀性好，耐磨性能好，胶黏强度高；抗收缩，使用方便，耐水洗性65‑85次螨虫趋避率92.5‑96.5%，柔韧性1mm，光泽度好；成本低廉，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率98.8‑99.2%，可以广泛生产并不断代替现有材料。

Description

一种刺绣用透气整理剂的制备方法
技术领域
本申请属于刺绣材料领域，尤其涉及一种刺绣用透气整理剂的制备方法。
背景技术
无甲醛防皱整理剂DPH适用于棉、麻、人造棉及其混纺织物的防皱和耐久压烫整理。经其整理后的织物具有良好的形态记忆和耐洗涤性，无游离甲醛，防缩防绉，外观挺括，手感丰满柔软，耐洗耐磨性好，高温下不泛黄，没有色变现象。弹性可提高70-90%，强力保留率70-80%，平挺度3.5级以上。织物穿着舒适，洗涤后不需再熨烫平整，压线长久保持。
顾绣针法，最主要继承了宋代最完备之已成绣法，更加以变化而运用之，可谓集针法之大成。用线主要仍多数用平线，有时亦用捻线，丝细如发，针脚平整，而所用色线种类之多，则非宋绣所能比拟。同时又使用中间色线，借色与补色，绣绘并用，力求逼真原稿。又视图案所需，可以随意取材，不拘成法，真草、暹罗斗鸡尾毛，薄金、头发均可入绣别创新意，尤其利用发绣完成绘画之制作，于世界染织史上从未一见，即此可知顾绣有极其巧妙精微之刺绣技术。
雕绣又称楼空绣，是一种有一定难度、效果十分别致的绣法。它的最大特点是在绣制过程中，按花纹需要修剪出孔洞，并在剪出的孔洞里以不同方法绣出多种图案组合，使绣面上既有洒脱大方的实地花，又有玲戏美观的楼空花，虚实相衬，富有情趣。绣品高雅、精致。
织物防水整理的历史悠久，我国在魏、晋、六朝时期就已经有了防水整理的产品，而含氟烷基化合物作为织物防水防油整理剂的实用化是在20世纪50年代。1950年，美国DuPont（杜邦）公司率先以聚四氟乙烯（PTFE）乳液作为织物整理剂，并发表专利。随后，美国3M公司成功合成了含氟烷基丙烯酸酯共聚物，用于织物防水防油整理。此后，越来越多的商品话防水整理剂问世，市场竞争也越来越激烈。
铝皂、石蜡/金属盐类整理剂（石蜡-铝盐、石蜡-锆盐等）：利用石蜡乳液和金属盐的水分散液浸渍织物，经烘干和热处理后生成金属盐氧化物或者氢氧化，与石蜡的混合物沉积于织物上，赋予织物的防水性。
对所有的纤维面料都有良好的防水防油性能。加工稳定性好。加工后，织物的手感柔软。无着火点，属非危险品类，使用更安全。不含有可能产生诱异作用的聚环氧乙烷苯酚醛物质等环境激素。适用于天然纤维（毛、丝、棉）、涤棉混纺、镜棉混纺、合成纤维（涤纶、尼龙）等织物面料的一般防水加工。
发明内容
解决的技术问题：
本申请针对上述技术问题，提供一种刺绣用透气整理剂的制备方法，解决现有刺绣用透气整理剂防霉效果差、光泽度低和透气性差等技术问题。
技术方案：
一种刺绣用透气整理剂的制备方法，包括如下步骤：
第一步：按照重量份数配比称取水100份、二硝基苯酚0.3-0.7份、活性剂3-7份、二元酸8-12份、羧甲基纤维素30-50份、聚乙二醇双硬脂酸酯15-35份、六水硫酸镁5-25份、乙基纤维素10-30份、海藻酸钠2-6份、双草酸酯5-15份和乙二醇4-8份；
第二步：将聚乙二醇双硬脂酸酯、乙基纤维素和海藻酸钠投入带有温度计、搅拌机和加热装置的反应釜中，升温至60-70℃，打开搅拌机混合，混合速度为200-300r/min，混合60-100min；
第三步：依次加入羧甲基纤维素、水和二硝基苯酚，调节混合速度至350-450 r/min，混合1-3h，升温至90-110℃，加入剩余原料，搅拌均匀后将混合均匀的产物投入砂磨机中，砂磨20-40min，筛网过滤后即得。
作为本发明的一种优选技术方案：所述第一步中刺绣用透气整理剂的原料按重量份数配比如下：水100份、二硝基苯酚0.3份、活性剂3份、二元酸8份、羧甲基纤维素30份、聚乙二醇双硬脂酸酯15份、六水硫酸镁5份、乙基纤维素10份、海藻酸钠2份、双草酸酯5份和乙二醇4份。
作为本发明的一种优选技术方案：所述第一步中刺绣用透气整理剂的原料按重量份数配比如下：水100份、二硝基苯酚0.7份、活性剂7份、二元酸12份、羧甲基纤维素50份、聚乙二醇双硬脂酸酯35份、六水硫酸镁25份、乙基纤维素30份、海藻酸钠6份、双草酸酯15份和乙二醇8份。
作为本发明的一种优选技术方案：所述第一步中刺绣用透气整理剂的原料按重量份数配比如下：水100份、二硝基苯酚0.5份、活性剂5份、二元酸10份、羧甲基纤维素40份、聚乙二醇双硬脂酸酯25份、六水硫酸镁15份、乙基纤维素20份、海藻酸钠4份、双草酸酯10份和乙二醇6份。
作为本发明的一种优选技术方案：所述活性剂采用氧化锌。
有益效果：
本发明所述一种刺绣用透气整理剂的制备方法采用以上技术方案与现有技术相比，具有以下技术效果：1、制备方法简单，透气性能好，防霉效果好，抗拉强度3-5MPa，抗潮气性优良；2、工艺简单，光泽度高，附着力1级，耐腐蚀性好，耐磨性能好，胶黏强度高；3、抗收缩，使用方便，耐水洗性65-85次螨虫趋避率92.5-96.5%，柔韧性1mm，光泽度好；4、成本低廉，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率98.8-99.2%，可以广泛生产并不断代替现有材料。
具体实施方式
实施例1:
按照重量份数配比称取水100份、二硝基苯酚0.3份、氧化锌3份、二元酸8份、羧甲基纤维素30份、聚乙二醇双硬脂酸酯15份、六水硫酸镁5份、乙基纤维素10份、海藻酸钠2份、双草酸酯5份和乙二醇4份。
将聚乙二醇双硬脂酸酯、乙基纤维素和海藻酸钠投入带有温度计、搅拌机和加热装置的反应釜中，升温至60℃，打开搅拌机混合，混合速度为200r/min，混合60min。
依次加入羧甲基纤维素、水和二硝基苯酚，调节混合速度至350r/min，混合1h，升温至90℃，加入剩余原料，搅拌均匀后将混合均匀的产物投入砂磨机中，砂磨20min，筛网过滤后即得。
制备方法简单，透气性能好，防霉效果好，抗拉强度3MPa，抗潮气性优良；工艺简单，光泽度高，附着力1级，耐腐蚀性好，耐磨性能好，胶黏强度高；抗收缩，使用方便，耐水洗性65次螨虫趋避率92.5%，柔韧性1mm，光泽度好；成本低廉，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率98.8%，可以广泛生产并不断代替现有材料。
实施例2:
按照重量份数配比称取水100份、二硝基苯酚0.7份、氧化锌7份、二元酸12份、羧甲基纤维素50份、聚乙二醇双硬脂酸酯35份、六水硫酸镁25份、乙基纤维素30份、海藻酸钠6份、双草酸酯15份和乙二醇8份。
将聚乙二醇双硬脂酸酯、乙基纤维素和海藻酸钠投入带有温度计、搅拌机和加热装置的反应釜中，升温至70℃，打开搅拌机混合，混合速度为300r/min，混合100min。
依次加入羧甲基纤维素、水和二硝基苯酚，调节混合速度至450 r/min，混合3h，升温至110℃，加入剩余原料，搅拌均匀后将混合均匀的产物投入砂磨机中，砂磨40min，筛网过滤后即得。
制备方法简单，透气性能好，防霉效果好，抗拉强度4MPa，抗潮气性优良；工艺简单，光泽度高，附着力1级，耐腐蚀性好，耐磨性能好，胶黏强度高；抗收缩，使用方便，耐水洗性75次螨虫趋避率94.5%，柔韧性1mm，光泽度好；成本低廉，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率99%，可以广泛生产并不断代替现有材料。
实施例3:
按照重量份数配比称取水100份、二硝基苯酚0.5份、氧化锌5份、二元酸10份、羧甲基纤维素40份、聚乙二醇双硬脂酸酯25份、六水硫酸镁15份、乙基纤维素20份、海藻酸钠4份、双草酸酯10份和乙二醇6份。
将聚乙二醇双硬脂酸酯、乙基纤维素和海藻酸钠投入带有温度计、搅拌机和加热装置的反应釜中，升温至65℃，打开搅拌机混合，混合速度为250r/min，混合80min。
依次加入羧甲基纤维素、水和二硝基苯酚，调节混合速度至400 r/min，混合2h，升温至100℃，加入剩余原料，搅拌均匀后将混合均匀的产物投入砂磨机中，砂磨30min，筛网过滤后即得。
制备方法简单，透气性能好，防霉效果好，抗拉强度5MPa，抗潮气性优良；工艺简单，光泽度高，附着力1级，耐腐蚀性好，耐磨性能好，胶黏强度高；抗收缩，使用方便，耐水洗性85次螨虫趋避率96.5%，柔韧性1mm，光泽度好；成本低廉，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率99.2%，可以广泛生产并不断代替现有材料。
以上实施例中的组合物所有组分均可以商业购买。
上述实施例只是用于对本发明的内容进行阐述，而不是限制，因此在与本发明的权利要求书相当的含义和范围内的任何改变，都应该认为是包括在权利要求书的范围内。

Claims (5)

1.一种刺绣用透气整理剂的制备方法，其特征在于，包括如下步骤：
第一步：按照重量份数配比称取水100份、二硝基苯酚0.3-0.7份、活性剂3-7份、二元酸8-12份、羧甲基纤维素30-50份、聚乙二醇双硬脂酸酯15-35份、六水硫酸镁5-25份、乙基纤维素10-30份、海藻酸钠2-6份、双草酸酯5-15份和乙二醇4-8份；
第二步：将聚乙二醇双硬脂酸酯、乙基纤维素和海藻酸钠投入带有温度计、搅拌机和加热装置的反应釜中，升温至60-70℃，打开搅拌机混合，混合速度为200-300r/min，混合60-100min；
第三步：依次加入羧甲基纤维素、水和二硝基苯酚，调节混合速度至350-450 r/min，混合1-3h，升温至90-110℃，加入剩余原料，搅拌均匀后将混合均匀的产物投入砂磨机中，砂磨20-40min，筛网过滤后即得。
2.根据权利要求1所述的刺绣用透气整理剂的制备方法，其特征在于：所述第一步中刺绣用透气整理剂的原料按重量份数配比如下：水100份、二硝基苯酚0.3份、活性剂3份、二元酸8份、羧甲基纤维素30份、聚乙二醇双硬脂酸酯15份、六水硫酸镁5份、乙基纤维素10份、海藻酸钠2份、双草酸酯5份和乙二醇4份。
3.根据权利要求1所述的刺绣用透气整理剂的制备方法，其特征在于：所述第一步中刺绣用透气整理剂的原料按重量份数配比如下：水100份、二硝基苯酚0.7份、活性剂7份、二元酸12份、羧甲基纤维素50份、聚乙二醇双硬脂酸酯35份、六水硫酸镁25份、乙基纤维素30份、海藻酸钠6份、双草酸酯15份和乙二醇8份。
4.根据权利要求1所述的刺绣用透气整理剂的制备方法，其特征在于：所述第一步中刺绣用透气整理剂的原料按重量份数配比如下：水100份、二硝基苯酚0.5份、活性剂5份、二元酸10份、羧甲基纤维素40份、聚乙二醇双硬脂酸酯25份、六水硫酸镁15份、乙基纤维素20份、海藻酸钠4份、双草酸酯10份和乙二醇6份。
5.根据权利要求1所述的刺绣用透气整理剂的制备方法，其特征在于：所述活性剂采用氧化锌。
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Publication number Priority date Publication date Assignee Title
CN1167177A (zh) * 1997-01-06 1997-12-10 刘采英 织物防水透气整理剂
CN103741452A (zh) * 2013-12-17 2014-04-23 江苏金太阳纺织科技有限公司 一种衬衫整理液及其制备方法
CN106637950A (zh) * 2016-12-15 2017-05-10 吴江市北厍盛源纺织品助剂厂 一种增强纺织物透气性的整理剂及其制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1167177A (zh) * 1997-01-06 1997-12-10 刘采英 织物防水透气整理剂
CN103741452A (zh) * 2013-12-17 2014-04-23 江苏金太阳纺织科技有限公司 一种衬衫整理液及其制备方法
CN106637950A (zh) * 2016-12-15 2017-05-10 吴江市北厍盛源纺织品助剂厂 一种增强纺织物透气性的整理剂及其制备方法

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