CN107822984A - A kind of black tea toothpaste with antiallergy reparation and preparation method thereof - Google Patents
A kind of black tea toothpaste with antiallergy reparation and preparation method thereof Download PDFInfo
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- CN107822984A CN107822984A CN201711249322.XA CN201711249322A CN107822984A CN 107822984 A CN107822984 A CN 107822984A CN 201711249322 A CN201711249322 A CN 201711249322A CN 107822984 A CN107822984 A CN 107822984A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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Abstract
The invention discloses a kind of black tea toothpaste with antiallergy reparation and preparation method thereof, including following component by weight percentage：Black tea extract 12~20%, hydrated silica 18~28%, calcium silicates 0.6~1%, sodium monofluorophosphate 1.25~1.6%, glycerine 18~25%, propane diols 9~15%, xylitol 6~10%, stevioside 3~5%, mint extract 2.2~5.2%, laruyl alcohol sodium sulfovinate 1.5~3.5%, and deionized water surplus.A kind of preparation method of black tea toothpaste with antiallergy reparation provided by the invention, using supercritical fluid extraction, extraction yield is high, active ingredient is enriched in toothpaste, with significant antibacterial bacteriostatic, alleviate and eliminate toothache, periodontitis, hemodia symptom, there is salubrious tea perfume, can long-acting holding oral cavity fresh and cool.
Description
Technical field
The invention belongs to toothpaste production field, and in particular to a kind of black tea toothpaste and its preparation side with antiallergy reparation
Method.
Background technology
The life of people as the improvement of people's living standards, varieties of food items is enriched constantly, and carious tooth, hemodia,
The mouth diseases such as periodontitis have also turned into one of disease common in people's life, and this is all due to neglecting for tooth daily nursing
Depending on dental surface breed bacteria forms bacterial plaque, and it is constantly destroyed to ultimately result in tooth structure.Toothpaste is the tooth that people commonly use
Nursing materials, in order to ensure dental health while diet, use the toothpaste day that can effectively take care of one's teeth with gum
Benefit is valued by people.
The principal item of black tea has Hunan black tea, the flat tea of Hubei man, Sichuan brick tea, Guangxi Liu Bao loose teas, yunnan puer tea,
It is a kind of to have long enjoyed a good reputation, the alkaline fermentation tea of decades can be deposited.The black tea extract of sophistication extraction, is rich in
Tea Polyphenols, flavones, multivitamin and trace element, these materials can effectively suppress bacteria breed, prevent bacterial plaque, tooth knot
Stone is formed, and to diseases such as resist gingivitis, periodontitis carious teeth, is protected the health of one's teeth；Meanwhile black tea extract has strong tea
Perfume (or spice), halitosis can be effectively removed, ensure that oral cavity is pleasant pleasant.
In the prior art, for example, the toothpaste containing black tea extract that is provided of application publication number CN105748338A and
Its preparation method, the black tea extract content added is few, the effect very unobvious of bactericidal, the black tea essence of addition, prevents
Rotten agent, saccharin sodium are natural constituents, easily cause consumer's misunderstanding, and finished product function is single, can not meet tooth and oral cavity shield
Manage many demands.
The content of the invention
The purpose of the present invention is the problem of presence for prior art, there is provided a kind of black tea toothpaste with antiallergy reparation
And preparation method thereof, the material and preparation method thereof significantly reaches by adding innate efficacy composition and suppresses oral bacteria, prevent
Bacterial plaque is formed, and decomposes bacterial plaque, the effect of fresh breath.
To achieve the above object, the present invention is achieved through the following technical solutions.
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract 12
~20%, hydrated silica 18~28%, calcium silicates 0.6~1%, sodium monofluorophosphate 1.25~1.6%, glycerine 18~25%, third
Glycol 9~15%, xylitol 6~10%, stevioside 3~5%, mint extract 2.2~5.2%, laruyl alcohol sodium sulfovinate 1.5
~3.5%, and deionized water surplus.
Preferably, including following component by weight percentage：Black tea extract 14~18%, hydrated silica 21~
25%th, calcium silicates 0.8%, sodium monofluorophosphate 1.45%, glycerine 22%, propane diols 12%, xylitol 8%, stevioside 4%, thin
Lotus extract 3.7%, laruyl alcohol sodium sulfovinate 2~3%, and deionized water surplus.
It is highly preferred that including following component by weight percentage：Black tea extract 16%, hydrated silica 23%, silicic acid
Calcium 0.8%, sodium monofluorophosphate 1.45%, glycerine 22%, propane diols 12%, xylitol 8%, stevioside 4%, mint extract
3.7%th, laruyl alcohol sodium sulfovinate 2.5%, and deionized water surplus.
Present invention also offers a kind of preparation method of the black tea toothpaste with antiallergy reparation, comprise the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction respectively, 55~65 DEG C of extraction temperature,
1~2h of extraction time, 25~35MPa of extracting pressure, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Preferably, the extraction temperature of supercritical fluid extraction is 60 DEG C in step S2.
Preferably, the extracting pressure of supercritical fluid extraction is 30MPa in step S2.
Compared with prior art, the beneficial effects of the invention are as follows：1st, natural materials are used containing abundant in toothpaste finished product
Black tea, peppermint are processed obtained corresponding extract, antibacterial, good to anti-plaque formation effect；2nd, black tea extract is realized
With the extraction to greatest extent of mint extract；3rd, the active ingredients such as calcium silicates, sodium monofluorophosphate are with the addition of, can effectively be repaired
The crackle of dental surface, protective layer is formed, reduce hemodia symptom；4th, toothpaste has strong naturally tea perfume and peppermint clear
Perfume (or spice), implication can be effectively removed, keep oral cavity fresh and cool.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.Unless stated otherwise, the reagent of the invention used, method and apparatus is the art conventional reagent, methods
And equipment.
Embodiment 1
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract
20%th, hydrated silica 18%, calcium silicates 1%, sodium monofluorophosphate 1.6%, glycerine 25%, propane diols 9%, xylitol 10%, sweet tea
Chrysanthemum glycosides 5%, mint extract 5.2%, laruyl alcohol sodium sulfovinate 3.5%, and deionized water surplus.
The preparation method of the above-mentioned black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 60 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 30MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Embodiment 2
The present embodiment is substantially the same manner as Example 1, and difference is following aspect.
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract
12%th, hydrated silica 28%, calcium silicates 0.8%, sodium monofluorophosphate 1.6%, glycerine 18%, propane diols 15%, xylitol 6%,
Stevioside 3%, mint extract 2.2%, laruyl alcohol sodium sulfovinate 1.5%, and deionized water surplus.
Embodiment 3
The present embodiment is substantially the same manner as Example 1, and difference is following aspect.
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract
18%th, hydrated silica 25%, calcium silicates 0.8%, sodium monofluorophosphate 1.45%, glycerine 22%, propane diols 12%, xylitol 8%,
Stevioside 4%, mint extract 3.7%, laruyl alcohol sodium sulfovinate 3%, and deionized water surplus.
Embodiment 4
The present embodiment is substantially the same manner as Example 1, and difference is following aspect.
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract
14%th, hydrated silica 21%, calcium silicates 0.8%, sodium monofluorophosphate 1.45%, glycerine 22%, propane diols 12%, xylitol 8%,
Stevioside 4%, mint extract 3.7%, laruyl alcohol sodium sulfovinate 2%, and deionized water surplus.
Embodiment 5
The present embodiment is substantially the same manner as Example 1, and difference is following aspect.
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract
16%th, hydrated silica 23%, calcium silicates 0.8%, sodium monofluorophosphate 1.45%, glycerine 22%, propane diols 12%, xylitol 8%,
Stevioside 4%, mint extract 3.7%, laruyl alcohol sodium sulfovinate 2.5%, and deionized water surplus, each component total amount are
100%.
Embodiment 6
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract
16%th, hydrated silica 23%, calcium silicates 0.8%, sodium monofluorophosphate 1.45%, glycerine 22%, propane diols 12%, xylitol 8%,
Stevioside 4%, mint extract 3.7%, laruyl alcohol sodium sulfovinate 2.5%, and deionized water surplus, each component total amount are
100%.
The preparation method of the above-mentioned black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 65 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 30MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Embodiment 7
The present embodiment is substantially the same manner as Example 6, and difference is in the following areas.
A kind of preparation method of the black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 55 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 30MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Embodiment 8
The present embodiment is substantially the same manner as Example 6, and difference is in the following areas.
A kind of preparation method of the black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 60 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 35MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Embodiment 9
The present embodiment is substantially the same manner as Example 6, and difference is in the following areas.
A kind of preparation method of the black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 60 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 25MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Comparative example 1
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract
22%th, hydrated silica 16%, calcium silicates 0.8%, sodium monofluorophosphate 1.45%, glycerine 27%, propane diols 17%, xylitol
12%th, stevioside 7%, mint extract 5.4%, laruyl alcohol sodium sulfovinate 4%, and deionized water surplus, each component total amount
For 100%.
The preparation method of the above-mentioned black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 60 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 30MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Comparative example 2
This comparative example and comparative example 1 are essentially identical, and difference is in the following areas.
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract
16%th, hydrated silica 23%, calcium silicates 0.8%, sodium monofluorophosphate 1.45%, glycerine 22%, propane diols 12%, xylitol 4%,
Stevioside 4%, mint extract 3.7%, laruyl alcohol sodium sulfovinate 2.5%, and deionized water surplus, each component total amount are
100%.Comparative example 3
A kind of black tea toothpaste with antiallergy reparation, including following component by weight percentage：Black tea extract
16%th, hydrated silica 23%, calcium silicates 0.8%, sodium monofluorophosphate 1.45%, glycerine 22%, propane diols 12%, xylitol 8%,
Stevioside 4%, mint extract 3.7%, laruyl alcohol sodium sulfovinate 2.5%, and deionized water surplus, each component total amount are
100%.
The preparation method of the above-mentioned black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 70 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 30MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Comparative example 4
This comparative example and comparative example 3 are essentially identical, and difference is in the following areas.
A kind of preparation method of the black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 50 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 30MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Comparative example 5
This comparative example and comparative example 3 are essentially identical, and difference is in the following areas.
A kind of preparation method of the black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 60 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 40MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Comparative example 6
This comparative example and comparative example 3 are essentially identical, and difference is in the following areas.
A kind of preparation method of the black tea toothpaste with antiallergy reparation comprises the following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 60 DEG C of extraction temperature, extraction respectively
1~2h of time, extracting pressure 20MPa, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mix
Close uniformly standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mix
Close uniform；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
Application examples 1
Toothpaste finished product sense organ and physical and chemical index evaluation obtained by embodiment 1~9 and comparative example 1~6.
(1) fragrance.Evaluation criteria is with obvious tea smell and cooling taste, free from extraneous odour.
(2) color and luster.Evaluation criteria is sepia.
(3) denseness.
1. method：The toothpaste of embodiment 1~9 and comparative example 1~6 is first extruded to 20mm and abandons it, then extrudes toothpaste again, will
Lotion bar crosses to remaining steel wire successively since first steel wire on denseness frame, makes cream bar crossbearer on steel wire, Mei Geshi
The toothpaste for applying example or comparative example continuously squeezes 3.1min is stood after having squeezed, observation lotion breaks from iron wire falls situation.
2. measurement result criterion：And have in 32 identicals be across the cream bar for not breaking to fall on steel wire it is maximum away from
It is single branch measurement result from (millimeter)；After 3 toothpaste all measure, take wherein 2 toothpaste denseness identicals to be used as and most terminate
Fruit.If less than 9mm (denseness is too small) or more than 33mm (denseness is excessive), it is determined as unqualified, if between 9~33mm, judges
To be qualified.
(4) extraction yield.The weight using supercritical fluid extraction technique extraction black tea extract and mint extract is weighed,
Calculate extraction yield.Extraction yield=extract weight × 100%/raw material gross weight.
As a result it see the table below 1.
The toothpaste finished product sense organ and physics and chemistry evaluation result summary sheet of the embodiment of table 1 and comparative example
According to the result of table 1, the fragrance of the toothpaste finished product of comparative example 1~5 and comparative example 1~2 under different formulations,
Color and luster and denseness, fragrance, color and luster and the denseness of the toothpaste finished product of embodiment 1~5 are substantially better than comparative example 1~2, therefore embodiment
1~5 formula is more excellent；The extraction yield of the toothpaste finished product of comparative example 5~7 and comparative example 3,4 under different extraction temperatures,
The extraction yield of embodiment 5~7 is apparently higher than comparative example 3,4, and the extraction yield highest of embodiment 5, therefore the extraction of embodiment 5~7
Take temperature more excellent, the extraction temperature of embodiment 5 is optimal；Comparative example 5,8,9 and comparative example 5,6 are under different extracting pressures
Toothpaste finished product extraction yield, the extraction yield of embodiment 5,8,9 is apparently higher than comparative example 5,6, and the extracting pressure of embodiment 5 is most
It is excellent, therefore the extracting pressure of embodiment 5,8,9 is more excellent, the extracting pressure of embodiment 5 is optimal.
In general, the formula of embodiment 1~5, extraction temperature and extracting pressure are more excellent, and wherein embodiment 5 is optimal,
Therefore, the effect of the formula of embodiment 1~5 is more preferable.
Application examples 2
Examine antiallergy reparation and the antibacterial of the toothpaste finished product prepared by the different formulations of embodiment 1~5 and comparative example 1,2
Antibacterial effect.
1st, checked object：Take with hemodia patient 160, toothache or patients with periodontitis 160.
2nd, the method for inspection：Hemodia patient is divided into 8 groups at random, tries out embodiment 1~5 and comparative example 1,2 respectively
Toothpaste finished product, be respectively designated as allergy implement 1~5 group, allergy compares 1,2 group；Toothache or patients with periodontitis are divided equally at random
For 8 groups, the toothpaste finished product of embodiment 1~5 and comparative example 1,2 is tried out respectively, is respectively designated as inflammation and is implemented 1~5 group, inflammation
Compare 1,2 group.
It is required that brushing teeth 2 times, each 5min daily, try out 3 months；Blank control group is set up in addition, is brushed teeth daily with clear water
2 times, each 5min, adhere to 3 months.
3rd, assay.The number of each group's hemodia, toothache or periodontitis symptom mitigation is counted, see the table below 2.
The antiallergy reparation of table 2 and antibacterial bacteriostatic effect summary sheet
| Numbering | Symptom mitigation or elimination |
| Allergy implements 1 | 15 |
| Allergy implements 2 | 15 |
| Allergy implements 3 | 16 |
| Allergy implements 4 | 16 |
| Allergy implements 5 | 20 |
| Allergy compares 1 | 10 |
| Allergy compares 2 | 11 |
| Inflammation implements 1 | 16 |
| Inflammation implements 2 | 16 |
| Inflammation implements 3 | 17 |
| Inflammation implements 4 | 17 |
| Inflammation implements 5 | 19 |
| Inflammation compares 1 | 10 |
| Inflammation compares 2 | 9 |
| Blank control | 4 |
The result of consolidated statement 2, the patient symptom of the hemodia of the toothpaste finished product of embodiment 1~5 on probation are mitigated or eliminated
The obvious unnecessary comparative example 1,2 of quantity, try out the toothpaste finished product of embodiment 1~5 toothache or patients with periodontitis symptom mitigation or
The quantity of elimination also obvious unnecessary comparative example 1,2, and gap is very big, wherein, the disparity of embodiment 5.Therefore, embodiment
Toothpaste finished product effect prepared by 1~5 formula is more excellent, and toothpaste finished product effect prepared by the formula of embodiment 5 is optimal.
The implementation of the present invention is described in detail in above example, comparative example and application examples, and still, the present invention is not limited to
State the detail in embodiment., can be to the skill of the present invention in claims of the present invention and range of the technology design
Art scheme carries out a variety of simple remodeling and changed, and these simple variants belong to protection scope of the present invention.
Claims (6)
1. a kind of black tea toothpaste with antiallergy reparation, it is characterised in that including following component by weight percentage：Black tea
Extract 12~20%, hydrated silica 18~28%, calcium silicates 0.6~1%, sodium monofluorophosphate 1.25~1.6%, glycerine 18~
25%th, propane diols 9~15%, xylitol 6~10%, stevioside 3~5%, mint extract 2.2~5.2%, laruyl alcohol sulfuric acid
Ester sodium 1.5~3.5%, and deionized water surplus.
2. a kind of black tea toothpaste with antiallergy reparation according to claim 1, it is characterised in that including below by weight
Measure the component of percentage：Black tea extract 14~18%, hydrated silica 21~25%, calcium silicates 0.8%, sodium monofluorophosphate
1.45%th, glycerine 22%, propane diols 12%, xylitol 8%, stevioside 4%, mint extract 3.7%, laruyl alcohol sodium sulfovinate
2~3%, and deionized water surplus.
3. a kind of black tea toothpaste with antiallergy reparation according to claim 1, it is characterised in that including below by weight
Measure the component of percentage：Black tea extract 16%, hydrated silica 23%, calcium silicates 0.8%, sodium monofluorophosphate 1.45%, glycerine
22%th, propane diols 12%, xylitol 8%, stevioside 4%, mint extract 3.7%, laruyl alcohol sodium sulfovinate 2.5%, and
Deionized water surplus.
A kind of 4. preparation method of black tea toothpaste with antiallergy reparation described in claims 1 to 3, it is characterised in that bag
Include following steps：
S1, black tea, peppermint are taken, cross 40~80 mesh sieves after crushing respectively, black tea powder is made respectively and Herba Menthae powder is standby；
S2, black tea powder and Herba Menthae powder made from S1 are taken, carry out supercritical fluid extraction, 55~65 DEG C of extraction temperature, extraction respectively
1~2h of time, 25~35MPa of extracting pressure, black tea extract is made respectively for recovery and mint extract is standby；
S3, black tea extract, glycerine, propane diols, mint extract, laruyl alcohol sodium sulfovinate are weighed in parts by weight, mixing is equal
It is even standby；
S4, calcium silicates, sodium monofluorophosphate, hydrated silica, xylitol, stevioside, deionized water are weighed in parts by weight, mixing is equal
It is even；
Lotion finished product is made after importing homogenizer homogeneous in S5, the mixture for preparing step S3 and S4.
A kind of 5. preparation method of the black tea toothpaste with antiallergy reparation as claimed in claim 4, it is characterised in that step
The extraction temperature of supercritical fluid extraction is 60 DEG C in S2.
A kind of 6. preparation method of the black tea toothpaste with antiallergy reparation as claimed in claim 5, it is characterised in that step
The extracting pressure of supercritical fluid extraction is 30MPa in S2.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105193674A (en) * | 2015-10-30 | 2015-12-30 | 成都顺发消洗科技有限公司 | Antiallergic toothpaste |
| CN105748338A (en) * | 2015-11-27 | 2016-07-13 | 肖建国 | Toothpaste with dark tea extract and method for preparing toothpaste |
-
2017
- 2017-12-01 CN CN201711249322.XA patent/CN107822984A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105193674A (en) * | 2015-10-30 | 2015-12-30 | 成都顺发消洗科技有限公司 | Antiallergic toothpaste |
| CN105748338A (en) * | 2015-11-27 | 2016-07-13 | 肖建国 | Toothpaste with dark tea extract and method for preparing toothpaste |
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