CN107780211A - 一种渗透剂及其制备方法 - Google Patents
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Abstract
本发明公开了一种渗透剂及其制备方法，所述渗透剂由如下重量份数的原料组成：仲烷基磺酸钠10‑20份、二乙二醇单丁醚3‑5份、琥珀酸二辛酯磺酸钠10‑15份、月桂醇醚磷酸酯5‑7份、聚乙烯吡咯烷酮5‑7份、氯化钙3‑5份、月桂酰胺丙基甜菜碱3‑7份、二甲基硅油3‑5份、去离子水30‑40份。本发明的渗透剂制造工艺简单易操作，原料价格低廉易获得，且无毒无害，对人体不刺激，挥发性低，且渗透力强，与其它助剂同时使用不产生冲突。
Description
技术领域
本发明属于纺织助剂技术领域，更具体是涉及一种渗透剂。
背景技术
渗透剂顾名思义是起渗透作用，也是具有固定的亲水亲油基团，在溶液的表面能定向排列，并能使表面张力显著下降的物质。
在染整加工过程中，为了使染料等物质快速的渗透到织物中去，需要添加渗透剂。但是现有的渗透剂耐碱度不高、毛效差，与其它助剂互配效果差，高温煮时会有白粉点产生，从而影响使用效果。有些渗透剂还含有APEO，不易生物降解，不利于环保。
发明内容
本发明的目的在于提供一种渗透剂及其制备方法，以解决上述背景技术中提出的问题。
为实现上述目的，本发明提供如下技术方案：
一种渗透剂，按照重要份数，包括以下组分：仲烷基磺酸钠10-20份、二乙二醇单丁醚3-5份、琥珀酸二辛酯磺酸钠10-15份、月桂醇醚磷酸酯5-7份、聚乙烯吡咯烷酮5-7份、氯化钙3-5份、月桂酰胺丙基甜菜碱3-7份、二甲基硅油3-5份、去离子水30-40份。
优选地，所述的渗透剂，按照重量份数，包括以下组分：仲烷基磺酸钠10份、二乙二醇单丁醚3份、琥珀酸二辛酯磺酸钠10份、月桂醇醚磷酸酯5份、聚乙烯吡咯烷酮5份、氯化钙3份、月桂酰胺丙基甜菜碱3份、二甲基硅油3份、去离子水30份。
优选地，所述的渗透剂，按照重量份数，包括以下组分：仲烷基磺酸钠15份、二乙二醇单丁醚4份、琥珀酸二辛酯磺酸钠13份、月桂醇醚磷酸酯6份、聚乙烯吡咯烷酮6份、氯化钙4份、月桂酰胺丙基甜菜碱5份、二甲基硅油4份、去离子水35份。
优选地，所述的渗透剂，按照重量份数，包括以下组分：仲烷基磺酸钠20份、二乙二醇单丁醚5份、琥珀酸二辛酯磺酸钠15份、月桂醇醚磷酸酯7份、聚乙烯吡咯烷酮7份、氯化钙5份、月桂酰胺丙基甜菜碱7份、二甲基硅油5份、去离子水40份。
优选地，所述的渗透剂的制备方法，具体步骤包括：
步骤1，在反应釜中加入去离子水30-40份，升高温度至50-60℃；
步骤2，加入仲烷基磺酸钠10-20份、二乙二醇单丁醚3-5份、琥珀酸二辛酯磺酸钠10-15份、月桂醇醚磷酸酯5-7份，500-1000转/分钟，搅拌10-20分钟；
步骤3，降温至30-40℃，加入聚乙烯吡咯烷酮5-7份、月桂酰胺丙基甜菜碱3-7份，500-1000转/分钟，搅拌20-30分钟；
步骤4，降温至20-30℃，加入氯化钙3-5份、二甲基硅油3-5份，500-1000转/分钟，搅拌20-30分钟；
步骤5，关停搅拌，得到配制好的液体渗透剂；
步骤6，静置冷却至搅拌釜中液体渗透剂低于20℃，放料封装，制得成品。
与现有技术相比，本发明的有益效果是：
1、本发明的渗透剂制造工艺简单易操作，原料价格低廉易获得，且无毒无害，挥发性低，对人体不刺激。
2、本发明的渗透剂所用各种原料之间相互配伍、协同作用，共同组成性能优异的产品。
3、本发明的渗透剂在应用过程中，不产生有毒的气体或固体物质。
4、本发明的渗透剂渗透力强，与其它助剂同时使用不产生冲突。
5、简化工艺，操作安全简单，易于工业化生产。
6、本发明的使用可收到良好的经济效益。
具体实施实例
本发明公开了一种渗透剂，按照重要份数，包括以下组分：仲烷基磺酸钠10-20份、二乙二醇单丁醚3-5份、琥珀酸二辛酯磺酸钠10-15份、月桂醇醚磷酸酯5-7份、聚乙烯吡咯烷酮5-7份、氯化钙3-5份、月桂酰胺丙基甜菜碱3-7份、二甲基硅油3-5份、去离子水30-40份。
本发明还提供了一种渗透剂的制备方法，具体步骤包括：
步骤1，在反应釜中加入去离子水30-40份，升高温度至50-60℃；
步骤2，加入仲烷基磺酸钠10-20份、二乙二醇单丁醚3-5份、琥珀酸二辛酯磺酸钠10-15份、月桂醇醚磷酸酯5-7份，500-1000转/分钟，搅拌10-20分钟；
步骤3，降温至30-40℃，加入聚乙烯吡咯烷酮5-7份、月桂酰胺丙基甜菜碱3-7份，500-1000转/分钟，搅拌20-30分钟；
步骤4，降温至20-30℃，加入氯化钙3-5份、二甲基硅油3-5份，500-1000转/分钟，搅拌20-30分钟；
步骤5，关停搅拌，得到配制好的液体渗透剂；
步骤6，静置冷却至搅拌釜中液体渗透剂低于20℃，放料封装，制得成品。
实施例1
本发明公开了一种渗透剂，按照重要份数，包括以下组分：仲烷基磺酸钠10份、二乙二醇单丁醚3份、琥珀酸二辛酯磺酸钠10份、月桂醇醚磷酸酯5份、聚乙烯吡咯烷酮5份、氯化钙3份、月桂酰胺丙基甜菜碱3份、二甲基硅油3份、去离子水30份。
本发明还提供了一种渗透剂的制备方法，具体步骤包括：
步骤1，在反应釜中加入去离子水30份，升高温度至50℃；
步骤2，加入仲烷基磺酸钠10份、二乙二醇单丁醚3份、琥珀酸二辛酯磺酸钠10份、月桂醇醚磷酸酯5份，500转/分钟，搅拌20分钟；
步骤3，降温至30℃，加入聚乙烯吡咯烷酮5份、月桂酰胺丙基甜菜碱3份，500转/分钟，搅拌20分钟；
步骤4，降温至20℃，加入氯化钙3份、二甲基硅油3份，500转/分钟，搅拌20分钟；
步骤5，关停搅拌，得到配制好的液体渗透剂；
步骤6，静置冷却至搅拌釜中液体渗透剂低于20℃，放料封装，制得成品。
实施例2
本发明公开了一种渗透剂，按照重要份数，包括以下组分：仲烷基磺酸钠15份、二乙二醇单丁醚4份、琥珀酸二辛酯磺酸钠13份、月桂醇醚磷酸酯6份、聚乙烯吡咯烷酮6份、氯化钙4份、月桂酰胺丙基甜菜碱5份、二甲基硅油4份、去离子水35份。
本发明还提供了一种渗透剂的制备方法，具体步骤包括：
步骤1，在反应釜中加入去离子水35份，升高温度至55℃；
步骤2，加入仲烷基磺酸钠15份、二乙二醇单丁醚4份、琥珀酸二辛酯磺酸钠13份、月桂醇醚磷酸酯6份，900转/分钟，搅拌15分钟；
步骤3，降温至35℃，加入聚乙烯吡咯烷酮6份、月桂酰胺丙基甜菜碱5份，900转/分钟，搅拌25分钟；
步骤4，降温至25℃，加入氯化钙4份、二甲基硅油4份，900转/分钟，搅拌25分钟；
步骤5，关停搅拌，得到配制好的液体渗透剂；
步骤6，静置冷却至搅拌釜中液体渗透剂低于20℃，放料封装，制得成品。
实施例3
本发明公开了一种渗透剂，按照重要份数，包括以下组分：仲烷基磺酸钠20份、二乙二醇单丁醚5份、琥珀酸二辛酯磺酸钠15份、月桂醇醚磷酸酯7份、聚乙烯吡咯烷酮7份、氯化钙5份、月桂酰胺丙基甜菜碱7份、二甲基硅油5份、去离子水40份。
本发明还提供了一种渗透剂的制备方法，具体步骤包括：
步骤1，在反应釜中加入去离子水40份，升高温度至60℃；
步骤2，加入仲烷基磺酸钠20份、二乙二醇单丁醚5份、琥珀酸二辛酯磺酸钠15份、月桂醇醚磷酸酯7份，1000转/分钟，搅拌10分钟；
步骤3，降温至40℃，加入聚乙烯吡咯烷酮7份、月桂酰胺丙基甜菜碱7份，1000转/分钟，搅拌30分钟；
步骤4，降温至30℃，加入氯化钙5份、二甲基硅油5份，1000转/分钟，搅拌30分钟；
步骤5，关停搅拌，得到配制好的液体渗透剂；
步骤6，静置冷却至搅拌釜中液体渗透剂低于20℃，放料封装，制得成品。
实施例4
本发明公开了一种渗透剂，按照重要份数，包括以下组分：仲烷基磺酸钠20份、二乙二醇单丁醚4份、琥珀酸二辛酯磺酸钠15份、月桂醇醚磷酸酯7份、聚乙烯吡咯烷酮7份、氯化钙3份、月桂酰胺丙基甜菜碱5份、二甲基硅油4份、去离子水30份。
本发明还提供了一种渗透剂的制备方法，具体步骤包括：
步骤1，在反应釜中加入去离子水30份，升高温度至60℃；
步骤2，加入仲烷基磺酸钠20份、二乙二醇单丁醚4份、琥珀酸二辛酯磺酸钠15份、月桂醇醚磷酸酯7份，1000转/分钟，搅拌10分钟；
步骤3，降温至30℃，加入聚乙烯吡咯烷酮7份、月桂酰胺丙基甜菜碱5份，900转/分钟，搅拌20分钟；
步骤4，降温至20℃，加入氯化钙3份、二甲基硅油4份，1000转/分钟，搅拌20分钟；
步骤5，关停搅拌，得到配制好的液体渗透剂；
步骤6，静置冷却至搅拌釜中液体渗透剂低于20℃，放料封装，制得成品。
将实施例1、2、3、4的渗透剂进行耐碱性(氢氧化钠浓度为50g/L)、沉降时间的测试，测试结果如下：
| 实施例 | 耐碱性 | 沉降时间(s) | 80℃下的沉降时间(s) |
| 1 | 有一点点絮状物，泡沫有一点 | 16.5 | 13.2 |
| 2 | 较为澄清，泡沫少 | 14.2 | 10.4 |
| 3 | 澄清，基本无泡沫 | 7.5 | 6.2 |
| 4 | 澄清，泡沫少 | 12.7 | 8.5 |
尽管已经示出和描述了本发明的实施例，对于本领域的普通技术人员而言，可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型，本发明的范围由所附权利要求及其等同物限定。
Claims (5)
1.一种渗透剂，其特征在于：所述渗透剂包括如下重量份数的原料：仲烷基磺酸钠10-20份、二乙二醇单丁醚3-5份、琥珀酸二辛酯磺酸钠10-15份、月桂醇醚磷酸酯5-7份、聚乙烯吡咯烷酮5-7份、氯化钙3-5份、月桂酰胺丙基甜菜碱3-7份、二甲基硅油3-5份、去离子水30-40份。
2.根据权利要求1所述的渗透剂，其特征在于：按照重量份数，包括以下组分：仲烷基磺酸钠10份、二乙二醇单丁醚3份、琥珀酸二辛酯磺酸钠10份、月桂醇醚磷酸酯5份、聚乙烯吡咯烷酮5份、氯化钙3份、月桂酰胺丙基甜菜碱3份、二甲基硅油3份、去离子水30份。
3.根据权利要求1所述的渗透剂，其特征在于：按照重量份数，包括以下组分：仲烷基磺酸钠15份、二乙二醇单丁醚4份、琥珀酸二辛酯磺酸钠13份、月桂醇醚磷酸酯6份、聚乙烯吡咯烷酮6份、氯化钙4份、月桂酰胺丙基甜菜碱5份、二甲基硅油4份、去离子水35份。
4.根据权利要求1所述的渗透剂，其特征在于：按照重量份数，包括以下组分：仲烷基磺酸钠20份、二乙二醇单丁醚5份、琥珀酸二辛酯磺酸钠15份、月桂醇醚磷酸酯7份、聚乙烯吡咯烷酮7份、氯化钙5份、月桂酰胺丙基甜菜碱7份、二甲基硅油5份、去离子水40份。
5.一种采用上述权利要求1-4中任一所述渗透剂的制备方法，其特征在于：具体步骤包括：
步骤1，在反应釜中加入去离子水30-40份，升高温度至50-60℃；
步骤2，加入仲烷基磺酸钠10-20份、二乙二醇单丁醚3-5份、琥珀酸二辛酯磺酸钠10-15份、月桂醇醚磷酸酯5-7份，500-1000转/分钟，搅拌10-20分钟；
步骤3，降温至30-40℃，加入聚乙烯吡咯烷酮5-7份、月桂酰胺丙基甜菜碱3-7份，500-1000转/分钟，搅拌20-30分钟；
步骤4，降温至20-30℃，加入氯化钙3-5份、二甲基硅油3-5份，500-1000转/分钟，搅拌20-30分钟；
步骤5，关停搅拌，得到配制好的液体渗透剂；
步骤6，静置冷却至搅拌釜中液体渗透剂低于20℃，放料封装，制得成品。
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109252401A (zh) * | 2018-09-14 | 2019-01-22 | 桐乡市濮院毛针织技术服务中心 | 一种高密度腈纶织物的紫色染色用渗透剂的制备方法 |
| CN109267398A (zh) * | 2018-09-14 | 2019-01-25 | 桐乡市濮院毛针织技术服务中心 | 一种高密度腈纶织物的紫色染色方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101725042A (zh) * | 2009-12-08 | 2010-06-09 | 山东金鲁化工有限公司 | 一种耐碱精炼渗透剂及其制备方法 |
| CN104549037A (zh) * | 2015-01-22 | 2015-04-29 | 南通优尼科化工有限公司 | 一种渗透剂 |
| CN105671946A (zh) * | 2016-02-26 | 2016-06-15 | 苏州三和开泰花线织造有限公司 | 一种用于织物前处理的高效环保渗透剂及其制备方法 |
| CN106120319A (zh) * | 2016-07-01 | 2016-11-16 | 潘明华 | 一种丝光渗透剂及其制备方法 |
-
2017
- 2017-10-20 CN CN201710983523.6A patent/CN107780211A/zh active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101725042A (zh) * | 2009-12-08 | 2010-06-09 | 山东金鲁化工有限公司 | 一种耐碱精炼渗透剂及其制备方法 |
| CN104549037A (zh) * | 2015-01-22 | 2015-04-29 | 南通优尼科化工有限公司 | 一种渗透剂 |
| CN105671946A (zh) * | 2016-02-26 | 2016-06-15 | 苏州三和开泰花线织造有限公司 | 一种用于织物前处理的高效环保渗透剂及其制备方法 |
| CN106120319A (zh) * | 2016-07-01 | 2016-11-16 | 潘明华 | 一种丝光渗透剂及其制备方法 |
Non-Patent Citations (1)
| Title |
|---|
| 《化学化工大辞典》编委会、化学工业出版社辞书编辑部编: "《化学化工大辞典（下）》", 31 January 2003, 化学工业出版社出版 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109252401A (zh) * | 2018-09-14 | 2019-01-22 | 桐乡市濮院毛针织技术服务中心 | 一种高密度腈纶织物的紫色染色用渗透剂的制备方法 |
| CN109267398A (zh) * | 2018-09-14 | 2019-01-25 | 桐乡市濮院毛针织技术服务中心 | 一种高密度腈纶织物的紫色染色方法 |
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