CN107724095A - A kind of microcapsules necktie finishing agent and preparation method thereof - Google Patents
A kind of microcapsules necktie finishing agent and preparation method thereof Download PDFInfo
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- CN107724095A CN107724095A CN201710833548.8A CN201710833548A CN107724095A CN 107724095 A CN107724095 A CN 107724095A CN 201710833548 A CN201710833548 A CN 201710833548A CN 107724095 A CN107724095 A CN 107724095A
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- Prior art keywords
- microcapsules
- necktie
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- finishing agent
- oil
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/005—Compositions containing perfumes; Compositions containing deodorants
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/15—Proteins or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Abstract
The invention discloses a kind of microcapsules necktie finishing agent and preparation method thereof, the microcapsules necktie finishing agent, mainly it is made up of microcapsules wick and the microcapsule wall material being coated on outside microcapsules wick, its preparation method comprises the following steps：S1, the preparation of the microcapsule wall material aqueous solution, S2, the preparation of microcapsules wick aqueous emulsion, S3, the preparation of microcapsule dressing agent；The microcapsules wick includes the component of following percentage by weight：Lemon oil 1% 50%, bergamot oil 1% 30%, limette oil 1% 30%, orange oil 1% 50%, petit grain oil 1% 20%, peach aldehyde 1% 10%, apple ester 1% 20%, geraniol 1% 30%, rhodinol 1% 30%, surfactant 1% 50%, other spices auxiliary agents 1% 30%.The present invention is using the plants essential oil extracted in various fruit as raw material, plants essential oil cladding is got up with high polymer material, it is prepared into the microcapsule dressing agent of functionalization textile, the lemon of highly volatile is overmolding to microcapsules, with slow-release function, the fragrance remaining time of necktie is extended, solves the problems, such as the long-term lasting of necktie.
Description
Technical field
The present invention relates to textile finish technical field, more particularly to a kind of microcapsules necktie finishing agent and its preparation side
Method.
Background technology
Necktie is man social life top grade ornaments, and particularly silk tie hand embroidering is very noble." Gulong perfume "
It is west man's favorite, primary flavor is natural lemon plants essential oil, and Gulong perfume is sprayed on suit collar band, even more a kind of body
The symbol of part.
The primary solvent of perfume is absolute ethyl alcohol, and perfume is sprayed directly on necktie, and fragrance remaining time only has 4-6h, second day
With regard to what fragrance also without such as outgoing also to need to spray perfume.Modern society's dog-eat-dog, the time is more valuable, everyday to necktie
On spray perfume over sth it is a little troublesome.If the fragrance that energy high-ranking military officer takes is retained for a long time, the time largely to spray perfume over sth can be saved.
The content of the invention
The invention aims to solve shortcoming present in prior art, and a kind of microcapsules necktie proposed arranges
Agent and preparation method thereof.
To achieve these goals, present invention employs following technical scheme：
A kind of microcapsules necktie finishing agent, mainly by microcapsules wick and the microcapsule wall material being coated on outside microcapsules wick
Composition, the microcapsules wick include the component of following percentage by weight：Lemon oil 1%-50%, bergamot oil 1%-30%,
Limette oil 1%-30%, orange oil 1%-50%, petit grain oil 1%-20%, peach aldehyde 1%-10%, apple ester 1%-20%, perfume (or spice)
Leaf-alcohol 1%-30%, rhodinol 1%-30%, surfactant 1%-50%, other spices auxiliary agents 1%-30%.
Preferably, the microcapsule wall material is animal gelatin or protein, and the protein is specially casein, soybean egg
In vain, one or both of wheat gluten, fibroin are combined.
Preferably, other described spices auxiliary agents are specially indoles, Thymol, eugenol, aldehyde perfume, benzoates
Any of spices or any several mixtures form.
Preferably, the lemon oil is process by lemon by cold press.
Preferably, the orange oil formed after cold press is processed, again with organic solvent purification by liquid extraction by sweet orange, be free of
The pure sweet orange pericarp essential oil of quick material.
Preferably, the surfactant is specially sorbitan trioleate, the stearic acid of anhydrous sorbitol three, second two
Alcohol fatty acid ester, sorbitan mono-laurate, polyoxyethylene 20 sorbitan monostearate, APEO dehydration mountain
One or both of pears alcohol monopalmitate compounding forms.
Preferably, a kind of preparation method of microcapsules necktie finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：High polymer material is added in 45-90 DEG C of deionized water, startup is stirred
Machine is mixed, under agitation, 45-90 DEG C of constant temperature, dissolution time 1-10h, multiplies heat filtering, removes water-insoluble, obtained filtrate exists
5-20h is aged at 45-90 DEG C, obtains the transparent microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：According to formula, microcapsules wick, agitating and heating are prepared, temperature reaches
At 45-90 DEG C, stirring and dissolving 5-60min under constant temperature, deionized water and lauryl sodium sulfate aqueous solution are added, with high shear breast
Change machine handles 2-10min, obtains microcapsules wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：Microcapsules wick aqueous emulsion is continued into high-speed shearing emulsion machine processing 2-
10min, the microcapsule wall material aqueous solution is added, and be heated to 45-90 DEG C, isothermal reaction 4-12h, cooled, obtain the micro- glue of finished product
Capsule finishing agent.
Preferably, in the S1, the rotating speed of agitation is 100-200r/min.
Preferably, in the S2, the rotating speed of stirring is 200-300r/min, the lauryl sodium sulfate aqueous solution it is dense
Spend for 0.2-10%.
Preferably, in the S2 and the S3, the rotating speed of high-shear emulsion machine is 9000-30000r/min, the side of heating
Formula is heating water bath.
Preferably, in the S3, the concentration 1%-10% of the microcapsule wall material aqueous solution.
Compared with prior art, the beneficial effects of the invention are as follows：
1. the present invention is using the plants essential oil extracted in various fruit as raw material, plants essential oil is coated with high polymer material
Get up, be prepared into the microcapsule dressing agent of functionalization textile, the lemon of highly volatile is overmolding to microcapsules, is allowed to have
There is slow-release function, extend the fragrance remaining time of necktie, solve the problems, such as the long-term lasting of necktie.
2. the present invention combines the preference of fragrance the note of west Gulong perfume with Asians, with lemon oil, perfume (or spice)
Lemon oil, limette oil, orange oil, petit grain oil and spices auxiliary combination optimization microcapsules wick formula, are allowed to be more easy to by east
People receives.
3. the present invention has selected protein-based high polymer material to make microcapsule wall material, because the knitted material majority of necktie is
Silk, acrylic fibers fiber, protein-based high polymer material can increase the pliability of necktie.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only part of the embodiment of the present invention, rather than whole embodiments.
Embodiment 1：
A kind of preparation method of microcapsules necktie finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Deionized water 480ml is measured, heats to 65 DEG C, adds silk element
(silk protein hydrolysate product) 7.5g, start mixer, 65 DEG C of constant temperature, dissolve 6h, be filtered to remove water-insoluble, 45 DEG C of filtrate is old
Change 16h, obtain the milky microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh lemon oil 80g, bergamot oil 150g, limette oil 30g, sweet orange
It is oily 40g, petit grain oil 30g, peach aldehyde 20g, apple ester 30g, geraniol 40g, rhodinol 60g, indoles 2g, Ergol 20g, poly-
Oxygen ethene (20) sorbitan monopalmitate 30g, Aceonon 300 MO 6g, transglutaminase 2g, prepare micro-
Capsule wick, agitating and heating, when temperature reaches 53 DEG C, stirring and dissolving 6h under constant temperature, deionized water 480ml is added, concentration 5%
Lauryl sodium sulfate aqueous solution 50ml, 5min is handled with high-shear emulsion machine 18000r/min rotating speed, obtains microcapsules
Wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, it is that 1.5% silk element is water-soluble to add concentration
Liquid 480ml, continue to handle 4min with high-speed shearing emulsion machine, be moved back to again on water-bath, start electric blender, rotating speed
170r/min, lower 53 DEG C of reaction 8h of constant temperature are stirred, cools, obtains finished lemon/lime essential oil microcapsules necktie finishing agent.
The present embodiment prepares the finished lemon/lime essential oil microcapsules necktie finishing agent of silk element parcel, finished product is micro- during use
Capsule finishing agent is diluted with water into 2%-5% weak solution, is 2% microcapsules with (45 DEG C) dilution modulation concentration of deionized water
Necktie finishing agent, add in ultra-fine directed spraying machine, be directly sprayed onto under stress on necktie, spouting liquid is by necktie weight
15% metering, it is sprayed, with 60 DEG C of hot blast dryings, pressed and shaped with vapour iron, after detection is qualified, packaging is dispatched from the factory, i.e., complete
The arrangement process of paired necktie.
Lemon has the effect of refreshing the mind, relieving fatigue, and the lemon of highly volatile is covered by micro- glue
It is intracapsular, with slow-release function, extend the fragrance remaining time of necktie, solve the problems, such as the long-term lasting of necktie.
Embodiment 2：
A kind of preparation method of microcapsules necktie finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Deionized water 480ml is measured, heats to 65 DEG C, adds casein
5g, start mixer, 65 DEG C of constant temperature, dissolve 6h, be filtered to remove water-insoluble, 45 DEG C of ageing 16h of filtrate, obtain milky micro-
The capsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh lemon oil 80g, bergamot oil 150g, limette oil 20g, sweet orange
It is oily 30g, petit grain oil 30g, peach aldehyde 20g, apple ester 30g, geraniol 40g, rhodinol 60g, indoles 2g, Ergol 20g, poly-
Oxygen ethene (20) sorbitan monopalmitate 20g, Aceonon 300 MO 5g, transglutaminase 2g, prepare micro-
Capsule wick, agitating and heating, when temperature reaches 53 DEG C, stirring and dissolving 6h under constant temperature, deionized water 480ml is added, concentration 5%
Lauryl sodium sulfate aqueous solution 50ml, 5min is handled with high-shear emulsion machine 20000r/min rotating speed, obtains microcapsules
Wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, it is 2% casein to add 480ml concentration
The aqueous solution, continue to handle 4min with high-speed shearing emulsion machine, be moved back to again on water-bath, start electric blender, rotating speed 170r/
Min, lower 53 DEG C of reaction 8h of constant temperature are stirred, cools, obtains finished lemon/lime essential oil microcapsules necktie finishing agent.
The present embodiment prepares the finished lemon/lime essential oil microcapsules necktie finishing agent of casein parcel, finished product is micro- during use
Capsule finishing agent is diluted with water into 2%-5% weak solution, is 2% microcapsules with (45 DEG C) dilution modulation concentration of deionized water
Necktie finishing agent, add in ultra-fine directed spraying machine, be directly sprayed onto under stress on necktie, spouting liquid is by necktie weight
15% metering, it is sprayed, with 60 DEG C of hot blast dryings, pressed and shaped with vapour iron, after detection is qualified, packaging is dispatched from the factory, i.e., complete
The arrangement process of paired necktie.
Lemon has the effect of refreshing the mind, relieving fatigue, and the lemon of highly volatile is covered by micro- glue
It is intracapsular, with slow-release function, extend the fragrance remaining time of necktie, solve the problems, such as the long-term lasting of necktie.
Embodiment 3：
A kind of preparation method of microcapsules necktie finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Deionized water 480ml is measured, heats to 65 DEG C, adds soybean egg
White 15g, start mixer, 65 DEG C of constant temperature, dissolve 6h, be filtered to remove water-insoluble, 45 DEG C of ageing 16h of filtrate, obtain milky
The microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh lemon oil 70g, bergamot oil 150g, limette oil 20g, sweet orange
It is oily 40g, petit grain oil 30g, peach aldehyde 20g, apple ester 30g, geraniol 40g, rhodinol 60g, indoles 2g, Ergol 20g, poly-
Oxygen ethene (5) sorbitan monopalmitate 30g, polyoxyethylene tristearate 3g, transglutaminase 2g, prepare micro-
Capsule wick, agitating and heating, when temperature reaches 45 DEG C, stirring and dissolving 6h under constant temperature, deionized water 480ml is added, concentration 5%
Lauryl sodium sulfate aqueous solution 50ml, 5min is handled with high-shear emulsion machine 25000r/min rotating speed, obtains microcapsules
Wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, it is 3% soybean egg to add 480ml concentration
White water solution, continue to handle 4min with high-speed shearing emulsion machine, be moved back to again on water-bath, start electric blender, rotating speed
200r/min, lower 50 DEG C of reaction 6h of constant temperature are stirred, cools, obtains finished lemon/lime essential oil microcapsules necktie finishing agent.
The present embodiment prepares the finished lemon/lime essential oil microcapsules necktie finishing agent of soybean protein parcel, soybean protein price
Cheaply, it is adapted to a wide range of use.Finished microcapsule finishing agent is diluted with water into 2%-5% weak solution during use, spend from
Sub- (45 DEG C) dilution modulation concentration of water are 2% microcapsules necktie finishing agent, are added in ultra-fine directed spraying machine, under stress directly
Connect and be sprayed onto on necktie, spouting liquid measures by the 15% of necktie weight, sprayed, with 60 DEG C of hot blast dryings, uses vapour iron
Flatiron sizing, after detection is qualified, packaging is dispatched from the factory, that is, completes the arrangement process to necktie.
Lemon has the effect of refreshing the mind, relieving fatigue, and the lemon of highly volatile is covered by micro- glue
It is intracapsular, with slow-release function, extend the fragrance remaining time of necktie, solve the problems, such as the long-term lasting of necktie.
Embodiment 4：
A kind of preparation method of microcapsules necktie finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Deionized water 480ml is measured, heats to 65 DEG C, adds wheat egg
White 20g, start mixer, 65 DEG C of constant temperature, dissolve 6h, be filtered to remove water-insoluble, 45 DEG C of ageing 20h of filtrate, obtain milky
The microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh lemon oil 90g, bergamot oil 120g, limette oil 30g, sweet orange
It is oily 30g, petit grain oil 30g, peach aldehyde 20g, apple ester 30g, geraniol 40g, rhodinol 60g, indoles 2g, Ergol 20g, poly-
Oxygen ethene (5) sorbitan monopalmitate 30g, Aceonon 300 MO 6g, transglutaminase 3g, prepare microcapsules
Wick, agitating and heating, when temperature reaches 70 DEG C, stirring and dissolving 6h under constant temperature, add deionized water 480ml, the 12 of concentration 5%
Alkylsurfuric acid sodium water solution 50ml, 5min is handled with high-shear emulsion machine 18000r/min rotating speed, obtains microcapsules wick
Aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, it is 1.5% wheat to add 480ml concentration
Protein solution, continue to handle 4min with high-speed shearing emulsion machine, be moved back to again on water-bath, start electric blender, rotating speed
250r/min, lower 70 DEG C of reaction 8h of constant temperature are stirred, cools, obtains finished lemon/lime essential oil microcapsules necktie finishing agent.
The present embodiment prepares the finished lemon/lime essential oil microcapsules necktie finishing agent of wheat gluten parcel, by finished product during use
Microcapsule dressing agent is diluted with water into 2%-5% weak solution, is 2% microcapsules with (45 DEG C) dilution modulation concentration of deionized water
Necktie finishing agent, add in ultra-fine directed spraying machine, be directly sprayed onto under stress on necktie, spouting liquid is by necktie weight
15% metering, it is sprayed, with 60 DEG C of hot blast dryings, pressed and shaped with vapour iron, after detection is qualified, packaging is dispatched from the factory, i.e., complete
The arrangement process of paired necktie.
Lemon has the effect of refreshing the mind, relieving fatigue, and the lemon of highly volatile is covered by micro- glue
It is intracapsular, with slow-release function, extend the fragrance remaining time of necktie, solve the problems, such as the long-term lasting of necktie.
Embodiment 5：
A kind of preparation method of microcapsules necktie finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Deionized water 480ml is measured, heats to 90 DEG C, it is bright to add pigskin
Glue 10g, start mixer, 90 DEG C of constant temperature, dissolve 6h, be filtered to remove water-insoluble, 45 DEG C of ageing 16h of filtrate, obtain milky
The microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh lemon oil 100g, bergamot oil 150g, limette oil 10g, sweet tea
Orange oil 20g, petit grain oil 20g, peach aldehyde 20g, apple ester 30g, geraniol 40g, rhodinol 60g, indoles 2g, Ergol 20g,
Polyoxyethylene (20) Span60 30g, Aceonon 300 MO 6g, transglutaminase 2g, prepare micro- glue
Capsule wick, agitating and heating, when temperature reaches 53 DEG C, stirring and dissolving 6h under constant temperature, add deionized water 480ml, the ten of concentration 5%
Sodium dialkyl sulfate aqueous solution 50ml, 5min is handled with high-shear emulsion machine 19000r/min rotating speed, obtain microcapsules oil
Core aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, it is that 5% pigskin is bright to add 480ml concentration
Glue solution, continue to handle 4min with high-speed shearing emulsion machine, be moved back to again on water-bath, start electric blender, rotating speed
170r/min, lower 53 DEG C of reaction 8h of constant temperature are stirred, cools, obtains finished lemon/lime essential oil microcapsules necktie finishing agent.
The present embodiment prepares the finished lemon/lime essential oil microcapsules necktie finishing agent of pigskin gelatin parcel, and its is cheap,
But easily cause necktie in necktie to be hardened.Finished microcapsule finishing agent is diluted with water into the dilute molten of 2%-5% during use
Liquid, it is 2% microcapsules necktie finishing agent with (45 DEG C) dilution modulation concentration of deionized water, adds in ultra-fine directed spraying machine,
Directly it is sprayed onto under pressure on necktie, spouting liquid measures by the 15% of necktie weight, sprayed, with 60 DEG C of hot blast dryings, uses
Vapour iron flatiron sizing, after detection is qualified, packaging is dispatched from the factory, that is, completes the arrangement process to necktie.
Lemon has the effect of refreshing the mind, relieving fatigue, and the lemon of highly volatile is covered by micro- glue
It is intracapsular, with slow-release function, extend the fragrance remaining time of necktie, solve the problems, such as the long-term lasting of necktie.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (11)
- A kind of 1. microcapsules necktie finishing agent, mainly by microcapsules wick and the microcapsule wall material group being coated on outside microcapsules wick Into, it is characterised in that the microcapsules wick includes the component of following percentage by weight：Lemon oil 1%-50%, bergamot oil 1%-30%, limette oil 1%-30%, orange oil 1%-50%, petit grain oil 1%-20%, peach aldehyde 1%-10%, apple ester 1%-20%, geraniol 1%-30%, rhodinol 1%-30%, surfactant 1%-50%, other spices auxiliary agents 1%- 30%.
- 2. a kind of microcapsules necktie finishing agent according to claim 1, it is characterised in that the microcapsule wall material is animal Gelatin or protein, the protein are specially one or both of casein, soybean protein, wheat gluten, fibroin It is combined.
- 3. a kind of microcapsules necktie finishing agent according to claim 1, it is characterised in that other described spices auxiliary agents are specific Formed for any of indoles, Thymol, eugenol, aldehyde perfume, benzoates spices or any several mixtures.
- 4. a kind of microcapsules necktie finishing agent according to claim 1, it is characterised in that the lemon oil is passed through by lemon Cold press is process.
- 5. a kind of microcapsules necktie finishing agent according to claim 1, it is characterised in that the orange oil is by sweet orange through cold After squeezing processing, formed again with organic solvent purification by liquid extraction, pure sweet orange pericarp essential oil without allergin.
- 6. a kind of microcapsules necktie finishing agent according to claim 1, it is characterised in that the surfactant is specially It is sorbitan trioleate, the stearic acid of anhydrous sorbitol three, glycol fatty acid ester, sorbitan mono-laurate, poly- One or both of oxygen ethene sorbitan monostearate, APEO sorbitan monopalmitate compound and Into.
- 7. the preparation method of a kind of microcapsules necktie finishing agent according to claim 1, it is characterised in that including following step Suddenly：S1, the preparation of the microcapsule wall material aqueous solution：High polymer material is added in 45-90 DEG C of deionized water, starts mixer, Under agitation, 45-90 DEG C of constant temperature, dissolution time 1-10h, multiply heat filtering, remove water-insoluble, obtained filtrate is in 45-90 5-20h is aged at DEG C, obtains the transparent microcapsule wall material aqueous solution；S2, the preparation of microcapsules wick aqueous emulsion：According to formula, microcapsules wick, agitating and heating are prepared, temperature reaches 45-90 DEG C when, stirring and dissolving 5-60min under constant temperature, add deionized water and lauryl sodium sulfate aqueous solution, use high-shear emulsion machine 2-10min is handled, obtains microcapsules wick aqueous emulsion；S3, the preparation of microcapsule dressing agent：Microcapsules wick aqueous emulsion is continued into high-speed shearing emulsion machine processing 2-10min, then The microcapsule wall material aqueous solution is added, and is heated to 45-90 DEG C, isothermal reaction 4-12h, cools, obtains finished microcapsule finishing agent.
- A kind of 8. preparation method of microcapsules necktie finishing agent according to claim 7, it is characterised in that in the S1, The rotating speed of agitation is 100-200r/min.
- A kind of 9. preparation method of microcapsules necktie finishing agent according to claim 7, it is characterised in that in the S2, The rotating speed of stirring is 200-300r/min, and the concentration of the lauryl sodium sulfate aqueous solution is 0.2-10%.
- A kind of 10. preparation method of microcapsules necktie finishing agent according to claim 7, it is characterised in that the S2 and In the S3, the rotating speed of high-shear emulsion machine is 9000-30000r/min, and the mode of heating is heating water bath.
- A kind of 11. preparation method of microcapsules necktie finishing agent according to claim 7, it is characterised in that in the S3, The concentration 1%-10% of the microcapsule wall material aqueous solution.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3092760A1 (en) * | 2019-02-19 | 2020-08-21 | Gerard Redziniak | PROCESS FOR PROLONGING THE PRESENCE OF OLFACTORY AND AROMATIC MOLECULES ON WOVEN OR NON-WOVEN SUBSTRATES |
| WO2022038322A1 (en) | 2020-08-20 | 2022-02-24 | Benu Blanc | Perfumed composition for making an olfactory support |
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| CN103290700A (en) * | 2013-05-31 | 2013-09-11 | 山东鲁普科技有限公司 | Aromatic rope and manufacturing method thereof |
| CN103689836A (en) * | 2013-12-11 | 2014-04-02 | 常熟市创裕印染有限公司 | Scarf |
| CN106035326A (en) * | 2016-06-06 | 2016-10-26 | 南通伟德动力电池研究所（普通合伙） | Preparation method of fragrance microcapsule spraying agent for dispelling houseflies |
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| FR3092760A1 (en) * | 2019-02-19 | 2020-08-21 | Gerard Redziniak | PROCESS FOR PROLONGING THE PRESENCE OF OLFACTORY AND AROMATIC MOLECULES ON WOVEN OR NON-WOVEN SUBSTRATES |
| WO2022038322A1 (en) | 2020-08-20 | 2022-02-24 | Benu Blanc | Perfumed composition for making an olfactory support |
| FR3113493A1 (en) | 2020-08-20 | 2022-02-25 | Benu Blanc | PERFUMED COMPOSITION FOR MANUFACTURING AN OLFACTORY SUPPORT |
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