CN103961272B - A kind of compounding skin care item based on white beeswax substrate and preparation method thereof - Google Patents
A kind of compounding skin care item based on white beeswax substrate and preparation method thereof Download PDFInfo
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- CN103961272B CN103961272B CN201410218308.3A CN201410218308A CN103961272B CN 103961272 B CN103961272 B CN 103961272B CN 201410218308 A CN201410218308 A CN 201410218308A CN 103961272 B CN103961272 B CN 103961272B
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Abstract
The present invention provides a kind of compounding skin care item based on white beeswax substrate and preparation method thereof, including following raw materials according: Cera Chinensis 0.8～10%, high triacontanol 0.03～1%, camellia seed oil 2～10%, collagen peptide 1.3～4%, medical ventolin 3～6%, glycerol 3～8%, enuatrol 0.5～5%, triethanolamine 0～2%, sodium carboxymethyl cellulose 0.5～3%, water are surplus.First get the raw materials ready, Cera Chinensis and high triacontanol are joined camellia seed oil carries out water-bath, add sodium hydroxide/ethyl alcohol solution and carry out saponification, medical ventolin, glycerol, triethanolamine and sodium carboxymethyl cellulose is added after water-bath is melted, mix under water-bath and add boiling water emulsifying, add collagen peptide aqueous solution after cooling, stir evenly and i.e. obtain compounding skin care item.The present invention has that effect is good, side effect is little, safety is high, it is to avoid the irreversible damage of the skin that synthetic life-time service may cause.
Description
Technical field
The present invention relates to a kind of cosmetics and preparation method thereof, specifically, relate to a kind of based on white beeswax substrate answer
Join skin care item and Preliminary development thereof, belong to daily cosmetics field.
Background technology
Since entering for 20th century, along with the progress of science and technology, it is more likely formed the chemosynthesis of large-scale production than natural product
Goods start large-scale application in cosmetic industry.But, bigger toxicity and zest is often had due to chemicals, it is long
The safety issue that phase uses is paid close attention to the most greatly, people start again again to pursue natural, green, have no side effect
And have the plant resources of multiple physiological, Nutrition.Exploitation plant resources active substance, development pure natural skin care item become
Cosmetic industry develops one of most active theme.
Cera Chinensis is the outstanding person in biowax, is China's distinctive resource insect product.Cera Chinensis granulation promoting is invigorated blood circulation, to skin
Skin has the effect moistening protection, has potential using value in terms of cosmetics.At present, Cera Chinensis is used to coordinate the compositions such as collagen
Compounding skin care item and related manufacturing processes, have not been reported.
Summary of the invention
There is the problem such as side effect and zest for solving existing skin care item, the present invention provides a kind of based on white beeswax substrate
Compounding skin care item and preparation method thereof, with provide one have natural, green, have no side effect and have multiple physiological, nutrition
The plant resources skin care item of effect.
The present invention is realized by following technical proposal: a kind of compounding skin care item based on white beeswax substrate, it is characterised in that bag
Include the raw material of following masses percentage ratio:
Cera Chinensis 0.8～10% high triacontanol 0.03～1%
Camellia seed oil 2～10% collagen peptide 1.3～4%
Medical ventolin 3～6% glycerol 3～8%
Enuatrol 0.5～5% triethanolamine 0～2%
Sodium carboxymethyl cellulose 0.5～3% water surplus.
Another object of the present invention is to provide the preparation method of a kind of compounding skin care item based on white beeswax substrate, its feature
It is through the following step:
(1) by the material preparation of following mass percent:
Cera Chinensis 0.8～10% high triacontanol 0.03～1%
Camellia seed oil 2～10% collagen peptide 1.3～4%
Medical ventolin 3～6% glycerol 3～8%
Enuatrol 0.5～5% triethanolamine 0～2%
Sodium carboxymethyl cellulose 0.5～3% water surplus；
(2), after Cera Chinensis being pulverized, join together with high triacontanol in camellia seed oil, 55～93 DEG C of water bath condition
Under, make Cera Chinensis and high triacontanol be dissolved in camellia seed oil to obtain mixed liquor, then add in mixed liquor mass concentration be 2～
The sodium hydroxide/ethyl alcohol mixed solution of 20% carries out saponification, until sporting gluing state from liquid, i.e. obtains Cera Chinensis water
Soluble base；
(3) by after melted for the water-bath at 55～93 DEG C of step (2) gained Cera Chinensis water-soluble base, medical all scholars are added
Woods, glycerol, triethanolamine and sodium carboxymethyl cellulose, then stirring and evenly mixing to add 2～7 times of Cera Chinensises water-soluble under water bath condition
The boiling water of property substrate quality, emulsifying 5～20min, be then cooled to room temperature, add be deployed into mass concentration be 10.1～
The room temperature collagen peptide aqueous solution of 31.6%, i.e. obtains compounding skin care item based on white beeswax substrate after stirring evenly.
The sodium hydroxide/ethyl alcohol mixed solution of described step (2) is with the ethanol dissolving hydrogen-oxygen that mass concentration is 50～95%
Change sodium to the mixed solution that mass concentration is 2～20%.
The compounding skin care item of described step (3) make the skincare products such as emulsion, frost or cream routinely.
The Cera Chinensis water-soluble base of described step (2) comprises enuatrol, as the composite emulsifier in step (3) it
One uses.
Wherein, in camellia seed oil, unsaturated fatty acid content is up to 90%, and unsaturated fatty acid has the title of " beauty treatment acid ".And
And, camellia seed oil contains higher vitamin E and antioxidant content, can protect skin, especially can prevent skin injury and aging,
Skin is made to have gloss.
High triacontanol also known as high fatty alcohol, be containing 12 carbon atoms more than chain saturated monohydroxy alcohol, at nature
In existence extremely wide, octacosanol therein be added in cosmetics can promote cutaneous circulation, improve oxygen defeated
Send ability, improve basal metabolic rate, activating cell, enhancement skin activity, eliminate wrinkle of skin, antiinflammatory and prevent and treat dermatosis (as
Eczema, pruritus, acne) etc. effect, its using effect is clearly.
Collagen peptide has good absorbability, dissolubility, water absorption and moisture retention, can keep keratodermatitis water
Point, add the moisture-keeping efficacy that has additional nutrients in cosmetic emulsion, increase skin elasticity and make skin beautiful smooth.
Sodium carboxymethyl cellulose odorless, tasteless, have hygroscopicity, be that in the world today, range is the widest, consumption is maximum
Cellulose kind, is used as thickening stabilizing agent in the present invention.
The present invention have the advantage that compared with existing skin care item in the present invention raw material Cera Chinensis used, high triacontanol,
The pure natural property of the plant extracts such as camellia seed oil and distinctive effect thereof, be complementary to one another, mutually promote so that it is at moistening skin-care
Aspect relatively synthetic has uniqueness and significant advantage, has that effect is good, side effect is little, safety is high, nontoxic, no
The feature such as carcinogenic, it is to avoid the irreversible damage of the skin that synthetic life-time service may cause, is a kind of to moisten nutrition
Type skin care item.On the other hand, this be also first by composite usages such as Cera Chinensis, high triacontanol, camellia seed oils in skin care item, expand
The big scope of plant source cosmetics.The compounding skin care item of the present invention are verified by experiments has the effect that nutrition is moistened.
Detailed description of the invention
Below by embodiment, the present invention will be further described.
Embodiment 1
(1) by the material preparation of following mass percent:
Cera Chinensis 3% high triacontanol 0.5%
Camellia seed oil 10% collagen peptide 1.3%
Medical ventolin 5% glycerol 3%
Enuatrol 4% triethanolamine 1%
Sodium carboxymethyl cellulose 3% water surplus；
(2), after Cera Chinensis being pulverized, join together with high triacontanol in camellia seed oil, under 70 DEG C of water bath condition, make
Cera Chinensis and high triacontanol are dissolved in camellia seed oil and obtain mixed liquor, then addition mass concentration is the hydrogen of 10% in mixed liquor
Sodium oxide/alcohol mixed solution carries out saponification, until it sports gluing state from liquid, i.e. obtains Cera Chinensis water solublity base
Matter, wherein sodium hydroxide/ethyl alcohol mixed solution is to be to mass concentration with the ethanol dissolved hydrogen sodium oxide that mass concentration is 50%
10%, Cera Chinensis water-soluble base comprises enuatrol, uses as one of composite emulsifier in step (3)；
(3) by after melted for the water-bath at 93 DEG C of step (2) gained Cera Chinensis water-soluble base, medical ventolin, sweet is added
Oil, triethanolamine and sodium carboxymethyl cellulose, then stirring and evenly mixing add 5 times of Cera Chinensis water-soluble base matter under water bath condition
The boiling water of amount, emulsifying 10min, it is then cooled to room temperature, adds and be deployed into the room temperature fish scale collagen that mass concentration is 16%
Peptide aqueous solution, i.e. obtains compounding skin care item based on white beeswax substrate after stirring evenly, compounding skin care item make emulsion skincare product routinely.
Embodiment 2
(1) by the material preparation of following mass percent:
Cera Chinensis 0.8% high triacontanol 1%
Camellia seed oil 8% collagen peptide 4%
Medical ventolin 3% glycerol 8%
Enuatrol 0.5% triethanolamine 2%
Sodium carboxymethyl cellulose 2% water surplus；
(2), after Cera Chinensis being pulverized, join together with high triacontanol in camellia seed oil, under 55 DEG C of water bath condition, make
Cera Chinensis and high triacontanol are dissolved in camellia seed oil and obtain mixed liquor, then addition mass concentration is the hydrogen of 20% in mixed liquor
Sodium oxide/alcohol mixed solution carries out saponification, until it sports gluing state from liquid, i.e. obtains Cera Chinensis water solublity base
Matter, wherein sodium hydroxide/ethyl alcohol mixed solution is to be to mass concentration with the ethanol dissolved hydrogen sodium oxide that mass concentration is 75%
20%, Cera Chinensis water-soluble base comprises enuatrol, uses as one of composite emulsifier in step (3)；
(3) by after melted for the water-bath at 80 DEG C of step (2) gained Cera Chinensis water-soluble base, medical ventolin, sweet is added
Oil, triethanolamine and sodium carboxymethyl cellulose, then stirring and evenly mixing add 7 times of Cera Chinensis water-soluble base matter under water bath condition
The boiling water of amount, emulsifying 20min, it is then cooled to room temperature, adds and be deployed into the room temperature scale collagen egg that mass concentration is 31.6%
White peptide aqueous solution, i.e. obtains compounding skin care item based on white beeswax substrate after stirring evenly, compounding skin care item are made frost shape skin protection routinely and used
Product.
Embodiment 3
(1) by the material preparation of following mass percent:
Cera Chinensis 10% high triacontanol 0.03%
Camellia seed oil 2% collagen peptide 2%
Medical ventolin 6% glycerol 6%
Enuatrol 5% sodium carboxymethyl cellulose 0.5%
Water surplus；
(2), after Cera Chinensis being pulverized, join together with high triacontanol in camellia seed oil, under 93 DEG C of water bath condition, make
Cera Chinensis and high triacontanol are dissolved in camellia seed oil and obtain mixed liquor, then addition mass concentration is the hydrogen-oxygen of 2% in mixed liquor
Change sodium/alcohol mixed solution and carry out saponification, until it sports gluing state from liquid, i.e. obtain Cera Chinensis water solublity base
Matter, wherein sodium hydroxide/ethyl alcohol mixed solution is to be to mass concentration with the ethanol dissolved hydrogen sodium oxide that mass concentration is 95%
2%, Cera Chinensis water-soluble base comprises enuatrol, uses as one of composite emulsifier in step (3)；
(3) by after melted for the water-bath at 55 DEG C of step (2) gained Cera Chinensis water-soluble base, medical ventolin, sweet is added
Oil, triethanolamine and sodium carboxymethyl cellulose, then stirring and evenly mixing add 2 times of Cera Chinensis water-soluble base matter under water bath condition
The boiling water of amount, emulsifying 5min, it is then cooled to room temperature, adds and be deployed into the room temperature scale collagen egg that mass concentration is 10.1%
White peptide aqueous solution, i.e. obtains compounding skin care item based on white beeswax substrate after stirring evenly, compounding skin care item are made paste skin protection routinely and used
Product.
Organoleptic indicator and the physical and chemical index of embodiment 1,2,3 skin care item are as follows:
Organoleptic indicator: this compounding skin care item color and luster is pale, mastic is fine and smooth, and uniformly, profit does not separates, and easily absorbs in coating.
1, physical and chemical index:
(1) pH value: the pH value of compounding skin care item is 6.5～7.5.
(2) heat-resistant experiment
Taking gained to compound skin care item and pour in 2 test tubes respectively, the cleanest cork, wherein examination to be checked
Pipe is placed in and is pre-adjusted to the calorstat of 40 ± 1 DEG C, takes out after 24h, carries out with sample in another test tube after recovering room temperature
Range estimation is compared, and finds without oil-water separation phenomenon, and character is without significant difference.
(3) cold-resistant experiment
The compounding skin care item taking preparation are poured in 2 test tubes respectively, the cleanest cork.According to cold-resistant index: excellent
Level product require-15 DEG C/24h, recover room temperature oil-free water segregation phenomenon；Primes requires-10 DEG C/24h, recovers room temperature oil-free moisture
From phenomenon；Certified products require-5 DEG C/24h, recover room temperature oil-free water segregation phenomenon.Wherein test tube to be checked is placed in advance
In the refrigerator that regulation is extremely-18 DEG C, take out after 24h, carry out range estimation with sample in another test tube after recovering room temperature and compare, find nothing
Oil-water separation phenomenon, character is without significant difference.
(4) heat-resisting cold-resistant alternately experiment
Finishing heat resistant test (or low temperature resistant test), then do low temperature resistant test (or heat resistant test), so referred to as one cold and hot
Circulation, the most repeatedly, until the phenomenons such as oil-water separation, color and luster change or permeability occur in institute's test sample product, records period.Will be compounding
Skin care item carry out heat-resisting cold-resistant alternately experiment, to circulation eight times, color and luster change and permeability phenomenon occur, do not occur that profit divides
From.Reach stability (cold cycling) index.
(5) centrifugal test
In centrifuge tube, inject compounding skin care item about 2/3rds height and fill reality, building lid, be then placed in adjusting in advance
Save the calorstat inside holding 1h of 38 ± 1 DEG C, move into centrifuge immediately and be adjusted to setting speed, rotate to take out after terminating and observe.
Test 2000r/min respectively and rotate 30min, 3000r/min rotation 30min, 4000r/min rotation 30min, 5000r/min
Rotate 30min, find that oil-water separation does not all occur, and sample property does not occurs significant change, reach the centrifugal stably finger of cosmetics
Mark.(according to the physical and chemical index of skin care item, in centrifugal test, 4000r/min rotation 30min is not stratified, for top grade product；3000r/
It is not stratified, for primes that min rotates 30min；It is not stratified for certified products that 2000r/min rotates 30min).
Embodiment 1,2,3 gained compounds skin care item carry out human efficiency and test as follows:
Experimental group have chosen the compounding skin care item that 86 volunteer's trial edition inventive embodiments 1 provide, wherein male 31 people,
Women 55 people.Additionally choose matched group 20 people, wherein male 10 people, women 10 people, during experiment, disable any skin care item.Will be real
Drying after the inboard arm wash clean of the volunteer testing group and matched group, the inboard arm experimental group volunteer draws a circle to approve one directly
Footpath is the border circular areas of 2.5cm, and with the sample size every about square centimeter 2mg, sample is beaten the inboard arm volunteer, it
Rear volunteer smears with the finger of another hands voluntarily.Meanwhile, volunteer's inboard arm of matched group does not smear any protecting
Skin product.During experiment, there is not untoward reaction in experimental group, and the inboard arm skin of experimental group volunteer is all than matched group
More moist, fine and smooth, glossy.
Claims (1)
1. compounding skin care item based on white beeswax substrate, it is characterised in that be made up of the raw material of following masses percentage ratio:
Cera Chinensis 0.8～10% high triacontanol 0.03～1%
Camellia seed oil 2～10% collagen peptide 1.3～4%
Medical ventolin 3～6% glycerol 3～8%
Enuatrol 0.5～5% triethanolamine 0～2%
Sodium carboxymethyl cellulose 0.5～3% water are surplus.
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| CN201410218308.3A CN103961272B (en) | 2014-05-22 | 2014-05-22 | A kind of compounding skin care item based on white beeswax substrate and preparation method thereof |
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| CN103961272B true CN103961272B (en) | 2016-09-14 |
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| CN105943474A (en) * | 2016-07-06 | 2016-09-21 | 广东工业大学 | Composition, as well as preparation method and application thereof |
| CN106038825B (en) * | 2016-08-01 | 2020-02-14 | 中国林业科学研究院资源昆虫研究所 | Ointment for promoting wound healing and preparation method thereof |
| CN108721199A (en) * | 2018-08-30 | 2018-11-02 | 项佳红 | A kind of freckle removing and whitening type health-care skin-protecting products and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101886106A (en) * | 2010-07-02 | 2010-11-17 | 湖北远成药业有限公司 | Method for extracting collagen peptide from fish scales |
| CN102908304A (en) * | 2012-11-19 | 2013-02-06 | 浙江省林业科学研究院 | Anti-ageing wrinkle reduction toning lotion enriched with active peptide, and preparation method thereof |
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2014
- 2014-05-22 CN CN201410218308.3A patent/CN103961272B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101886106A (en) * | 2010-07-02 | 2010-11-17 | 湖北远成药业有限公司 | Method for extracting collagen peptide from fish scales |
| CN102908304A (en) * | 2012-11-19 | 2013-02-06 | 浙江省林业科学研究院 | Anti-ageing wrinkle reduction toning lotion enriched with active peptide, and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 鱼鳞胶原蛋白的研究进展和应用前景;曹俊;《水产科技情报》;20091231;第36卷(第1期);第41-44页 * |
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Inventor after: Ma Jinju Inventor after: Ma Liyi Inventor after: Chen Xiaoming Inventor after: Zhang Hong Inventor after: Zhang Zhongquan Inventor after: Wang Youqiong Inventor after: Duan Qiongfen Inventor before: Ma Jinju Inventor before: Ma Liyi Inventor before: Zhang Hong Inventor before: Zhang Zhongquan Inventor before: Wang Youqiong Inventor before: Duan Qiongfen |
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Free format text: CORRECT: INVENTOR; FROM: MA JINJU MA LIYI ZHANG HONG ZHANG ZHONGQUAN WANG YOUQIONG DUAN QIONGFEN TO: MA JINJU MA LIYI CHEN XIAOMING ZHANG HONG ZHANG ZHONGQUAN WANG YOUQIONG DUAN QIONGFEN |
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