CN102784068B - BB cream and preparation method thereof - Google Patents
BB cream and preparation method thereof Download PDFInfo
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- CN102784068B CN102784068B CN201110127193.3A CN201110127193A CN102784068B CN 102784068 B CN102784068 B CN 102784068B CN 201110127193 A CN201110127193 A CN 201110127193A CN 102784068 B CN102784068 B CN 102784068B
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- frost
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- capsule
- granule
- titanium white
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- 239000006071 cream Substances 0.000 title abstract description 11
- 238000002360 preparation method Methods 0.000 title abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 46
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
- 238000003756 stirring Methods 0.000 claims abstract description 28
- 239000000758 substrate Substances 0.000 claims abstract description 18
- 239000008367 deionised water Substances 0.000 claims abstract description 16
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 16
- 239000002245 particle Substances 0.000 claims abstract description 10
- 239000002270 dispersing agent Substances 0.000 claims abstract description 9
- 230000002421 anti-septic effect Effects 0.000 claims abstract description 8
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 8
- 239000002904 solvent Substances 0.000 claims abstract description 8
- 239000008187 granular material Substances 0.000 claims description 47
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 41
- 235000010215 titanium dioxide Nutrition 0.000 claims description 38
- 230000002087 whitening effect Effects 0.000 claims description 36
- 239000002775 capsule Substances 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 12
- 230000001804 emulsifying effect Effects 0.000 claims description 8
- 239000003974 emollient agent Substances 0.000 claims description 7
- 239000000080 wetting agent Substances 0.000 claims description 7
- 230000005484 gravity Effects 0.000 claims description 6
- 230000008569 process Effects 0.000 claims description 6
- 238000000518 rheometry Methods 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 abstract description 9
- 239000002537 cosmetic Substances 0.000 abstract description 5
- 239000003995 emulsifying agent Substances 0.000 abstract description 3
- 239000002738 chelating agent Substances 0.000 abstract 2
- 238000001816 cooling Methods 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerol group Chemical group OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 18
- 238000002474 experimental method Methods 0.000 description 14
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical group NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 description 12
- 239000003921 oil Substances 0.000 description 11
- OWPUOLBODXJOKH-UHFFFAOYSA-N 2,3-dihydroxypropyl prop-2-enoate Chemical group OCC(O)COC(=O)C=C OWPUOLBODXJOKH-UHFFFAOYSA-N 0.000 description 8
- 230000000694 effects Effects 0.000 description 8
- 238000004945 emulsification Methods 0.000 description 8
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 description 6
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 description 6
- 241000221095 Simmondsia Species 0.000 description 6
- 235000004433 Simmondsia californica Nutrition 0.000 description 6
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical group OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 6
- 229920006243 acrylic copolymer Polymers 0.000 description 6
- 229960000458 allantoin Drugs 0.000 description 6
- 239000004359 castor oil Substances 0.000 description 6
- 235000019438 castor oil Nutrition 0.000 description 6
- 230000002354 daily effect Effects 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 150000002148 esters Chemical class 0.000 description 6
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 6
- 230000007062 hydrolysis Effects 0.000 description 6
- 238000006460 hydrolysis reaction Methods 0.000 description 6
- 229940069338 potassium sorbate Drugs 0.000 description 6
- 235000010241 potassium sorbate Nutrition 0.000 description 6
- 239000004302 potassium sorbate Substances 0.000 description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical group OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 5
- 239000002552 dosage form Substances 0.000 description 5
- 230000006872 improvement Effects 0.000 description 5
- 238000012423 maintenance Methods 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 description 5
- 239000000047 product Substances 0.000 description 4
- 230000015556 catabolic process Effects 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 239000004408 titanium dioxide Substances 0.000 description 3
- 229920002126 Acrylic acid copolymer Polymers 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 229920002261 Corn starch Polymers 0.000 description 2
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 description 2
- 229930195725 Mannitol Natural products 0.000 description 2
- 229920000168 Microcrystalline cellulose Polymers 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- 230000003796 beauty Effects 0.000 description 2
- 229960001631 carbomer Drugs 0.000 description 2
- 239000008120 corn starch Substances 0.000 description 2
- 230000009977 dual effect Effects 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 239000000594 mannitol Substances 0.000 description 2
- 235000010355 mannitol Nutrition 0.000 description 2
- 235000019813 microcrystalline cellulose Nutrition 0.000 description 2
- 239000008108 microcrystalline cellulose Substances 0.000 description 2
- 229940016286 microcrystalline cellulose Drugs 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 230000008929 regeneration Effects 0.000 description 2
- 238000011069 regeneration method Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- OSCJHTSDLYVCQC-UHFFFAOYSA-N 2-ethylhexyl 4-[[4-[4-(tert-butylcarbamoyl)anilino]-6-[4-(2-ethylhexoxycarbonyl)anilino]-1,3,5-triazin-2-yl]amino]benzoate Chemical compound C1=CC(C(=O)OCC(CC)CCCC)=CC=C1NC1=NC(NC=2C=CC(=CC=2)C(=O)NC(C)(C)C)=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=N1 OSCJHTSDLYVCQC-UHFFFAOYSA-N 0.000 description 1
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 description 1
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 244000062730 Melissa officinalis Species 0.000 description 1
- 235000010654 Melissa officinalis Nutrition 0.000 description 1
- 241000700647 Variola virus Species 0.000 description 1
- 206010048222 Xerosis Diseases 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000003044 adaptive effect Effects 0.000 description 1
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- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005282 brightening Methods 0.000 description 1
- -1 card ripple 980 Chemical compound 0.000 description 1
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- 239000003086 colorant Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 239000007863 gel particle Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 239000000865 liniment Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
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- 238000004806 packaging method and process Methods 0.000 description 1
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- 230000001835 salubrious effect Effects 0.000 description 1
- 231100000241 scar Toxicity 0.000 description 1
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- 239000013589 supplement Substances 0.000 description 1
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Landscapes
- Cosmetics (AREA)
Abstract
The invention relates to a cosmetic, and especially relates to a BB cream and its preparation method. The BB cream is a gel type BB cream, and raw materials of the BB cream mainly comprise a gel substrate, a dispersant, and BB cream particles, wherein the raw materials of the gel substrate mainly comprise deionized water, a rheological adjustment agent, a chelating agent, a neutralizer, an antiseptic and a solubilizer. The preparation method of the BB cream comprises the following steps: uniformly mixing the deionized water, the rheological adjustment agent, the chelating agent and the dispersant at room temperature, stirring, and heating to 80-85DEG C; adding the neutralizer, uniformly stirring, and maintaining the temperature for 20-25min; cooling to 40-45DEG C, adding the antiseptic and the solubilizer, and uniformly stirring; and cooling to 38-40DEG C, adding the BB cream particles, and uniformly stirring. The preparation method solves technical problems of instability and excess oil content of present emulsifier type BB creams.
Description
Technical field
The present invention relates to a kind of cosmetics, relate in particular to a kind of BB frost.The invention still further relates to a kind of preparation method of cosmetics, relate in particular to the preparation method of this BB frost.
Background technology
In recent years, along with the increase of the development of cosmetics and the women's that likes to be beautiful demand, BB frost was pursued by people more and more and was become fashion trend.Its underlying cause is that BB frost is not only easy to use, and has effect of foundation cream, sun-proof and isolated product concurrently.The women who likes to be beautiful only need use BB frost just can have flawless skin quality and skinfeel.BB frost can allow female friend go out in proud array; More can help the women who likes to be beautiful to make adornment of the perfect end, keep lastingly the dressing of a day.
BB frost, is the abbreviation of Blemish Balm, and effect is mainly to hide the flaw, the adjustment colour of skin, sun-proof, careful pore, can create the sensation of Nude Look (naked adornment effect).BB frost is originally after peeling or whitening (brightening), the protection of the skin to impaired and damage and the regeneration frost that maintenance is used.This regeneration frost can be given and improve rapidly in time the problem of skin, can improve and make up the shortcoming of skin, thereby the BB frost of gaining the name.
BB frost is developed so far, and has experienced first generation BB frost (scar maintenance frost), and second filial generation BB frost (having merged the dual identity of skin care products and foundation cream), has released third generation BB frost now.Science and technology is innovation constantly, by initial airtight after using on the face, the even BB frost and the white combination of maintenance of life-time service skin president small pox of xerosis cutis, has formed third generation BB frost.Third generation BB frost has the following advantages: 1, make newborn skin permeability good; Because the third generation BB frost molecular weight decomposing by up-to-date beauty treatment science and technology is less, be used on the face and can not stop up pore later, breathability is fine.2, deep layer is nourished: little by sub-molecular weight, the basal layer of the skin that can go directly, directly acts on cell, is conducive to the absorption of nutritional labeling, and absorbtivity is the three-to-four-fold of second filial generation BB frost; On this basis, third generation BB frost, also add the concept of deep moisturizing, in BB frost, add the best molecule of maintenance composition and moisturizing, micromolecular water, utilizes up-to-date most advanced and sophisticated composition embedding techniques can better supplement moisture of skin inside, makes skin for a long time in moistening state, performance of keeping humidity is good, and life-time service skin can not be dried.3, easily makeup removing; Because nutritional labeling is completely absorbed, thus general makeup removing liquid for makeup removing, or warm water to add facial milk cleanser just passable.
BB frost itself has maintenance and the dual identity that hides the flaw, and the impression of the ignoring skin in order to reach the effect that hides the flaw, this belongs to a kind of phenomenon of contradiction at beauty treatment fields, so the technology innovation of BB frost is regenerated extremely urgent.
Existing BB frost is all Water-In-Oil or oil-in-water emulsification system on the market, is to form stable system by oil phase and water by emulsifying agent.But emulsification system is subject to external environment as larger in the impact of temperature and air pressure, larger temperature Change may be destroyed the stable of emulsification system, occurs the phenomenon of breakdown of emulsion, shows as emulsification system and occurs obvious layering.Breakdown of emulsion is the problem that emulsification system the most easily produces.In addition in emulsification system, oil content is essential.Oil content is also necessary for skin, but excessive oil content can make skin, over-burden.Skin be oiliness or summer skin too easily go out under oil condition, everybody wishes to use salubrious BB frost, wishes that BB frost has the effect of the appearance of repairing simultaneously.Therefore just need a kind of dosage form of brand-new BB frost to solve these problems and reach good result of use.
Under this background and demand, this case inventor has expected suspending to have by this dosage form of gel repairing the titanium dioxide granule that holds effect.First gel is the formula of pure water phase, has avoided containing oil content in BB frost, is more applicable to summer and oiliness skin and uses.In addition the dosage form of gel particle does not need emulsifying agent to stablize, and it is just very little that BB frost is subject to the impact of external environment like this, can not make BB frost occur the problem of stability because of sharply changing of temperature.
Summary of the invention
A first aspect of the present invention object is to provide a kind of BB frost, and this BB frost is subject to the impact of external environment little, not containing excessive oil content, has solved the technical problem that BB frost is unstable, oil-containing is excessive of present emulsifying dosage form.
The present invention solves the problems of the technologies described above by the following technical programs, reaches a first aspect of the present invention object.
A kind of BB frost, described BB frost is gel type BB frost, it is as follows that the component that the raw material of described gel type BB frost mainly comprises and this component account for the mass percent of raw material of described gel type BB frost:
Gel substrate 91-95.5%
Dispersant 1.0-3.0%
BB frost granule 2.5-6.0%.
In the present invention, it is as follows that the component that the raw material of described gel substrate mainly comprises and this component account for the mass percent of raw material of described gel type BB frost:
In the present invention, described BB frost granule is BB frost embedding capsule and two kinds of BB frost granules of titanium white whitening capsule.BB frost embedding capsule mainly comprises titanium dioxide, microcrystalline Cellulose, and mannitol, corn starch, hydrolecithin and pigment, titanium white whitening capsule mainly comprises titanium dioxide, microcrystalline Cellulose, mannitol, Kaolin corn starch and pigment.The particle diameter of two kinds of BB frost granules of described BB frost embedding capsule and titanium white whitening capsule is 0.5mm-3mm.Described titanium white whitening capsule is 1.2-1.5 with respect to the specific gravity range of water, and described BB frost embedding capsule is 1.2-1.4 with respect to the specific gravity range of water.Gel system is the system of pure water matter, its density has a specific scope, the BB frost granule of not every particle diameter and weight can stable existence in gel system, therefore determining after the component content of gel substrate, need to carry out the test of BB frost granule stability, select the BB frost granule of suitable particle diameter and weight.With formula test, BB frost of the present invention preferably uses the BB frost granule of particle diameter between 0.5mm-3mm by experiment, and such BB frost granule proportion and density are all relatively applicable to gel substrate of the present invention, can in system, suspend more stablely and keep to suspend.
Further, the preferred BB frost of described BB frost embedding capsule embedding capsule-yellow 12, the preferred titanium white whitening capsule-green 12 of described titanium white whitening capsule, the quality ratio range of described titanium white whitening capsule-green 12 and described BB frost embedding capsule-yellow 12 preferably 2: 3-3: 1.
The color of BB frost granule selects to have comprised two aspects, the color of the powder wrapping up in the firstth, BB frost granule, the powder of the preferred colour of skin of the present invention and ivory white two kinds of colors, the BB frost granule that wraps up respectively these two kinds of powder by certain proportioning after, can form more natural color, substantially be suitable for most Asia women; The secondth, BB frost particle appearance color, the selection of outward appearance is mainly to consider visual effect.The present invention is titanium white whitening capsule-green 12 and BB frost embedding capsule-yellow 12 preferably; What titanium white whitening capsule-green 12 was wrapped up is the powder of the colour of skin, and the color of outward appearance is green, and what BB frost embedding capsule-yellow 12 was wrapped up is white powder, and the color of outward appearance is yellow.Inventor find surprisingly when the proportioning of titanium white whitening capsule-green 12 and BB frost embedding capsule-yellow 12 in reasonable and suitable scope as 2: 3-3: in 1 scope time, (colour of skin of Asia women is generally more yellow can be applicable to most of Asia women, after the BB frost of the application of the invention, the colour of skin all can have obvious improvement, and this improvement is accepted by most of Asia women).Through test, when the proportioning of titanium white whitening capsule-green 12 and BB frost embedding capsule-yellow 12 is 2: 3-3: in 1 scope time, its skinfeel and whiteness of skin after using can be accepted by 92% tester (improvement that acceptance refers to this colour of skin is user approval, feel acceptable).
In the present invention, the component that the raw material of described gel type BB frost also comprises is emollient, and the mass percent that described emollient accounts for the raw material of described gel type BB frost is 1.0-3.0%.
In the present invention, the component that the raw material of described gel substrate also comprises is Derma-Guard, and the mass percent that described Derma-Guard accounts for the raw material of described gel type BB frost is 0.2-0.5%.
In the present invention, the component that the raw material of described gel substrate also comprises is wetting agent, and the mass percent that described wetting agent accounts for the raw material of described gel type BB frost is 2.0-6.0%.
In the present invention, the component that the raw material of described gel substrate also comprises is essence, and the mass percent that described essence accounts for the raw material of described gel type BB frost is 0.02-0.1%.
In the present invention, described emollient is preferably hydrolysis Jojoba esters.
In the present invention, described dispersant is preferably glycerol acrylate/acrylic copolymer (English name: Glyceryl acrylate/acrylic acid copolymer is a kind of glycerol acrylate and acrylic acid copolymer).
In the present invention, described rheology control agent is preferably carbomer.
In the present invention, described chelating agen is preferably EDETATE SODIUM.
In the present invention, described Derma-Guard is preferably allantoin.
In the present invention, described wetting agent is preferably glycerol.
In the present invention, described nertralizer is preferably triethanolamine.
In the present invention, described antiseptic is preferably potassium sorbate.
In the present invention, described solubilizing agent is preferably castor oil hydrogenated.
In the present invention, described essence is preferably daily essence.
A second aspect of the present invention object is to propose the preparation method of aforementioned BB frost.
The present invention reaches a second aspect of the present invention object by the following technical programs.
A kind of method of preparing aforementioned BB frost, the method is at room temperature described deionized water, described rheology control agent, described chelating agen, described dispersant to be added in vacuum emulsifying pot successively, then homogenizing is uniformly dispersed raw material, stirs and is warming up to 80-85 ℃; Add described nertralizer to stir, insulation 20-25 minute; In 30-60 minute, be cooled to 40-45 ℃ and add described antiseptic, described solubilizing agent, stir; Be cooled to 38-40 ℃, then add described BB frost granule, stir and obtain described BB frost.
In the present invention, the described method of preparing BB frost also comprises the pretreatment process of described BB frost granule, and the pretreatment process of described BB frost granule is to soak described BB frost granule 2-4 hour with the deionized water of 20-40 ℃.
BB frost of the present invention is take gel as carrier and the BB frost of substrate, is particularly suitable for oiliness skin and other various skin and uses in summer.The beneficial effect of BB frost of the present invention is: (1) is frost carrier and substrate using gel as BB, because gel is the formula of pure water matter, avoid having too much oil content in BB frost, while using BB frost, just can not produce greasy feeling, made skin more merrily and lightheartedly exquisitely carved; (2) BB of gel substrate frost texture is very sparkling and crystal-clear, and the BB frost profit that more adds water can meet the moistening effect of skin; (3) suspend in the gel brand-new system of BB frost granule, after effect mix homogeneously by pump head, very convenient when use, and (pump head is parts on packaging bottle can to make skin present more natural outward appearance, BB frost granule in BB frost of the present invention is by after the extruding of pump head, can be disperseed more equably, be Powdered rather than original graininess during like this with contact skin, while therefore use, facilitated); (4) in gel, the system of particle is more stable compared with traditional BB frost, is not vulnerable to the impact of external environment, can make the sharply variation of BB frost adaptive temperature.
BB frost of the present invention is carried out to heat-resisting cold-resistant circulation experiment: BB frost of the present invention is put into constant incubator, carry out heat-resisting (40 ± 1 ℃) experiment, place after one month, take out to return to and observe after room temperature without separating, without metachromatism, then put into the experiment (5～-15 ℃) of resisting cold in refrigerator, place after one month, taking-up is observed without separation, without metachromatism after returning to room temperature; This process is a circulation experiment.Carry out after three circulation experiments, recovered to observe BB frost of the present invention after room temperature, without separating and metachromatism.
The BB frost of emulsifying dosage form of the prior art generally only does once heat-resisting cold-resistant circulation experiment, because circulation repeatedly can make emulsification system breakdown of emulsion, finally causes system to occur that water is separating of oil.Can stand heat-resisting cold-resistant circulation experiment at least 3 times take the Gel mile of BB frost as carrier, illustrate that the stability of Gel mile of system surpasses general emulsification system.
The specific embodiment
A kind of BB frost, this BB frost is gel type BB frost, it is as follows that the component that the raw material of gel type BB frost mainly comprises and this component account for the mass percent of raw material of gel type BB frost:
In above-mentioned component, the mass percent that the raw material of gel substrate accounts for the raw material of gel type BB frost is preferably 91-95.5%.
In above-mentioned component, BB frost granule is BB frost embedding capsule and two kinds of BB frost granules of titanium white whitening capsule, the particle diameter of two kinds of BB frost granules of BB frost embedding capsule and titanium white whitening capsule is 0.5mm-3mm, titanium white whitening capsule is 1.2-1.5 with respect to the specific gravity range of water, and BB frost embedding capsule is 1.2-1.4 with respect to the specific gravity range of water.BB frost embedding capsule is BB frost embedding capsule-yellow 12, and titanium white whitening capsule is titanium white whitening capsule-green 12, and the quality ratio range of titanium white whitening capsule-green 12 and BB frost embedding capsule-yellow 12 is 2: 3-3: 1.BB frost granule has carried out pretreatment.Pretreatment is to soak BB frost granule 2-4 hour with the deionized water of 20-40 ℃; Pretreatment can make BB frost granule have applicable hardness and applicable loft; Pretreated object is to strengthen BB frost of the present invention comfort level in use.
In above-mentioned component, emollient is hydrolysis Jojoba esters.Dispersant is glycerol acrylate/acrylic copolymer.Rheology control agent is carbomer, is preferably the one in card ripple U21, carbopol 940 and Ka Bo 980.Chelating agen is EDETATE SODIUM.Derma-Guard is allantoin.Wetting agent is glycerol.Nertralizer is triethanolamine.Antiseptic is potassium sorbate.Solubilizing agent is castor oil hydrogenated.Essence is daily essence.
The preparation method of this BB frost is: with the deionized water immersion BB frost granule 2-4 hour of 20-40 ℃; Under room temperature, deionized water, rheology control agent, chelating agen, Derma-Guard, wetting agent, emollient, dispersant are added successively in vacuum emulsifying pot, then homogenizing is uniformly dispersed raw material, stirring is warming up to 80-85 ℃, and mixing speed is 2000-2500 rev/min; Add nertralizer to stir, insulation 20-25 minute; In 30-60 minute, be cooled to 40-45 ℃ and add antiseptic, solubilizing agent and essence, stir; Be cooled to 38-40 ℃, slow down mixing speed to 1500-1800 rev/min, then add BB frost granule, stir.
Organoleptic indicator and the relevant physical and chemical parameter of the BB frost preparing according to this specific embodiment are as follows:
Organoleptic indicator: color and luster: water white transparency includes color grains
Abnormal smells from the patient: peat-reek
Outward appearance: uniform and smooth, water white transparency include the gel of color grains
Physical and chemical parameter: pH (25 ℃): 5.5-7.0
Heat-resisting (40 ± 1 ℃, 24h): recover after room temperature without separating, without metachromatism
Cold-resistant (5～-15 ℃, 24h): recover after room temperature without separating, without metachromatism
Density (25 ℃): 1.000-1.500g/ml
Embodiment 1
A kind of BB frost, BB frost is gel type BB frost, it is as follows that the component that the raw material of gel type BB frost comprises and component account for the mass percent of this raw material:
Wherein, BB frost granule is BB frost embedding capsule-yellow 12,12 two kinds of BB frost granules of titanium white whitening capsule-green, and the quality proportioning of titanium white whitening capsule-green 12 and BB frost embedding capsule-yellow 12 is 3:2.Prepare BB frost with 100kg raw material, by above-mentioned mass percent feeding, wherein BB frost granule is the BB frost granule having soaked with the deionized water of 20 ℃ 4 hours; Under room temperature, deionized water, card ripple U21, EDTA disodium, allantoin, glycerol, hydrolysis Jojoba esters, glycerol acrylate/acrylic copolymer are added in vacuum emulsifying pot successively, then homogenizing is uniformly dispersed raw material, stirring is warming up to 80 ℃, and mixing speed is 2000 revs/min; Add triethanolamine to stir, be incubated 25 minutes; In 30 minutes, be cooled to 40 ℃ and add potassium sorbate, castor oil hydrogenated and daily essence, stir; Be cooled to 40 ℃, slow down mixing speed to 1500 rev/min, then add BB frost embedding capsule-yellow 12 and titanium white whitening capsule-green 12, stir, make BB frost 96.1kg.
The BB frost of the present embodiment is carried out to heat-resisting cold-resistant circulation experiment: the BB frost of the present embodiment is put into constant incubator, carry out heat-resisting (40 ± 1 ℃) experiment, place after one month, take out to return to and observe after room temperature without separating, without metachromatism, then put into the experiment (5～-15 ℃) of resisting cold in refrigerator, place after one month, taking-up is observed without separation, without metachromatism after returning to room temperature; This process is a circulation experiment.Carry out after three circulation experiments, after recovery room temperature, observed the BB frost of the present embodiment, without separating and metachromatism.
By the BB frost of the present embodiment, offer volunteer and try out (on probation maintaining secrecy); Volunteer is the yellow race at Asia random choose; Period of time for approval is three months, and every day is on probation once.Questionnaire after use shows, without allergic phenomena, without greasy feeling, 99% volunteer's the colour of skin all can have obvious improvement, skinfeel after wherein using and the whiteness of skin can be by 92% volunteers received (improvement that acceptance refers to this colour of skin be that volunteer approves, feel acceptable).
Embodiment 2
A kind of BB frost, BB frost is gel type BB frost, it is as follows that the component that the raw material of gel type BB frost comprises and component account for the mass percent of this raw material:
Wherein, BB frost granule is BB frost embedding capsule-yellow 12,12 two kinds of BB frost granules of titanium white whitening capsule-green, and the quality proportioning of titanium white whitening capsule-green 12 and BB frost embedding capsule-yellow 12 is 7:3.Prepare BB frost with 100kg raw material, by above-mentioned mass percent feeding, wherein BB frost granule is the BB frost granule having soaked with the deionized water of 40 ℃ 2 hours; Under room temperature, deionized water, carbopol 940, EDETATE SODIUM, allantoin, glycerol, hydrolysis Jojoba esters, glycerol acrylate/acrylic copolymer are added in vacuum emulsifying pot successively, then homogenizing is uniformly dispersed raw material, stirring is warming up to 85 ℃, and mixing speed is 2500 revs/min; Add triethanolamine to stir, be incubated 20 minutes; In 60 minutes, be cooled to 45 ℃ and add potassium sorbate, castor oil hydrogenated and daily essence, stir; Be cooled to 38 ℃, slow down mixing speed to 1800 rev/min, then add BB frost embedding capsule-yellow 12 and titanium white whitening capsule-green 12, stir, make BB frost 95.5kg.
Embodiment 3
A kind of BB frost, BB frost is gel type BB frost, it is as follows that the component that the raw material of gel type BB frost comprises and component account for the mass percent of this raw material:
Wherein, BB frost granule is BB frost embedding capsule-yellow 12,12 two kinds of BB frost granules of titanium white whitening capsule-green, and the quality proportioning of titanium white whitening capsule-green 12 and BB frost embedding capsule-yellow 12 is 2:1.Prepare BB frost with 100kg raw material, by above-mentioned mass percent feeding, wherein BB frost granule is the BB frost granule having soaked with the deionized water of 30 ℃ 3 hours; Under room temperature, deionized water, card ripple 980, EDETATE SODIUM, allantoin, glycerol, hydrolysis Jojoba esters, glycerol acrylate/acrylic copolymer are added in vacuum emulsifying pot successively, then homogenizing is uniformly dispersed raw material, stirring is warming up to 83 ℃, and mixing speed is 2200 revs/min; Add triethanolamine to stir, be incubated 23 minutes; In 45 minutes, be cooled to 43 ℃ and add potassium sorbate, castor oil hydrogenated and daily essence, stir; Be cooled to 39 ℃, slow down mixing speed to 1600 rev/min, then add BB frost embedding capsule-yellow 12 and titanium white whitening capsule-green 12, stir, make BB frost 95.8kg.
In this specific embodiment, the source of raw material is as follows:
The Noveon company (Noveon, Inc) of card ripple U21, carbopol 940, the Ka Bo980You U.S. produces;
EDETATE SODIUM is produced by Shanghai company of Zhi Rou Chemical Co., Ltd.;
Allantoin is produced by the International Specialty Products company (ISP) of the U.S.;
Glycerol is produced by Shanghai Zhi Rou Chemical Co., Ltd.;
Triethanolamine is produced by Shanghai Zhi Rou Chemical Co., Ltd.;
Hydrolysis Jojoba esters is produced by the Fu Bo Chemical Co., Ltd. of Taiwan;
Glycerol acrylate/acrylic copolymer is produced by the International Specialty Products company (ISP) of the U.S.;
Potassium sorbate is produced by Evonik Degussa (China) Co., Ltd. (EVONIK INDUSTRIES);
Castor oil hydrogenated is produced by Evonik Degussa (China) Co., Ltd. (EVONIK INDUSTRIES);
Daily essence is produced by German De Leman essence corporation (DROM);
The Magic50-BY12 that BB frost embedding capsule-yellow 12 is produced by KPT company of Korea S's (strain) (KPT Co., Ltd.);
The Magic30-WG12 that titanium white whitening capsule-green 12 is produced by KPT company of Korea S's (strain) (KPT Co., Ltd.);
The component content (mass percent) of titanium white whitening capsule-green 12 and BB frost embedding capsule-yellow 12 is as follows:
INCI is international name cosmetic material; CAS No. is that U.S. chemical abstract is served the registration number that society (Chemical Abstracts Service, CAS) works out for chemical substance.
More than describe preferred embodiment of the present invention in detail.The ordinary skill that should be appreciated that this area just can design according to the present invention be made many modifications and variations without creative work.Therefore, all technical staff in the art, all should be in by the determined protection domain of claims under this invention's idea on the basis of existing technology by the available technical scheme of logical analysis, reasoning, or a limited experiment.
Claims (8)
1. a BB frost, is characterized in that, described BB frost is gel type BB frost, and it is as follows that the component that the raw material of described gel type BB frost mainly comprises and this component account for the mass percent of raw material of described gel type BB frost:
Gel substrate 91-95.5%
Dispersant 1.0-3.0%
BB frost granule 2.5-6.0%;
Described BB frost granule is BB frost embedding capsule and two kinds of BB frost granules of titanium white whitening capsule, the particle diameter of two kinds of BB frost granules of described BB frost embedding capsule and titanium white whitening capsule is 0.5mm-3mm, described titanium white whitening capsule is 1.2-1.5 with respect to the specific gravity range of water, and described BB frost embedding capsule is 1.2-1.4 with respect to the specific gravity range of water;
Described BB frost embedding capsule is BB frost embedding capsule-yellow 12, and described titanium white whitening capsule is titanium white whitening capsule-green 12, and the quality ratio range of described titanium white whitening capsule-green 12 and described BB frost embedding capsule-yellow 12 is 2:3-3:1;
Described BB frost embedding capsule-yellow 12 is the Magic50-BY12 that produced by KPT company of Korea S's (strain) (KPT Co., Ltd.); And
Titanium white whitening capsule-green 12 is the Magic30-WG12 that produced by KPT company of Korea S's (strain) (KPT Co., Ltd.).
2. BB frost as claimed in claim 1, is characterized in that, it is as follows that the component that the raw material of described gel substrate mainly comprises and this component account for the mass percent of raw material of described gel type BB frost:
Rheology control agent 0.2-0.8%
Chelating agen 0.05-0.1%
Nertralizer 0.2-0.8%
Antiseptic 0.1-0.3%
Solubilizing agent 0.1-0.4%
Deionized water surplus.
3. BB frost as claimed in claim 1, is characterized in that, the component that the raw material of described gel type BB frost also comprises is emollient, and the mass percent that described emollient accounts for the raw material of described gel type BB frost is 1.0-3.0%.
4. BB frost as claimed in claim 2, is characterized in that, the component that the raw material of described gel substrate also comprises is Derma-Guard, and the mass percent that described Derma-Guard accounts for the raw material of described gel type BB frost is 0.2-0.5%.
5. BB frost as claimed in claim 2, is characterized in that, the component that the raw material of described gel substrate also comprises is wetting agent, and the mass percent that described wetting agent accounts for the raw material of described gel type BB frost is 2.0-6.0%.
6. BB frost as claimed in claim 2, is characterized in that, the component that the raw material of described gel substrate also comprises is essence, and the mass percent that described essence accounts for the raw material of described gel type BB frost is 0.02-0.1%.
7. prepare the method for BB frost as claimed in claim 2 for one kind, it is characterized in that: under room temperature, described deionized water, described rheology control agent, described chelating agen, described dispersant are added in vacuum emulsifying pot successively, then homogenizing is uniformly dispersed raw material, stirs and is warming up to 80-85 ℃; Add described nertralizer to stir, insulation 20-25 minute; In 30-60 minute, be cooled to 40-45 ℃ and add described antiseptic, described solubilizing agent, stir; Be cooled to 38-40 ℃, then add described BB frost granule, stir and obtain described BB frost.
8. the method for preparing BB frost as claimed in claim 7, is characterized in that, also comprises the pretreatment process of described BB frost granule, and the pretreatment process of described BB frost granule is to soak described BB frost granule 2-4 hour with the deionized water of 20-40 ℃.
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| CN201110127193.3A CN102784068B (en) | 2011-05-17 | 2011-05-17 | BB cream and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101375830A (en) * | 2007-08-31 | 2009-03-04 | 天津天狮生物发展有限公司 | Aloe moisture-keeping nutrient skin-care cream and preparation method thereof |
| CN101773458A (en) * | 2009-01-12 | 2010-07-14 | 孙海 | Skin-refreshing jelly whitening and protective creamy foundation |
| CN101773460A (en) * | 2009-01-12 | 2010-07-14 | 孙海 | Transparent gel skin-care product |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101375830A (en) * | 2007-08-31 | 2009-03-04 | 天津天狮生物发展有限公司 | Aloe moisture-keeping nutrient skin-care cream and preparation method thereof |
| CN101773458A (en) * | 2009-01-12 | 2010-07-14 | 孙海 | Skin-refreshing jelly whitening and protective creamy foundation |
| CN101773460A (en) * | 2009-01-12 | 2010-07-14 | 孙海 | Transparent gel skin-care product |
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