CN112057354A - Blush and preparation method thereof - Google Patents

Blush and preparation method thereof Download PDF

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Publication number
CN112057354A
CN112057354A CN202010842731.6A CN202010842731A CN112057354A CN 112057354 A CN112057354 A CN 112057354A CN 202010842731 A CN202010842731 A CN 202010842731A CN 112057354 A CN112057354 A CN 112057354A
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blush
silica
mica
seed oil
stirring
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何晓志
骆妙如
骆承甫
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Shanghai Zhixin Biotechnology Co ltd
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Shanghai Zhixin Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25Silicon; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/466Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/85Polyesters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/08Preparations containing skin colorants, e.g. pigments for cheeks, e.g. rouge
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The invention discloses a blush and a preparation method thereof, which relate to the field of cosmetics, and the blush is prepared from the following raw materials in parts by weight: silicon elastomer, mica, silica, diisostearyl malate, di-diglycerol polyacyladipate-2, vegetable gel, oryzanol, polyhydroxystearic acid, phenoxyethanol, Spanish sage seed oil, and toner; the makeup cream has the advantages of smooth and fine touch feeling, light, thin and transparent makeup, good air permeability, lasting makeup effect, capability of moisturizing and brightening the skin, natural makeup surface and full skin health and luster; a blush preparation method comprises the steps of weighing raw materials, stirring a silicon elastomer, a plant gel, Spanish sage seed oil, oryzanol and phenoxyethanol, adding ground toner, diisostearyl malate, bis-diglycerol polyacyladipate-2 and polyhydroxystearic acid, stirring, adding mica and silica after stirring, continuously stirring, and then placing in a grinding tool for forming to obtain a finished product.

Description

Blush and preparation method thereof
Technical Field
The invention relates to the field of cosmetics, in particular to blush and a preparation method thereof.
Background
The blush is the best tool for modifying the face shape and beautifying the skin color, can add good complexion, increase the red and moist feeling of the face skin and produce the tender and transparent skin color.
The types of blush products on the market are mostly seen in dry powder, oil cream and emulsified blush; the dry powder blush is easy to be pulverized in the makeup process, and the pulverized powder is easy to be inhaled by the nasal cavity of a human body so as to influence the health of the human body; compared with dry powder blushers, the oil cream blushers have the advantage of no powder flying, but the oil cream blushers are greasy, are not refreshing enough on makeup, and have matte makeup surfaces and no normal gloss of skin; compared with the cream blush, the emulsified blush has the advantages of less greasy feeling and easy coating, but is not easy to make up uniformly.
Disclosure of Invention
Aiming at the defects in the prior art, the first purpose of the invention is to provide a blush which has the advantages of no powder flying, smooth and fine touch, light, thin and transparent makeup, good air permeability, lasting makeup effect, capability of moisturizing and brightening skin, uniform and natural makeup surface and skin health and luster.
A second object of the present invention is to provide a method for preparing a blush, which has advantages of simple operation and easy production.
In order to achieve the first object, the invention provides the following technical scheme: a blush is prepared from the following raw materials in parts by weight: 36-40 parts of silicon elastomer, 22-30 parts of mica, 8-12 parts of silica, 4-8 parts of diisostearyl malate, 22-3 parts of bis-diglycerol polyacyladipate, 3-5 parts of plant gel, 0.1-0.4 part of oryzanol, 0.3-0.8 part of polyhydroxystearic acid, 0.3-0.8 part of phenoxyethanol, 1-5 parts of salvia hispida seed oil and 8-10 parts of toner.
By adopting the technical scheme, the prepared blush is soft and smooth in touch, soft and glutinous in texture, light, thin and transparent in makeup and good in air permeability under the synergistic action of the silicon elastomer and the silica, and the viscosity of the blush can be reduced; under the synergistic effect of the mica and the silicon elastomer, the blush has transparent, glossy, fluffy and soft make-up feeling, and the glossiness of the skin can be stimulated; under the synergistic action of the silicon elastomer and the plant gel, the prepared blush has moderate viscosity and good moisturizing degree and moisturizing effect, so that the skin is not dry and unsmooth; under the synergistic effect of the plant gel, the Spanish sage and the oryzanol, the prepared blush has good effects of calming, relieving and resisting ultraviolet rays, and the glossiness of the skin can be enhanced on the premise of keeping the stability of the product; the synergistic effect of the plant gel, the silica and the oryzanol ensures that the nutrient components of the blush are absorbed, the water-oil balance of the skin is ensured, and the surface of the skin is moist, smooth, breathable and elastic; under the synergistic action of diisostearyl malate, bis-diglycerol polyacyladipate-2 and polyhydroxystearic acid, the dispersion agent can well disperse pigments, silica, mica and silicon elastomers, and can also be used as an emollient to ensure the water-oil balance of skin.
Silica and mica have porous structures, and the silicon elastomer, the mica and the silica are all hydrophilic and oleophobic types, and because the skin moistening components of the vegetable gel and the Spanish sage seed oil are lipid substances, the silicon elastomer can be positioned in the pore structure of the silica and the layer structure of the mica, and the silicon elastomer ensures that the blush makeup has the advantages of being light, thin and transparent, improving skin color and good in air permeability, and simultaneously prevents the silicon elastomer from blocking pores; under the synergistic effect of the silicon elastomer, the mica and the silica, the skin is promoted to absorb the skin moistening components of the plant gel and the Spanish sage seed oil, so that the phenomena of dry and astringent make-up and peeling of the skin are avoided; and the emollient components of the plant gel and the spanish sage seed oil contain partial moisture, so that the water-oil balance of the skin can be ensured under the synergistic action of the silicon elastomer, the plant gel and the spanish sage seed oil, and the skin is smooth and elastic.
Because the skin of a human body is always in a breathing state, when the skin produces oil, part of bacteria and dust can be easily adhered to the surface of the skin, and bacteria and microorganisms can easily enter the skin, so that the problems of acne growth, more cutin and more blackheads appear on the skin; make blush have antibiotic, anti-inflammatory effect under the synergistic effect of utilizing spanish sage and plant gel, the oil absorption performance of the silkiness degree of cooperation silicon elastomer and silica prevents that the bacterium from attaching to the skin top layer and kills the bacterium of attaching to the skin top layer, avoids the bacterium to breathe through the skin and gets into inside the skin to avoid the phenomenon of the skin to appear and to play pox, blackhead to take place, guarantee the frivolous sense and the air permeability of skin.
Further, the plant gel is composed of sunflower seed oil, safflower seed oil and a styrene-butadiene copolymer in a weight ratio of 2:2: 1.
By adopting the technical scheme, the sunflower seed oil, the safflower seed oil and the styrene-butadiene copolymer are prepared into the plant gel under the synergistic effect, the cohesive force of the product can be enhanced, and the plant oil and the skin moistening components which are easily absorbed by the skin in the sunflower seed oil and the safflower seed oil enable the skin to be moist, glossy and good in moisturizing effect.
The stratum corneum of the skin is a lipid bilayer and is hydrophobic in structure, so the surface layer of the skin is often easy to lack water; the synergistic effect of the sunflower seed oil, the Spanish sage seed oil and the silicon elastomer can quickly seal and lock the moisture of the skin and supply natural nutrient elements to the skin, and a certain water retention capacity required by a skin barrier is achieved, so that the skin is moist and glossy.
The blush has good oxidation resistance under the synergistic effect of the sunflower seed oil, the safflower seed oil, the spanish sage and the oryzanol, can promote the skin to retain water and control oil for a long time, repair the damaged skin surface layer, and avoid the phenomena that the skin is sensitive, easy to be stimulated and the immunity is reduced because the skin is rough and thin due to long-time water shortage.
Further, the silicon elastomer was composed of polydimethylsiloxane and polysiloxane-11 in a weight ratio of 1: 1.
By adopting the technical scheme, the silicon elastomer is an organosilicon elastic gel body formed by polymerizing polydimethylsiloxane and polysiloxane-11, and the organosilicon elastic gel body has the advantages of smoothness, fineness and non-stickiness.
The cake body of the blush is continuously pressed in the using process, so that powdery particles are gathered, the powdery particles are compacted, and the coloring effect is poor; by utilizing the synergistic effect of the organic silicon elastic gel, the mica and the silica, the blush has good elastic performance, and the powder is prevented from being compacted, so that the coloring effect of the blush after long-time use is ensured.
Further, the blush also comprises 1-3 parts of taurine.
By adopting the technical scheme, the blush can have stronger antioxidation under the synergistic action of the taurine and the sunflower seed oil, the taurine is sulfur-containing amino acid, the sunflower seed oil contains neutral amino acids such as glycine, proline and the like, the synergistic action of the taurine and the sunflower seed oil is a material basis for forming a poly-anion-group structure, the poly-anion is utilized to remove free radicals, so that the blush has the antioxidation function, and the prepared blush also has the function of repairing cheek injury muscles.
Furthermore, the mica is spherical powder, and the particle size of the mica is 40-45 microns.
By adopting the technical scheme, the particle size of the mica is limited to be 40-45 microns, the blush can be ensured to have transparent luster, good fluffy feeling and the performance of adsorbing the silicon elastomer to a large extent, the elasticity of the cake can be kept, and the phenomenon that the cake is not uniform in makeup after being compacted is avoided.
Further, the silica is spherical powder with a particle size of 8-12 μm.
By adopting the technical scheme, the blush can be smoother by limiting the spherical powder with the particle size of silica being 8-12 microns.
In order to achieve the second object, the invention provides the following technical scheme: a preparation method of blush comprises the following steps:
s1, weighing silicon elastomer, mica, silica, diisostearyl malate, di-diglycerol polyacyladipate-2, plant gel, oryzanol, polyhydroxystearic acid, phenoxyethanol, Spanish sage seed oil and toner according to the proportion;
s2, stirring the silicon elastomer, the plant gel, the Spanish sage seed oil, the oryzanol and the phenoxyethanol to obtain a mixture A;
s3, grinding the toner, diisostearyl malate, di-diglycerol polyacyl adipate-2 and polyhydroxystearic acid for 2-4 times to prepare color paste;
s4, placing the color paste prepared in the S3 into the mixture A prepared in the S2, and stirring uniformly until toner particles cannot be seen by naked eyes to prepare a mixture B;
s5, placing mica and silica into the mixture B prepared by the S4, stirring until dough is soft and glutinous, and preparing the pre-treated cake;
and S6, placing the pretreated cakes prepared in the S5 into a mould, and prepressing for forming to obtain a finished product.
By adopting the technical scheme, the silicon elastomer, the plant gel, the Spanish sage seed oil, the oryzanol and the phenoxyethanol are mixed and stirred to prepare the mixture A, so that the nutrient components can be uniformly distributed, and the blush is ensured to have the characteristics of smoothness and softness; then adding toner to endow the blush with unique color, and uniformly dispersing the toner in the mixture A by matching with diisostearyl malate, bis-diglycerol polyacyladipate-2 and polyhydroxystearic acid, so that the uniformity of the blush chroma is ensured conveniently; then adding mica and silica into the mixture B for stirring, ensuring that the blush has good permeability and air permeability and leading the blush to have good oxidation resistance; the operation process is simple and convenient, and the processing efficiency is higher.
Further, the stirring speed in S2 is 1500r/min, and the stirring time is 10-18 min.
By adopting the technical scheme, the silicon elastomer, the plant gel, the Spanish sage seed oil, the oryzanol and the phenoxyethanol are conveniently and efficiently mixed by limiting the stirring speed, so that the effective components can be uniformly dispersed in the mixture A, and the uniformity and the smoothness of the blush makeup are ensured.
Further, in S5, silica and mica were previously stirred at a stirring speed of 1500r/min for 15 seconds, then at a stirring speed of 800r/min for 10 seconds, and then at a stirring speed of 1500r/min for 15 seconds to prepare a powder, and then the powder was placed in the mixture B prepared in S4.
By adopting the technical scheme, as the particle sizes of the silica and the mica are larger and are not easy to be uniformly mixed, the mica and the silica are stirred in advance, so that the mica and the silica are uniformly mixed, and the glossiness, the smoothness and the fluffy feeling of the blush are ensured.
In conclusion, the invention has the following beneficial effects:
1. the prepared blush is soft and smooth in touch, soft and glutinous in texture, light, thin and transparent in makeup and good in air permeability by utilizing the synergistic effect of the silicon elastomer and the silica, and the viscosity of the blush can be reduced; under the synergistic effect of the mica and the silicon elastomer, the blush has transparent, glossy, fluffy and soft make-up feeling, and the glossiness of the skin can be stimulated; under the synergistic action of the silicon elastomer and the plant gel, the prepared blush has moderate viscosity and good moisturizing degree and moisturizing effect, so that the skin is not dry and unsmooth; under the synergistic effect of the plant gel, the Spanish sage and the oryzanol, the prepared blush has good effects of calming, relieving and resisting ultraviolet rays, and the glossiness of the skin can be enhanced on the premise of keeping the stability of the product; the synergistic effect of the plant gel, the silica and the oryzanol ensures that the nutrient components of the blush are absorbed, the water-oil balance of the skin is ensured, and the surface of the skin is moist, smooth, breathable and elastic; under the synergistic effect of the diisostearyl malate, the di-diglycerol polyacyladipate-2 and the polyhydroxystearic acid, the aqueous emulsion can well disperse pigments, silica, mica and silicon elastomers, and can also be used as an emollient to ensure the water-oil balance of skin;
2. the synergistic effect of the Spanish sage and the plant gel is utilized to enable the blush to have antibacterial and anti-inflammatory effects, and the silkiness of the silicon elastomer and the oil absorption performance of silica are matched to prevent bacteria from attaching to the surface layer of the skin and kill the bacteria attached to the surface layer of the skin, so that the bacteria are prevented from entering the interior of the skin through skin respiration, and the phenomena of acne and more blackheads of the skin are avoided;
3. the sunflower seed oil, the Spanish sage seed oil and the silicon elastomer can quickly seal and lock water for the skin and supply natural nutrient elements for the skin under the synergistic effect, and a certain water retention force required by a skin barrier is achieved, so that the skin is moist and glossy;
4. the self-repairing ability of damaged and sensitive skin can be promoted under the synergistic effect of the sunflower seed oil, the polydimethylsiloxane and the polysiloxane-11, and the skin lipid layer can be ensured to resist the stimulation of various substances and chemical substances in the external environment, so that the skin inflammation phenomenon is slowed down;
5. under the synergistic action of the organosilicon elastic gel, the mica and the silica, the blush has good elastic performance, and the cake body of the blush is prevented from being compacted, so that the blush is ensured to still have good coloring effect after being used for a long time;
6. under the synergistic action of taurine and sunflower seed oil, the blush has stronger antioxidation, the taurine is sulfur-containing amino acid, the sunflower seed oil contains neutral amino acid such as glycine, proline and the like, the synergistic action of the taurine and the sunflower seed oil is a material basis for forming a poly-anion-based structure, the poly-anion is utilized to remove free radicals, so that the blush has the antioxidation function, and the prepared blush also has the effect of repairing damaged muscles.
Detailed Description
The present invention will be described in further detail with reference to examples.
Examples
Example 1: a blush is prepared by the following method:
s1, weighing 38kg of silicon elastomer, 28kg of mica (selected from Nippon Shankou company), 10kg of silica (selected), 6kg of diisostearyl malate (selected from RYOO official flagship store), 4kg of plant gel, 0.25kg of oryzanol (selected from Zhejiang Dabiol science and technology Co., Ltd., gamma-oryzanol), 0.5kg of polyhydroxystearic acid (selected from Shantou Sono chemical technology Co., Ltd., model number NcenasiilUC-SPT), 0.5kg of phenoxyethanol (selected from Guangzhou Bairui International Inc.), 3kg of Spanish sage seed oil (selected from Shenzhen Bordete import and export Co., Ltd.), and 9kg of toner; the plant gel comprises sunflower seed oil (selected from Guangzhou Beri International trade company, Inc.), safflower seed oil (selected from Guangzhou Xinzhilian cosmetics, Inc.), and styrene-butadiene copolymer (selected from Kaixili plastics, Inc. of Dongguan city, No. 825) at a weight ratio of 2:2: 1; the silicone elastomer consisted of 1:1 by weight polydimethylsiloxane (from Glant, USA, type 530) and polysiloxane-11 (from Glant, USA); the mica is spherical powder with the grain diameter of 40-45 microns; the silica is spherical powder with the grain diameter of 8-12 microns; disperse red is selected as the toner;
s2, sequentially placing the silicon elastomer, the plant gel, the Spanish sage seed oil, the oryzanol and the phenoxyethanol into an oil phase pot (a Shijiazhuangyen Kuai mechanical equipment factory, model 190504) at normal temperature of 25 ℃, and stirring at a stirring speed of 1500r/min for 15min to prepare a mixture A;
s3, placing the toner, diisostearyl malate, di-diglycerol polyacyladipate-2 and polyhydroxystearic acid in a three-roll grinding machine (selecting Tabang mechanical equipment, Inc., Ri, China) to grind for 15min at a speed of 600r/min, wherein the grinding is the first grinding; then grinding for 10min at the speed of 800r/min, which is the second grinding; grinding at 1000r/min for 8min, which is the third grinding; preparing color paste;
s4, placing the color paste prepared in the S3 into the mixture A prepared in the S2, and stirring at the speed of 500r/min for 5min to prepare a mixture B;
s5, placing mica and silica into a stirring pot, stirring for 15S at a speed of 1500r/min, then stirring for 10S at a speed of 800r/min, and then stirring for 15S at a speed of 1500r/min to prepare powder;
s6, adding the powder prepared in the S5 and the mixture B prepared in the S4 into a dough mixer (the Shanghai Limai mechanical equipment Co., Ltd., model HF80 is selected) and mixing for 25min at the rotating speed of 100r/min to prepare soft waxy pretreated cakes;
and S7, placing the pretreated cakes prepared in the S6 into a mould, and prepressing for forming to obtain a finished product.
Example 2
S1, weighing 36kg of silicon elastomer, 22kg of mica, 8kg of silica, 4kg of diisostearyl malate, 22kg of diglycerol polyacyladipate, 3kg of plant gel, 0.1kg of oryzanol, 0.3kg of polyhydroxystearic acid, 0.3kg of phenoxyethanol, 1kg of salvia Spanish seed oil and 8kg of toner; the plant gel consists of sunflower seed oil, safflower seed oil and styrene-butadiene copolymer in a weight ratio of 2:2: 1; the silicon elastomer consists of polydimethylsiloxane and polysiloxane-11 in a weight ratio of 1: 1; the mica is spherical powder with the grain diameter of 40-45 microns; the silica is spherical powder with the grain diameter of 8-12 microns; disperse red is selected as the toner;
s2, sequentially placing the silicon elastomer, the plant gel, the Spanish sage seed oil, the oryzanol and the phenoxyethanol in an oil phase pot at normal temperature of 25 ℃, and stirring at a stirring speed of 1500r/min for 10min to prepare a mixture A;
s3, grinding the toner, diisostearyl malate, di-diglycerol polyacyladipate-2 and polyhydroxystearic acid in a three-roll grinder at a speed of 600r/min for 15min, wherein the grinding is the first grinding; then grinding for 10min at the speed of 800r/min, which is the second grinding; preparing color paste;
s4, placing the color paste prepared in the S3 into the mixture A prepared in the S2, and stirring at the speed of 500r/min for 5min to prepare a mixture B;
s5, placing mica and silica into a stirring pot, stirring for 15S at a speed of 1500r/min, then stirring for 10S at a speed of 800r/min, and then stirring for 15S at a speed of 1500r/min to prepare powder;
s6, adding the powder prepared in the step S5 and the mixture B prepared in the step S4 into a dough mixer, and mixing for 25min at the rotating speed of 100r/min to prepare soft waxy pretreated cakes;
and S7, placing the pretreated cakes prepared in the S6 into a mould, and prepressing for forming to obtain a finished product.
Example 3
S1, weighing 40kg of silicon elastomer, 30kg of mica, 12kg of silica, 8kg of diisostearyl malate, 23kg of diglycerol polyacyladipate, 5kg of plant gel, 0.4kg of oryzanol, 0.8kg of polyhydroxystearic acid, 0.8kg of phenoxyethanol, 5kg of Spanish sage seed oil and 10kg of toner; the plant gel consists of sunflower seed oil, safflower seed oil and styrene-butadiene copolymer in a weight ratio of 2:2: 1; the silicon elastomer consists of polydimethylsiloxane and polysiloxane-11 in a weight ratio of 1: 1; the mica is spherical powder with the grain diameter of 40-45 microns; the silica is spherical powder with the grain diameter of 8-12 microns; disperse red is selected as the toner;
s2, sequentially placing the silicon elastomer, the plant gel, the Spanish sage seed oil, the oryzanol and the phenoxyethanol in an oil phase pot at normal temperature of 25 ℃, and stirring at a stirring speed of 1500r/min for 18min to prepare a mixture A;
s3, placing the toner, diisostearyl malate, di-diglycerol polyacyladipate-2 and polyhydroxystearic acid into a three-roll grinding machine, grinding for 15min at the speed of 600r/min, then grinding for 10min at the speed of 800r/min, then grinding for 8min at the speed of 1000r/min, and finally grinding for 5min at the speed of 1100r/min to obtain the color paste;
s4, placing the color paste prepared in the S3 into the mixture A prepared in the S2, and stirring at the speed of 500r/min for 5min to prepare a mixture B;
s5, placing mica and silica into a stirring pot, stirring for 15S at a speed of 1500r/min, then stirring for 10S at a speed of 800r/min, and then stirring for 15S at a speed of 1500r/min to prepare powder;
s6, adding the powder prepared in the step S5 and the mixture B prepared in the step S4 into a dough mixer, and mixing for 25min at the rotating speed of 100r/min to prepare soft waxy pretreated cakes;
and S7, placing the pretreated cakes prepared in the S6 into a mould, and prepressing for forming to obtain a finished product.
Example 4: the present embodiment is different from embodiment 1 in that:
s1, adding 2kg of taurine into the raw materials;
s2, sequentially placing the silicon elastomer, the plant gel, the Spanish sage seed oil, the taurine, the oryzanol and the phenoxyethanol in an oil phase pot at normal temperature of 25 ℃, and stirring for 15min at a stirring speed of 1500r/min to obtain a mixture A.
Example 5: the present embodiment is different from embodiment 1 in that:
s1, adding 1kg of taurine into the raw materials;
s2, sequentially placing the silicon elastomer, the plant gel, the Spanish sage seed oil, the taurine, the oryzanol and the phenoxyethanol in an oil phase pot at normal temperature of 25 ℃, and stirring for 15min at a stirring speed of 1500r/min to obtain a mixture A.
Example 6: the present embodiment is different from embodiment 1 in that:
s1, adding 3kg of taurine in the raw materials;
s2, sequentially placing the silicon elastomer, the plant gel, the Spanish sage seed oil, the taurine, the oryzanol and the phenoxyethanol in an oil phase pot at normal temperature of 25 ℃, and stirring for 15min at a stirring speed of 1500r/min to obtain a mixture A.
Note: the toner includes dispersed red but is not limited to dispersed red.
Comparative example
Comparative example 1: this comparative example differs from example 4 in that no silicon elastomer and no silica were added to the raw materials.
Comparative example 2: this comparative example differs from example 4 in that no silicon elastomer and no mica were added to the raw materials.
Comparative example 3: this comparative example differs from example 4 in that no silicon elastomer, silica and mica were added to the raw materials.
Comparative example 4: this comparative example is different from example 4 in that no silicone elastomer or vegetable gel was added to the raw materials.
Comparative example 5: this comparative example differs from example 4 in that no vegetable gel, spanish sage, was added to the raw material.
Comparative example 6: this comparative example differs from example 4 in that no plant gel, spanish sage and oryzanol were added to the raw materials.
Comparative example 7: this comparative example differs from example 4 in that no plant gel, silica and oryzanol were added to the raw materials.
Comparative example 8: this comparative example differs from example 4 in that sunflower, spanish sage and silicone elastomer were not added to the feed.
Comparative example 9: this comparative example differs from example 4 in that taurine and sunflower oil were not added to the raw materials.
Comparative example 10: this comparative example differs from example 4 in that the mica and silica were added directly to mix B without mixing and stirring.
Performance test
1. DHHP method for detecting oxidation resistance of blush
Preparation of DPPH solution: weighing DPPH3.5mg, dissolving with absolute ethyl alcohol, transferring into a volumetric flask quantitatively, fixing the volume to a scale with the absolute ethyl alcohol, placing 2ml in a 100ml volumetric flask, shaking up to obtain DPPH solution with the concentration of 0.0178mmol/L, and placing in a refrigerator for storage.
Preparation of blush test solution: 5.5mg of blush samples prepared in examples 1-6 and comparative examples 1-10 were weighed, dissolved in absolute ethanol, and quantitatively transferred to a 50ml volumetric flask, quantified to the scale with absolute ethanol, 15ml of the quantified blush sample was placed in a 100ml volumetric flask, and shaken up.
Determination of DPPH radical scavenging Rate: adding 4.0ml of DPPH solution and 5ml of blush test solution into a 10ml colorimetric tube in sequence, adding absolute ethyl alcohol to scale, immediately mixing, measuring a light absorption value (A) at a wavelength of 517nm by using a 1cm cuvette, wherein the light absorption value is Ai, storing at room temperature in a dark place for 30min, and measuring the light absorption value to obtain Aj, and the light absorption value is marked as Ac by using an ethanol solution only added with DPPH in a contrast test.
The formula for calculating the free radical clearance is as follows:
K(%)=[1-(Ai-Aj)/Ac]×100%
the experiment was repeated three times and the data averaged.
2. Cheek red cake coloring effect test
160 female volunteers aged 20-30 were searched, 160 volunteers were divided into 16 groups, and 16 groups of volunteers used the blushers prepared in examples 1-6 and comparative examples 1-10, respectively, and the coloring effect of the blushers was scored at 15 days, 30 days, and 45 days of use of the blushers, respectively, according to the following scoring criteria: the coloring effect is good, and the blush cake body does not have the phenomenon of agglomeration for 7-10 minutes; the coloring effect is general, and the blush cake body has the caking tendency of 4-7 minutes; the coloring effect is poor, and the blush cake body is caked for 0-4 minutes.
TABLE 1 blush free radical scavenging rate and blush coloring effect testing table
Figure BDA0002642027800000091
3. Blush make-up performance measurement
160 female volunteers aged 20-30 were searched, 160 volunteers were divided into 16 groups, and 16 groups of volunteers used the blushers prepared in examples 1-6 and comparative examples 1-10, respectively, and scored for the texture, uniformity, breathability, extensibility, skin gloss, makeup retention, and makeup naturalness of the blushers at 8 hours after use, respectively.
The scoring criteria for each item of content were: 5 min-very good; 4 min-better; 3 min-general; 2 min-poor; 1 min-very poor.
Table 2 blush make-up performance test table
Figure BDA0002642027800000092
Figure BDA0002642027800000101
According to the data in tables 1 and 2, the radical scavenging rates of examples 1-3 are reduced compared to examples 4-6 by comparing examples 1-3 with comparative examples 4-6, which shows that the combination of taurine and sunflower seed oil can provide a blush having a good antioxidant ability.
By comparing examples 4-6 with comparative examples 1-10, the raw material of comparative example 1 is not added with silicon elastomer and silica, and compared with example 4, the radical clearance of comparative example 1 is reduced compared with that of example 4, which shows that the combination of silicon elastomer and silica can make blush have good oxidation resistance; the blush coloring effect of comparative example 1 is lower than that of example 4, indicating that the combination of the silicon elastomer and silica can impart a certain degree of elasticity to the blush, ensuring that the blush still has a good elastic function after being used for a long time, and not affecting the blush coloring effect due to the bonding condition of the blush cake; the texture, uniformity, air permeability, extensibility, color satisfaction, makeup retention, and naturalness of comparative example 1 were all reduced from those of example 4, where the greater variation in uniformity, air permeability, makeup retention, and naturalness indicates that the combination of the silicon elastomer and silica makes the prepared blush soft and sticky to the touch when made up, the makeup is light, thin, and transparent, the air permeability is good, and the stickiness of the blush can be reduced.
The raw material of the comparative example 2 is not added with the silicon elastomer and the mica, compared with the example 4, the free radical clearance rate of the comparative example 2 is reduced compared with that of the example 4, which shows that the combination of the silicon elastomer and the mica can ensure that the blush has the oxidation resistance; the coloring effect of the blush of comparative example 2 is reduced compared with that of example 4, which shows that the combination of the silicon elastomer and the mica can endow the blush with a certain degree of elasticity, ensure that the blush still has a good elastic function after being used for a long time, and cannot influence the coloring effect of the blush due to the bonding condition of the blush cake body; the texture, uniformity, air permeability, extensibility, color satisfaction, makeup duration, and naturalness of comparative example 2 were all reduced compared to example 4, where the uniformity, air permeability, makeup duration, and naturalness were greatly varied, indicating that the combination of the silicone elastomer and mica provides a transparent, glossy, fluffy, and soft makeup feeling to the blush and can stimulate the glossiness of the skin itself.
The raw material of the comparative example 3 is not added with the silicon elastomer, the mica and the silica, compared with the example 4, the free radical clearance rate of the comparative example 3 is reduced compared with that of the example 4, which shows that the combination of the silicon elastomer, the mica and the silica can ensure that the blush has the anti-oxidation performance; comparative example 3 the coloring effect of the blush was reduced compared to example 4, which shows that the combination of the silicon elastomer, mica and silica can give a certain degree of elasticity to the blush, ensuring that the blush still has a good elastic function after long-term use, and the coloring effect of the blush is not affected by the bonding condition of the blush cake; the texture, uniformity, air permeability, extensibility, color satisfaction, makeup-holding degree, and naturalness of comparative example 3 were all reduced compared to example 4, indicating that the combination of the silicon elastomer and mica makes the blush have a makeup feeling of good texture, light and thin makeup, good air permeability, moist and glossy face, fluffy, and soft, and can stimulate the skin's own glossiness.
The raw materials of the comparative example 4 are not added with the silicon elastomer and the vegetable gel, compared with the example 4, the free radical clearance rate of the comparative example 4 is reduced compared with that of the example 4, and the matching of the silicon elastomer and the vegetable gel can ensure that the blush has good oxidation resistance; comparative example 4 the coloring effect of the blush was reduced compared to example 4, which shows that the combination of the silicon elastomer and the plant gel can impart a certain degree of elasticity to the blush, ensuring that the blush still has a good elastic function after long-term use; the texture, uniformity, air permeability, extensibility, color satisfaction, make-up retention and naturalness of comparative example 4 were all reduced from those of example 4, with greater variations in uniformity, air permeability, make-up retention and naturalness, indicating that the combination of silicone elastomer and vegetable gel resulted in a blush with moderate viscosity, good moisture retention and moisturizing effect, and thus no dry and uneven skin.
Comparative example 5 without addition of the vegetable gel, spanish sage, the radical scavenging rate of comparative example 5 was reduced compared to that of example 4, indicating that the combination of spanish sage and vegetable gel can provide blush with good antioxidant properties; comparative example 5 the coloring effect of the blush was reduced compared to example 4, indicating that the combination of spanish sage and vegetable gel had an effect on the elasticity of the blush cake; the texture, uniformity, air permeability, extensibility, color satisfaction, make-up retention, and naturalness of comparative example 5 were all reduced from those of example 4, where the uniformity, air permeability, and skin gloss were greatly varied, indicating that the combination of spanish sage and vegetable gel provided a good moisturizing effect on the prepared blush, stimulating the naturalness of the skin.
Comparative example 6 the raw materials were not added with vegetable gel, spanish sage and oryzanol, and compared with example 4, the radical scavenging rate of comparative example 6 was greatly reduced compared with that of example 4, indicating that the combination of the silicone elastomer and the vegetable gel can make blush have good antioxidant property; comparative example 6 the coloring effect of blush was reduced compared to example 4, indicating that the combination of vegetable gel, spanish sage and oryzanol has an effect on the elasticity of the blush cake; the texture, evenness, breathability, extensibility, color satisfaction, make-up retention, and naturalness of comparative example 6 were all reduced from those of example 4, with greater variations in evenness, breathability, and naturalness, indicating that the combination of the plant gel, spanish sage, and oryzanol provides a good skin moisturizing effect to the blush and ensures water and oil balance to the skin.
Comparative example 7 the raw material was not added with vegetable gel, silica and oryzanol, and the radical scavenging rate of comparative example 7 was reduced compared to that of example 4, compared to example 4, indicating that the combination of the silicone elastomer and the vegetable gel can provide a blush with good antioxidant properties; comparative example 7 the coloring effect of the blush was reduced compared to example 4, indicating that the combination of the plant gel, silica and oryzanol has an effect on the elasticity of the blush; the texture, uniformity, breathability, extensibility, color satisfaction, make-up retention, and naturalness of comparative example 7 were all reduced from those of example 4, where the texture, uniformity, breathability, and extensibility were varied significantly, indicating that the combination of the plant gel, silica, and oryzanol absorbed the nutrients of blush, ensured the moisture-oil balance of skin, and made the skin surface moist, smooth, breathable, and elastic.
Comparative example 8 the raw materials without sunflower seed oil, spanish sage and silicone elastomer, compared to example 4, the radical scavenging rate of comparative example 8 is reduced compared to that of example 4, indicating that the combination of silicone elastomer and vegetable gel can make blush have good antioxidant properties; comparative example 8 the color effect of blush was reduced compared to example 4, indicating that the combination of sunflower seed oil, spanish sage and silicon elastomer had some effect on the elasticity of the blush cake; the texture, uniformity, breathability, extensibility, color satisfaction, make-up retention, and naturalness of comparative example 8 were all reduced from those of example 4, where the greater variation in uniformity, breathability, extensibility, and naturalness, and the synergistic effect of silicone elastomer, phytogel, and chia oil, ensured a water-oil balance of the skin, and thus, the skin was smooth and elastic.
Compared with example 4, the radical scavenging rate of the comparative example 9 is greatly reduced compared with that of example 4, which indicates that the blush has good oxidation resistance due to the matching of the taurine and the sunflower seed oil; comparative example 9 the coloring effect of blush was reduced compared to example 4, indicating that the combination of taurine and sunflower seed oil has an effect on the elasticity of the blush cake; the texture, uniformity, breathability, extensibility, color satisfaction, make-up retention, and naturalness of comparative example 9 were all reduced compared to example 4, indicating that the combination of taurine and sunflower seed oil has an effect on the texture, uniformity, breathability, extensibility, color satisfaction, make-up retention, and naturalness of blush.
Comparative example 10 no pre-agitation of silica and mica, and the radical clearance of comparative example 10 changed less than that of example 4 compared to example 4, indicating that the uniformity of the silica and mica distribution had an effect on the oxidation resistance; the texture, evenness, breathability, extensibility, color satisfaction, make-up retention, and naturalness of comparative example 10 were all reduced from those of example 4, indicating that the uniformly distributed mica and silica enable the emollient ingredients of plant gel and spanish sage to be more effectively absorbed by the skin, and the silicone elastomer to be more uniformly distributed in the pore structure of silica and mica, ensuring the naturalness, breathability, smooth texture, and stimulating the skin's own gloss of the blush make-up.
The present embodiment is only for explaining the present invention, and it is not limited to the present invention, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present invention.

Claims (9)

1. The blush is characterized by being prepared from the following raw materials in parts by weight: 36-40 parts of silicon elastomer, 22-30 parts of mica, 8-12 parts of silica, 4-8 parts of diisostearyl malate, 22-3 parts of bis-diglycerol polyacyladipate, 3-5 parts of plant gel, 0.1-0.4 part of oryzanol, 0.3-0.8 part of polyhydroxystearic acid, 0.3-0.8 part of phenoxyethanol, 1-5 parts of salvia hispida seed oil and 8-10 parts of toner.
2. The blush as claimed in claim 1, wherein said plant gel is composed of sunflower seed oil, safflower seed oil, styrene-butadiene copolymer in a weight ratio of 2:2: 1.
3. The blush as claimed in claim 1 wherein the silicone elastomer is comprised of polydimethylsiloxane and polysiloxane-11 in a weight ratio of 1: 1.
4. The blush as claimed in claim 1, wherein said blush further comprises 1-3 parts taurine.
5. The blush as claimed in claim 1, wherein said mica is a spherical powder with a particle size of 40-45 μm.
6. The blush as claimed in claim 1 wherein said silica is spherical powder having a particle size of 8-12 microns.
7. A method of preparing a blush as claimed in claim 1, comprising the steps of:
s1, weighing silicon elastomer, mica, silica, diisostearyl malate, di-diglycerol polyacyladipate-2, plant gel, oryzanol, polyhydroxystearic acid, phenoxyethanol, Spanish sage seed oil and toner according to the proportion;
s2, stirring the silicon elastomer, the plant gel, the Spanish sage seed oil, the oryzanol and the phenoxyethanol to obtain a mixture A;
s3, grinding the toner, diisostearyl malate, di-diglycerol polyacyl adipate-2 and polyhydroxystearic acid for 2-4 times to prepare color paste;
s4, placing the color paste prepared in the S3 into the mixture A prepared in the S2, and stirring uniformly until toner particles cannot be seen by naked eyes to prepare a mixture B;
s5, placing mica and silica into the mixture B prepared by the S4, stirring until dough is soft and glutinous, and preparing the pre-treated cake;
and S6, placing the pretreated cakes prepared in the S5 into a mould, and prepressing for forming to obtain a finished product.
8. The method of preparing a blush as set forth in claim 7, wherein the stirring speed in S2 is 1500r/min and the stirring time is 10-18 min.
9. The method of preparing a blush as claimed in claim 7, wherein the silica and mica are previously stirred at 1500r/min for 15S in S5, and then at 800r/min for 10S, and then at 1500r/min for 15S to obtain powder, and then the powder is put into the mixture B prepared in S4.
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Application publication date: 20201211