CN108852959B - Preparation method of natural multi-effect lip mask - Google Patents
Preparation method of natural multi-effect lip mask Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
Abstract
The invention discloses a preparation method of a natural multi-effect lip film, which comprises the following steps: (1) mixing two oily substances including olive oil and grape seed oil to obtain an oil phase, mixing glycerol and water to obtain a water phase, mixing pectin as an emulsifier, heating to 70-80 deg.C, stirring, shearing at high speed, and homogenizing under high pressure to obtain a uniform and stable oil-in-water emulsion; (2) preparing a vitamin E microcapsule by taking chitosan and maltodextrin as wall materials through spray drying; (3) mixing the emulsion obtained in the step (1) with vitamin E microcapsules, glycolic acid, honey and chitosan, and uniformly stirring; (4) preparing a frosting agent; (5) fully mixing and stirring the product obtained in the step (3) and the abrasive agent uniformly; (6) sterilizing; (7) cooling and subpackaging to obtain the lip film product. The lip mask prepared by the invention has good moisturizing and moistening properties, oxidation resistance, antibacterial property and exfoliating effect.
Description
(I) technical field
The invention belongs to the field of daily chemical products, and particularly relates to a preparation method of a natural multi-effect lip mask.
(II) technical background
The lip mask is a novel lip care product, and is used for moistening and softening, removing old waste cutin, fading pigmentation of lips and providing nutrition and gloss for lips. Without removing the dead skin cutin, the nutrition cannot be absorbed, and thus the nutrition cannot be nourished to the lip skin. And old waste cutin makes skin rough, unsmooth, dark and dim, and influences the beauty. The common lip mask does not add keratolytic ingredients, and the abrasive is directly used to forcibly remove aged cutin, so that the removal is not thorough and has large damage to lip mucosa, and lips cannot be well protected.
A mature lip film not only has the care problem of lips, but also has the smearing effect and the sanitary safety problem. The traditional lip mask has simple process and single effect, and the raw materials are ground into powder and mixed with water into paste to be applied to lips. The effective components in the raw materials cannot be well utilized by simply grinding the raw materials into powder, and the raw materials are not fresh and comfortable enough and are easy to crack. The lip skin is tender and fragile, is easy to be damaged, pigments are easy to deposit, the problem of lip color cannot be fundamentally solved because the problem of pigment deposition is not considered in the traditional lip film, and a part of products use single antioxidants, cannot play a good role in resisting oxidation and improve the lip color and the fine lines of the lips. In addition, many lip film products use many chemically synthesized substances in order to obtain their desired effects, which may cause irritation of the skin of the lips, allergy, etc.
Patent CN107569406A discloses a lip film and a preparation method thereof, and the technical scheme is that the lip film is prepared and comprises the following components: petrolatum, beeswax, synthetic wax, polyisobutylene, polyethylene, ethylhexyl palmitate, phenoxyethanol, piroctone olamine. The patent has the functions of moistening and removing aged cutin, but the use of chemical components can stimulate the skin and cause certain harm. Patent CN106880575A discloses a method for making a frosted lip film, which comprises the steps of making frosted particles, dissolving functional components, mixing, sterilizing, subpackaging and cooling to obtain the frosted lip film. This patent is got rid of the cutin through the physical action of abrasive, can only get rid of skin top layer dead skin, can't go deep into the clearance, directly uses abrasive moreover and easily causes lip skin impaired.
Disclosure of the invention
The technical problem to be solved by the invention is to provide a preparation method of a natural multi-effect lip mask, and the lip mask has good moisturizing and moistening properties, oxidation resistance, antibacterial property and exfoliating effect.
In order to solve the technical problems, the invention adopts the following technical scheme:
the invention provides a preparation method of a natural multi-effect lip film, which comprises the following steps:
(1) preparing an emulsion: mixing olive oil and grape seed oil at a mass ratio of 3-5:1.5-2.5, heating to 80-90 deg.C, and stirring to obtain oil phase; mixing glycerol and water to obtain water phase, using pectin as emulsifier, mixing oil phase, water phase and emulsifier, heating to 70-80 deg.C, stirring, high-speed shearing, and high-pressure homogenizing to obtain uniform and stable oil-in-water emulsion; wherein, the mass percentages of the glycerin, the water and the emulsifier are respectively 15-25%, 30-40% and 5-10% and the balance is oil phase, wherein the total mass of the fed materials of the components is 100%;
(2) preparing a vitamin E microcapsule by taking chitosan and maltodextrin as wall materials through spray drying: mixing vitamin E and an emulsifier, wherein the emulsifier is lecithin and gelatin in a mass ratio of 4:2, shearing and stirring at a high speed to obtain a core material solution, adding a chitosan solution into the core material solution while stirring, adding a maltodextrin solution, shearing at a high speed, homogenizing at a high pressure to obtain a microcapsule emulsion, and spray-drying to obtain a vitamin E microcapsule; the total mass of the emulsifier, the chitosan, the maltodextrin and the vitamin E is 100 percent, and the mass percentage of each component is as follows: 3-5% of chitosan, 60-70% of maltodextrin, 15-20% of vitamin E and 5-15% of emulsifier;
(3) mixing materials: controlling the temperature to be 55-65 ℃, mixing the emulsion obtained in the step (1) with vitamin E microcapsules, glycolic acid, honey and chitosan, wherein the mass ratio of the vitamin E microcapsules, the glycolic acid, the honey and the chitosan is 1-2:0.3-0.6:2-3:3-4, the amount of the emulsion accounts for 80-95% of the total mass of the materials, and uniformly stirring;
(4) preparing a frosting agent: the method comprises the following steps of (1) adopting natural frosted particles, wherein the natural frosted particles are one or a combination of any more of walnut powder, oat powder, olive kernel powder, apricot kernel powder and cherry kernel powder in any proportion, and crushing the frosted particles into uniform particles of 150-350 microns by using a micron crusher to obtain the frosting agent;
(5) mixing materials: fully mixing the product obtained in the step (3) with the abrasive agent obtained in the step (4) to ensure that the mass fraction of the abrasive agent in the mixture is between 3 and 5 percent, and uniformly stirring;
(6) sterilizing the mixture obtained in the step (5) at the temperature of 60-70 ℃;
(7) cooling (preferably to 30 deg.C) the sterilized product, and packaging to obtain lip film product.
Further, in the step (1), the high-speed shearing conditions are as follows: shearing for 2-3min by using a high-speed shearing machine with 26000-30000 rpm; the high-pressure homogenizing conditions are as follows: and circularly homogenizing for 5-6 times under 70-80 MPa by using a high-pressure homogenizer to obtain the uniform and stable oil-in-water emulsion.
Further, in the step (2), the high-speed shearing conditions are as follows: 13000r/min-15000r/min, 2-4 min; the high-pressure homogenizing conditions are as follows: 40-60 Mpa for 3-5 times; the spray drying conditions were: the air inlet temperature of spray drying is 170-190 ℃, and the air outlet temperature is 80-90 ℃.
Further, in the step (6), the temperature is controlled to be 60-70 ℃ and kept for 0.5-1 hour, and most of microorganisms can be killed.
In the invention, in order to obtain better lip protecting effect of the lip mask, the moisturizing and moistening performance of the lip mask is increased by increasing the using amount of the emulsion, the oxidation resistance of the lip mask is increased by increasing the using amount of the grape seed oil and the vitamin E, and the antibacterial property of the lip mask is increased by increasing the using amount of the chitosan. Therefore, in the step (1), the oil phase is preferably 30-35%, wherein the optimal ratio of the olive oil to the grape seed oil is 3-4: 2-2.5. In the step (3), the mixing mass ratio of the vitamin E microcapsules, the glycolic acid, the honey and the chitosan is preferably 1.5-2:0.3-0.5:2.5-3:3.5-4, and the dosage of the emulsion is preferably 90-95%. The advantages and the beneficial effects of the invention are as follows:
(1) according to the invention, the oil-in-water emulsion is added, and active substances such as vitamin E microcapsules, honey, chitosan and the like are added, so that better moistening, moisturizing, antioxidant and antibacterial effects are achieved, and lips are comprehensively maintained.
Specifically, ordinary lips have a single effect, and lips cannot be maintained in all aspects. The scheme takes olive oil and grape seed oil as base oil, and the oil-in-water emulsion is prepared by using a natural emulsifier by using a method for preparing the emulsion. The water can be supplemented, and the absorption of fat-soluble substances can be enhanced, so that the lip skin can be deeply nourished. After the lip mask is smeared by the oil-in-water system, the skin of the lips is more moist and glossy, is not greasy and is not easy to crack.
The olive oil is rich in squalene with excellent affinity with skin and essential fatty acid of human body, and has the advantages of rapid absorption, good moistening property, and effective maintenance of skin elasticity and moistening. Linoleic acid in grape seeds is a fatty acid which is necessary for human bodies and cannot be synthesized by the human bodies, and can resist free radicals, resist aging, prevent melanin from precipitating and help to absorb vitamin C and E. The vitamin E is insoluble in water and easy to oxidize, and the vitamin E microcapsule is prepared by microcapsule embedding technology and added, so that the vitamin E microcapsule is more stable in a system, the bioactivity utilization rate of the vitamin E is obviously improved, and the skin state is improved. Meanwhile, the vitamin E can continuously act on the lip skin due to the slow release effect of the microcapsule. The grape seed oil helps to absorb vitamin E, and can prolong and enhance antioxidant effect. Chitosan acts on thallus cells from the outside, and positively charged amino exists in the molecular structure, so that the chitosan is easy to adsorb with negatively charged thallus and can also enter the thallus, and the chitosan is combined with components such as protein and the like necessary for the survival of bacteria to destroy the metabolic balance of the bacteria, thereby generating the bacteriostatic effect.
(2) The polishing agent and the fruit acid are used together, so that the skin can be deeply cleaned, aged cutin can be effectively removed, lips can be protected, and the skin of the lips is smooth and tender.
Specifically, the frosting agent adopts natural frosted particles, such as walnut powder, oat powder, olive kernel powder, apricot kernel powder, cherry kernel powder and the like, a micron pulverizer is used for pulverizing the frosted particles into uniform particles of 150-350 microns, and the particles are pulverized and classified simultaneously through mechanical pulverization and airflow screening, so that the uniform and proper particle size of the frosted particles is ensured, pain is caused by excessive friction of the particles, and the over-small cutin removal effect of the particles is not obviously improved. The abrasive removes cutin by physical action, acts on the outermost layer of skin, and the abrasive particles continuously rub with lips to cut off the connection between the tilted skin and the cutin, thereby achieving the purpose of removing cutin. When getting rid of the cutin, dull polish particle is constantly slided at the lip, increases the friction comfort, promotes lip blood circulation, is favorable to the metabolism.
The natural active ingredients such as fruit acid are added, the fruit acid removes cutin through chemical action, the fruit acid can destroy the connection between cuticle cells, the adhesion between cornelian cells is weakened through the interference of iron atoms on the surface of the cells, the adhesion of cuticle is weakened, and dead skin accumulated on the skin is removed. The high-concentration tartaric acid has quite strong permeability and can peel off aged cutin at one time, but lip skin is tender, and the high-concentration tartaric acid causes strong irritation to the skin and possibly damages to the skin. In order to solve the problem, the low-concentration glycolic acid is matched with the abrasive agent for use, no stimulation is caused to the skin, and the glycolic acid has the smallest chemical structure in the fruit acid and only has two carbon atoms; the lowest molecular weight is only 76.05, so the surface layer of the skin is easy to permeate, the absorption effect is most obvious, the low-concentration glycolic acid can reduce the coagulation force among epidermal corneocytes, soften old and waste corneas of the skin, destroy the connection among the corneocytes, generate easy-to-fall corneous crumbs, and the exfoliative crusts can be effectively removed by slight friction of the abrasive. Meanwhile, the lip polishing liquid avoids the damage of a single polishing agent to the lips, protects the two lips and enables the skin of the lips to be smooth and tender.
(IV) description of the drawings
FIG. 1 is a flow chart of a conventional lip film production process;
FIG. 2 is a flow chart of the lip film production process of the present invention.
(V) detailed description of the preferred embodiment
The invention will be further described with reference to specific examples, but the scope of the invention is not limited thereto:
example 1:
(1) preparing an emulsion: mixing 18.5g of olive oil and 11.5g of grape seed oil according to the mass ratio of 4:2.5, heating to 85 ℃, and uniformly stirring to obtain an oil phase. Mixing 25g of glycerol and 40g of water to obtain a water phase, mixing 5g of pectin to obtain an emulsifier, heating the oil phase, the water phase and the emulsifier to 80 ℃, uniformly stirring, shearing for 2min by using a high-speed shearing machine with the speed of 26000rpm, and circularly homogenizing for 5 times by using a high-pressure homogenizer under the pressure of 70MPa to obtain a uniform and stable oil-in-water emulsion;
(2) preparing vitamin E microcapsules: preparing a vitamin E microcapsule by taking chitosan and maltodextrin as wall materials through spray drying, wherein lecithin and gelatin are used as an emulsifier in a mass ratio of 4:2, and the chitosan: maltodextrin, 2: vitamin E: emulsifier 3%: 70%: 15%: 12 percent. Mixing 1.5g of vitamin E, 0.8g of lecithin and 0.4g of gelatin, carrying out high-speed shearing and stirring (13000r/min, 3min) to obtain a core material solution, adding 3g of chitosan solution with the mass concentration of 10% into the core material solution while stirring, adding 10g of maltodextrin solution with the mass concentration of 70%, carrying out high-speed shearing and stirring (13000r/min, 3min), carrying out high-pressure homogenization to obtain a microcapsule emulsion (40Mpa, 3 times, 30min), finally carrying out spray drying, wherein the air inlet temperature of the spray drying is 180 ℃, and the air outlet temperature is 80 ℃ to obtain a vitamin E microcapsule;
(3) mixing materials: cooling to 55 ℃, mixing 90g of the emulsion obtained in the step (1) with 1.1g of vitamin E microcapsule, 0.4g of glycolic acid, 2.2g of honey and 3.3g of chitosan, wherein the mixing mass ratio of the vitamin E microcapsule, the glycolic acid, the honey and the chitosan is 1:0.33:2:3, the dosage of the emulsion accounts for 92.8 percent of the total mass of the materials, and uniformly stirring;
(4) preparing a frosting agent: adopting natural frosted particles selected from any combination of walnut powder, oat powder and olive kernel powder, and crushing the frosted particles into uniform particles of 200 microns by using a micron crusher;
(5) mixing materials: fully mixing 97g of the product obtained in the step (3) with 3g of the abrasive agent obtained in the step (4), and uniformly stirring;
(6) and (3) sterilization: the low-temperature sterilization method is adopted, the temperature is controlled at 60 ℃ and kept for 1 hour, and most microorganisms can be killed;
(7) cooling and subpackaging: cooling to 30 deg.C, and packaging to obtain lip film product.
Example 2:
(1) preparing an emulsion: mixing two oily substances of 19.2g of olive oil and 12.8g of grape seed oil according to the mass ratio of 3:2, heating to 90 ℃, and uniformly stirring to obtain an oil phase. Mixing 25g of glycerol and 35g of water to obtain a water phase, mixing 8g of pectin to obtain an emulsifier, heating the oil phase, the water phase and the emulsifier to 80 ℃, uniformly stirring, shearing for 3min by using a high-speed shearing machine at 30000rpm, and circularly homogenizing for 5 times under the pressure of 70MPa by using a high-pressure homogenizer to obtain a uniform and stable oil-in-water emulsion;
(2) preparing vitamin E microcapsules: preparing a vitamin E microcapsule by taking chitosan and maltodextrin as wall materials through spray drying, wherein lecithin and gelatin are used as an emulsifier in a mass ratio of 4:2, and the chitosan: maltodextrin, 2: vitamin E: emulsifier is 4%: 60%: 20%: 15 percent. Mixing vitamin E2g, lecithin 1g and gelatin 0.5g, performing high-speed shearing and stirring (14000r/min, 3min) to obtain a core material solution, adding chitosan solution 5g with the mass concentration of 10% into the core material solution while stirring, adding maltodextrin solution 10g with the mass concentration of 60%, performing high-speed shearing and stirring (14000r/min, 3min), performing high-pressure homogenization to obtain microcapsule emulsion (50Mpa, 4 times, 25min), finally performing spray drying, wherein the inlet air temperature of the spray drying is 185 ℃, and the outlet air temperature is 85 ℃ to obtain vitamin E microcapsules;
(3) cooling to 60 ℃, mixing 88g of the emulsion obtained in the step (1) with 1.5g of vitamin E microcapsules, 0.5g of glycolic acid, 2.5g of honey and 3.5g of chitosan, wherein the mixing mass ratio of the vitamin E microcapsules, the glycolic acid, the honey and the chitosan is 1.5:0.5:2.5:3.5, the dosage of the emulsion accounts for 91.7 percent of the total mass of the materials, and uniformly stirring;
(4) preparing a frosting agent: adopting natural frosted particles selected from any combination of walnut powder, olive pit powder and cherry pit powder, and crushing the frosted particles into uniform particles of 350 microns by using a micron crusher;
(5) mixing materials: fully mixing 96g of the product obtained in the step (3) with 4g of the abrasive agent obtained in the step (4), and uniformly stirring;
(6) and (3) sterilization: the low-temperature sterilization method is adopted, the temperature is controlled to be 65 ℃ and kept for 1 hour, and most microorganisms can be killed;
(7) cooling and subpackaging: cooling to 30 deg.C, and packaging to obtain lip film product.
Example 3:
(1) preparing an emulsion: mixing 26.9g of olive oil and 8.1g of grape seed oil according to the mass ratio of 5:1.5, heating to 75 ℃, and uniformly stirring to obtain an oil phase. Mixing 15g of glycerol and 40g of water to obtain a water phase, mixing 10g of pectin to obtain an emulsifier, heating the oil phase, the water phase and the emulsifier to 75 ℃, uniformly stirring, shearing for 2-3min by using a 28000rpm high-speed shearing machine, and circularly homogenizing for 5 times under the pressure of 70MPa by using a high-pressure homogenizer to obtain a uniform and stable oil-in-water emulsion;
(2) preparing vitamin E microcapsules: preparing a vitamin E microcapsule by taking chitosan and maltodextrin as wall materials through spray drying, wherein the emulsifier is lecithin and gelatin in a mass ratio of 4:2, and the weight ratio of chitosan: maltodextrin, 2: vitamin E: emulsifier is 4%: 65%: 18%: 13 percent. Mixing 1.8g of vitamin E, 0.9g of lecithin and 0.4g of gelatin, carrying out high-speed shearing and stirring (15000r/min, 3min) to obtain a core material solution, adding 4g of a chitosan solution with the mass concentration of 10% into the core material solution while stirring, adding 10g of a maltodextrin solution with the mass concentration of 65%, carrying out high-speed shearing and stirring (15000r/min, 3min), carrying out high-pressure homogenization to obtain a microcapsule emulsion (60Mpa, 5 times, 20min), finally carrying out spray drying, wherein the air inlet temperature of the spray drying is 180 ℃, and the air outlet temperature is 80 ℃ to obtain a vitamin E microcapsule;
(3) cooling to 65 ℃, mixing 85g of the emulsion obtained in the step (1) with 2.1g of vitamin E microcapsules, 0.6g of glycolic acid, 3.1g of honey and 4.2g of chitosan, wherein the mixing mass ratio of the vitamin E microcapsules, the glycolic acid, the honey and the chitosan is 2:0.6:3:4, the dosage of the emulsion accounts for 89.5 percent of the total mass of the materials, and uniformly stirring;
(4) preparing a frosting agent: adopting natural frosted particles selected from any combination of oat flour, olive kernel powder, apricot kernel powder and cherry kernel powder, and crushing the frosted particles into uniform particles of 150 microns by using a micron crusher;
(5) mixing materials: fully mixing 95g of the product obtained in the step (3) with 5g of the abrasive agent obtained in the step (4), and uniformly stirring;
(6) and (3) sterilization: the low-temperature sterilization method is adopted, the temperature is controlled at 70 ℃ and kept for 0.5 hour, and most of microorganisms can be killed;
(7) cooling and subpackaging: cooling to 30 deg.C, and packaging to obtain lip film product.
The experimental effect is as follows:
and (3) moisture retention rate determination: in order to control the humidity, saturated potassium acetate is placed in a dryer, the humidity is controlled to be about 60%, and in order to better simulate the actual situation of the skin, the saturated potassium acetate is selectedSticking 3M adhesive tape on a glass plate (50mm × 100mm), uniformly coating 200mg of sample on the surface of the adhesive tape, putting into a dryer for a certain time, weighing, and standing until the water content is M1Mass of water m after standing2The moisture retention was calculated as follows: rm ═ m2/m1×100％
Determination of radical clearance: using a DPPH method, sequentially adding 4ml of DPPH solution and 2ml (1:50) of lip membrane diluent into a 10ml colorimetric tube, adding absolute ethyl alcohol for constant volume, measuring the light absorption value at 517nm, recording the light absorption value Ai, keeping away from light for 30min to measure the light absorption value Aj, adding only DPPH ethanol solution in a contrast test, and calculating the clearance rate according to the following formula: k (%) [1- (Ai-Aj)/Ac ] x 100%
And (3) testing the exfoliating effect: the corneocytes on the skin surface before and after the lip mask is used are peeled off by special conductive adhesive, and the obtained product is scanned on a scanning electron microscope to obtain a clear image, and the quantity change of the corneocytes before and after the lip mask is used is compared.
And (3) determination of antibacterial rate: 2g of lip membrane is weighed, 0.2ml of escherichia coli bacterial suspension and staphylococcus aureus bacterial suspension are respectively added, 17.8ml of normal saline is added into a 50ml triangular flask, the flask is fixed on a shaking table and shaken for 2 hours at 200 r/min. The samples were diluted (1: 10) before and after shaking, and inoculated onto petri dishes for viable cell culture counting. The antibacterial rate was calculated as follows: the bacteriostatic rate is (average number of colonies before sample shaking-average number of colonies after sample shaking)/average number of colonies before sample shaking × 100%.
Lip film performance characterization data are shown in the following table:
TABLE 1
The experimental result shows that the lip mask has good moisturizing and moistening properties, oxidation resistance, antibacterial property and good exfoliating effect.
Claims (8)
1. A preparation method of a natural multi-effect lip mask comprises the following steps:
(1) preparing an emulsion: mixing olive oil and grape seed oil at a mass ratio of 3-5:1.5-2.5, heating to 80-90 deg.C, and stirring to obtain oil phase; mixing glycerol and water to obtain water phase, using pectin as emulsifier, mixing oil phase, water phase and emulsifier, heating to 70-80 deg.C, stirring, high-speed shearing, and high-pressure homogenizing to obtain uniform and stable oil-in-water emulsion; wherein, the mass percentages of the glycerin, the water and the emulsifier are respectively 15-25%, 30-40% and 5-10% and the balance is oil phase, wherein the total mass of the fed materials of the components is 100%;
(2) preparing a vitamin E microcapsule by taking chitosan and maltodextrin as wall materials through spray drying: mixing vitamin E and an emulsifier, wherein the emulsifier is lecithin and gelatin in a mass ratio of 4:2, shearing and stirring at a high speed to obtain a core material solution, adding a chitosan solution into the core material solution while stirring, adding a maltodextrin solution, shearing at a high speed, homogenizing at a high pressure to obtain a microcapsule emulsion, and spray-drying to obtain a vitamin E microcapsule; the total mass of the emulsifier, the chitosan, the maltodextrin and the vitamin E is 100 percent, and the mass percentage of each component is as follows: 3-5% of chitosan, 60-70% of maltodextrin, 15-20% of vitamin E and 5-15% of emulsifier;
(3) mixing materials: controlling the temperature to be 55-65 ℃, mixing the emulsion obtained in the step (1) with vitamin E microcapsules, glycolic acid, honey and chitosan, wherein the mass ratio of the vitamin E microcapsules, the glycolic acid, the honey and the chitosan is 1-2:0.3-0.6:2-3:3-4, the amount of the emulsion accounts for 80-95% of the total mass of the materials, and uniformly stirring;
(4) preparing a frosting agent: the method comprises the following steps of (1) adopting natural frosted particles, wherein the natural frosted particles are one or a combination of any more of walnut powder, oat powder, olive kernel powder, apricot kernel powder and cherry kernel powder in any proportion, and crushing the frosted particles into uniform particles of 150-350 microns by using a micron crusher to obtain the frosting agent;
(5) mixing materials: fully mixing the product obtained in the step (3) with the abrasive agent obtained in the step (4) to ensure that the mass fraction of the abrasive agent in the mixture is between 3 and 5 percent, and uniformly stirring;
(6) sterilizing the mixture obtained in the step (5) at the temperature of 60-70 ℃;
(7) and cooling and subpackaging the sterilized product to obtain a lip mask product.
2. The method of claim 1, wherein: in the step (1), the high-speed shearing conditions are as follows: shearing for 2-3min by using a high-speed shearing machine with 26000-30000 rpm; the high-pressure homogenizing conditions are as follows: circularly homogenizing for 5-6 times under 70-80 MPa with a high-pressure homogenizer to obtain uniform and stable oil-in-water emulsion.
3. The method of claim 1, wherein: in the step (2), the high-speed shearing conditions are as follows: 13000r/min-15000r/min, 2-4 min; the high-pressure homogenizing conditions are as follows: 40MPa-60MPa for 3-5 times; the spray drying conditions were: the air inlet temperature of spray drying is 170-190 ℃, and the air outlet temperature is 80-90 ℃.
4. The method of claim 2, wherein: in the step (2), the high-speed shearing conditions are as follows: 13000r/min-15000r/min, 2-4 min; the high-pressure homogenizing conditions are as follows: 40MPa-60MPa for 3-5 times; the spray drying conditions were: the air inlet temperature of spray drying is 170-190 ℃, and the air outlet temperature is 80-90 ℃.
5. The method according to any one of claims 1 to 4, wherein: in the step (1), the oil phase accounts for 30-35% by mass, wherein the mass ratio of the olive oil to the grape seed oil is 3-4: 2-2.5.
6. The method according to any one of claims 1 to 4, wherein: in the step (3), the mixing mass ratio of the vitamin E microcapsules, the glycolic acid, the honey and the chitosan is 1.5-2:0.3-0.5:2.5-3:3.5-4, and the dosage of the emulsion accounts for 90-95% of the total mass of the materials.
7. The method according to any one of claims 1 to 4, wherein: in the step (1), the oil phase accounts for 30-35% by mass, wherein the mass ratio of the olive oil to the grape seed oil is 3-4: 2-2.5; in the step (3), the mixing mass ratio of the vitamin E microcapsules, the glycolic acid, the honey and the chitosan is 1.5-2:0.3-0.5:2.5-3:3.5-4, and the dosage of the emulsion accounts for 90-95% of the total mass of the materials.
8. The method according to any one of claims 1 to 4, wherein: in the step (6), the temperature is controlled to be 60-70 ℃ and kept for 0.5-1 hour.
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