FR3092760A1 - PROCESS FOR PROLONGING THE PRESENCE OF OLFACTORY AND AROMATIC MOLECULES ON WOVEN OR NON-WOVEN SUBSTRATES - Google Patents
PROCESS FOR PROLONGING THE PRESENCE OF OLFACTORY AND AROMATIC MOLECULES ON WOVEN OR NON-WOVEN SUBSTRATES Download PDFInfo
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- FR3092760A1 FR3092760A1 FR1901662A FR1901662A FR3092760A1 FR 3092760 A1 FR3092760 A1 FR 3092760A1 FR 1901662 A FR1901662 A FR 1901662A FR 1901662 A FR1901662 A FR 1901662A FR 3092760 A1 FR3092760 A1 FR 3092760A1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/015—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
- A61L9/04—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air without heating
- A61L9/044—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air without heating with the help of an organic compound other than a macromolecular compound
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/005—Compositions containing perfumes; Compositions containing deodorants
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/15—Proteins or derivatives thereof
Abstract
La présente invention concerne le domaine des procédés et produits pour Textiles et Cosméto-Textiles afin d’obtenir un effet prolongé des produits de traitement, tel que le parfum d’ambiance ou des préparations donnant des résultats cosmétiques, après application sur des supports tissés ou non tissés.The present invention relates to the field of processes and products for Textiles and Cosmeto-Textiles in order to obtain a prolonged effect of treatment products, such as room fragrance or preparations giving cosmetic results, after application to woven or woven supports. non-woven.
Description
La présente invention concerne le domaine des procédés et produits pour Textiles et Cosméto-Textiles afin d’obtenir un effet prolongé des produits de traitement, tel que le parfum d’ambiance ou des préparations donnant des résultats cosmétiques, après application sur des supports tissés ou non tissés.The present invention relates to the field of processes and products for Textiles and Cosmeto-Textiles in order to obtain a prolonged effect of treatment products, such as home fragrances or preparations giving cosmetic results, after application to woven or nonwovens.
Ce procédé augmente la présence et l’efficacité des molécules et extraits naturels appliqués sur ces dits supports.This process increases the presence and effectiveness of molecules and natural extracts applied to these so-called supports.
Il est connu par l’homme de l’art qu’après vaporisation ou brumisation à l’aide d’un spray ou d’un atomiseur sous pression de gaz, un liquide parfumé , à base de molécules odorantes de type aromatiques, a une durée de présence très éphémère (quelques minutes à une ou deux heures maximum) après application sur un support tissé ou non tissé comme la soie naturelle ou le coton.It is known by those skilled in the art that after vaporization or misting using a spray or an atomizer under gas pressure, a perfumed liquid, based on odorous molecules of the aromatic type, has a very short-lived presence (a few minutes to one or two hours maximum) after application on a woven or non-woven support such as natural silk or cotton.
Afin de prolonger la présence de ces molécules olfactives ayant des propriétés calmantes , relaxantes et agissant sur la beauté de la peau – anti-rides , cicatrisantes, régénérantes - après vaporisation ou brumisation le soir sur une taie d’oreiller en soie ou en coton , le demandeur a découvert de façon fortuite qu’en additionnant dans la solution odorante à appliquer des protéines naturelles ou peptides, naturels ou synthétiques, ou hydrolysats de protéines après hydrolyse enzymatique, les molécules aromatiques persistaient au moins 8 heures sur le support traité.
Le procédé fait appel à des protéines , hydrolysats de protéines ou peptides d’origine naturelle ou synthétique qui sont constitués ou enrichis en particulier d’acides aminés hydrophobes tels que la Glycine, l’Alanine, la Valine , la Leucine ou l’Isoleucine.
Le procédé fait appel à des protéines , hydrolysats de protéines et peptides qui sont extraits de la soie comme la Séricyne , du blé comme les Gliadines, du maïs comme la Zéine.
Le procédé utilise ces protéines , hydrolysats de protéines et peptides qui sont mélangés à la hauteur de O,1 à 10% en poids ou masse , et plus particulièrement à 1% pour l’hydrolysat de Séricyne dans la solution hydro-alcoolique contenant les molécules odorantes et aromatiques à pulvériser par atomisation ou brumisation au moment de l’emploi.
Le procédé fait appel à des molécules odorantes et aromatiques qui constituent la base parfumée hydro-alcoolique et font partie des composés et molécules suivant :
-gamma undécalactone, mélonal, trans-2-hexenal,acetate de linalyl,trans-2-décénal,aldéhyde cyclamen, hydroxycitronellal, hexen-1-ol, méthyl ionone, 2-6 nonadien-1-ol, géraniol, alcool phenyl-éthylique, limonène,2-6-diméthyl-2-heptanol,gamma décalactone,3-hydroxy-2-butanone,beta ionone,hédione,hélional, limonène,aldéhydes C8 à C10,citral,acétate de linalyle,angélate d’isoamyle, angélate d’isobutyle,farnésol,acétate de benzyl,cis-3-hexenol,alpha-ionone,indole,lilial, santalol.
La composition parfumée hydro-alcoolique peut également contenir des huiles essentielles connues pour leurs propriétés relaxantes et calmantes comme des extraits de :
-Mandarine, Petitgrain bigarade,lavande,lavandin, ylang-ylang,néroli,camomille romaine,Marjolaine à coquille, Verveine odorante, Santal.In order to prolong the presence of these olfactory molecules with calming, relaxing properties and acting on the beauty of the skin - anti-wrinkle, healing, regenerating - after vaporization or misting in the evening on a silk or cotton pillowcase, the applicant discovered by chance that by adding in the fragrant solution to be applied natural proteins or peptides, natural or synthetic, or protein hydrolysates after enzymatic hydrolysis, the aromatic molecules persisted for at least 8 hours on the treated support.
The method makes use of proteins, protein hydrolysates or peptides of natural or synthetic origin which are constituted or enriched in particular with hydrophobic amino acids such as Glycine, Alanine, Valine, Leucine or Isoleucine.
The process uses proteins, protein hydrolysates and peptides which are extracted from silk such as Sericyne, wheat such as Gliadins, corn such as Zein.
The process uses these proteins, protein hydrolysates and peptides which are mixed up to 0.1 to 10% by weight or mass, and more particularly at 1% for the hydrolyzate of Sericyne in the hydro-alcoholic solution containing the molecules fragrant and aromatic to be sprayed by atomization or misting at the time of use.
The process uses fragrant and aromatic molecules which constitute the hydro-alcoholic perfumed base and are part of the following compounds and molecules:
-gamma undecalactone, melonal, trans-2-hexenal, linalyl acetate, trans-2-decenal, cyclamen aldehyde, hydroxycitronellal, hexen-1-ol, methyl ionone, 2-6 nonadien-1-ol, geraniol, phenyl alcohol- ethyl, limonene, 2-6-dimethyl-2-heptanol, gamma decalactone, 3-hydroxy-2-butanone, beta ionone, hedione, helional, limonene, C8 to C10 aldehydes, citral, linalyl acetate, isoamyl angelate, isobutyl angelate, farnesol, benzyl acetate, cis-3-hexenol, alpha-ionone, indole, lilial, santalol.
The hydro-alcoholic perfumed composition may also contain essential oils known for their relaxing and calming properties, such as extracts of:
- Mandarin, Petitgrain Bigarade, Lavender, Lavandin, Ylang-Ylang, Neroli, Roman Chamomile, Marjoram, Scented Verbena, Sandalwood.
Les exemples suivant permettent d’illustrer le dit procédé :The following examples illustrate this process:
Exemple 1 : Néo-Perles Aromatiques de Soie pour la BeautéExample 1: Aromatic Silk Neo-Pearls for Beauty
1-1Préparation des bases aromatiques:
200ml d’un mélange d’huiles essentielles de lavande, lavandin, ylang-ylang, néroli , et chacune à 1% en volume , auquel est ajouté 0,1% en volume de santalol ,d’angélate d’isoamyle et d’angélate d’isobutyle, est préparé dans une solution hydro-alcoolique à 70% en volume d’éthanol dénaturé.
On sépare cette base en deux volumes égaux :
Dans 100ml de cette base aromatique sont solubilisés 2% en poids d’hydrolysat de protéines de soie, la Séricyne traitée par une protéase et sous forme de poudre. Les autres 100ml sont conservés sans ajout de protéines. Les deux solutions sont placées dans des flacons pompes puis vaporisées sur 10 taies d’oreiller en soie.1-1 Preparation of aromatic bases :
200ml of a mixture of essential oils of lavender, lavandin, ylang-ylang, neroli, each at 1% by volume, to which is added 0.1% by volume of santalol, isoamyl angelate and angelate of isobutyl, is prepared in a hydro-alcoholic solution at 70% by volume of denatured ethanol.
This base is separated into two equal volumes:
In 100ml of this aromatic base are dissolved 2% by weight of silk protein hydrolyzate, Sericyne treated with a protease and in powder form. The other 100ml are kept without adding protein. The two solutions are placed in pump bottles and then sprayed on 10 silk pillowcases.
1-2 Test olfactif : Un panel de 3 experts en analyse sensorielle a évalué toutes les heures la présence olfactive des deux solutions sur les taies en soie et constaté que la solution, contenant la base aromatique et l’hydrolysat de Séricyne, était toujours présente après 8 heures alors que la solution ne contenant pas d’hydrolysat avait disparu après 1 heure.1-2 Olfactory test: A panel of 3 experts in sensory analysis evaluated the olfactory presence of the two solutions on the silk pillowcases every hour and found that the solution, containing the aromatic base and the hydrolyzate of Sericyne, was always present. after 8 hours whereas the solution containing no hydrolyzate had disappeared after 1 hour.
1-3Test visuel par Microscopie Electronique à Balayage:
Des fragments de tissus de soie ont été placés sur deux supports pour l’analyse en Microscopie Electronique à Balayage . Un support a été traité par vaporisation avec la solution aromatique contenant l’hydrolysat de Séricyne et l’autre avec la solution n’en contenant pas. Sur le support qui a été traité par la solution aromatique contenant l’hydrolysat de Séricyne on observe la présence de « perles » microscopiques de quelques microns qui se sont formées extemporanément après la pulvérisation. Sur le support traité par la solution ne contenant pas l’hydrolysat de Séricyne nous n’observons pas la présence de ces « néo-perles » mais plutôt des formes amorphes comme des « flaques huileuses » microscopiques.1-3 Visual test by Scanning Electron Microscopy :
Silk fabric fragments were placed on two supports for Scanning Electron Microscopy analysis. One support was treated by vaporization with the aromatic solution containing the Sericyne hydrolyzate and the other with the solution not containing it. On the support which has been treated with the aromatic solution containing the hydrolyzate of Sericyne, the presence of microscopic “pearls” of a few microns in size which formed extemporaneously after the spraying is observed. On the support treated with the solution not containing the Sericyne hydrolyzate, we do not observe the presence of these "neo-pearls" but rather amorphous forms such as microscopic "oily puddles".
Exemple 2 : Formulation d’une Brume Essentielle favorisant le sommeil et son maintienExample 2: Formulation of an Essential Mist promoting sleep and its maintenance
2-1Préparation des bases aromatiques:
200ml d’un mélange d’huiles essentielles de Mandarine, Petitgrain bigarade, lavande, lavandin, ykang-ylang, néroli, camomille romaine, Marjolaine à coquille et Verveine odorante chacune à 1% en volume , est préparé dans une solution hydro-alcoolique à 70% en volume d’éthanol dénaturé. On sépare cette base en deux volumes égaux : Dans 100ml de cette base aromatique sont solubilisés 0,5% en poids de protéines de blé, des gliadines. Les autres 100ml sont conservés sans ajout de protéines. Les deux solutions sont placées dans des flacons pompes puis vaporisées sur 10 taies d’oreiller en coton.2-1 Preparation of aromatic bases :
200ml of a mixture of Mandarin, Petitgrain bigarade, lavender, lavandin, ykang-ylang, neroli, Roman chamomile, shell marjoram and fragrant verbena essential oils, each at 1% by volume, is prepared in a hydro-alcoholic solution at 70% by volume of denatured ethanol. This base is separated into two equal volumes: In 100ml of this aromatic base are dissolved 0.5% by weight of wheat proteins, gliadins. The other 100ml are kept without adding protein. The two solutions are placed in pump bottles and then sprayed on 10 cotton pillowcases.
2-2Test olfactif: Un panel de 3 experts en analyse sensorielle a évalué toutes les heures la présence olfactive des deux solutions sur les taies en coton et constaté que la solution , contenant la base aromatique et les gliadines, était toujours présente après 8 heures alors que la solution ne contenant pas de protéines de blé avait disparu après 2 heures.2-2 Olfactory test : A panel of 3 experts in sensory analysis evaluated the olfactory presence of the two solutions on the cotton pillowcases every hour and found that the solution, containing the aromatic base and the gliadins, was still present after 8 hours. whereas the solution containing no wheat protein had disappeared after 2 hours.
Exemple 3 : Micro-Poudres AromatiquesExample 3: Aromatic Micro-Powders
3-1Préparation des bases aromatiques:
200ml d’un mélange d’huiles essentielles de lavande, lavandin, ylang-ylang, néroli , et chacune à 1% en volume , auquel est ajouté 0,1% en volume de santalol ,d’angélate d’isoamyle et d’angélate d’isobutyle, est préparé dans une solution hydro-alcoolique à 70% en volume d’éthanol dénaturé.
On sépare cette base en deux volumes égaux :
Dans 100ml de cette base aromatique sont solubilisés 5% en poids d’un tri-peptide de synthèse constitué d’un tiers de Glycine, d’un tiers d’Alanine, d’un tiers de Valine. Les autres 100ml sont conservés sans ajout de protéines. Les deux solutions sont placées dans des flacons pompes puis vaporisées sur 10 taies d’oreiller en soie.3-1 Preparation of aromatic bases :
200ml of a mixture of essential oils of lavender, lavandin, ylang-ylang, neroli, each at 1% by volume, to which is added 0.1% by volume of santalol, isoamyl angelate and angelate of isobutyl, is prepared in a hydro-alcoholic solution at 70% by volume of denatured ethanol.
This base is separated into two equal volumes:
In 100ml of this aromatic base are dissolved 5% by weight of a synthetic tri-peptide consisting of one third of Glycine, one third of Alanine, one third of Valine. The other 100ml are kept without adding protein. The two solutions are placed in pump bottles and then sprayed on 10 silk pillowcases.
3-2Test olfactif: Un panel de 3 experts en analyse sensorielle a évalué toutes les heures la présence olfactive des deux solutions sur les taies en soie et constaté que la solution, contenant la base aromatique et le peptide de synthèse, était toujours présente après 8 heures alors que la solution ne contenant pas d’hydrolysat avait disparu après 1 heure.3-2 Olfactory test : A panel of 3 experts in sensory analysis evaluated the olfactory presence of the two solutions on the silk pillowcases every hour and found that the solution, containing the aromatic base and the synthetic peptide, was still present after 8 hours whereas the solution containing no hydrolyzate had disappeared after 1 hour.
3-3Test visuel par Microscopie Electronique à Balayage:
Des fragments de tissus de soie ont été placés sur deux supports pour l’analyse en Microscopie Electronique à Balayage. Un support a été traité par vaporisation avec la solution aromatique contenant le peptide de synthèse et l’autre avec la solution n’en contenant pas. Sur le support qui a été traité par la solution aromatique contenant le peptide on observe la présence de « micro-poudres » microscopiques de quelques microns qui se sont formées extemporanément après la pulvérisation. Sur le support traité par la solution ne contenant pas le peptide nous n’observons pas la présence de ces « micro-poudres» mais plutôt des formes amorphes comme des « flaques huileuses » microscopiques.3-3 Visual test by Scanning Electron Microscopy :
Fragments of silk fabrics were placed on two supports for analysis by Scanning Electron Microscopy. One support was treated by spraying with the aromatic solution containing the synthetic peptide and the other with the solution not containing it. On the support which has been treated with the aromatic solution containing the peptide, the presence of microscopic “micro-powders” of a few microns in size which formed extemporaneously after the spraying is observed. On the support treated with the solution not containing the peptide, we do not observe the presence of these "micro-powders" but rather amorphous forms such as microscopic "oily puddles".
Claims (6)
-gamma undécalactone, mélonal, trans-2-hexenal,acetate de linalyl,trans-2-décénal,aldéhyde cyclamen, hydroxycitronellal, hexen-1-ol, méthyl ionone, 2-6 nonadien-1-ol, géraniol, alcool phenyl-éthylique, limonène,2-6-diméthyl-2-heptanol,gamma décalactone,3-hydroxy-2-butanone,beta ionone,hédione,hélional, limonène,aldéhydes C8 à C10,citral,acétate de linalyle,angélate d’isoamyle, angélate d’isobutyle,farnésol,acétate de benzyl,cis-3-hexenol,alpha-ionone,indole,lilial, santalol.Process according to Claim 1, characterized in that the odorous and aromatic molecules which constitute the hydro-alcoholic perfumed base consist of the following compounds:
-gamma undecalactone, melonal, trans-2-hexenal, linalyl acetate, trans-2-decenal, cyclamen aldehyde, hydroxycitronellal, hexen-1-ol, methyl ionone, 2-6 nonadien-1-ol, geraniol, phenyl alcohol- ethyl, limonene, 2-6-dimethyl-2-heptanol, gamma decalactone, 3-hydroxy-2-butanone, beta ionone, hedione, helional, limonene, C8 to C10 aldehydes, citral, linalyl acetate, isoamyl angelate, isobutyl angelate, farnesol, benzyl acetate, cis-3-hexenol, alpha-ionone, indole, lilial, santalol.
-Mandarine , Petitgrain bigarade ,lavande, lavandin, ylang-ylang, néroli, camomille romaine, Marjolaine à coquille, Verveine odorante, Santal.Process according to Claim 1, characterized in that the hydro-alcoholic perfumed composition may also contain essential oils known for their relaxing and calming properties, such as extracts of:
- Mandarin, Petitgrain bigarade, lavender, lavandin, ylang-ylang, neroli, Roman chamomile, marjoram, fragrant verbena, sandalwood.
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SILVA CARLA ET AL: "Odorant binding proteins: a biotechnological tool for odour control", APPLIED MICROBIOLOGY AND BIOTECHNOLOGY, SPRINGER BERLIN HEIDELBERG, BERLIN/HEIDELBERG, vol. 98, no. 8, 5 October 2013 (2013-10-05), pages 3629 - 3638, XP035328978, ISSN: 0175-7598, [retrieved on 20131005], DOI: 10.1007/S00253-013-5243-9 * |
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