CN103290700A - Aromatic rope and manufacturing method thereof - Google Patents
Aromatic rope and manufacturing method thereof Download PDFInfo
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- CN103290700A CN103290700A CN2013102123482A CN201310212348A CN103290700A CN 103290700 A CN103290700 A CN 103290700A CN 2013102123482 A CN2013102123482 A CN 2013102123482A CN 201310212348 A CN201310212348 A CN 201310212348A CN 103290700 A CN103290700 A CN 103290700A
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Abstract
The invention discloses an aromatic rope and a manufacturing method of the aromatic rope. The method comprises the steps of preparation of microcapsules, fragrance finishing and aftertreatment technology. The method is reasonable in technological process arrangement and scientific, simple and convenient in implementation, and adopts the microcapsule technology to carry out fragrance finishing on the rope; the manufactured rope has the good characteristics of being long in fragrance lasting time and good in durability, and can be widely applied to the aspects such as entertainment, interior decoration and jewelries.
Description
Technical field
The present invention relates to the daily living article field, specifically a kind of fragrant rope and preparation method thereof.
Background technology
At present, rope is in the extensive use of entertainment field such as household, open air, physical culture, leisure, and its mounting or dismounting are easy, convenient carrying is that it is in the numerous areas extensive use.Along with the raising day by day of people's living standard and cultural taste, amusement and recreation class rope requires also to have had new variation, transformed to decoration, enjoyment, health by the practical of past, and the rope perfuming has been complied with this trend.
Because the fragrance rope has antibacterial expelling parasite, covering smell, makes the comfortable effect of body and mind, thereby is subjected to liking of people.If adopt the mode of adding spices to realize fragrance effect, spices is highly volatile at normal temperatures, and fragrance is difficult to permanent preservation, poor durability, and also fragrance effect is subject to the washing influence.
Summary of the invention
For solving the technical problem of above-mentioned existence, the invention provides a kind of fragrant rope and preparation method thereof, simple to operate, the fragrance longer duration, improve user's level of comfort, make it in the bigger use value of entertainment field such as household, open air, physical culture, leisure performance.
For achieving the above object, the technical solution used in the present invention is as follows:
A kind of fragrant rope comprises rope matrix and spices slow release layer, and described spices slow release layer is coated on the outside of described rope matrix by PVC or PU coating.
Described rope matrix is nylon torsade, terylene torsade, polypropylene fibre torsade, cotton torsade, nylon sennit, terylene sennit, polypropylene fibre sennit and cotton sennit.
A kind of preparation method of fragrant rope, realize as follows:
1) preparation slowly-releasing perfume microcapsule, at first take by weighing gelatin, essence and OP-10 that weight proportion is 90-98%:1-5%:1-5%, adding distilled water mixes the back 55-70 ℃ of dissolving down, 5000 rev/mins rotating speed emulsification, the emulsion that emulsification obtains is poured in the there-necked flask after the dissolving, adding distil water, regulating the pH value is 6.0-6.5, and 60 ℃ of reactions added glutaraldehyde cross-linking 1-2 hour at last, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid adds functional aid and distilled water with slowly-releasing perfume microcapsule solution, and magnetic agitation is to mixing in beaker;
3) rope matrix is put into cleaning solution and soaks, the oil stain on the flush away rope, with slowly-releasing perfume microcapsule dressing liquid by coating, pad or immersion coating on rope matrix, under 35-90 ℃, bake 10min-30min, dry, form the spices slow release layer;
4) coated rope matrix is put into cleaning solution and soak, dry and get product.
Coating in the described step 3) adopts a kind of in blade coating, spraying, flow coat or the electro-deposition.
Described step 2) function additive that adopts in adopts tackifier, flexibilizer, plasticizer, thickener, diluent, solvent, coupling agent, emulsifying agent, filler, reinforcing agent, curing agent, crosslinking agent, initator, light trigger, catalyst, promoter, polymerization inhibitor, oxidant, softening agent, age resistor, dispersant, blowing agent, defoamer, levelling agent, colouring agent, toner, bleeding agent, wetting agent, neutralizer, sagging inhibitor, anti skinning agent, drier, anti-adhesion agent, antifreezing agent, antistatic additive, the flavor agent disappears, antiseptic, mould inhibitor, mite-proof agent, anophelifuge, in fire retardant or the ultra-violet absorber one or more.
Technique process arrangement of the present invention is reasonable, simple to operate, with low cost, by microcapsules technology rope matrix is carried out Aroma finishing, utilize filmogen that spices is wrapped to form small-particle, wall film by airtight or semi-hermetic is isolated rope matrix core and external environment, thereby reach protection and stable rope matrix core, odor barrier and color, control discharges the purpose of fragrance, it is long that the rope that makes has fragrance remaining time, and the characteristics of good endurance are applied to live more widely, field such as leisure, amusement, decoration; Preparation method of the present invention is not limited to the Aroma finishing in cord material field in addition, also is applicable to the Aroma finishing of materials such as fiber, silk, line, cloth, obtains close effect.
Description of drawings
Fig. 1 is structural representation of the present invention.
The specific embodiment
Describe the present invention below in conjunction with the drawings and specific embodiments:
Be illustrated in figure 1 as specific embodiments of the invention, this fragrance rope comprises rope matrix 1 and spices slow release layer 2, and described spices slow release layer 2 is coated on the outside of described rope matrix 1 by PVC or PU coating.
Described rope matrix 1 is nylon torsade, terylene torsade, polypropylene fibre torsade, cotton torsade, nylon sennit, terylene sennit, polypropylene fibre sennit and cotton sennit.
The preparation method of this fragrance rope, realize as follows:
1) preparation slowly-releasing perfume microcapsule, at first take by weighing gelatin, essence and OP-10 that weight proportion is 90-98%:1-5%:1-5%, add distilled water and mix the back 55-70 ℃ of dissolving down, dissolving back emulsification under 5000-2500 rev/min rotating speed is poured the emulsion that emulsification obtains in the there-necked flask into, adding distil water, regulating the pH value is 6.0-6.5, and 60-50 ℃ of reaction added glutaraldehyde cross-linking 1-2 hour at last, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid adds functional aid and distilled water with slowly-releasing perfume microcapsule solution, and magnetic agitation is to mixing in beaker;
3) rope matrix is put into cleaning solution and soaks, the oil stain on the flush away rope, with slowly-releasing perfume microcapsule dressing liquid by coating, pad or immersion coating on rope matrix, under 35-90 ℃, bake 10min-30min, dry, form the spices slow release layer;
4) coated rope matrix is put into cleaning solution and soak, dry and get product.
Coating in the described step 3) adopts a kind of in blade coating, spraying, flow coat or the electro-deposition.
Described step 2) the described function additive that adopts in adopts tackifier, flexibilizer, plasticizer, thickener, diluent, solvent, coupling agent, emulsifying agent, filler, reinforcing agent, curing agent, crosslinking agent, initator, light trigger, catalyst, promoter, polymerization inhibitor, oxidant, softening agent, age resistor, dispersant, blowing agent, defoamer, levelling agent, colouring agent, toner, bleeding agent, wetting agent, neutralizer, sagging inhibitor, anti skinning agent, drier, anti-adhesion agent, antifreezing agent, antistatic additive, the flavor agent disappears, antiseptic, mould inhibitor, mite-proof agent, anophelifuge, in fire retardant or the ultra-violet absorber one or more.
The preparation method of the present invention's fragrance rope is described below by several specific embodiments:
Embodiment 1:
1) preparation slowly-releasing perfume microcapsule, 90g gelatin, 5g essence, 5g OP-10 are added D500mL distilled water mix the back 60 ℃ of dissolvings down, dissolving back is 5000 rev/mins rotating speed emulsification, the emulsion that emulsification obtains is poured in the there-necked flask, adding distil water, regulating the pH value is 6.2,60 ℃ of reactions, added glutaraldehyde cross-linking at last 2 hours, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid, get the above-mentioned spices slow-release microcapsule that makes and be configured to 10% solution, 30% water-borne acrylic resin (ApA-518), 2% levelling agent (GSK-588), 4% antioxidant, 32% pigment, magnetic agitation is to mixing in beaker;
3) rope matrix is put into 40 ℃, the cleaning solution of 1g/L and soaked 0.5min, stir 2min with glass bar again, dry, with oil stain on the flush away rope, above-mentioned slowly-releasing perfume microcapsule dressing liquid is uniformly coated on the nylon rope matrix, coating weight is 100g/m
2, bake 30min under 60 ℃, dry, form the spices slow release layer;
4) rope that step 3) is made is put into 40 ℃, the cleaning solution of 1g/L and is soaked 0.5min, stirs 2min with glass bar again, dries, and gets product.
Embodiment 2:
1) preparation slowly-releasing perfume microcapsule, 95g gelatin, 2.5g essence, 2.5g OP-10 are added 200mL distilled water mix the back 60 ℃ of dissolvings down, dissolving back is 5000 rev/mins rotating speed emulsification, the emulsion that emulsification obtains is poured in the there-necked flask, adding distil water, regulating the pH value is 6.0,60 ℃ of reactions, added glutaraldehyde cross-linking at last 1 hour, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid is got the above-mentioned slowly-releasing perfume microcapsule that makes and is configured to 10% solution, adds 0.2% bleeding agent, 20% PU resin, 4.5% thickener (690048) in beaker magnetic agitation to mixing;
3) rope matrix is put into 40 ℃, the cleaning solution of 1g/L and soaked 0.5min, stir 2min with glass bar again, dry, with oil stain on the flush away rope, above-mentioned slowly-releasing perfume microcapsule dressing liquid is uniformly coated on the nylon rope matrix, coating weight is 100g/m
2, bake 30min under 60 ℃, dry, form the spices slow release layer;
4) rope that step 3) is made is put into 40 ℃, the cleaning solution of 1g/L and is soaked 0.5min, stirs 2min with glass bar again, dries, and gets product.
Embodiment 3:
1) preparation slowly-releasing perfume microcapsule, 98g gelatin, 1g essence, 1g OP-10 are added 200mL distilled water mix the back 60 ℃ of dissolvings down, dissolving back is 5000 rev/mins rotating speed emulsification, the emulsion that emulsification obtains is poured in the there-necked flask, adding distil water, regulating the pH value is 6.5,60 ℃ of reactions, added glutaraldehyde cross-linking at last 1.5 hours, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid is got the above-mentioned slowly-releasing perfume microcapsule that makes and is configured to 10% solution, 30% water-borne acrylic resin (ApA-518), 2% levelling agent (GSK-588) in beaker magnetic agitation to mixing;
3) rope matrix is put into 40 ℃, the cleaning solution of 1g/L and soaked 0.5min, stir 2min with glass bar again, dry, with oil stain on the flush away rope, above-mentioned slowly-releasing perfume microcapsule dressing liquid is uniformly coated on the nylon rope matrix, coating weight is 100g/m
2, bake 30min under 65 ℃, dry, form the spices slow release layer;
4) rope that step 3) is made is put into 40 ℃, the cleaning solution of 1g/L and is soaked 0.5min, stirs 2min with glass bar again, dries, and gets product.
Embodiment 4:
1) preparation slowly-releasing perfume microcapsule, 98g gelatin, 1g essence, 1g OP-10 are added 200mL distilled water mix the back 60 ℃ of dissolvings down, dissolving back is 5000 rev/mins rotating speed emulsification, the emulsion that emulsification obtains is poured in the there-necked flask, adding distil water, regulating the pH value is 6.5,60 ℃ of reactions, added glutaraldehyde cross-linking at last 1.5 hours, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid, get the above-mentioned slowly-releasing perfume microcapsule that makes and be configured to 10% solution, 30% water-borne acrylic resin (ApA-518), 2% levelling agent (GSK-588), 4% antioxidant, 32% pigment, magnetic agitation is to mixing in beaker;
3) rope matrix is put into 40 ℃, the cleaning solution of 1g/L and soaked 0.5min, stir 2min with glass bar again, dry, with oil stain on the flush away rope, above-mentioned slowly-releasing perfume microcapsule dressing liquid is uniformly coated on the nylon rope matrix, coating weight is 100g/m
2, bake 15min under 70 ℃, dry, form the spices slow release layer;
4) rope that step 3) is made is put into 40 ℃, the cleaning solution of 1g/L and is soaked 0.5min, stirs 2min with glass bar again, dries, and gets product.
Embodiment 5:
1) preparation slowly-releasing perfume microcapsule: 95g gelatin, 2.5g essence, 2.5g OP-10 are added distilled water mix the back 60 ℃ of dissolvings down, dissolving back is 5000 rev/mins rotating speed emulsification, the emulsion that emulsification obtains is poured in the there-necked flask, adding distil water, regulating the pH value is 6.0,60 ℃ of reactions, will add glutaraldehyde cross-linking at last 1 hour, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid: get above-mentioned 20% the slowly-releasing perfume microcapsule solution that makes, add 0.2% bleeding agent, 4% low-temperature adhesive, 1.0% fire retardant (FPK8078), 1.0% dispersant (S-2108) and an amount of water, magnetic agitation is to mixing in beaker;
3) cotton cord rope matrix is put into 40 ℃, the cleaning solution of 1g/L and soaked 0.5min, stir 2min with glass bar again, dry, with oil stain on the flush away rope, rope matrix is put into slowly-releasing perfume microcapsule dressing liquid dipping rope matrix, bath raio 1:8, adopt two to soak two roll process, under 90 ℃, bake 10min during dipping, dry, form the spices slow release layer;
4) rope that step 3) is made is put into 40 ℃, the cleaning solution of 1g/L and is soaked 0.5min, stirs 2min with glass bar again, dries, and gets product.
Embodiment 6:
1) preparation slowly-releasing perfume microcapsule, 98g gelatin, 1g essence, 1g OP-10 are added 200mL distilled water mix the back 60 ℃ of dissolvings down, dissolving back is 5000 rev/mins rotating speed emulsification, the emulsion that emulsification obtains is poured in the there-necked flask, adding distil water, regulating the pH value is 6.5,60 ℃ of reactions, added glutaraldehyde cross-linking at last 1.5 hours, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid: get above-mentioned 20% the slowly-releasing perfume microcapsule solution that makes, add 3% low-temperature adhesive, 13% ultra-violet absorber (UV-531), 1.2% pest-control finishing agent (AI), 0.8% dispersant (LM-5040)
With an amount of water, magnetic agitation is to mixing in beaker;
3) rope matrix is put into 40 ℃, the cleaning solution of 1g/L and soaked 0.5min, stir 2min with glass bar again, dry, with oil stain on the flush away rope, rope matrix is put into slowly-releasing perfume microcapsule dressing liquid dipping rope matrix, bath raio 1:8, adopt two to soak two roll process, under 90 ℃, bake 10min during dipping, dry, form the spices slow release layer;
4) rope that step 3) is made is put into 40 ℃, the cleaning solution of 1g/L and is soaked 0.5min, stirs 2min with glass bar again, dries, and gets product.
Embodiment 7:
1) preparation slowly-releasing perfume microcapsule: 95g gelatin, 2.5g essence, 2.5g OP-10 are added distilled water mix the back 60 ℃ of dissolvings down, dissolving back is 5000 rev/mins rotating speed emulsification, the emulsion that emulsification obtains is poured in the there-necked flask, adding distil water, regulating the pH value is 6.0,60 ℃ of reactions, will add glutaraldehyde cross-linking at last 1 hour, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid: get above-mentioned 20% the slowly-releasing perfume microcapsule solution that makes, add 0.2% bleeding agent, 0.45% low-temperature adhesive and an amount of water, magnetic agitation is to mixing in beaker;
3) rope matrix is put into 40 ℃, the cleaning solution of 1g/L and soaked 0.5min, stir 2min with glass bar again, dry, with oil stain on the flush away rope, rope matrix put into slowly-releasing perfume microcapsule dressing liquid dipping rope matrix; bath raio 1:10; dipping 1h, then rope matrix is dried (liquid carrying rate is 80%), bake 30min under 35 ℃; dry, form the spices slow release layer;
4) rope that step 3) is made is put into 40 ℃, the cleaning solution of 1g/L and is soaked 0.5min, stirs 2min with glass bar again, dries, and gets product.
Need to prove that in the preparation slowly-releasing perfume microcapsule process, regulate the pH value and react afterwards, those skilled in the art controlled voluntarily and got final product as the case may be the time of reaction, did not do the restriction of further time here under 60 ℃ of situations.
Also savory after fragrant 24 weeks of rope placement that method for sorting obtains according to the method described above; According to technology washing methods washing 10 times, 30 times, fragrance successively decreases after 50 times, still has faint fragrance after washing 50 times.
This fragrance rope solved spices at normal temperatures volatile, fragrance be difficult to permanent preservation, poor durability, fragrance are subject to problems such as washing influence, fragrance slowly-releasing and holding time are permanent, good endurance, be widely used in fields such as amusement and recreation, interior decoration, jewellery ornaments more, comfortable, fashion, cost is low, easily promotes.
Certainly, above-mentioned explanation is not to be limitation of the present invention, and the present invention also is not limited in above-mentioned giving an example, and the variation that those skilled in the art make in essential scope of the present invention, remodeling, interpolation or replacement also should belong to protection scope of the present invention.
Claims (5)
1. a fragrant rope is characterized in that, comprises rope matrix (1) and spices slow release layer (2), and described spices slow release layer (2) is coated on the outside of described rope matrix (1) by PVC or PU coating.
2. fragrant rope according to claim 1 is characterized in that, described rope matrix (1) is nylon torsade, terylene torsade, polypropylene fibre torsade, cotton torsade, nylon sennit, terylene sennit, polypropylene fibre sennit and cotton sennit.
3. the preparation method of fragrant rope according to claim 1 is characterized in that, realizes as follows:
1) preparation slowly-releasing perfume microcapsule, at first take by weighing gelatin, essence and OP-10 that weight proportion is 90-98%:1-5%:1-5%, adding distilled water mixes the back 55-70 ℃ of dissolving down, 5000 rev/mins rotating speed emulsification, the emulsion that emulsification obtains is poured in the there-necked flask after the dissolving, adding distil water, regulating the pH value is 6.0-6.5, and 60 ℃ of reactions added glutaraldehyde cross-linking 1-2 hour at last, suction filtration, oven dry obtains microcapsules;
2) preparation slowly-releasing perfume microcapsule dressing liquid adds functional aid and distilled water with slowly-releasing perfume microcapsule solution, and magnetic agitation is to mixing in beaker;
3) rope matrix is put into cleaning solution and soaks, the oil stain on the flush away rope, with slowly-releasing perfume microcapsule dressing liquid by coating, pad or immersion coating on rope matrix, under 35-90 ℃, bake 10min-30min, dry, form the spices slow release layer;
4) coated rope matrix is put into cleaning solution and soak, dry and get product.
4. the preparation method of fragrant rope according to claim 3 is characterized in that, coating in the described step 3) adopts a kind of in blade coating, spraying, flow coat or the electro-deposition.
5. the preparation method of fragrant rope according to claim 3, it is characterized in that described step 2) the middle function additive employing tackifier that adopt, flexibilizer, plasticizer, thickener, diluent, solvent, coupling agent, emulsifying agent, filler, reinforcing agent, curing agent, crosslinking agent, initator, light trigger, catalyst, promoter, polymerization inhibitor, oxidant, softening agent, age resistor, dispersant, blowing agent, defoamer, levelling agent, colouring agent, toner, bleeding agent, wetting agent, neutralizer, sagging inhibitor, anti skinning agent, drier, anti-adhesion agent, antifreezing agent, antistatic additive, the flavor agent disappears, antiseptic, mould inhibitor, mite-proof agent, anophelifuge, in fire retardant or the ultra-violet absorber one or more.
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| CN105369609A (en) * | 2015-12-21 | 2016-03-02 | 常熟市一心无纺制品有限公司 | Fragrant non-woven fabric |
| CN105887387A (en) * | 2016-04-25 | 2016-08-24 | 广东鹏运实业有限公司 | After-finishing method for increasing nano-antibacterial effect of knitting garments |
| CN107724095A (en) * | 2017-09-15 | 2018-02-23 | 南通香佳纺织科技有限公司 | A kind of microcapsules necktie finishing agent and preparation method thereof |
| CN107916567A (en) * | 2017-12-18 | 2018-04-17 | 太和县双飞绳业有限公司 | A kind of preparation method of the fragrant rope made of hemp |
| CN109403108A (en) * | 2018-09-04 | 2019-03-01 | 李丹 | A kind of pre-buried rope removing plastics peculiar smell |
| CN109750498A (en) * | 2017-11-02 | 2019-05-14 | 丹阳八紫光能有限公司 | A kind of sofa cloth with aromatic odor |
| CN110592801A (en) * | 2019-10-09 | 2019-12-20 | 鲁普耐特集团有限公司 | Multifunctional decorative rope and manufacturing method thereof |
| CN111074550A (en) * | 2019-12-20 | 2020-04-28 | 陈强 | Textile processing technology |
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| CN110592801A (en) * | 2019-10-09 | 2019-12-20 | 鲁普耐特集团有限公司 | Multifunctional decorative rope and manufacturing method thereof |
| CN111074550A (en) * | 2019-12-20 | 2020-04-28 | 陈强 | Textile processing technology |
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