CN102493207A - Method for preparing regenerated cellulose fabric with calming healthcare effect - Google Patents
Method for preparing regenerated cellulose fabric with calming healthcare effect Download PDFInfo
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- CN102493207A CN102493207A CN2011104011514A CN201110401151A CN102493207A CN 102493207 A CN102493207 A CN 102493207A CN 2011104011514 A CN2011104011514 A CN 2011104011514A CN 201110401151 A CN201110401151 A CN 201110401151A CN 102493207 A CN102493207 A CN 102493207A
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- regenerated cellulose
- sweet orange
- essential oil
- lining
- orange essential
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Abstract
The invention relates to a method for preparing a regenerated cellulose fabric with a calming healthcare effect. The method comprises the following steps of: (1) adding sweet orange oil into polyurethane and water, stirring, adding a microcapsule solution, fully stirring, adding a dispersing agent, an adhesive and a softening agent, and stirring to obtain a sweet orange oil microcapsule finishing agent; (2) coating the sweet orange oil microcapsule finishing agent on a regenerated cellulose fabric; and (3) performing after finishing on the regenerated cellulose fabric coated with the sweet orange oil microcapsule finishing agent in the step (2). The preparation method is easy to operate; a natural extract, namely the sweet orange oil is prepared into the microcapsule finishing agent safely in an environment-friendly way; and the regenerated cellulose fabric with the calming healthcare effect can durably and uniformly release sweet orange fragrance, and has a wide application prospect.
Description
Technical field
The invention belongs to the preparation field of functional regenerated cellulose lining, particularly a kind of preparation method with regenerated cellulose lining of calm health-care function.
Background technology
The pure natural plant essential oil is little with its character mitigation, beauty treatment, health care, toxic and side effect, more and more receives people's favor.Sweet orange essential oil (orange) extracts from pericarp.Sweet orange is that minority is proved to be one of contrastimulant essential oil; The sweet orange essential oil that sweet orange fragrance is arranged, this essential oil molecule is very little, and the tiny ability rapid permeability that arrives is to blood vessel and lymph; Stimulate circulation, the carbon dioxide and the metabolic waste metabolism of being detained are in vivo come out.Can expel intense strain and pressure, improve the caused insomnia of anxiety; Owing to contain a large amount of Vitamin Cs in the orange peel; Can preventing cold, to skin have moistening effect, can balancing skin sour salty value, help collagen to form, for systemic growth and reparation favorable effects is arranged.Can promote sweating, thereby the skin that can help to block discharges toxin, all helpful to oiliness, dark sore or dry skin person.Yet the sweet orange essential oil is volatile, and smell is dense, and active ingredient is very easily oxidation in air, instability, and loss easily is not easy to storage, has limited the variation and the range of application thereof of transportation and formulation.
In the last few years, along with the raising of living standards of the people and rhythm of life, people required increasingly high to comfortableness, health, security and the feature of environmental protection etc. of textiles.After-finishing of textile products has become and has improved functions of textile fabrics and one of important channel of improving the product surcharge.Utilizing the capsule of nano technology to make textiles have functional is one of the focus of future development.The application of microcapsules technology in weaving mainly is aspect the arrangement of back; Various lining post-finishing agents can be processed the back arrangement that is used for lining behind the microcapsules, like depilation, gas defence, antifog, anti-soil, wrinkle resistant, shrinkproof, deodorization, heat storing and heat preserving, softness, fragrance, fire-retardant, antibiotic, antiultraviolet etc.Most modes with co-blended spinning or coating put on fiber or the lining, but co-blended spinning has relatively high expectations to equipment and technology content, also do not obtain large-scale production application.
At present also not with the sweet orange essential oil as the microcapsules inclusions, adopt certain process method for sorting that covers, process a kind of technology with regenerated cellulose lining of calm health-care function.
Summary of the invention
Technical problem to be solved by this invention provides a kind of preparation method with regenerated cellulose lining of calm health-care function; This method is simple to operate; Safety and environmental protection, this lining can lastingly, evenly discharge sweet orange fragrance, can expel intense strain and pressure, improve the caused insomnia of anxiety; For systemic growth and reparation favorable effects is arranged, have a extensive future.
A kind of preparation method with regenerated cellulose lining of calm health-care function of the present invention comprises:
(1) preparation sweet orange essential oil microcapsules finishing agent
Under 35-45 ℃, the sweet orange essential oil is added in polyurethanes and the water, stirred 1～2 minute; Add microcapsule solution then, fully stir into emulsion form after, add dispersant; Stirred 1～3 minute, and added adhesive, stirred 3～5 minutes; Stirred 3～5 minutes after adding softener again, obtain sweet orange essential oil microcapsules finishing agent;
(2) above-mentioned sweet orange essential oil microcapsules finishing agent is covered be added on the regenerated cellulose lining, the process that obtains is covered the regenerated cellulose lining with sweet orange essential oil microcapsules finishing agent;
(3) the regenerated cellulose lining that above-mentioned process is covered with sweet orange essential oil microcapsules finishing agent carries out the back arrangement, promptly gets the regenerated cellulose lining of the health-care function of calming.
The component of the sweet orange essential oil microcapsules finishing agent described in the step (1) comprises by mass percentage: sweet orange essential oil 20～30%, adhesive 10～25%, polyurethanes 3%, softener 3～5%, microcapsule solution 20%, dispersant 1～3%, water surplus.
Sweet orange essential oil described in the step (1) is the orange peel natural extract; Described adhesive is an acrylic resin; Described softener can adopt silicon series softener, organosilicon; Described microcapsule solution is for adopting the preparation of gelatin or instant Arabic gum; Described dispersant is the ZD resin.
The described speed that stirs in the emulsion form that fully stirs into of step (1) is 1500～2000 rev/mins.
Covering described in the step (2) adds for adopting spraying process, padding method or infusion process to handle; Wherein spraying process is handled for directly spray oven dry at fiber surface; Liquid carrying rate is 100% in the padding method; Infusion process is earlier through dipping, then after the calendering in 80-100 ℃ of dehydration.
Back arrangement described in the step (3) is carried out calendering for regenerated cellulose lining that described process is covered with sweet orange essential oil microcapsules finishing agent, through 80～100 ℃ of preliminary dryings 3～5 minutes, finalizes the design in 140～160 ℃ at last and cures 3～5 minutes then.
Sweet orange essential oil microcapsules finishing agent of the present invention through covering process, makes the microcapsules that contain the sweet orange essential oil get in the regenerated celulose fibre under the effect of described softener, adhesive, dispersant.
The microcapsules particle diameter that contains the sweet orange essential oil that sweet orange essential oil and microcapsule solution form has different-diameter and wall thickness at 1～50 mu m range.Change the composition and the thickness of wall material, can control the rate of release and the quantity of microcapsules, prolong wear life.Can know according to detecting the gained data, when microcapsules quantity is 2,000,000/m
2When above, can wash more than 50 times by anti-washing machine.Mode of appearance is good; Be smooth, spherical; Covered effect, dispersiveness, slow release are good, add under the effect of adhesive, softener, dispersant, cover process through certain; The microcapsules that contain the sweet orange essential oil that make get in the regenerated celulose fibre, can discharge sweet orange fragrance for a long time, lentamente, equably.
In sum; Because the microcapsules particle diameter that contains the sweet orange essential oil that sweet orange essential oil and microcapsule solution form at 1～50 mu m range, has different-diameter and wall thickness, mode of appearance is good among the present invention; Be smooth, spherical; Covered effect, favorable dispersibility very easily get into and are attached in the regenerated celulose fibre, therefore can discharge sweet orange fragrance for a long time, lentamente, equably.Lining of the present invention is made into clothing; Bedding, medical supplies and other textiless are through the friction in the process of taking with deflect; The microcapsules rupture that contains the sweet orange essential oil; Discharge sweet orange fragrance, get into the brain nervous centralis, can expel intense strain and pressure, improve the caused insomnia of anxiety through respiratory system.Through with the contacting of skin, the sour salty value of balancing skin, help collagen to form, for systemic growth and reparation favorable effects is arranged.
Preparation method of the present invention has the pure natural of employing extract and does not contain any chemical harmful components, with state-of-the-art capsule of nano slow release method, can lastingly, evenly discharge sweet orange fragrance.Adopt the nanoscale microcapsules, can not influence the comfort level of fabric itself.
Beneficial effect
(1) preparation method of the present invention is simple to operate, adopts pure natural extract sweet orange essential oil to prepare microcapsule dressing agent, safety and environmental protection;
(2) the regenerated cellulose lining of calm health-care function of the present invention can lastingly, evenly discharge sweet orange fragrance; Can expel intense strain and pressure, improve the caused insomnia of anxiety; For systemic growth and reparation favorable effects is arranged, have a extensive future.
The specific embodiment
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only to be used to the present invention is described and be not used in the restriction scope of the present invention.Should be understood that in addition those skilled in the art can do various changes or modification to the present invention after the content of having read the present invention's instruction, these equivalent form of values fall within the application's appended claims institute restricted portion equally.
Embodiment 1
With following each component as follows according to the mass percent batching: sweet orange essential oil 20Kg, adhesive-107 glue 11Kg, polyurethanes 3Kg, softener-organosilicon 3Kg, microcapsule solution 20Kg, dispersant-ZD 3Kg, water 40Kg amounts to 100Kg.
Under 35 ℃, earlier 20Kg sweet orange essential oil is put into 3Kg polyurethanes and 40Kg water, stirred 1 minute with 1500 rev/mins rotating speeds; Add microcapsule solution and fully stir, after becoming emulsion form, add ZD 3Kg successively after; Stirred 1-3 minute, add 107 glue 11Kg after, stirred 5 minutes; Stirred 3 minutes after adding organosilicon 3Kg again, it is subsequent use to process sweet orange essential oil microcapsules finishing agent;
The woven lining of cotton type viscose staple fibre two is soaked two and rolls in microcapsule dressing agent, take out lining, the wherein liquid carrying rate 100% of lining.After the lining that will in microcapsule dressing agent, pad carries out calendering, get into qualitative the curing 3 minutes of 140 degree after 3 minutes through 80 degree preliminary dryings; Promptly obtain microcapsules artificial cotton lining with the sweet orange essential oil.
Embodiment 2
With following each component as follows according to the mass percent batching: sweet orange essential oil 25Kg, adhesive-107 glue 15Kg, polyurethanes 3Kg, softener-organosilicon 4Kg, microcapsule solution 20Kg, dispersant-ZD3Kg, water 30Kg amounts to 100Kg.
Under 40 ℃, earlier 25Kg sweet orange essential oil is put into the water of 3Kg polyurethanes and 30Kg, stirred 1 minute with 1700 rev/mins rotating speeds; Add microcapsule solution and fully stir, after becoming emulsion form, add ZD 3Kg successively after; Stirred 1-3 minute, add 107 glue 15Kg after, stirred 5 minutes; Stirred 3 minutes after adding organosilicon 4Kg again, it is subsequent use to process sweet orange essential oil microcapsules finishing agent;
Adopt spraying coating process with microcapsule dressing agent, be sprayed on the woven lining of koplon (polynosic), take out lining, the wherein coverage rate 100% of microcapsule dressing agent on the lining.After will carrying out calendering with the lining that microcapsule dressing agent sprayed, get into qualitative the curing 4 minutes of 150 degree after 4 minutes through 90 degree preliminary dryings; Promptly obtain microcapsules high wet modulus viscosity glue lining with the sweet orange essential oil.
Embodiment 3
With following each component as follows according to the mass percent batching: sweet orange essential oil 20Kg, adhesive-107 glue 25Kg, polyurethanes 3Kg, softener-organosilicon 5Kg, microcapsule solution 20Kg, dispersant-ZD 1Kg, water 26Kg amounts to 100Kg.
Under 45 ℃, earlier 20Kg sweet orange essential oil is put into the water of 3Kg polyurethanes and 26Kg, stirred 2 minutes with 1800 rev/mins rotating speeds; Add microcapsule solution and fully stir, after becoming emulsion form, add ZD 1Kg successively after; Stirred 1-3 minute, add 107 glue 25Kg after, stirred 5 minutes; Stirred 3 minutes after adding organosilicon 3Kg again, it is subsequent use to process sweet orange essential oil microcapsules finishing agent;
Adopt impregnation technology with microcapsule dressing agent, evenly be coated with on the woven lining of shop solvent-borne type regenerated celulose fibre (Lyocell), take out lining, the wherein coverage rate 100% of microcapsule dressing agent on the lining; After will carrying out calendering with the lining that the microcapsule dressing agent coating is crossed, dehydration is 5 minutes under 80 degree, gets into qualitative the curing 5 minutes of 160 degree after 5 minutes through 100 degree preliminary dryings; Promptly obtain microcapsules regenerated cellulose lining with the sweet orange essential oil.
Claims (6)
1. preparation method with regenerated cellulose lining of calm health-care function comprises:
(1) under 35-45 ℃, the sweet orange essential oil is added in polyurethanes and the water, stirred 1～2 minute; Add microcapsule solution then, fully stir into emulsion form after, add dispersant; Stirred 1～3 minute, and added adhesive, stirred 3～5 minutes; Stirred 3～5 minutes after adding softener again, obtain sweet orange essential oil microcapsules finishing agent;
(2) above-mentioned sweet orange essential oil microcapsules finishing agent is covered be added on the regenerated cellulose lining, the process that obtains is covered the regenerated cellulose lining with sweet orange essential oil microcapsules finishing agent;
(3) the regenerated cellulose lining that above-mentioned process is covered with sweet orange essential oil microcapsules finishing agent carries out the back arrangement, promptly gets the regenerated cellulose lining of the health-care function of calming.
2. a kind of preparation method with regenerated cellulose lining of calm health-care function according to claim 1 is characterized in that: the component of the sweet orange essential oil microcapsules finishing agent described in the step (1) comprises: sweet orange essential oil 20～30% by mass percentage; Adhesive 10～25%; Polyurethanes 3%, softener 3～5%, microcapsule solution 20%; Dispersant 1～3%, water surplus.
3. a kind of preparation method according to claim 1 with regenerated cellulose lining of calm health-care function, it is characterized in that: the sweet orange essential oil described in the step (1) is the orange peel natural extract; Described adhesive is an acrylic resin; Described softener is an organosilicon; Described microcapsule solution is for adopting the preparation of gelatin or instant Arabic gum; Described dispersant is the ZD resin.
4. a kind of preparation method with regenerated cellulose lining of calm health-care function according to claim 1 is characterized in that: the described speed that stirs in the emulsion form that fully stirs into of step (1) is 1500～2000 rev/mins.
5. a kind of preparation method with regenerated cellulose lining of calm health-care function according to claim 1 is characterized in that: covering described in the step (2) adds for adopting spraying process, padding method or infusion process to handle; Wherein spraying process is handled for directly spray oven dry at fiber surface; Liquid carrying rate is 100% in the padding method; Infusion process is earlier through dipping, then after the calendering in 80-100 ℃ of dehydration.
6. a kind of preparation method according to claim 1 with regenerated cellulose lining of calm health-care function; It is characterized in that: the back arrangement described in the step (3) is carried out calendering for the regenerated cellulose lining that described process is covered with sweet orange essential oil microcapsules finishing agent; Through 80～100 ℃ of preliminary dryings 3～5 minutes, finalize the design in 140～160 ℃ at last and cure 3～5 minutes then.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2011104011514A CN102493207A (en) | 2011-12-06 | 2011-12-06 | Method for preparing regenerated cellulose fabric with calming healthcare effect |
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| CN2011104011514A CN102493207A (en) | 2011-12-06 | 2011-12-06 | Method for preparing regenerated cellulose fabric with calming healthcare effect |
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| CN102493207A true CN102493207A (en) | 2012-06-13 |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103290700A (en) * | 2013-05-31 | 2013-09-11 | 山东鲁普科技有限公司 | Aromatic rope and manufacturing method thereof |
| CN103343455A (en) * | 2013-06-21 | 2013-10-09 | 黄惠标 | Aromatic fabric production method |
| CN107345365A (en) * | 2016-05-04 | 2017-11-14 | 无限手巾有限公司 | Fragrant towel manufacture method and fragrant towel |
| CN110804859A (en) * | 2019-10-25 | 2020-02-18 | 嘉兴市秀洲恒丰纺织有限公司 | Finishing process of vitamin skin-care health-care cellulose fabric |
| CN110820358A (en) * | 2019-10-25 | 2020-02-21 | 嘉兴市秀洲恒丰纺织有限公司 | Finishing process of vitamin skin-care health-care real silk fabric |
| CN111020868A (en) * | 2019-12-30 | 2020-04-17 | 稳健医疗用品股份有限公司 | Mask, mask lining and mask manufacturing method |
| CN115522392A (en) * | 2022-06-16 | 2022-12-27 | 李庆生 | Aromatic fiber containing rose essential oil and preparation method thereof |
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| JP2005248410A (en) * | 2004-03-01 | 2005-09-15 | Aoki International Co Ltd | Method for producing aromatic fabric |
| CN101403182A (en) * | 2008-11-06 | 2009-04-08 | 吴张江 | Skin-protection health-care fabric functional finishing agent and use thereof |
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Patent Citations (4)
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| JP2005248410A (en) * | 2004-03-01 | 2005-09-15 | Aoki International Co Ltd | Method for producing aromatic fabric |
| CN101403182A (en) * | 2008-11-06 | 2009-04-08 | 吴张江 | Skin-protection health-care fabric functional finishing agent and use thereof |
| CN101838933A (en) * | 2009-03-20 | 2010-09-22 | 李江陵 | Sleeping-aided fabric and manufacturing method thereof |
| CN102008149A (en) * | 2011-01-08 | 2011-04-13 | 石国明 | Method for manufacturing deodorant shoe and deodorant shoe |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103290700A (en) * | 2013-05-31 | 2013-09-11 | 山东鲁普科技有限公司 | Aromatic rope and manufacturing method thereof |
| CN103343455A (en) * | 2013-06-21 | 2013-10-09 | 黄惠标 | Aromatic fabric production method |
| CN103343455B (en) * | 2013-06-21 | 2015-07-29 | 江苏圣夫岛纺织生物科技有限公司 | A kind of production method of aromatic fabrics |
| CN107345365A (en) * | 2016-05-04 | 2017-11-14 | 无限手巾有限公司 | Fragrant towel manufacture method and fragrant towel |
| CN110804859A (en) * | 2019-10-25 | 2020-02-18 | 嘉兴市秀洲恒丰纺织有限公司 | Finishing process of vitamin skin-care health-care cellulose fabric |
| CN110820358A (en) * | 2019-10-25 | 2020-02-21 | 嘉兴市秀洲恒丰纺织有限公司 | Finishing process of vitamin skin-care health-care real silk fabric |
| CN111020868A (en) * | 2019-12-30 | 2020-04-17 | 稳健医疗用品股份有限公司 | Mask, mask lining and mask manufacturing method |
| CN115522392A (en) * | 2022-06-16 | 2022-12-27 | 李庆生 | Aromatic fiber containing rose essential oil and preparation method thereof |
| CN115522392B (en) * | 2022-06-16 | 2024-03-01 | 李庆生 | Aromatic fiber containing rose essential oil and preparation method thereof |
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Application publication date: 20120613 |