JP2005248410A - Method for producing aromatic fabric - Google Patents
Method for producing aromatic fabric Download PDFInfo
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- JP2005248410A JP2005248410A JP2004093731A JP2004093731A JP2005248410A JP 2005248410 A JP2005248410 A JP 2005248410A JP 2004093731 A JP2004093731 A JP 2004093731A JP 2004093731 A JP2004093731 A JP 2004093731A JP 2005248410 A JP2005248410 A JP 2005248410A
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- fabric
- aromatic
- microcapsules
- essential oil
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- 239000004744 fabric Substances 0.000 title claims abstract description 28
- 125000003118 aryl group Chemical group 0.000 title claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 title abstract description 8
- 239000003094 microcapsule Substances 0.000 claims abstract description 23
- 239000000341 volatile oil Substances 0.000 claims abstract description 11
- 239000002245 particle Substances 0.000 claims abstract description 10
- 239000011230 binding agent Substances 0.000 claims abstract description 6
- 229920005989 resin Polymers 0.000 claims abstract description 6
- 239000011347 resin Substances 0.000 claims abstract description 6
- 235000013311 vegetables Nutrition 0.000 claims abstract description 6
- 229920001059 synthetic polymer Polymers 0.000 claims abstract description 3
- 238000000034 method Methods 0.000 claims description 10
- 239000000126 substance Substances 0.000 claims description 3
- 239000000835 fiber Substances 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 5
- 238000000222 aromatherapy Methods 0.000 abstract description 3
- 239000002759 woven fabric Substances 0.000 abstract description 3
- 230000002688 persistence Effects 0.000 abstract 1
- 238000002386 leaching Methods 0.000 description 5
- 210000002268 wool Anatomy 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 2
- 244000178870 Lavandula angustifolia Species 0.000 description 2
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 230000035876 healing Effects 0.000 description 2
- 239000001102 lavandula vera Substances 0.000 description 2
- 235000018219 lavender Nutrition 0.000 description 2
- 241001474374 Blennius Species 0.000 description 1
- 240000008564 Boehmeria nivea Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 description 1
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 description 1
- 235000007866 Chamaemelum nobile Nutrition 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 244000004281 Eucalyptus maculata Species 0.000 description 1
- 241000219146 Gossypium Species 0.000 description 1
- 238000012695 Interfacial polymerization Methods 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- 244000042664 Matricaria chamomilla Species 0.000 description 1
- 235000007232 Matricaria chamomilla Nutrition 0.000 description 1
- 229920000877 Melamine resin Polymers 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 244000179970 Monarda didyma Species 0.000 description 1
- 235000010672 Monarda didyma Nutrition 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 235000010676 Ocimum basilicum Nutrition 0.000 description 1
- 240000007926 Ocimum gratissimum Species 0.000 description 1
- 235000011203 Origanum Nutrition 0.000 description 1
- 240000000783 Origanum majorana Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 244000178231 Rosmarinus officinalis Species 0.000 description 1
- 240000000513 Santalum album Species 0.000 description 1
- 235000008632 Santalum album Nutrition 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 229940035676 analgesics Drugs 0.000 description 1
- 239000000730 antalgic agent Substances 0.000 description 1
- 230000001139 anti-pruritic effect Effects 0.000 description 1
- 239000003908 antipruritic agent Substances 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 125000003289 ascorbyl group Chemical class [H]O[C@@]([H])(C([H])([H])O*)[C@@]1([H])OC(=O)C(O*)=C1O* 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 235000005607 chanvre indien Nutrition 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000007730 finishing process Methods 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000006996 mental state Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 230000008433 psychological processes and functions Effects 0.000 description 1
- 239000002964 rayon Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 125000002640 tocopherol group Chemical class 0.000 description 1
- 235000019149 tocopherols Nutrition 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- -1 wool Substances 0.000 description 1
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- Fats And Perfumes (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
Description
本発明は、人の心身を癒すという生理心理学機能性を布帛に持たせる芳香布帛の製造方法に関する。 The present invention relates to a method for producing an aromatic fabric in which the fabric has a physiological psychological function of healing human mind and body.
従来、皮膚の生理的状態(痒み、痛み、かさつき等)を改善する作用を有する物質(例えば、アスコルビン酸類、トコフェロール類、海藻エキス、鎮痒剤、鎮痛剤)や芳香剤を内蔵したマイクロカプセルを、繊維製品(例えば、ストッキング、下着類、まくら等)に付着させ、着用あるいは使用時に、意図的な摩擦でマイクロカプセルを破砕、ひび割れさせることで、内蔵の成分を徐々に浸出させ、皮膚の生理的状態の改善や快眠を導くといった技術が開示されている(特許第2562233号)。 Conventionally, microcapsules containing substances (such as ascorbic acids, tocopherols, seaweed extracts, antipruritics, analgesics) and fragrances that have an effect of improving the physiological state of the skin (itch, pain, roughness, etc.) It is attached to textile products (eg, stockings, underwear, pillows, etc.), and when worn or used, the microcapsules are crushed and cracked with intentional friction to gradually leach out the built-in components, thereby physiology of the skin A technique for improving the mental state and leading to a good sleep is disclosed (Japanese Patent No. 2562233).
ところが、上記従来技術によるマイクロカプセルは、その粒子径が2〜300μmと大きいため、これを繊維の一本々に確実に付着させることができず、その結果、織物などの繊維集合体には高密度付着が困難となって、マイクロカプセル破砕による浸出内蔵成分の余芳性や浸出持続性を向上させることができない。また、その壁膜の膜厚も0.3〜4μmと厚いため、大きな粒子径と相俟って、これを繊維に付着させても繊維の風合いが硬くなるおそれも生じている。 However, the microcapsules according to the above prior art have a particle size as large as 2 to 300 μm, so that they cannot be reliably attached to individual fibers. It becomes difficult to adhere to the density, and it is not possible to improve the fragility and leaching sustainability of the leaching built-in component by crushing the microcapsules. Moreover, since the wall film thickness is as thick as 0.3 to 4 μm, there is a possibility that the texture of the fiber becomes hard even if it is attached to the fiber, coupled with the large particle diameter.
本発明者は、上記の課題がマイクロカプセルの粒子径と壁膜の膜厚にあることを突き止め、これらを微小値で形成し、内臓の成分を天然植物性芳香精油にすることで、上記課題を解決でき、アロマテラピー効果をも実現することができることを見出し、本発明を完成させた。 The present inventor has found that the above problems are the particle size of the microcapsule and the film thickness of the wall film, and that these are formed with minute values, and the components of the internal organs are natural plant aromatic essential oils. And the present invention has been completed by finding that an aromatherapy effect can be realized.
すなわち、上記課題を解決する本発明は、天然植物性芳香精油を内蔵させた合成高分子物質からなるマイクロカプセルであって、粒子径が平均1μm以下の範囲にあり、壁膜が平均0.1μm以下の膜厚を持つマイクロカプセルを、織物の仕上加工段階において、バインダー樹脂によって布帛に担持させることを特徴とする芳香布帛の製造方法である。 That is, the present invention for solving the above-mentioned problems is a microcapsule made of a synthetic polymer substance containing a natural vegetable aromatic essential oil, having an average particle size of 1 μm or less and an average wall membrane of 0.1 μm. A method for producing an aromatic fabric, characterized in that a microcapsule having the following film thickness is supported on a fabric by a binder resin in a finishing process of the fabric.
本発明方法によると、マイクロカプセルを、繊維の一本々に確実に付着させることができ、繊維集合体としても高密度付着が実現するので、織物などの繊維集合体の風合いをソフトに仕上げることができる。また、マイクロカプセルの粒子径や壁膜の膜厚の微小値化は、内蔵の天然植物性芳香精油の浸出を緩やかにするので、長時間に亘って芳香を放散させることができ、その余芳性や浸出持続性が遥かに向上する。さらに、天然植物性芳香精油の浸出が、これを嗅ぐ人の心身を癒し、アロマテラピー効果を実現することができる。 According to the method of the present invention, the microcapsules can be reliably attached to individual fibers, and high-density adhesion can be realized as a fiber assembly, so that the texture of the fiber assembly such as a fabric can be finished softly. Can do. The microcapsule particle size and the wall film thickness are made minute, which slows the leaching of the built-in natural plant aromatic essential oil, allowing the fragrance to be diffused over a long period of time. And the leaching sustainability is greatly improved. Furthermore, the leaching of natural vegetable aromatic essential oils can heal the mind and body of the person who smells it and realize an aromatherapy effect.
本発明方法を実現させるマイクロカプセルは、IN SITE重合法や界面重合法などの公知の方法によって製造することができる。その際、粒子径を平均1μm以下の範囲にするには、マイクロカプセル製造時の撹拌の強弱や乳化剤の濃度設定により行なうことができる。また、壁膜の膜厚を平均0.1μm以下にするには、油滴中の尿素又はメラミンの濃度コントロールにより行なうことができる。 The microcapsule for realizing the method of the present invention can be produced by a known method such as an IN SITE polymerization method or an interfacial polymerization method. At that time, the average particle size can be adjusted to 1 μm or less by adjusting the strength of stirring during the production of the microcapsules and setting the concentration of the emulsifier. Further, the average film thickness of the wall film can be 0.1 μm or less by controlling the concentration of urea or melamine in the oil droplets.
マイクロカプセルに内蔵させる天然植物性芳香精油としては、ラベンダー精油が最も好ましいが、この他、例えば、カモミール、レモン、サンダルウッド、ジャスミン、バジル、ローズ、ペパーミント、ベルガモット、マージョラム、ユーカリ、ローズマリーなどの精油を使用することも可能である。 Lavender essential oil is most preferable as a natural vegetable aromatic essential oil incorporated in the microcapsule, but other examples include chamomile, lemon, sandalwood, jasmine, basil, rose, peppermint, bergamot, marjoram, eucalyptus, rosemary and the like. It is also possible to use essential oils.
マイクロカプセルを布帛に担持させるバインダー樹脂は、シリコン系、ウレタン系、酢酸ビニル系、アクリル系、フェノール系など公知のものであれば特に限定されるものではないが、ゴム状皮膚を形成するシリコン系やウレタン系などの樹脂が耐久性及び圧力緩衝性の点で好ましい。 The binder resin for supporting the microcapsules on the cloth is not particularly limited as long as it is a known one such as silicon, urethane, vinyl acetate, acrylic, phenol, etc., but is a silicone that forms rubbery skin. And urethane resins are preferred in terms of durability and pressure buffering properties.
また、マイクロカプセルを担持させる布帛としては、ウール、ウールと他繊維の混紡、ウールと他繊維との交織あるいは交編、綿、麻、ラミーなどのセルロース系天然繊維、ポリエステル、レーヨン、ナイロンなどの合成繊維が適用される。 In addition, as fabrics for supporting microcapsules, wool, blends of wool and other fibers, woven or knitted wool and other fibers, cellulosic natural fibers such as cotton, hemp, ramie, polyester, rayon, nylon, etc. Synthetic fibers are applied.
ラベンダー精油を内蔵し、粒子径平均1μm以下で、壁膜が平均0.1μm以下の膜厚を持つマイクロカプセルを公知の製造方法により得た。このラベンダー内蔵マイクロカプセルの適宜量を、0.5〜5%溶液のウレタン系バインダー樹脂とともに適宜量の水の入ったパッド槽1内に入れ、撹拌して処理溶液とした。布帛Cは複数のガイドローラ2によってパッド槽1内の付着溶液中を経て絞りローラ3に導かれた後、乾燥機4を通過するようになっている。布帛Cがパッド槽1内の処理溶液を通過する間に、布帛Cはバインダー樹脂によってラベンダー内蔵マイクロカプセルを吸収、吸着する。その後、布帛Cは乾燥機4に導かれ、80℃〜120℃で乾燥され、これで、布帛Cにはラベンダー内蔵マイクロカプセルが熱固着され、担持される。布帛Cに担持されたラベンダー内蔵マイクロカプセルは、上記のようにその粒子径と膜厚が微小値となっているため、布帛Cへの高密度付着が実現し、布帛C自体の風合いがソフトに仕上がっていた。 Microcapsules containing lavender essential oil, having an average particle size of 1 μm or less and a wall film thickness of 0.1 μm or less were obtained by a known production method. An appropriate amount of the lavender-embedded microcapsule was placed in a
22〜27歳の男性被験者20名により、本発明方法により製造した芳香布帛(織物)と未加工織物を用いて官能検査を行なった。検査は、対象物を直接嗅ぐ方法を採用した。その結果、未加工織物については何ら官能的回答はなかったが、芳香布帛では、「癒し」と答えた被験者が22%、「落ち着く」が16%、「さわやか」が27%、「清潔感」が22%「その他」が13%となり、87%の被験者がやすらぎ感による快適感を感じることが分かった。 A sensory test was performed by 20 male subjects aged 22-27 years old using an aromatic fabric (woven fabric) produced by the method of the present invention and a raw fabric. The inspection adopted a method of sniffing the object directly. As a result, there was no sensual answer for raw fabrics, but for aromatic fabrics, 22% of subjects answered “healing”, 16% “settled”, 27% “freshness”, “cleanliness” It was found that 22% of “Others” was 13%, and 87% of subjects felt a comfortable feeling of comfort.
1 パッド槽
2 ガイドローラ
3 絞りローラ
4 乾燥機
C 布帛1 Pad tank
2 Guide rollers
3 Drawing roller
4 dryers
C fabric
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JP2004093731A JP2005248410A (en) | 2004-03-01 | 2004-03-01 | Method for producing aromatic fabric |
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JP2004093731A JP2005248410A (en) | 2004-03-01 | 2004-03-01 | Method for producing aromatic fabric |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2008017957A (en) * | 2006-07-12 | 2008-01-31 | Aroma Space:Kk | Method for producing aroma generating mask |
CN102493207A (en) * | 2011-12-06 | 2012-06-13 | 东华大学 | Method for preparing regenerated cellulose fabric with calming healthcare effect |
ES2849826A1 (en) * | 2020-02-22 | 2021-08-23 | Patino Marcela Viviana Sinisterra | PAJAMAS WITH INTELLIGENT FABRIC (Machine-translation by Google Translate, not legally binding) |
-
2004
- 2004-03-01 JP JP2004093731A patent/JP2005248410A/en active Pending
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2008017957A (en) * | 2006-07-12 | 2008-01-31 | Aroma Space:Kk | Method for producing aroma generating mask |
CN102493207A (en) * | 2011-12-06 | 2012-06-13 | 东华大学 | Method for preparing regenerated cellulose fabric with calming healthcare effect |
ES2849826A1 (en) * | 2020-02-22 | 2021-08-23 | Patino Marcela Viviana Sinisterra | PAJAMAS WITH INTELLIGENT FABRIC (Machine-translation by Google Translate, not legally binding) |
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