CN102720070A - Esthetic carpet fragrance microcapsule finishing agent and preparation thereof - Google Patents
Esthetic carpet fragrance microcapsule finishing agent and preparation thereof Download PDFInfo
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- CN102720070A CN102720070A CN201210228818XA CN201210228818A CN102720070A CN 102720070 A CN102720070 A CN 102720070A CN 201210228818X A CN201210228818X A CN 201210228818XA CN 201210228818 A CN201210228818 A CN 201210228818A CN 102720070 A CN102720070 A CN 102720070A
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Abstract
The invention relates to an esthetic carpet fragrance microcapsule finishing agent and preparation thereof. The finishing agent comprises, by mass, 5% -30% of fragrance microcapsules, 4%-50% of synthetic rubber latex, and the balance water. The method specifically comprises that the fragrance microcapsule finishing agent is added to backing lining glue of an esthetic carpet fabric, performing drying trough a coating process, and the method is completed. According to the esthetic carpet fragrance microcapsule finishing agent and the preparation thereof, the process is simple, the method can be applied to the esthetic carpet fabric conveniently, no special device is added, dehydration is not required, the processing temperature is easy to achieved, continuous production can be conducted, the esthetic carpet fabrics finished by the method have lasting fragrance, the villose surface appearance effects of small carpets are not effected, the effect is good and free from damage, and the fragrance can last for more than one year.
Description
Technical field
The invention belongs to odor type art square field, particularly a kind of art square fragrant microcapsule finishing agent and application thereof.
Background technology
Aromatic props has the function of adjustment nerve system of human body because it produces psychology and physiological health-care function to the people, receives people's welcome, has occurred a lot of fragrant fabrics on the market in succession.Its technology generally is divided into two kinds: 1, adopt liquid essence or other organic solution, make its essence can be coated with slip and carry out evenly miscible and anchor at by the effect of adhesive in the coating; 2, in order to protect essence to avoid the influence of external environment, control or prolong it and release the fragrant time limit and reach the application target of people spices, essence is carried out microencapsulation handle.For example; Disclosed a kind of fragrant fabric of Chinese invention patent application CN1301898A and manufacturing approach thereof adopt the mixture of microcapsules, adhesive and the water of aromatic component that fabric is flooded, after the roll compacting dehydration; Under 100 ~ 160 ℃, carry out drying; Obtain fragrant fabric, the adhesive that wherein adopts belongs to high temperature adhesive, need under 100 ~ 160 ℃, just can work.And a kind of fragrance after-finishing production process of silk flosssilk wadding is disclosed among the Chinese invention patent ZL200410065870.3, preparation perfume microcapsule maceration extract, the technical process of carrying out essence dipping, centrifugal dehydration, drying, dry to silk flosssilk wadding.For the art square fabric, these technical process all are not suitable for.High temperature drying can bring essence to volatilize in a large number, and aroma-keeping time is short.And technologies such as employing centrifugal dehydration only are fit to the production of batch (-type), easy water absorbing fabric, and the particle of essence microcapsule is too small, and the spices of its parcel is limited, holds perfume (or spice) and releases fragrant limited time; Particle is excessive, especially to the art square fabric, solids occur at the art square fiber surface easily, influences appearance effect.
Summary of the invention
Technical problem to be solved by this invention provides a kind of art square fragrant microcapsule finishing agent and application thereof; The art square fabric of putting in order through the present invention has lasting fragrance; And do not influence little, carpet matte appearance effect, powerful not damaged, fragrance can keep more than 1 year.
A kind of art square fragrant microcapsule finishing agent of the present invention, its component comprises: by mass percentage,
Nano fragrant microcapsules 5% ~ 30%;
Synthetic rubber latex 4% ~ 50%;
Water surplus.
Fragrant microcapsule finishing agent component comprises: by mass percentage,
Nano fragrant microcapsules 5%;
Synthetic rubber latex 15%;
Water surplus.
Said nano fragrant microcapsules are grapefruit essence microcapsule, lemon extract microcapsules, strawberry essence microcapsules, flavoring pineapple essence microcapsules, hundred Cupid's essence microcapsules, ancient imperial essence microcapsule, Forest Bath essence microcapsule, lavender essence microcapsule, cream jasmin france microcapsules, flavoring rose essence microcapsules, aloe essence microcapsule or sandalwood fragrance microcapsules.
Said nano fragrant microcapsules as wall material raw material, obtain nano fragrant microcapsules through situ aggregation method parcel essence by etherificate melamine resin performed polymer.
The concrete technology of preparation nano fragrant microcapsules: in the 250mL beaker, add 10g essence and 22g PDA (macromolecule emulsifier); Add deionized water to 100mL, at room temperature with 16, the speed emulsification 10min of 000r/min; Use the vinegar acid for adjusting pH value to 4-5 then, get the core emulsion;
Above-mentioned emulsion is poured in the 250mL round-bottomed flask, 7g trihydroxy melamine formal performed polymer dropwise is added in the above-mentioned emulsion, and then under the 200r/min mechanical agitation, slowly is warming up to 65 ℃, and insulation reaction 1.5h; After temperature is reduced to room temperature, 3g hexahydroxy melamine formal prepolymer solution slowly is added in the reaction system, is warming up to 75 ℃, and insulation reaction 2h.Reaction finishes after the cooling, with ammoniacal liquor regulate the pH value to 7-8 to finish reaction, microcapsules are filtered and use respectively benzinum and deionized water cyclic washing, filter, drying can obtain white capsule of nano powder.
Said synthetic rubber latex is commercially available.
A kind of application of art square fragrant microcapsule finishing agent, concrete steps are following: in the backing gluing of art square fabric, add the fragrant microcapsule finishing agent, through the photoresist coating process oven dry, get final product.
Purpose of design: a kind of art square fabric is provided, and through the arrangement of gum perfuming, art square can discharge fragrance, antibacterial for a long time, does not influence its matte appearance effect simultaneously.
Design:
1, adopting nanometer etherificate melamine resin essence microcapsule as one of composition of backing gluing, is one of technical characterictic of the present invention.The purpose of doing like this is: the fresh fragrance various health-care such as intense strain, calmness, deodorization, sterilization of releiving.In ancient times, people put the leaf of fragrant plant, flower etc. together with clothing, make the fragrance volatilization infiltrate the hole of clothes fiber, reach the purpose of clothing lasting.Perfume, face powder etc. had been arranged afterwards; People just are sprinkled upon these materials that contain essence on the clothing; But the perfuming textiles that these methods obtain, fragrance remaining time is very short, and washing back fragrance will disappear; Its reason be since in the essence organic principle complicacy that contains and chemical property extremely unstable, using with lay up period is volatile, scatter and disappear or decompose and go bad.Discover that essence microcapsule is a kind of novel functional fabric finishing agent.The nano fragrant microcapsules that the present inventor uses are as wall material raw material with etherificate melamine resin performed polymer; Wrap up the capsule of nano that liquid essence obtains through situ aggregation method; Melamine resin is a thermosetting resin; Heat resisting temperature>230 ℃, insoluble molten in the gum technical process, and have certain mechanical performance.
2, the carpet coating technique is the pith of putting in order behind the carpet, directly influences the quality of quality of carpet, as: fall hair, micelle, rubber, distortion, peculiar smell, soft durometer all is the quality problems that in photoresist coating process, very easily cause.The purpose of carpet backsizing is through applying latex suede bunch to be fixed with the blanket base; Prevent that carpet hooks two pile loops of the pile loop or the blanket back side because of hard thing in carrying or use junction is with the pile loop elongation or widen; Cause contiguous pile loop to dwindle, pile just differs.Gluing can increase the hardness of carpet simultaneously, and is abundant and smooth, increases the DIMENSIONAL STABILITY and the robustness of carpet, increases the service life.The gum main component of art square fabric is used latex exactly, and latex is divided into two types of natural rubber and synthetic rubber: synthetic rubber can dispose according to purposes, and applies easily, so be widely used in the carpet backing gluing.Emulsion has contained when dispatching from the factory outside the pesticide water softener, also should add filler (its granularity will at 5 μ m ~ 20 μ m) during configuration, surfactant, thickener and water.
Beneficial effect
(1) the art square fabric of putting in order through the present invention has lasting fragrance, and does not influence little, carpet matte appearance effect, and powerful not damaged, fragrance can keep more than 1 year;
(2) the art square fabric of putting in order through the present invention progressively discharges fragrance, and the pleasant aroma has fungistatic effect, and to human non-toxic, non-stimulated, no allergic reaction, is the environmental type technology;
(3) technology of the present invention is simple, and is especially convenient for the art square fabric, need not to add special installation, need not dehydration, and its processing temperature is prone to realize, can carries out continous mode production;
(4) because of the present invention contains nanometer technology and material, have characteristics such as high dispersive, can repeatedly wash practicality.
Description of drawings
Fig. 1 is the structural representation of art square fabric of the present invention; Wherein, 1 is the art square fabric face; 2 for containing the gum of nano essence microcapsules.
The specific embodiment
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only to be used to the present invention is described and be not used in the restriction scope of the present invention.Should be understood that in addition those skilled in the art can do various changes or modification to the present invention after the content of having read the present invention's instruction, these equivalent form of values fall within the application's appended claims institute restricted portion equally.
Embodiment 1
Gum technology: base blanket bottom surface gluing, hothouse oven dry, cooling.
Gum prescription: 5 parts of nanometer lavender essence microcapsules; 15 parts in synthetic rubber latex; Residue is water.Art square appearance of fabrics no change before and after the lavender spice finish, the bathroom pad blanket of processing gives out pleasant fragrance, gets into the toilet as getting into as the lavender garden sustainable 1 year of fragrance.
Gum technology: base blanket bottom surface gluing, hothouse oven dry, cooling.
The gum prescription: nanoforest is bathed 5 parts of essence microcapsules; 15 parts in synthetic rubber latex; Residue is water.Art square appearance of fabrics no change before and after the Forest Bath spice finish, blanket gives out pleasant fragrance before the bed of processing, and gets into the room as getting into forest, and fragrance is sustainable more than 1 year.
Claims (5)
1. art square fragrant microcapsule finishing agent, its component comprises: by mass percentage,
Nano fragrant microcapsules 5% ~ 30%;
Synthetic rubber latex 4% ~ 50%;
Water surplus.
2. a kind of art square fragrant microcapsule finishing agent according to claim 1, it is characterized in that: its component comprises: by mass percentage,
Nano fragrant microcapsules 5%;
Synthetic rubber latex 15%;
Water surplus.
3. a kind of art square fragrant microcapsule finishing agent according to claim 1 and 2 is characterized in that: said nano fragrant microcapsules are grapefruit essence microcapsule, lemon extract microcapsules, strawberry essence microcapsules, flavoring pineapple essence microcapsules, hundred Cupid's essence microcapsules, ancient imperial essence microcapsule, Forest Bath essence microcapsule, lavender essence microcapsule, cream jasmin france microcapsules, flavoring rose essence microcapsules, aloe essence microcapsule or sandalwood fragrance microcapsules.
4. a kind of art square fragrant microcapsule finishing agent according to claim 3 is characterized in that: said nano fragrant microcapsules as wall material raw material, obtain nano fragrant microcapsules through situ aggregation method parcel essence by etherificate melamine resin performed polymer.
5. the application of an art square fragrant microcapsule finishing agent as claimed in claim 1, it is characterized in that: concrete steps are following: in the backing gluing of art square fabric, add the fragrant microcapsule finishing agent, through the photoresist coating process oven dry, get final product.
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103184694A (en) * | 2013-03-19 | 2013-07-03 | 无锡翔隆高分子面料有限公司 | Nano microcapsule type dry garment piece, and preparation method and application thereof |
CN103233368A (en) * | 2013-05-08 | 2013-08-07 | 天津城市建设学院 | Preparation and applications of modified melamine resin essence microcapsule finishing agent |
CN103290700A (en) * | 2013-05-31 | 2013-09-11 | 山东鲁普科技有限公司 | Aromatic rope and manufacturing method thereof |
CN105369609A (en) * | 2015-12-21 | 2016-03-02 | 常熟市一心无纺制品有限公司 | Fragrant non-woven fabric |
CN106235817A (en) * | 2016-08-12 | 2016-12-21 | 张太平 | A kind of functional quilt core and processing technique thereof |
CN107119540A (en) * | 2017-05-22 | 2017-09-01 | 江苏共创人造草坪有限公司 | A kind of mosquito dispersing chinampa |
CN110130112A (en) * | 2019-05-27 | 2019-08-16 | 林炜 | A kind of embroidery lace screen cloth aromatizing process |
WO2020206989A1 (en) * | 2019-04-12 | 2020-10-15 | 江苏意瑞达纺织科技有限公司 | Preparation method for aromatic flannel household textile fabric |
CN113736371A (en) * | 2020-05-27 | 2021-12-03 | 深圳市准能新材料有限公司 | Environment-friendly water-based carpet back adhesive composition, back adhesive, preparation method of back adhesive and carpet |
CN114161809A (en) * | 2021-12-17 | 2022-03-11 | 罗秀芝 | Production process of antibacterial composite fabric and antibacterial composite fabric |
CN114230403A (en) * | 2022-01-18 | 2022-03-25 | 深圳市帝拓电子有限公司 | Product capable of emitting preparation for a long time |
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Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103184694A (en) * | 2013-03-19 | 2013-07-03 | 无锡翔隆高分子面料有限公司 | Nano microcapsule type dry garment piece, and preparation method and application thereof |
CN103184694B (en) * | 2013-03-19 | 2016-01-20 | 无锡翔隆高分子面料有限公司 | A kind of capsule of nano drying sheet, preparation method and its usage |
CN103233368A (en) * | 2013-05-08 | 2013-08-07 | 天津城市建设学院 | Preparation and applications of modified melamine resin essence microcapsule finishing agent |
CN103290700A (en) * | 2013-05-31 | 2013-09-11 | 山东鲁普科技有限公司 | Aromatic rope and manufacturing method thereof |
CN105369609A (en) * | 2015-12-21 | 2016-03-02 | 常熟市一心无纺制品有限公司 | Fragrant non-woven fabric |
CN106235817A (en) * | 2016-08-12 | 2016-12-21 | 张太平 | A kind of functional quilt core and processing technique thereof |
CN107119540A (en) * | 2017-05-22 | 2017-09-01 | 江苏共创人造草坪有限公司 | A kind of mosquito dispersing chinampa |
CN107119540B (en) * | 2017-05-22 | 2020-07-21 | 江苏共创人造草坪股份有限公司 | Mosquito-repelling artificial lawn |
WO2020206989A1 (en) * | 2019-04-12 | 2020-10-15 | 江苏意瑞达纺织科技有限公司 | Preparation method for aromatic flannel household textile fabric |
CN110130112A (en) * | 2019-05-27 | 2019-08-16 | 林炜 | A kind of embroidery lace screen cloth aromatizing process |
CN113736371A (en) * | 2020-05-27 | 2021-12-03 | 深圳市准能新材料有限公司 | Environment-friendly water-based carpet back adhesive composition, back adhesive, preparation method of back adhesive and carpet |
CN113736371B (en) * | 2020-05-27 | 2023-04-07 | 深圳市准能新材料有限公司 | Environment-friendly water-based carpet back adhesive composition, back adhesive, preparation method of back adhesive and carpet |
CN114161809A (en) * | 2021-12-17 | 2022-03-11 | 罗秀芝 | Production process of antibacterial composite fabric and antibacterial composite fabric |
CN114230403A (en) * | 2022-01-18 | 2022-03-25 | 深圳市帝拓电子有限公司 | Product capable of emitting preparation for a long time |
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Application publication date: 20121010 |