CN107675512A - A kind of microcapsules children down toy finishing agent and preparation method thereof - Google Patents
A kind of microcapsules children down toy finishing agent and preparation method thereof Download PDFInfo
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- CN107675512A CN107675512A CN201710832847.XA CN201710832847A CN107675512A CN 107675512 A CN107675512 A CN 107675512A CN 201710832847 A CN201710832847 A CN 201710832847A CN 107675512 A CN107675512 A CN 107675512A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/13—Alginic acid or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/15—Proteins or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
Abstract
The invention discloses a kind of microcapsules children down toy finishing agent and preparation method thereof, the microcapsules children down toy finishing agent, mainly it is made up of microcapsules wick and the microcapsule wall material being coated on outside microcapsules wick, its preparation method comprises the following steps：S1, the preparation of the microcapsule wall material aqueous solution, S2, the preparation of microcapsules wick aqueous emulsion, S3, the preparation of microcapsule dressing agent；The microcapsules wick includes the component of following percentage by weight：Chamomile essential oil 1% 80%, lose essential oil 1% 50%, linalool 1% 50%, bergamio 1% 60%, indoles 1% 10%, Thymol 1% 10%, eugenol 1% 10%, ethylhexyl glycerine 1% 30%, geraniol 1% 30%, citronellol 1% 30%, surfactant 1% 40%.The present invention is coated chamomile essential oil with losing essential oil by microcapsules technology, it is prepared into microcapsules children's down toy finishing agent, make chamomile, lose essential oil fragrance remaining time on toy and exceed half a year, can routinely play beneficial effect of the essential oil to children's spirit psychology.
Description
Technical field
The present invention relates to textile finish technical field, more particularly to a kind of microcapsules children down toy finishing agent and
Its preparation method.
Background technology
Chamomile essential oil is the plant extracted from the fresh flower of feverfew chamomile with CO 2 supercritical technique
Thing essential oil, contain light chrysanthemum fragrance and soft medicinal herbs breath.Recorded according to foreign data, chamomile essential oil can excite children
Curiosity and desire for knowledge, the traditional Chinese medical science think that chamomile plays the role of clearing heat and removing internal heat, tranquilization and refreshment pair.
Lose save of vanilla south has wild or artificial cultivation resource more, has from the essential oil that is extracted in vanilla is lost
Antibacterial, the effect of sterilization.According to information, juvenile student can be improved more than mathematics achievement 5 divides often in contact with essential oil is lost.
Chamomile essential oil has certain help to make the Mental health of children certainly with losing vanilla essential oil compounding
With consumer it is expected to have the fragrance of above two essential oil on toy for children and can retained for a long time.Because essential oil easily plays, effectively
Time, one kilogram of chamomile essential oil thousand yuan was relatively valuable, considers from financial cost, is directly sprayed on toy less than one day
Chamomile essential oil be also it is worthless, more can not industrialized production.
The content of the invention
The invention aims to solve shortcoming present in prior art, and a kind of microcapsules children lint proposed
Toy finishing agent and preparation method thereof.
To achieve these goals, present invention employs following technical scheme：
A kind of microcapsules children down toy finishing agent, mainly by microcapsules wick and it is coated on micro- outside microcapsules wick
Capsule wall material forms, and the microcapsules wick includes the component of following percentage by weight：Chamomile essential oil 1%-80%, Alecrim
Essential oil 1%-50%, linalool 1%-50%, bergamio 1%-60%, indoles 1%-10%, Thymol 1%-10%,
Eugenol 1%-10%, ethylhexyl glycerine 1%-30%, geraniol 1%-30%, citronellol 1%-30%, surfactant
1%-40%.
Preferably, the microcapsule wall material is natural macromolecular material or synthesizes high polymer material, the natural polymer
Material is specially that one or both of animal gelatin, natural plant gum, algin, Arabic gum, peach gum, xanthans are combined,
The synthesis high polymer material is specially one in acrylic acid, polyacrylic acid, polypropylene, polyethylene, polystyrene, polyacrylonitrile
Plant or two kinds are combined.
Preferably, the chamomile essential oil is specially that the flower of chamomile passes through boiling and steam distillation PROCESS FOR TREATMENT, is received
The oil water mixture of the collection pure plant essential oil through normal hexane extract and separate again.
Preferably, the chamomile essential oil is specially plant essence of the flower of chamomile through organic solvent ether soak extraction
Oil.
Preferably, the chamomile essential oil is specially that the flower of chamomile extracts by carbon dioxide supercritical extraction technique
Plants essential oil.
Preferably, the surfactant be specially maleic acid higher alcohol monoesters acid sodium, polyoxyethylene fatty acid calcium,
It is sorbitan trioleate, the stearic acid of anhydrous sorbitol three, glycol fatty acid ester, sorbitan mono-laurate, poly-
One or both of oxygen ethene sorbitan monostearate, APEO sorbitan monopalmitate compound and
Into.
Preferably, a kind of preparation method of microcapsules children down toy finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：High polymer material is added in 40-100 DEG C of deionized water, startup is stirred
Machine is mixed, under agitation, 40-100 DEG C of constant temperature, dissolution time 2-10h, multiplies heat filtering, removes water-insoluble, obtain transparent
The microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Microcapsules wick is configured to according to formula, is dissolved by heating, addition helps breast
Agent, continue agitating and heating, when temperature reaches 40-100 DEG C, stirring and dissolving 10-20min under constant temperature, deionized water is added, with height
Emulsification pretreatment machine handles 5-10min, obtains microcapsules wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：Microcapsules wick aqueous emulsion is continued into high-speed shearing emulsion machine processing 3-5min,
And 40-100 DEG C is heated to, after isothermal reaction 4h, continue 40-100 DEG C of constant temperature, stir lower reaction 2-8h, cool, obtain finished product
Microcapsule dressing agent.
Preferably, in the S1, the rotating speed of agitation is 120-1500r/min.
Preferably, in the S2, the rotating speed of stirring is 280-450r/min, and the assistant for emulsifying agent is specially dodecyl sulphur
Acid sodium aqueous solution, its concentration are 0.2-10%.
Preferably, in the S2 and the S3, the rotating speed of high-shear emulsion machine is 1200-1600r/min, the side of heating
Formula is heating water bath.
Preferably, in the S3, the rotating speed of stirring is specially 100-800r/min.
Compared with prior art, the beneficial effects of the invention are as follows：
1. the present invention designs chamomile essential oil and loses the microcapsules wick formula of essential oil compounding, and uses microcapsules
Technology, by chamomile essential oil with losing essential oil cladding, it is prepared into microcapsules children's down toy finishing agent, its formula section
Learn, safety and sanitation, easily cause the interest of children, improve children educational effect.
2. the present invention, by final finishing technology, microcapsules is arranged onto toy fiber, made by rational process conditions
Chamomile, lose essential oil fragrance remaining time on toy and exceed half a year, solve children's push toy and chamomile essential oil, lose
The combination problem of essential oil, make toy for children functionalization, play beneficial effect of the essential oil to children's spirit psychology, play Chinese children
Tool upgrading, lift the inherent scientific and technological content of product.
3. in the formula of the microcapsules wick of the present invention, linalool and bergamio are also added, both spices tool
There is very high antibacterial activity, while also improve the fragrance of Alecrim, children is preferred this toy for having special aroma.
Embodiment
The technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described implementation
Example only part of the embodiment of the present invention, rather than whole embodiments.
Embodiment 1：
A kind of preparation method of microcapsules children down toy finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Edible gelatin 7.5g is weighed, adds deionized water 500ml, stirring is lower to be added
Heat is warming up to 65 DEG C, and 8h is dissolved in water-bath, multiplies heat filtering, removes water-insoluble, obtains the transparent microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh chamomile essential oil 120g, lose essential oil 30g, linalool 20g,
Bergamio 20g, indoles 1g, Thymol 2g, eugenol 4g, ethylhexyl glycerine 10g, geraniol 60g, citronellol 40g,
Surfactant maleic acid higher alcohol monoesters acid sodium 20g, polyoxyethylene fatty acid calcium 12g, 60 DEG C of constant temperature is dissolved by heating, it is molten
10min is solved, adds 60 DEG C of deionized water 161ml, 5min is handled with high-speed shearing emulsion machine, obtains microcapsules wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, the edible gelatin water that concentration is 5% is added
Solution 500ml, continue to handle 3min with high-speed shearing emulsion machine, be transferred on water-soluble pot, start electric blender, rotating speed
230r/min, 55 DEG C of reaction 6h of constant temperature, cools, obtains finished microcapsule finishing agent.
The present embodiment is using chamomile essential oil and loses essential oil compounding, is wrapped up with edible gelatin, it is micro- to obtain finished product
Capsule finishing agent.30% deionized water is measured by children's down toy weight during use, be heated to 50 DEG C, add down toy
The finished microcapsule finishing agent of weight 1.5%, is stirred evenly, the object for appreciation being sprayed onto above-mentioned aqueous with double shower nozzle power sprayes on conveyer belt
It is uniformly thoughtful during sprinkling on tool.Toy can dry de- for 60 seconds under 120 DEG C of high temperature after being baked with conveying immersion
Water.Toy conveyer belt falls into collector through air cooling area, through examining, is packaged as finished product, that is, completes the arrangement to down toy and add
Work process.
Toy after being arranged using finished microcapsule finishing agent manufactured in the present embodiment, fragrance remaining time exceed half a year.
Embodiment 2：
A kind of preparation method of microcapsules children down toy finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Sodium alginate 5g is weighed, adds deionized water 500ml, stirs lower heat
75 DEG C are warming up to, 8h is dissolved in water-bath, multiplies heat filtering, water-insoluble is removed, obtains the transparent microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh chamomile essential oil 110g, lose essential oil 40g, linalool 40g,
Bergamio 10g, indoles 1g, Thymol 1g, eugenol 4g, ethylhexyl glycerine 10g, geraniol 50g, citronellol 40g,
Surfactant maleic acid higher alcohol monoesters acid sodium 25g, polyoxyethylene fatty acid calcium 10g, 60 DEG C of constant temperature is dissolved by heating, it is molten
10min is solved, adds 60 DEG C of deionized water 161ml, 5min is handled with high-speed shearing emulsion machine, obtains microcapsules wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, the sodium alginate water that concentration is 2% is added
Solution 500ml, continue to handle 3min with high-speed shearing emulsion machine, be transferred on water-soluble pot, start electric blender, rotating speed
230r/min, 55 DEG C of reaction 6h of constant temperature, cools, obtains finished microcapsule finishing agent.
The present embodiment is using chamomile essential oil and loses essential oil compounding, is wrapped up with sodium alginate, it is micro- to obtain finished product
Capsule finishing agent.30% deionized water is measured by children's down toy weight during use, be heated to 50 DEG C, add down toy
The finished microcapsule finishing agent of weight 1.5%, is stirred evenly, the object for appreciation being sprayed onto above-mentioned aqueous with double shower nozzle power sprayes on conveyer belt
It is uniformly thoughtful during sprinkling on tool.Toy can dry de- for 60 seconds under 120 DEG C of high temperature after being baked with conveying immersion
Water.Toy conveyer belt falls into collector through air cooling area, through examining, is packaged as finished product, that is, completes the arrangement to down toy and add
Work process.
Toy after being arranged using finished microcapsule finishing agent manufactured in the present embodiment, fragrance remaining time exceed half a year.
Embodiment 3：
A kind of preparation method of microcapsules children down toy finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Polyurethane 15g is weighed, adds deionized water 450ml, stirs lower heat
65 DEG C are warming up to, 8h is dissolved in water-bath, multiplies heat filtering, water-insoluble is removed, obtains the transparent microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh chamomile essential oil 110g, lose essential oil 40g, linalool 40g,
Bergamio 10g, indoles 1g, Thymol 1g, eugenol 4g, ethylhexyl glycerine 10g, geraniol 50g, citronellol 40g,
Surfactant maleic acid higher alcohol monoesters acid sodium 25g, polyoxyethylene fatty acid calcium 10g, 60 DEG C of constant temperature is dissolved by heating, it is molten
10min is solved, adds 60 DEG C of deionized water 165ml, 5min is handled with high-speed shearing emulsion machine, obtains microcapsules wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, it is water-soluble to add the polyurethane that concentration is 8%
Liquid 500ml, continue to handle 3min with high-speed shearing emulsion machine, be transferred on water-soluble pot, start electric blender, rotating speed 230r/
Min, 55 DEG C of reaction 6h of constant temperature, cools, obtains finished microcapsule finishing agent.
The present embodiment is using chamomile essential oil and loses essential oil compounding, is wrapped up with polyurethane, obtains the micro- glue of finished product
Capsule finishing agent.30% deionized water is measured by children's down toy weight during use, be heated to 50 DEG C, add down toy weight
The finished microcapsule finishing agent of amount 1.5%, is stirred evenly, the toy being sprayed onto above-mentioned aqueous with double shower nozzle power sprayes on conveyer belt
On, it is uniformly thoughtful during sprinkling.Toy 60 seconds under 120 DEG C of high temperature can drying and dewatering after being baked with conveying immersion.
Toy conveyer belt falls into collector through air cooling area, through examining, is packaged as finished product, that is, the arrangement completed to down toy is processed
Journey.
Toy after being arranged using finished microcapsule finishing agent manufactured in the present embodiment, fragrance remaining time exceed half a year.
Embodiment 4：
A kind of preparation method of microcapsules children down toy finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Chitosan 5g is weighed, deionized water 450ml is added, under stirring
75 DEG C are heated to, 8h is dissolved in water-bath, multiplies heat filtering, water-insoluble is removed, obtains the transparent microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh chamomile essential oil 130g, lose essential oil 20g, linalool 50g,
Bergamio 10g, indoles 1g, Thymol 1g, eugenol 4g, ethylhexyl glycerine 10g, geraniol 50g, citronellol 40g,
Surfactant maleic acid higher alcohol monoesters acid sodium 35g, polyoxyethylene fatty acid calcium 10g, 60 DEG C of constant temperature is dissolved by heating, it is molten
10min is solved, adds 60 DEG C of deionized water 165ml, 5min is handled with high-speed shearing emulsion machine, obtains microcapsules wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, the deacetylated first that concentration is 2.5% is added
Shell element aqueous solution 500ml, continue to handle 3min with high-speed shearing emulsion machine, be transferred on water-soluble pot, start electric blender,
Rotating speed 230r/min, 55 DEG C of reaction 6h of constant temperature, cools, obtains finished microcapsule finishing agent.
The present embodiment is using chamomile essential oil and loses essential oil compounding, is wrapped up, obtained into chitosan
Product microcapsule dressing agent.30% deionized water is measured by children's down toy weight during use, be heated to 50 DEG C, add lint
The finished microcapsule finishing agent of toy weight 1.5%, is stirred evenly, and above-mentioned aqueous is sprayed onto on conveyer belt with double shower nozzle power sprayes
Toy on, it is uniformly thoughtful during sprinkling.Toy can dry for 60 seconds under 120 DEG C of high temperature after being baked with conveying immersion
Dehydration.Toy conveyer belt falls into collector through air cooling area, through examining, is packaged as finished product, that is, completes the arrangement to down toy
Process.
Toy after being arranged using finished microcapsule finishing agent manufactured in the present embodiment, fragrance remaining time exceed half a year.
Embodiment 5：
A kind of preparation method of microcapsules children down toy finishing agent, comprises the following steps：
S1, the preparation of the microcapsule wall material aqueous solution：Casein 5g is weighed, adds deionized water 450ml, stirs lower heat
66 DEG C are warming up to, 8h is dissolved in water-bath, multiplies heat filtering, water-insoluble is removed, obtains the transparent microcapsule wall material aqueous solution；
S2, the preparation of microcapsules wick aqueous emulsion：Weigh chamomile essential oil 150g, lose essential oil 10g, linalool 30g,
Bergamio 10g, indoles 1g, Thymol 1g, eugenol 4g, ethylhexyl glycerine 10g, geraniol 40, citronellol 40g,
Surfactant maleic acid higher alcohol monoesters acid sodium 35g, polyoxyethylene fatty acid calcium 10g, 60 DEG C of constant temperature is dissolved by heating, it is molten
10min is solved, adds 60 DEG C of deionized water 160ml, 5min is handled with high-speed shearing emulsion machine, obtains microcapsules wick aqueous emulsion；
S3, the preparation of microcapsule dressing agent：In microcapsules wick aqueous emulsion, the casein water that concentration is 2.5% is added
Solution 500ml, continue to handle 3min with high-speed shearing emulsion machine, be transferred on water-soluble pot, start electric blender, rotating speed
230r/min, 58 DEG C of reaction 6h of constant temperature, cools, obtains finished microcapsule finishing agent.
The present embodiment is using chamomile essential oil and loses essential oil compounding, is wrapped up with casein, obtains the micro- glue of finished product
Capsule finishing agent.30% deionized water is measured by children's down toy weight during use, be heated to 50 DEG C, add down toy weight
The finished microcapsule finishing agent of amount 1.5%, is stirred evenly, the toy being sprayed onto above-mentioned aqueous with double shower nozzle power sprayes on conveyer belt
On, it is uniformly thoughtful during sprinkling.Toy 60 seconds under 120 DEG C of high temperature can drying and dewatering after being baked with conveying immersion.
Toy conveyer belt falls into collector through air cooling area, through examining, is packaged as finished product, that is, the arrangement completed to down toy is processed
Journey.
Toy after being arranged using finished microcapsule finishing agent manufactured in the present embodiment, fragrance remaining time exceed half a year.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (11)
- A kind of 1. microcapsules children down toy finishing agent, mainly by microcapsules wick and the micro- glue being coated on outside microcapsules wick Cyst wall material forms, it is characterised in that the microcapsules wick includes the component of following percentage by weight：Chamomile essential oil 1%- 80%th, essential oil 1%-50%, linalool 1%-50%, bergamio 1%-60%, indoles 1%-10%, thyme are lost Phenol 1%-10%, eugenol 1%-10%, ethylhexyl glycerine 1%-30%, geraniol 1%-30%, citronellol 1%-30%, Surfactant 1%-40%.
- A kind of 2. microcapsules children down toy finishing agent according to claim 1, it is characterised in that the microcapsule wall Material is natural macromolecular material or synthesis high polymer material, and the natural macromolecular material is specially animal gelatin, natural plant gum, sea One or both of phycocolloid, Arabic gum, peach gum, xanthans are combined, and the synthesis high polymer material is specially propylene One or both of acid, polyacrylic acid, polypropylene, polyethylene, polystyrene, polyacrylonitrile are combined.
- A kind of 3. microcapsules children down toy finishing agent according to claim 1, it is characterised in that the chamomile essence Oil is specially that the flower of chamomile passes through boiling and steam distillation PROCESS FOR TREATMENT, and the oil water mixture of collection extracts through normal hexane again The pure plant essential oil of separation.
- A kind of 4. microcapsules children down toy finishing agent according to claim 1, it is characterised in that the chamomile essence Oil is specially plants essential oil of the flower of chamomile through organic solvent ether soak extraction.
- A kind of 5. microcapsules children down toy finishing agent according to claim 1, it is characterised in that the chamomile essence Oil is specially that the flower of chamomile passes through the plants essential oil of carbon dioxide supercritical extraction technique extraction.
- A kind of 6. microcapsules children down toy finishing agent according to claim 1, it is characterised in that the surface-active Agent is specially maleic acid higher alcohol monoesters acid sodium, polyoxyethylene fatty acid calcium, sorbitan trioleate, Sorbitan The stearic acid of alcohol three, glycol fatty acid ester, sorbitan mono-laurate, polyoxyethylene 20 sorbitan monostearate, One or both of APEO sorbitan monopalmitate compounding forms.
- A kind of 7. preparation method of microcapsules children down toy finishing agent according to claim 1, it is characterised in that bag Include following steps：S1, the preparation of the microcapsule wall material aqueous solution：High polymer material is added in 40-100 DEG C of deionized water, starts stirring Machine, under agitation, 40-100 DEG C of constant temperature, dissolution time 2-10h, multiply heat filtering, remove water-insoluble, obtain transparent micro- glue The cyst wall material aqueous solution；S2, the preparation of microcapsules wick aqueous emulsion：Microcapsules wick is configured to according to formula, is dissolved by heating, adds assistant for emulsifying agent, Continue agitating and heating, when temperature reaches 40-100 DEG C, stirring and dissolving 10-20min under constant temperature, add deionized water, use high shear Mulser handles 5-10min, obtains microcapsules wick aqueous emulsion；S3, the preparation of microcapsule dressing agent：Microcapsules wick aqueous emulsion is continued into high-speed shearing emulsion machine processing 3-5min, and added Heat arrives 40-100 DEG C, after isothermal reaction 4h, continues 40-100 DEG C of constant temperature, stirs lower reaction 2-8h, cools, obtain finished microcapsule Finishing agent.
- A kind of 8. preparation method of microcapsules children down toy finishing agent according to claim 7, it is characterised in that institute State in S1, the rotating speed of agitation is 120-1500r/min.
- A kind of 9. preparation method of microcapsules children down toy finishing agent according to claim 7, it is characterised in that institute State in S2, the rotating speed of stirring is 280-450r/min, and the assistant for emulsifying agent is specially lauryl sodium sulfate aqueous solution, its concentration For 0.2-10%.
- A kind of 10. preparation method of microcapsules children down toy finishing agent according to claim 7, it is characterised in that In the S2 and the S3, the rotating speed of high-shear emulsion machine is 1200-1600r/min, and the mode of heating is heating water bath.
- A kind of 11. preparation method of microcapsules children down toy finishing agent according to claim 7, it is characterised in that In the S3, the rotating speed of stirring is specially 100-800r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710832847.XA CN107675512A (en) | 2017-09-15 | 2017-09-15 | A kind of microcapsules children down toy finishing agent and preparation method thereof |
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| CN201710832847.XA CN107675512A (en) | 2017-09-15 | 2017-09-15 | A kind of microcapsules children down toy finishing agent and preparation method thereof |
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| CN107675512A true CN107675512A (en) | 2018-02-09 |
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|---|---|---|---|
| CN201710832847.XA Pending CN107675512A (en) | 2017-09-15 | 2017-09-15 | A kind of microcapsules children down toy finishing agent and preparation method thereof |
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| Country | Link |
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| CN (1) | CN107675512A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110777540A (en) * | 2019-11-21 | 2020-02-11 | 广州市迅泰通信设备有限公司 | Chamomile sanitary surface layer |
| CN112609466A (en) * | 2020-11-27 | 2021-04-06 | 江苏金太阳纺织科技股份有限公司 | Stomach-invigorating bedding fabric and preparation method thereof |
| CN113403008A (en) * | 2021-07-01 | 2021-09-17 | 凯鑫森(上海)功能性薄膜产业有限公司 | Anti-ultraviolet splicing adhesive tape and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110777540A (en) * | 2019-11-21 | 2020-02-11 | 广州市迅泰通信设备有限公司 | Chamomile sanitary surface layer |
| CN112609466A (en) * | 2020-11-27 | 2021-04-06 | 江苏金太阳纺织科技股份有限公司 | Stomach-invigorating bedding fabric and preparation method thereof |
| CN113403008A (en) * | 2021-07-01 | 2021-09-17 | 凯鑫森(上海)功能性薄膜产业有限公司 | Anti-ultraviolet splicing adhesive tape and preparation method thereof |
| CN113403008B (en) * | 2021-07-01 | 2022-09-27 | 凯鑫森(上海)功能性薄膜产业股份有限公司 | Anti-ultraviolet splicing adhesive tape and preparation method thereof |
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Application publication date: 20180209 |