CN107691956A - A kind of mulberry leaf beverage particle and preparation method thereof - Google Patents
A kind of mulberry leaf beverage particle and preparation method thereof Download PDFInfo
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- CN107691956A CN107691956A CN201710892102.2A CN201710892102A CN107691956A CN 107691956 A CN107691956 A CN 107691956A CN 201710892102 A CN201710892102 A CN 201710892102A CN 107691956 A CN107691956 A CN 107691956A
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- 235000008708 Morus alba Nutrition 0.000 title claims abstract description 123
- 239000002245 particle Substances 0.000 title claims abstract description 76
- 235000013361 beverage Nutrition 0.000 title claims abstract description 63
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 35
- 240000002948 Ophiopogon intermedius Species 0.000 claims abstract description 25
- 241000234435 Lilium Species 0.000 claims abstract description 24
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 20
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 20
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 20
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 17
- 239000008103 glucose Substances 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 41
- 239000000284 extract Substances 0.000 claims description 33
- 241000196324 Embryophyta Species 0.000 claims description 22
- 238000001035 drying Methods 0.000 claims description 18
- 238000000605 extraction Methods 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 18
- 238000005469 granulation Methods 0.000 claims description 12
- 230000003179 granulation Effects 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 11
- 239000000463 material Substances 0.000 claims description 11
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 10
- 101000693530 Staphylococcus aureus Staphylokinase Proteins 0.000 claims description 10
- 238000007710 freezing Methods 0.000 claims description 6
- 230000008014 freezing Effects 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 229910052786 argon Inorganic materials 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 5
- 239000000706 filtrate Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 239000007789 gas Substances 0.000 claims description 5
- 238000001291 vacuum drying Methods 0.000 claims description 5
- 238000009777 vacuum freeze-drying Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 3
- 238000000265 homogenisation Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- 238000010521 absorption reaction Methods 0.000 abstract description 6
- 239000004615 ingredient Substances 0.000 abstract description 6
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- 230000000052 comparative effect Effects 0.000 description 9
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- 244000025254 Cannabis sativa Species 0.000 description 3
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- BTCSSZJGUNDROE-UHFFFAOYSA-N gamma-aminobutyric acid Chemical compound NCCCC(O)=O BTCSSZJGUNDROE-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 210000002784 stomach Anatomy 0.000 description 2
- OGNSCSPNOLGXSM-UHFFFAOYSA-N (+/-)-DABA Natural products NCCC(N)C(O)=O OGNSCSPNOLGXSM-UHFFFAOYSA-N 0.000 description 1
- 108090000145 Bacillolysin Proteins 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- LXBIFEVIBLOUGU-UHFFFAOYSA-N Deoxymannojirimycin Natural products OCC1NCC(O)C(O)C1O LXBIFEVIBLOUGU-UHFFFAOYSA-N 0.000 description 1
- 102100024295 Maltase-glucoamylase Human genes 0.000 description 1
- 102000035092 Neutral proteases Human genes 0.000 description 1
- 108091005507 Neutral proteases Proteins 0.000 description 1
- 244000170916 Paeonia officinalis Species 0.000 description 1
- 235000006484 Paeonia officinalis Nutrition 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 206010036790 Productive cough Diseases 0.000 description 1
- 241000405414 Rehmannia Species 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 125000003158 alcohol group Chemical group 0.000 description 1
- 108010028144 alpha-Glucosidases Proteins 0.000 description 1
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- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003276 anti-hypertensive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
- 239000002934 diuretic Substances 0.000 description 1
- 230000001882 diuretic effect Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 229960003692 gamma aminobutyric acid Drugs 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
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- 108090000623 proteins and genes Proteins 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The present invention provides a kind of mulberry leaf beverage particle and preparation method thereof, belongs to food processing field, the mulberry leaf beverage particle is made up of the raw material of following parts by weight:180 200 parts of mulberry leaf, 15 20 parts of radix glycyrrhizae, 12 16 parts of the radix paeoniae rubrathe, 10 12 parts of lily, 46 parts of the root bark of white mulberry, 58 parts of the tuber of dwarf lilyturf, 48 parts of radix rehmanniae recen, 12 15 parts of glucose, 8 10 parts of maltodextrin, appropriate amount of water.The preparation method that the present invention also provides the mulberry leaf beverage particle.Formula provided by the invention and preparation method more can completely keep nutritional ingredient therein in manufacturing process, the mulberry leaf beverage particle produced is nutritious, instant, dissolubility and good in taste, and it is not easy the moisture absorption in atmosphere, suitable various people eat.
Description
【Technical field】
The present invention relates to teabag drink manufacture field, especially a kind of mulberry leaf beverage particle and preparation method thereof.
【Technical background】
The mulberry leaf resource in China is enriched, and contains a kind of alkaloid for being called 1-DNJ in mulberry leaf, and this is a kind of
A kind of alkaloid existed only in mulberry leaf, content about 100mg/100g, this alkaloid are a kind of inhibitor of alpha-glucosidase,
In addition, pure containing abundant gamma aminobutyric acid and plant in mulberry leaf, its content is 3-4 times of green tea, has fat-reducing, U.S.
Hold, hypoglycemic effect.
At present, the eating method of mulberry leaf is typically formed into Mulberry-leaf Tea and drunk, and also has and carries out Baoshang as health-care flavouring food materials
The methods of, it is but not convenient enough, therefore, the present inventor by largely testing and study, breaches traditional preparation method,
Like mulberry leaf taste personage to provide a kind of mulberry leaf beverage particle with unique oral sensations for vast, can drink at any time, the side of brewing
Just, the economic value added of mulberry leaf is improved.
【The content of the invention】
In view of posed problems above, the invention provides a kind of mulberry leaf beverage particle and preparation method thereof, methods described
Nutritional ingredient therein more can be completely kept in manufacturing process, the mulberry leaf beverage particle produced is nutritious, food
With convenient, dissolubility and good in taste, and it is not easy the moisture absorption in atmosphere, suitable various people eat.
Technical scheme is as follows:
A kind of mulberry leaf beverage particle, the mulberry leaf beverage particle are made up of the raw material of following parts by weight:Mulberry leaf 180-200
Part, radix glycyrrhizae 15-20 parts, radix paeoniae rubrathe 12-16 parts, lily 10-12 parts, root bark of white mulberry 4-6 parts, tuber of dwarf lilyturf 5-8 part, radix rehmanniae recen 4-8 parts, grape
Sugared 12-15 parts, maltodextrin 8-10 parts, appropriate amount of water.
Further, the mulberry leaf beverage particle is made up of the raw material of following parts by weight:It is 190 parts of mulberry leaf, 16 parts of radix glycyrrhizae, red
14 parts of Chinese herbaceous peony, 11 parts of lily, 5 parts of the root bark of white mulberry, 6 parts of the tuber of dwarf lilyturf, 6 parts of radix rehmanniae recen, 13 parts of glucose, 9 parts of maltodextrin, appropriate amount of water.
The present invention provides a kind of preparation method of mulberry leaf beverage particle, comprises the following steps:
(1) it is placed in desinfection chamber and dries after mulberry leaf are cleaned up, it is 2-3mm that the mulberry leaf after drying are broken into granularity, is adopted
Use supercritical CO2Extraction, the mulberry leaf after crushing are put into extractor, add ethanol, in temperature be 36-40 DEG C, pressure be
24-26MPa、CO2Volume flow extracts 60-80min under conditions of being 120-150ml/min, then separates CO in filter liquor2With
Ethanol, that is, obtain mulberry-leaf extract;Wherein, the volumetric concentration of the ethanol is 55-60%, and the usage amount of ethanol is the mixing
2.5-3 times of thing b mass;
(2) segment that the radix paeoniae rubrathe, the root bark of white mulberry, radix rehmanniae recen are cut into 5-8mm mixes, by the mixed radix paeoniae rubrathe, the root bark of white mulberry, the dried rhizome of rehmannia
Huang is put in the water of 8-10 times of quality of its gross mass, and simmer in water 20-25min, filtering, filter residue is repeated after boiling 2 times, by gained
Filtrate mixing is concentrated into the solution that room temperature measuring relative density is 1.15-1.25, as primary extract;Primary extract is put into super-pressure
In homogenizer, neutral proteinase is added, 5-10min is handled under conditions of pressure is 140-160MPa, obtains plant extraction liquid;
(3) radix glycyrrhizae, lily and the tuber of dwarf lilyturf are mixed and are dried using the method for vacuum freeze drying, by radix glycyrrhizae, lily and
The tuber of dwarf lilyturf is put in freezing room, and the central temperature that the material is freezed under conditions of being -28 DEG C in temperature is -16 DEG C, then will be frozen
Material after knot is put in vacuum drying cabinet, dries 5-5.5h under conditions of being 53-57 DEG C in temperature, high energy is placed into after taking-up
In nanometer impact tank, argon gas protection is passed through, 1.5-1.8h is ground, obtains plant freeze-dried powder;
(4) step (1) mulberry-leaf extract, step (2) plant extraction liquid, step (3) described plant are freezed
Stirred after adding glucose, maltodextrin in powder, obtain premix;Premix is put into granulator granulation, put after granulation
Enter be 60-65 DEG C in temperature in drying tank under the conditions of dry for the first time to particle water content be 18-22%, then place nothing
Bacterium room stands 1.5h, and it is 56-60 DEG C of dry 1.2-1.5h that the particle after standing, which is put to drying box in temperature, obtains the mulberry leaf
Beverage particles.
Further, in step (2), the usage amount of the neutral proteinase is the amount of primary extract described in 3-5wt%.
Further, in step (4), 40-60 mesh sieves are crossed after the premix granulation.
Further, in step (4), the water content of the mulberry leaf beverage particle is less than 4%.
The invention provides a kind of mulberry leaf beverage particle and preparation method thereof, compared with prior art, has beneficial below
Effect:
The raw material of mulberry leaf beverage particle of the present invention includes mulberry leaf, radix glycyrrhizae, the radix paeoniae rubrathe, lily, the root bark of white mulberry, the tuber of dwarf lilyturf, radix rehmanniae recen, Portugal
Grape sugar, maltodextrin, appropriate amount of water;Wherein, using supercritical extraction in specified conditions after mulberry leaf are crushed in manufacturing process
Lower extraction obtains mulberry-leaf extract, and this extracting method can be such that nutritional ingredient in mulberry leaf fully discharges, can be effectively from mulberry leaf
Middle extraction bioactive molecule, ethanol is used as extractant, can be being soluble in the isoreactivity thing composition of alcohol in mulberry leaf to greatest extent
Extract, so as to improve the nutritive value of product so as to improve its absorption rate, strengthen the nutritive value of product, gained
Mulberry-leaf extract has the effect of dispelling wind and heat from the body, clearing away the lungheat and moisturizing, clear liver and improve vision;The radix paeoniae rubrathe has clearing heat and cooling blood, the work(of blood stasis removing analgesic
Effect, the root bark of white mulberry have the function that antihypertensive diuretic, calm antibacterial, and radix rehmanniae recen can clearing heat and promoting fluid, nourishing yin and nourishing blood;Will in manufacturing process
The radix paeoniae rubrathe, the root bark of white mulberry, the water extract of radix rehmanniae recen obtain plant extraction liquid by neutral protease enzymolysis, by neutral proteinase enzyme
Solution is advantageous to accelerated decomposition macromolecular substances, makes extract be easier to be absorbed;Radix glycyrrhizae have moisten the lung and relieve the cough, the work(of QI invigorating stomach invigorating
Effect, and energy coordinating the drug actions of a prescription, radix glycyrrhizae sweet flavor can also lift products taste;Lily has the effect of Yin nourishing and lung moistening, clearing away the heart fire and tranquillizing,
The tuber of dwarf lilyturf can moistening lung clears away heart-fire, purge heat promote the production of body fluid, resolving sputum preventing or arresting vomiting;Radix glycyrrhizae, lily and the tuber of dwarf lilyturf are done using vacuum refrigeration in manufacturing process
Dry method is sloughed after freeze-dried powder is made in moisture, is put into during the impact of high energy nanometer fills and is ground into nano level powder, make by radix glycyrrhizae,
Macromolecular in lily and the tuber of dwarf lilyturf is fully degraded into small molecule, so as to promote absorption of the human body to nutritional ingredient, strengthens medicine again
The effect of effect, it can also make the mouthfeel of beverage particles more fine and smooth;The present invention compounds several raw materials together, and major ingredient is done with mulberry leaf
Manufactured new beverage particle, not only nutritive value is high, and by the complementation on pharmacological function, plays a part of Synergistic,
Instant, mouthfeel is excellent, and there are abundant nutritive value and good health-care effect, suitable various people to eat;The present invention
The harmony of product can be strengthened by maltodextrin as drying aids by being added in manufacturing process, ensure the mouthfeel and flavor of product,
Strengthen the nutritive value of product;Present invention also offers the usage amount of maltodextrin used, the usage amount can extend mulberry leaf beverage
The retention time of particle, it is set to be not easy the moisture absorption in atmosphere in addition, the addition of drying aids is very heavy to the quality of beverage particles
Will, and different types of beverage particles raw material, adapt to use different drying aids;In a word, it is of the present invention each
Technological means all cooperates, mutually promoted, and camps step by step, be all linked with one another, and caused total technique effect is remote
Far above technological means caused by single technological means simple plus and.
The invention provides a kind of mulberry leaf beverage particle and preparation method thereof, methods described can be more in manufacturing process
Completely keep nutritional ingredient therein, the mulberry leaf beverage particle produced is nutritious, have dispelling wind and heat from the body, clearing away the lungheat and moisturizing,
The effect of stomach invigorating diuresis, instant, dissolubility and good in taste, and it is not easy the moisture absorption in atmosphere, it is adapted to various people's food
With.
【Embodiment】
The following examples can help those skilled in the art that the present invention is more completely understood, but cannot be with any
Mode limits the present invention.
Embodiment 1
A kind of mulberry leaf beverage particle, the mulberry leaf beverage particle are made up of the raw material of following parts by weight:It is 180 parts of mulberry leaf, sweet
Grass 15 parts, 12 parts of the radix paeoniae rubrathe, 10 parts of lily, 4 parts of the root bark of white mulberry, 5 parts of the tuber of dwarf lilyturf, 4 parts of radix rehmanniae recen, 12 parts of glucose, maltodextrin 8- parts,
Appropriate amount of water.
The preparation method of mulberry leaf beverage particle, comprises the following steps:
(1) it is placed in desinfection chamber and dries after mulberry leaf are cleaned up, it is 2mm that the mulberry leaf after drying are broken into granularity, is used
Supercritical CO2Extraction, the mulberry leaf after crushing are put into extractor, add ethanol, in temperature be 36 DEG C, pressure 24MPa,
CO2Volume flow extracts 60min under conditions of being 120ml/min, then separates CO in filter liquor2And ethanol, that is, obtain mulberry leaf and carry
Take thing;Wherein, the volumetric concentration of the ethanol is 55%, and the usage amount of ethanol is 2.5 times of the mixture b mass;
(2) segment that the radix paeoniae rubrathe, the root bark of white mulberry, radix rehmanniae recen are cut into 5mm mixes, by the mixed radix paeoniae rubrathe, the root bark of white mulberry, radix rehmanniae recen
It is put in the water of its 8 times of quality of gross mass, simmered in water 20min, filtering, and filter residue is repeated after boiling 2 times, gained filtrate is mixed
It is concentrated into the solution that room temperature measuring relative density is 1.15, as primary extract;Primary extract is put into superhigh-voltage homogenizing machine, added
Neutral proteinase, 5min is handled under conditions of pressure is 140MPa, obtains plant extraction liquid;Wherein, the neutral proteinase
Usage amount be primary extract described in 3wt% amount;
(3) radix glycyrrhizae, lily and the tuber of dwarf lilyturf are mixed and are dried using the method for vacuum freeze drying, by radix glycyrrhizae, lily and
The tuber of dwarf lilyturf is put in freezing room, and the central temperature that the material is freezed under conditions of being -28 DEG C in temperature is -16 DEG C, then will be frozen
Material after knot is put in vacuum drying cabinet, dries 5h under conditions of being 53 DEG C in temperature, the punching of high energy nanometer is placed into after taking-up
Hit in tank, be passed through argon gas protection, grind 1.5h, obtain plant freeze-dried powder;
(4) step (1) mulberry-leaf extract, step (2) plant extraction liquid, step (3) described plant are freezed
Stirred after adding glucose, maltodextrin in powder, obtain premix;Premix is put into granulator granulation, gained particle
40 mesh sieves, be put into after granulation in drying tank be 60 DEG C in temperature under the conditions of carry out for the first time dry to particle water content be 18%,
Then place desinfection chamber and stand 1.5h, it be 56 DEG C of dry 1.2h that the particle after standing, which is put to drying box in temperature, obtain described in
The water content of mulberry leaf beverage particle is less than 4%.
Embodiment 2
A kind of mulberry leaf beverage particle, the mulberry leaf beverage particle are made up of the raw material of following parts by weight:It is 200 parts of mulberry leaf, sweet
Grass 20 parts, 16 parts of the radix paeoniae rubrathe, 12 parts of lily, 6 parts of the root bark of white mulberry, 8 parts of the tuber of dwarf lilyturf, 8 parts of radix rehmanniae recen, 15 parts of glucose, 10 parts of maltodextrin,
Appropriate amount of water.
The preparation method of mulberry leaf beverage particle, comprises the following steps:
(1) it is placed in desinfection chamber and dries after mulberry leaf are cleaned up, it is 3mm that the mulberry leaf after drying are broken into granularity, is used
Supercritical CO2Extraction, the mulberry leaf after crushing are put into extractor, add ethanol, in temperature be 40 DEG C, pressure 26MPa,
CO2Volume flow extracts 80min under conditions of being 150ml/min, then separates CO in filter liquor2And ethanol, that is, obtain mulberry leaf and carry
Take thing;Wherein, the volumetric concentration of the ethanol is 60%, and the usage amount of ethanol is 3 times of the mixture b mass;
(2) segment that the radix paeoniae rubrathe, the root bark of white mulberry, radix rehmanniae recen are cut into 8mm mixes, by the mixed radix paeoniae rubrathe, the root bark of white mulberry, radix rehmanniae recen
It is put in the water of its 10 times of quality of gross mass, simmered in water 25min, filtering, and filter residue is repeated after boiling 2 times, gained filtrate is mixed
Close the solution for being concentrated into that room temperature measuring relative density is 1.25, as primary extract;Primary extract is put into superhigh-voltage homogenizing machine, added
Enter neutral proteinase, handle 10min under conditions of pressure is 160MPa, obtain plant extraction liquid;Wherein, the neutral protein
The usage amount of enzyme is the amount of primary extract described in 5wt%;
(3) radix glycyrrhizae, lily and the tuber of dwarf lilyturf are mixed and are dried using the method for vacuum freeze drying, by radix glycyrrhizae, lily and
The tuber of dwarf lilyturf is put in freezing room, and the central temperature that the material is freezed under conditions of being -28 DEG C in temperature is -16 DEG C, then will be frozen
Material after knot is put in vacuum drying cabinet, dries 5.5h under conditions of being 57 DEG C in temperature, high energy nanometer is placed into after taking-up
Impact in tank, be passed through argon gas protection, grind 1.8h, obtain plant freeze-dried powder;
(4) step (1) mulberry-leaf extract, step (2) plant extraction liquid, step (3) described plant are freezed
Stirred after adding glucose, maltodextrin in powder, obtain premix;Premix is put into granulator granulation, gained particle
60 mesh sieves, be put into after granulation in drying tank be 65 DEG C in temperature under the conditions of carry out for the first time dry to particle water content be 22%,
Then place desinfection chamber and stand 1.5h, it be 60 DEG C of dry 1.5h that the particle after standing, which is put to drying box in temperature, obtain described in
The water content of mulberry leaf beverage particle is less than 4%.
Embodiment 3
A kind of mulberry leaf beverage particle, the mulberry leaf beverage particle are made up of the raw material of following parts by weight:It is 190 parts of mulberry leaf, sweet
Grass 16 parts, 14 parts of the radix paeoniae rubrathe, 11 parts of lily, 5 parts of the root bark of white mulberry, 6 parts of the tuber of dwarf lilyturf, 6 parts of radix rehmanniae recen, 13 parts of glucose, 9 parts of maltodextrin,
Appropriate amount of water.
The preparation method of mulberry leaf beverage particle, comprises the following steps:
(1) it is placed in desinfection chamber and dries after mulberry leaf are cleaned up, it is 2.5mm that the mulberry leaf after drying are broken into granularity, is adopted
Use supercritical CO2Extraction, the mulberry leaf after crushing are put into extractor, add ethanol, in temperature be 38 DEG C, pressure be
25MPa、CO2Volume flow extracts 70min under conditions of being 140ml/min, then separates CO in filter liquor2And ethanol, that is, obtain
Mulberry-leaf extract;Wherein, the volumetric concentration of the ethanol is 58%, and the usage amount of ethanol is the 2.7 of the mixture b mass
Times;
(2) segment that the radix paeoniae rubrathe, the root bark of white mulberry, radix rehmanniae recen are cut into 6mm mixes, by the mixed radix paeoniae rubrathe, the root bark of white mulberry, radix rehmanniae recen
It is put in the water of its 9 times of quality of gross mass, simmered in water 22min, filtering, and filter residue is repeated after boiling 2 times, gained filtrate is mixed
It is concentrated into the solution that room temperature measuring relative density is 1.2, as primary extract;Primary extract is put into superhigh-voltage homogenizing machine, added
Neutral proteinase, 8min is handled under conditions of pressure is 150MPa, obtains plant extraction liquid;Wherein, the neutral proteinase
Usage amount be primary extract described in 4wt% amount;
(3) radix glycyrrhizae, lily and the tuber of dwarf lilyturf are mixed and are dried using the method for vacuum freeze drying, by radix glycyrrhizae, lily and
The tuber of dwarf lilyturf is put in freezing room, and the central temperature that the material is freezed under conditions of being -28 DEG C in temperature is -16 DEG C, then will be frozen
Material after knot is put in vacuum drying cabinet, dries 5.2h under conditions of being 56 DEG C in temperature, high energy nanometer is placed into after taking-up
Impact in tank, be passed through argon gas protection, grind 1.6h, obtain plant freeze-dried powder;
(4) step (1) mulberry-leaf extract, step (2) plant extraction liquid, step (3) described plant are freezed
Stirred after adding glucose, maltodextrin in powder, obtain premix;Premix is put into granulator granulation, gained particle
50 mesh sieves, be put into after granulation in drying tank be 62 DEG C in temperature under the conditions of carry out for the first time dry to particle water content be 20%,
Then place desinfection chamber and stand 1.5h, it be 58 DEG C of dry 1.4h that the particle after standing, which is put to drying box in temperature, obtain described in
The water content of mulberry leaf beverage particle is less than 4%.
Comparative example 1
A kind of mulberry leaf beverage particle, the mulberry leaf beverage particle are made up of the raw material of following parts by weight:190 parts of mulberry leaf, hundred
11 parts of conjunction, 5 parts of the root bark of white mulberry, 6 parts of the tuber of dwarf lilyturf, 6 parts of radix rehmanniae recen, 13 parts of glucose, 9 parts of maltodextrin, appropriate amount of water;Other method with
Embodiment 3 is consistent.
Comparative example 2
A kind of mulberry leaf beverage particle, the mulberry leaf beverage particle are made up of the raw material of following parts by weight:It is 190 parts of mulberry leaf, sweet
16 parts of grass, 14 parts of the radix paeoniae rubrathe, 6 parts of the tuber of dwarf lilyturf, 6 parts of radix rehmanniae recen, 13 parts of glucose, 9 parts of maltodextrin, appropriate amount of water;Other method with
Embodiment 3 is consistent.
Comparative example 3
A kind of mulberry leaf beverage particle, the mulberry leaf beverage particle are made up of the raw material of following parts by weight:It is 190 parts of mulberry leaf, sweet
16 parts of grass, 14 parts of the radix paeoniae rubrathe, 11 parts of lily, 5 parts of the root bark of white mulberry, 13 parts of glucose, 9 parts of maltodextrin, appropriate amount of water;Other method with
Embodiment 3 is consistent.
Comparative example 4
A kind of mulberry leaf beverage particle, the mulberry leaf beverage particle are made up of the raw material of following parts by weight:It is 190 parts of mulberry leaf, sweet
16 parts of grass, 11 parts of lily, 6 parts of the tuber of dwarf lilyturf, 13 parts of glucose, 9 parts of maltodextrin, appropriate amount of water;Other method with the phase one of embodiment 3
Cause.
Sensory evaluation is tested
Using system point system, group is evaluated for the composition of personnel of Food Science by 50 specialties, by embodiment 1-3 with it is right
Ratio 1-4 preparation method prepares mulberry leaf beverage particle, and subjective appreciation is carried out after brewing, and method for pouring is by beverage particles and water
According to 1:15 mass ratio is well mixed, and deliberated index is outward appearance, flavour, smell, takes the total score of its each individual event average value
As appraisal result, total score is 30 points, and standards of grading are shown in Table 1, and appraisal result is shown in Table 2.
The sensory evaluation scores standard of the mulberry leaf beverage particle of table 1
The sensory evaluation scores result of the mulberry leaf beverage particle of table 2
Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | |
Outward appearance (10 points) | 10 | 10 | 10 | 8 | 7 | 5 | 3 |
Flavour (10 points) | 10 | 10 | 10 | 8 | 7 | 7 | 5 |
Smell (10 points) | 10 | 9 | 10 | 6 | 6 | 6 | 4 |
Amount to | 30 | 29 | 30 | 22 | 20 | 18 | 12 |
The result of table 2 shows:Total score is higher, illustrates that the quality of the mulberry leaf beverage particle of preparation is better.Embodiment 1-3 mulberry
The scoring of leaf beverage particle is higher, illustrates essential higher, the nothing of mulberry leaf beverage particle obtained according to the preparation method of the present invention
By the aspect for being outward appearance, flavour and smell, it is better than the mulberry leaf beverage particle that comparative example methods described obtains.
Although above the present invention is described in detail with a general description of the specific embodiments,
On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause
This, these modifications or improvements, belong to the scope of protection of present invention without departing from theon the basis of the spirit of the present invention.
Claims (6)
1. a kind of mulberry leaf beverage particle, it is characterised in that the mulberry leaf beverage particle is made up of the raw material of following parts by weight:Mulberry leaf
180-200 parts, radix glycyrrhizae 15-20 parts, radix paeoniae rubrathe 12-16 parts, lily 10-12 parts, root bark of white mulberry 4-6 parts, tuber of dwarf lilyturf 5-8 part, radix rehmanniae recen 4-8
Part, glucose 12-15 parts, maltodextrin 8-10 parts, appropriate amount of water.
2. a kind of mulberry leaf beverage particle according to claim 1, it is characterised in that the mulberry leaf beverage particle is by following heavy
The raw material of amount part is made:190 parts of mulberry leaf, 16 parts of radix glycyrrhizae, 14 parts of the radix paeoniae rubrathe, 11 parts of lily, 5 parts of the root bark of white mulberry, 6 parts of the tuber of dwarf lilyturf, radix rehmanniae recen 6
Part, 13 parts of glucose, 9 parts of maltodextrin, appropriate amount of water.
A kind of 3. preparation method of mulberry leaf beverage particle according to claim any one of 1-2, it is characterised in that including with
Lower step:
(1) it is placed in desinfection chamber and dries after mulberry leaf are cleaned up, it is 2-3mm that the mulberry leaf after drying are broken into granularity, using super
Critical CO2Extraction, the mulberry leaf after crushing are put into extractor, add ethanol, in temperature be 36-40 DEG C, pressure 24-
26MPa、CO2Volume flow extracts 60-80min under conditions of being 120-150ml/min, then separates CO in filter liquor2And second
Alcohol, that is, obtain mulberry-leaf extract;Wherein, the volumetric concentration of the ethanol is 55-60%, and the usage amount of ethanol is the mixture
2.5-3 times of b mass;
(2) segment that the radix paeoniae rubrathe, the root bark of white mulberry, radix rehmanniae recen are cut into 5-8mm is mixed, and the mixed radix paeoniae rubrathe, the root bark of white mulberry, radix rehmanniae recen are put
In the water of 8-10 times of quality of its gross mass, simmer in water 20-25min, filtering, filter residue is repeated after boiling 2 times, by gained filtrate
Mixing is concentrated into the solution that room temperature measuring relative density is 1.15-1.25, as primary extract;Primary extract is put into super-high-pressure homogenization
In machine, neutral proteinase is added, 5-10min is handled under conditions of pressure is 140-160MPa, obtains plant extraction liquid;
(3) radix glycyrrhizae, lily and the tuber of dwarf lilyturf are mixed and are dried using the method for vacuum freeze drying, by radix glycyrrhizae, lily and the tuber of dwarf lilyturf
It is put in freezing room, the central temperature that the material is freezed under conditions of being -28 DEG C in temperature is -16 DEG C, then after freezing
Material be put in vacuum drying cabinet, in temperature be 53-57 DEG C under conditions of dry 5-5.5h, high energy nanometer is placed into after taking-up
Impact in tank, be passed through argon gas protection, grind 1.5-1.8h, obtain plant freeze-dried powder;
(4) by step (1) mulberry-leaf extract, step (2) plant extraction liquid, step (3) the plant freeze-dried powder
Stirred after adding glucose, maltodextrin, obtain premix;Premix is put into granulator granulation, baking is put into after granulation
It is 18-22% to carry out drying to particle water content for the first time under the conditions of being 60-65 DEG C in temperature in dry groove, then places desinfection chamber
1.5h is stood, it is 56-60 DEG C of dry 1.2-1.5h that the particle after standing, which is put to drying box in temperature, obtains the mulberry leaf beverage
Particle.
4. a kind of preparation method of mulberry leaf beverage particle according to claim 3, it is characterised in that described in step (2)
The usage amount of neutral proteinase is the amount of primary extract described in 3-5wt%.
5. a kind of preparation method of mulberry leaf beverage particle according to claim 3, it is characterised in that described in step (4)
40-60 mesh sieves are crossed after premix granulation.
6. a kind of preparation method of mulberry leaf beverage particle according to claim 3, it is characterised in that described in step (4)
The water content of mulberry leaf beverage particle is less than 4%.
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CN109170754A (en) * | 2018-10-30 | 2019-01-11 | 广西万寿谷投资集团股份有限公司 | A kind of seafood chicken soup and its production technology |
CN110663952A (en) * | 2019-10-29 | 2020-01-10 | 海宁纪亨保健食品有限公司 | Production process of mulberry leaf chrysanthemum crystal |
WO2021086271A1 (en) * | 2019-10-31 | 2021-05-06 | Mark One Innovation Center Company Limited | A composition containing mulberry extract and production method thereof |
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