CN107663420A - A kind of preparation method of anti-aging paint - Google Patents
A kind of preparation method of anti-aging paint Download PDFInfo
- Publication number
- CN107663420A CN107663420A CN201711006708.8A CN201711006708A CN107663420A CN 107663420 A CN107663420 A CN 107663420A CN 201711006708 A CN201711006708 A CN 201711006708A CN 107663420 A CN107663420 A CN 107663420A
- Authority
- CN
- China
- Prior art keywords
- parts
- ludox
- resin
- titanium dioxide
- glycol monoethyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
- C09D191/005—Drying oils
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of preparation method of anti-aging paint, including titanium dioxide, powdered whiting, polyoxyethylene oleic acid ester, glycol monoethyl ether, styrene-acrylic emulsion, trbasic zinc phosphate, barium chromate, aluminium nitride, rosin resin, anti-yellowing resin, hydroxyethyl cellulose, Ludox, triphenyl phosphite, linseed oil and dimethyl malenate are configured by weight；Stirring is uniformly mixed and heated after solid matter is crushed with liquid.The beneficial effects of the invention are as follows：The present invention has the advantages of oxidation resistance is strong, paint can be avoided because exposure aoxidizes in atmosphere, so as to extend the service life of paint, and suitable for the adverse circumstances such as high temperature, humidity, pH-value be higher, it has formula simple, low manufacture cost, applied widely, the advantages of being readily produced, and is easy to promote the use of.
Description
Technical field
It is a kind of preparation method of anti-aging paint specifically the present invention relates to paint field.
Background technology
Paint is that one kind can firmly be covered in body surface, and the chemistry for playing protection, decoration, mark and other specific uses mixes
Compound coating.Paint as viscous oily pigment, it is inflammable in the case of not dry, it is not soluble in water, be slightly soluble in fat, dissolve in alcohol, aldehyde,
Ether, benzene, alkane, it is soluble in gasoline, kerosene, diesel oil.
All it is by three kinds of film forming matter, subsidiary film forming matter and auxiliary film forming matter no matter painting kind or form
Base substance forms：
Film forming matter：Also referred to as binding agent, it is organic high molecular compound such as natural resin that film forming matter is most of（It is rosin, big
Paint）, coating（Tung oil, linseed oil, soya-bean oil, fish oil etc.）, the mix such as synthetic resin, form by pyroreaction, also whether there is
The paint of machine thing combination（Such as：Inorganic zinc rich paint）.Various film forming matters press the common xxx classes of national standard.It is the master for forming paint
Body, decide the performance of paint film.If without film forming matter, simple pigment and auxiliary material can not form paint film.
Subsidiary film forming matter：Including various pigment, extender pigment, rust resisting pigment.Pigment provides color and covering for paint film
Power, improves the protective value and decorative effect of paint, and the pigment of good weatherability can improve the service life of paint.Extender pigment can
It is folded multiple by the accumulation of pigment using the performance of itself " sheet, needle-like " structure to increase the thickness of paint film, form fish scale
The paint film of shape, the service life of paint film is improved, improve water proofing property and rust-proof effect.Rust resisting pigment passes through itself physics and chemistry
Anti-rust action, prevent that metal surface is by corrosion by air, chemicals attack for body surface.
Auxiliary film forming matter：Including various auxiliary agents, solvent, various auxiliary agents are in the production process of paint, storage process, use
Process and the forming process of paint film play very important effect.Although the amount used is all seldom, to the performance shadow of paint film
Ring very big.Even it can not form paint film such as：Do not do, sink to the bottom caking, skinning.
Paint can be reacted and be led with the oxygen in air due to exposure for a long time in atmosphere under the conditions of prior art
Cause aging, come off.
The content of the invention
It is an object of the invention to provide a kind of service life it is long, can avoid reacting with oxygen and cause aging
The preparation method of anti-aging paint.
The present invention is achieved through the following technical solutions：A kind of preparation method of anti-aging paint, including following steps：
Step S1:By weight configure 20 ~ 26 parts of titanium dioxide, 10 ~ 15 parts of powdered whiting, 3 ~ 6 parts of polyoxyethylene oleic acid ester,
5 ~ 7 parts of glycol monoethyl ether, 2 ~ 4 parts of styrene-acrylic emulsion, 5 ~ 7 parts of trbasic zinc phosphate, 8 ~ 12 parts of barium chromate, 6 ~ 10 parts of aluminium nitride, rosin tree
3 ~ 7 parts of fat, 1 ~ 2 part of anti-yellowing resin, 5 ~ 7 parts of hydroxyethyl cellulose, 10 ~ 12 parts of Ludox, 6 ~ 8 parts of triphenyl phosphite, flax
3 ~ 5 parts of 12 ~ 18 parts of oil and dimethyl malenate；
Step S2：Titanium dioxide, powdered whiting, trbasic zinc phosphate, barium chromate, aluminium nitride, rosin resin, Ludox are well mixed,
Uniform mixed mixture is crushed to more than 800 mesh；
Step S3：By mixture and polyoxyethylene oleic acid ester after being crushed in step S2, glycol monoethyl ether, styrene-acrylic emulsion, anti-
Muntenite, hydroxy ethyl fiber, triphenyl phosphite, linseed oil and dimethyl malenate are uniformly mixed and heated to 120 DEG C ~ 150
℃；
Step S4：The mixture in step S3 is set to be incubated 10 ~ 15 minutes in the environment of 120 DEG C ~ 150 DEG C, soaking time terminates
Afterwards, stirred 20 minutes ~ 35 minutes in the environment of 120 DEG C ~ 150 DEG C, mixing speed is 800 ~ 1200 revs/min；
Step S5：After stirring, Temperature fall is painted.
Described 20 parts of titanium dioxide, 10 parts of powdered whiting, 3 parts of polyoxyethylene oleic acid ester, 5 parts of glycol monoethyl ether, benzene
2 parts of acrylic emulsion, 5 parts of trbasic zinc phosphate, 8 parts of barium chromate, 6 parts of aluminium nitride, 3 parts of rosin resin, 1 part of anti-yellowing resin, hydroxyethyl cellulose 5
Part, 10 parts of Ludox, 6 parts of triphenyl phosphite, 12 parts of linseed oil and 3 parts of dimethyl malenate.
Described 22 parts of titanium dioxide, 12 parts of powdered whiting, 3 parts of polyoxyethylene oleic acid ester, 6 parts of glycol monoethyl ether, benzene
2 parts of acrylic emulsion, 5 parts of trbasic zinc phosphate, 9 parts of barium chromate, 7 parts of aluminium nitride, 4 parts of rosin resin, 1 part of anti-yellowing resin, hydroxyethyl cellulose 6
Part, 11 parts of Ludox, 6 parts of triphenyl phosphite, 14 parts of linseed oil and 3 parts of dimethyl malenate.
Described 24 parts of titanium dioxide, 14 parts of powdered whiting, 5 parts of polyoxyethylene oleic acid ester, 6 parts of glycol monoethyl ether, benzene
2 parts of acrylic emulsion, 5 parts of trbasic zinc phosphate, 10 parts of barium chromate, 8 parts of aluminium nitride, 4 parts of rosin resin, 1 part of anti-yellowing resin, hydroxyethyl cellulose
3 parts of 6 parts, 10 parts of Ludox, 7 parts of triphenyl phosphite, 16 parts of linseed oil and dimethyl malenate.
Described 26 parts of titanium dioxide, 15 parts of powdered whiting, 6 parts of polyoxyethylene oleic acid ester, 7 parts of glycol monoethyl ether, benzene
4 parts of acrylic emulsion, 7 parts of trbasic zinc phosphate, 12 parts of barium chromate, 10 parts of aluminium nitride, 7 parts of rosin resin, 2 parts of anti-yellowing resin, hydroxy ethyl fiber
5 parts of 7 parts of element, 12 parts of Ludox, 8 parts of triphenyl phosphite, 18 parts of linseed oil and dimethyl malenate.
The present invention compared with prior art, has advantages below and beneficial effect：
The present invention has the advantages of oxidation resistance is strong, can avoid paint because exposure aoxidizes in atmosphere, so as to
Extend the service life of paint, and suitable for the adverse circumstances such as high temperature, humidity, pH-value be higher, its have formula it is simple,
Low manufacture cost, applied widely, the advantages of being readily produced, it is easy to promote the use of.
Embodiment
The present invention is described in further detail with reference to embodiment, but the implementation of the present invention is not limited to this.
Embodiment 1：
In the present embodiment, a kind of preparation method of anti-aging paint, including following steps：
Step S1:By weight configure 20 ~ 26 parts of titanium dioxide, 10 ~ 15 parts of powdered whiting, 3 ~ 6 parts of polyoxyethylene oleic acid ester,
5 ~ 7 parts of glycol monoethyl ether, 2 ~ 4 parts of styrene-acrylic emulsion, 5 ~ 7 parts of trbasic zinc phosphate, 8 ~ 12 parts of barium chromate, 6 ~ 10 parts of aluminium nitride, rosin tree
3 ~ 7 parts of fat, 1 ~ 2 part of anti-yellowing resin, 5 ~ 7 parts of hydroxyethyl cellulose, 10 ~ 12 parts of Ludox, 6 ~ 8 parts of triphenyl phosphite, flax
3 ~ 5 parts of 12 ~ 18 parts of oil and dimethyl malenate；
Step S2：Titanium dioxide, powdered whiting, trbasic zinc phosphate, barium chromate, aluminium nitride, rosin resin, Ludox are well mixed,
Uniform mixed mixture is crushed to more than 800 mesh；
Step S3：By mixture and polyoxyethylene oleic acid ester after being crushed in step S2, glycol monoethyl ether, styrene-acrylic emulsion, anti-
Muntenite, hydroxy ethyl fiber, triphenyl phosphite, linseed oil and dimethyl malenate are uniformly mixed and heated to 120 DEG C ~ 150
℃；
Step S4：The mixture in step S3 is set to be incubated 10 ~ 15 minutes in the environment of 120 DEG C ~ 150 DEG C, soaking time terminates
Afterwards, stirred 20 minutes ~ 35 minutes in the environment of 120 DEG C ~ 150 DEG C, mixing speed is 800 ~ 1200 revs/min；
Step S5：After stirring, Temperature fall is painted.
Described 20 parts of titanium dioxide, 10 parts of powdered whiting, 2 parts of polyoxyethylene oleic acid ester, 5 parts of glycol monoethyl ether, benzene
2 parts of acrylic emulsion, 5 parts of trbasic zinc phosphate, 8 parts of barium chromate, 6 parts of aluminium nitride, 3 parts of rosin resin, 1 part of anti-yellowing resin, hydroxyethyl cellulose 5
Part, 10 parts of Ludox, 6 parts of triphenyl phosphite, 12 parts of linseed oil and 3 parts of present invention of dimethyl malenate have high temperature resistant, resisted
The advantages of combustion ability is strong, the risk for triggering fire can be reduced, consequently facilitating storage and managenent, and it is painted on furniture, wall coverings, wall
After body, can when fire occurs from fire retardation, loss caused by reduce fire, it has, and formula is simple, is fabricated to
This is low, applied widely, the advantages of being readily produced, and is easy to promote the use of.
Embodiment 2：
On the basis of above-described embodiment, in the present embodiment, a kind of preparation method of anti-aging paint, including by weight
20 parts of titanium dioxide, 10 parts of powdered whiting, 3 parts of polyoxyethylene oleic acid ester, 5 parts of glycol monoethyl ether, 2 parts of styrene-acrylic emulsion, phosphoric acid
5 parts of zinc, 8 parts of barium chromate, 6 parts of aluminium nitride, 3 parts of rosin resin, 1 part of anti-yellowing resin, 5 parts of hydroxyethyl cellulose, 10 parts of Ludox,
3 parts of 6 parts of triphenyl phosphite, 12 parts of linseed oil and dimethyl malenate.
Embodiment 3：
On the basis of above-described embodiment, in the present embodiment, a kind of preparation method of anti-aging paint, including by weight
22 parts of titanium dioxide, 12 parts of powdered whiting, 3 parts of polyoxyethylene oleic acid ester, 6 parts of glycol monoethyl ether, 2 parts of styrene-acrylic emulsion, phosphoric acid
5 parts of zinc, 9 parts of barium chromate, 7 parts of aluminium nitride, 4 parts of rosin resin, 1 part of anti-yellowing resin, 6 parts of hydroxyethyl cellulose, 11 parts of Ludox,
3 parts of 6 parts of triphenyl phosphite, 14 parts of linseed oil and dimethyl malenate.
Embodiment 4：
On the basis of above-described embodiment, in the present embodiment, a kind of preparation method of anti-aging paint, including by weight
24 parts of titanium dioxide, 14 parts of powdered whiting, 5 parts of polyoxyethylene oleic acid ester, 6 parts of glycol monoethyl ether, 2 parts of styrene-acrylic emulsion, phosphoric acid
5 parts of zinc, 10 parts of barium chromate, 8 parts of aluminium nitride, 4 parts of rosin resin, 1 part of anti-yellowing resin, 6 parts of hydroxyethyl cellulose, Ludox 10
Part, 7 parts of triphenyl phosphite, 16 parts of linseed oil and 3 parts of dimethyl malenate.
Embodiment 5：
On the basis of above-described embodiment, in the present embodiment, a kind of preparation method of anti-aging paint, including by weight
26 parts of titanium dioxide, 15 parts of powdered whiting, 6 parts of polyoxyethylene oleic acid ester, 7 parts of glycol monoethyl ether, 4 parts of styrene-acrylic emulsion, phosphoric acid
7 parts of zinc, 12 parts of barium chromate, 10 parts of aluminium nitride, 7 parts of rosin resin, 2 parts of anti-yellowing resin, 7 parts of hydroxyethyl cellulose, Ludox 12
Part, 8 parts of triphenyl phosphite, 18 parts of linseed oil and 5 parts of dimethyl malenate.
It is described above, be only presently preferred embodiments of the present invention, any formal limitation not done to the present invention, it is every according to
Any simply modification, the equivalent variations made according to the technical spirit of the present invention to above example, each fall within the protection of the present invention
Within the scope of.
Claims (5)
- A kind of 1. preparation method of anti-aging paint, it is characterised in that：Including following steps：Step S1:By weight configure 20 ~ 26 parts of titanium dioxide, 10 ~ 15 parts of powdered whiting, 3 ~ 6 parts of polyoxyethylene oleic acid ester, 5 ~ 7 parts of glycol monoethyl ether, 2 ~ 4 parts of styrene-acrylic emulsion, 5 ~ 7 parts of trbasic zinc phosphate, 8 ~ 12 parts of barium chromate, 6 ~ 10 parts of aluminium nitride, rosin tree 3 ~ 7 parts of fat, 1 ~ 2 part of anti-yellowing resin, 5 ~ 7 parts of hydroxyethyl cellulose, 10 ~ 12 parts of Ludox, 6 ~ 8 parts of triphenyl phosphite, flax 3 ~ 5 parts of 12 ~ 18 parts of oil and dimethyl malenate；Step S2：Titanium dioxide, powdered whiting, trbasic zinc phosphate, barium chromate, aluminium nitride, rosin resin, Ludox are well mixed, Uniform mixed mixture is crushed to more than 800 mesh；Step S3：By mixture and polyoxyethylene oleic acid ester after being crushed in step S2, glycol monoethyl ether, styrene-acrylic emulsion, anti- Muntenite, hydroxy ethyl fiber, triphenyl phosphite, linseed oil and dimethyl malenate are uniformly mixed and heated to 120 DEG C ~ 150 ℃；Step S4：The mixture in step S3 is set to be incubated 10 ~ 15 minutes in the environment of 120 DEG C ~ 150 DEG C, soaking time terminates Afterwards, stirred 20 minutes ~ 35 minutes in the environment of 120 DEG C ~ 150 DEG C, mixing speed is 800 ~ 1200 revs/min；Step S5：After stirring, Temperature fall is painted.
- A kind of 2. preparation method of anti-aging paint according to claim 1, it is characterised in that：Described titanium dioxide 20 Part, 10 parts of powdered whiting, 3 parts of polyoxyethylene oleic acid ester, 5 parts of glycol monoethyl ether, 2 parts of styrene-acrylic emulsion, 5 parts of trbasic zinc phosphate, chromium Sour 8 parts of barium, 6 parts of aluminium nitride, 3 parts of rosin resin, 1 part of anti-yellowing resin, 5 parts of hydroxyethyl cellulose, 10 parts of Ludox, phosphorous acid three 3 parts of 6 parts of phenyl ester, 12 parts of linseed oil and dimethyl malenate.
- A kind of 3. preparation method of anti-aging paint according to claim 1, it is characterised in that：Described titanium dioxide 22 Part, 12 parts of powdered whiting, 3 parts of polyoxyethylene oleic acid ester, 6 parts of glycol monoethyl ether, 2 parts of styrene-acrylic emulsion, 5 parts of trbasic zinc phosphate, chromium Sour 9 parts of barium, 7 parts of aluminium nitride, 4 parts of rosin resin, 1 part of anti-yellowing resin, 6 parts of hydroxyethyl cellulose, 11 parts of Ludox, phosphorous acid three 3 parts of 6 parts of phenyl ester, 14 parts of linseed oil and dimethyl malenate.
- A kind of 4. preparation method of anti-aging paint according to claim 1, it is characterised in that：Described titanium dioxide 24 Part, 14 parts of powdered whiting, 5 parts of polyoxyethylene oleic acid ester, 6 parts of glycol monoethyl ether, 2 parts of styrene-acrylic emulsion, 5 parts of trbasic zinc phosphate, chromium Sour 10 parts of barium, 8 parts of aluminium nitride, 4 parts of rosin resin, 1 part of anti-yellowing resin, 6 parts of hydroxyethyl cellulose, 10 parts of Ludox, phosphorous acid 3 parts of 7 parts of triphenylmethyl methacrylate, 16 parts of linseed oil and dimethyl malenate.
- A kind of 5. preparation method of anti-aging paint according to claim 1, it is characterised in that：Described titanium dioxide 26 Part, 15 parts of powdered whiting, 6 parts of polyoxyethylene oleic acid ester, 7 parts of glycol monoethyl ether, 4 parts of styrene-acrylic emulsion, 7 parts of trbasic zinc phosphate, chromium Sour 12 parts of barium, 10 parts of aluminium nitride, 7 parts of rosin resin, 2 parts of anti-yellowing resin, 7 parts of hydroxyethyl cellulose, 12 parts of Ludox, phosphorous acid 5 parts of 8 parts of triphenylmethyl methacrylate, 18 parts of linseed oil and dimethyl malenate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711006708.8A CN107663420A (en) | 2017-10-25 | 2017-10-25 | A kind of preparation method of anti-aging paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711006708.8A CN107663420A (en) | 2017-10-25 | 2017-10-25 | A kind of preparation method of anti-aging paint |
Publications (1)
| Publication Number | Publication Date |
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| CN107663420A true CN107663420A (en) | 2018-02-06 |
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| CN201711006708.8A Withdrawn CN107663420A (en) | 2017-10-25 | 2017-10-25 | A kind of preparation method of anti-aging paint |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108610973A (en) * | 2018-05-10 | 2018-10-02 | 诸城市福日机械有限公司 | A kind of vehicle frame protection paint and preparation method thereof |
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| CN107057565A (en) * | 2017-06-26 | 2017-08-18 | 郑堂玲 | A kind of paint formulation containing Ludox |
| CN107216785A (en) * | 2017-08-08 | 2017-09-29 | 合肥安力电力工程有限公司 | It is a kind of for fire-resistant anticorrosion paint of power cable and preparation method thereof |
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| CN103408971A (en) * | 2013-07-03 | 2013-11-27 | 青阳县恒源化工原料有限责任公司 | Anti-aging modified calcium carbonate for paint-latex paint and preparation method thereof |
| CN104073041A (en) * | 2014-07-24 | 2014-10-01 | 周彩球 | Steel surface treatment paint |
| CN104194600A (en) * | 2014-08-27 | 2014-12-10 | 句容市石狮冲压件厂 | Antibacterial fluorescent coating for outdoor deck chair and preparation method of antibacterial fluorescent coating |
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| CN106810971A (en) * | 2015-11-27 | 2017-06-09 | 沈阳顺风新城建筑材料有限公司 | A kind of general emulsion paint of organic-silicon-modified inner-outer wall and preparation method thereof |
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| CN107033682A (en) * | 2016-11-25 | 2017-08-11 | 中山摩尔化学工业有限公司 | A kind of environment-friendly type styrene-acrylate emulsion coating and preparation method thereof |
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Application publication date: 20180206 |