CN107661223A - A kind of Wrinkle removing eye cream containing perfluorodecalin and preparation method thereof - Google Patents
A kind of Wrinkle removing eye cream containing perfluorodecalin and preparation method thereof Download PDFInfo
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- CN107661223A CN107661223A CN201711115607.4A CN201711115607A CN107661223A CN 107661223 A CN107661223 A CN 107661223A CN 201711115607 A CN201711115607 A CN 201711115607A CN 107661223 A CN107661223 A CN 107661223A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
- A61K8/21—Fluorides; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention discloses a kind of Wrinkle removing eye cream containing perfluorodecalin and preparation method thereof, and it includes each raw material components of following percentage by weight：Oil phase component：O/W types emulsifying agent 0.1 3%；16/18 alcohol 0.1 3%；Isononyl isononanoate 0.1 5%；Saualane 0.1 5%；Polydimethyl siloxane fluid 0.5 5%；Water phase components：Glycerine 0.1 10%；Butanediol 0.1 10%；Water phase thickener 0.1 2%；Deionized water 50 80%；Additive：Perfluorodecalin 0.1 20%；Preservative 0.5%.The grease of Wrinkle removing eye cream provided by the invention is controlled 1 15% by isononyl isononanoate, saualane, dimethyl silicone polymer compounded combination, the dosage of oil mass；Meet that grease will clearly, easily absorb, not increase the burden of eye skin, while add the skin optimization breathing that perfluorodecalin helps circumference of eyes, CO2 that can be in purifying skin and improve oxygen level so as to reduce wrinkle of skin.
Description
Technical field
The present invention relates to daily chemical product technical field, more particularly to a kind of Wrinkle removing eye cream and its system containing perfluorodecalin
Preparation Method.
Background technology
Wrinkle is to pursue the problem of fashion personage of young posture takes notice of the most, with age, Skin Cell activity
Decline, cell propagation weakens, then those are deposited in the horn cell on top layer with regard to difficult for drop-off；It is in addition, continuous in skin surface
Ground thickeies, and cuticula, which is constantly exposed to wind and rain, in addition, the sun shines etc. stimulates, and causes skin water shortage, flexibility worse and worse, most
, there is wrinkle in the intensity and flexibility decrease of whole skin.Therefore, for internal cause, the appearance of wrinkle is under Skin Cell activity
Caused by drop.External cause is that skin starts obvious aging, thinning of skin, is hardened, dries, tension force reduction.Corium elastic fibrosis, break
Split, the tension force and elasticity for making skin reduce, and so as to which after expression muscular relaxation, skin can not restore quickly, it is " solidifying that long then makes wrinkle
Gu " get off, shrinkage mark does not exist still mimetic muscle.Increase with the age, skin and hypodermis more relax, and are propped up plus face
Hold atrophy or the missing of tissue, and muscle is soft, skin will slide pendant under gravity, form deeper wrinkle
Line.
Particularly canthus fishtail line, with advancing age, due to endocrinopathy, elastomer transformation, collagen
The many reasons such as fracture, crow's feet can progressively occur at canthus, so make one to present a weathered appearance, lose beauty.In order to dispel fish tail
Line, people employ diversified mode, such as massage, physical extension, the various skin care materials of supplement, or even using operation, note
Penetrating etc. has the mode of injury to human body, and maximally efficient and safe mode is using the skin care item of eye cream etc, existing eye
Frost typically contains Argireline, Dermox SRC, DMAE, Firm agent ST, LipoLight OAP, these factors for
Confrontation skin, which improves oxidation resistance confrontation, especially has back cover effect, while supplements certain collagen.But these eye creams produce
The effect that product dispel crow's feet is not so good as the product of eye sticker class, and it is general to dispel the effect of crow's feet, therefore, it is necessary to constantly optimizes eye
White product into subassembly, preferably dispel effect so as to obtain.
The content of the invention
, can the technical problem to be solved in the present invention is to provide a kind of Wrinkle removing eye cream containing perfluorodecalin and preparation method thereof
The skin optimization breathing of circumference of eyes is helped, CO2 that can be in purifying skin and raising oxygen level are so as to reducing skin around eyes
The wrinkle of skin.
In order to solve the above-mentioned technical problem, it has been found that breathing is the key of skin toxin expelling, and perfluorodecalin can solve the problem that eye
Skin optimization breathing around portion, and the more preferable self-control in contaminated environment, so that the CO2 in purifying skin,
Enzyme and coenzyme in particularly CO2；Oxygen level is improved, preferably composition collagen is helped, the electric current in skin can be suppressed,
So as to reach the effect of blowdown and anti-aging.
Specifically, the invention provides a kind of Wrinkle removing eye cream containing perfluorodecalin, it includes each of following percentage by weight
Raw material components：
Oil phase component：
O/W type emulsifying agents 0.1-3%；
16/18 alcohol 0.1-3%；
Isononyl isononanoate 0.1-5%；
Saualane 0.1-5%；
Polydimethyl siloxane fluid 0.5-5%；
Water phase components：
Glycerine 0.1-10%；
Butanediol 0.1-10%；
Water phase thickener 0.1-2%；
Deionized water 50-80%；
Additive：
Perfluorodecalin 0.1-20%；
Preservative 0.5%.
Further, the O/W types emulsifying agent is cetostearyl alcohol glucoside, stearine and PEG-100 stearic
The mixture of acid esters.
Further, the polydimethyl siloxane fluid is DC200 silicone oil.
Further, the water phase thickener is hydroxy-ethyl acrylate and the Taurate Copolymer of acryloyl two.
Further, the preservative is that methyl hydroxybenzoate, Nipasol, 4 kinds of Sensiva SC50, Phenoxyethanol components are mixed
The preservative of conjunction.Preferably German Shu Mei Euxyl K350 cosmetics top grade preservatives.
Another aspect of the present invention, in order to prepare the above-mentioned Wrinkle removing eye cream containing perfluorodecalin, present invention also offers one kind
The preparation method of Wrinkle removing eye cream containing perfluorodecalin, the described method comprises the following steps：
S101, prepare recipe ingredient：Oil phase component：O/W types emulsifying agent 0.1-3%, isononyl isononanoate 0.1-5%, angle
Shark alkane 0.1-5%, polydimethyl siloxane fluid 0.5-5%, 16/18 alcohol 0.1-3%；Water phase components：Deionized water 50-80%, glycerine
0.1-10%, butanediol 0.1-10%, water phase thickener 0.1-2%；Additive：Perfluorodecalin 0.1-20%, preservative
0.5%.
S102, by oil phase component：O/W types emulsifying agent 0.1-3%, isononyl isononanoate 0.1-5%, saualane 0.1-5%,
Polydimethyl siloxane fluid 0.5-5%%, 16/18 alcohol 0.1-3%, sequentially add heating stirring in oil phase pot and are dissolved to 85 DEG C；
S103, water phase components：Deionized water 50-80%, glycerine 0.1-10%, butanediol 0.1-10%, water phase thickener
0.1-2%, sequentially add heating stirring in aqueous phase pot and be dissolved to 85 DEG C；
S104, the water phase components in the oil phase component in oil phase pot and aqueous phase pot are added in emulsification pot, and stir homogeneous
5-8min is well mixed to oil phase component and water phase components；
S105, continue stirring and be cooled to 45 DEG C, add perfluorodecalin 0.1-20%, preservative 0.5%.And with rotating speed
4000-6000rpm stirs.
S106, standing are filling after 2 hours.
To reach the purpose that the above solves problem, inventive formulation is from raw material selection, production technology, technical parameter etc.
Allocated, controlled.
Perfluorodecalin is the liquid oxygen being perfectly safe of U.S. FDA accreditation, is a kind of molecule that can extend self structure,
Gas O2, CO2 etc. can be loaded, 0.1-20% perfluorodecalin is added in salubrious eye cream matrix, notices that vacuum produces, very
Empty package, perfluorodecalin are reached in skin by being applied to, and are penetrated into immediately in skin, point of the oxygen from perfluorodecalin in process of osmosis
Discharged in son, due to the difference of gas partial pressure, oxygen can be contaminated thing CO2 and be substituted, and be moved to the skin histology of deep layer, this
When the perfluorodecalin comprising pollutant and free oxygen molecule continue through skin histology, shifted to blood circulation system, and lead to
It is external to cross lung's respiratory system exhalation., can be in the outer layer shape of skin meanwhile perfluorodecalin is the NMF of a long-acting efficient
Into oxygen store.
So far skin have passed through the cleaning of deep layer and recover life, so as to promote and recover metabolism.After tested, smear
The wrinkle of the subject of content 0.1-20% perfluorodecalin after 28 days reduces 50% in quantity and the depth of wrinkle.
The advantageous effects of the present invention：
A kind of grease of Wrinkle removing eye cream containing perfluorodecalin provided by the invention is by isononyl isononanoate, saualane, DC200
Compounded combination, the dosage of oil mass are controlled in 1-15%；Meet that grease will clearly, easily absorb, do not cause the burden of eye part skin.Add
Enter the skin optimization breathing that perfluorodecalin helps circumference of eyes, CO2 that can be in purifying skin and improve oxygen level so as to reduce
Wrinkle of skin.
Embodiment
The embodiment of the present invention is described further below.Herein it should be noted that for these implementations
The explanation of mode is used to help understand the present invention, but does not form limitation of the invention.In addition, invention described below
As long as involved technical characteristic does not form conflict can and is mutually combined each other in each embodiment.
The invention provides a kind of Wrinkle removing eye cream containing perfluorodecalin, and it includes each raw material group of following percentage by weight
Point：
Oil phase component：O/W type emulsifying agents 0.1-3%；16/18 alcohol 0.1-3%；Isononyl isononanoate 0.1-5%；Saualane
0.1-5%；Polydimethyl siloxane fluid 0.5-5%；
Water phase components：Glycerine 0.1-10%；Butanediol 0.1-10%；Water phase thickener 0.1-2%；Deionized water 50-
80%；
Additive：Perfluorodecalin 0.1-20%；Preservative 0.5%.
O/W types emulsifying agent selection in eye cream is critically important, and cetostearyl alcohol glucoside, glyceryl stearate are selected through test of many times
The mixture of acid esters and PEG-100 stearates, can stable emulsifying polyelectrolyte material and the stabilization below 45 DEG C and -15 DEG C.
The thickening stabilizing agent of aqueous phase needs to meet following principle：Heat stabilization test (40 DEG C 30 days) is thicker without being layered；It is cold
Stability test (- 5 DEG C, 30 days) is thicker without being layered；(4000-6000rpm) stirring it can be produced at 45 DEG C without influenceing at a high speed
Product quality, this product have selected hydroxy-ethyl acrylate and the Taurate Copolymer of acryloyl two.
Illustrated below by taking 3 embodiments as an example, the gross mass of wherein component is defined by 100g.
Embodiment 1
A kind of Wrinkle removing eye cream containing perfluorodecalin of embodiment 1, it includes each raw material components of following percentage by weight：
Oil phase component：O/W types emulsifying agent 1.5%, isononyl isononanoate 2.5%, saualane 2.5%, polydimethyl siloxane fluid
3%, 16/18 alcohol 1.5%；
Water phase components：Deionized water 72.7%, glycerine 5%, butanediol 5%, water phase thickener 0.8%；
Additive：Perfluorodecalin 5%, preservative 0.5%.
The step of preparing above-mentioned Wrinkle removing eye cream is as follows：
S101, prepare recipe ingredient：Oil phase component：O/W types emulsifying agent 1.5%, isononyl isononanoate 2.5%, saualane
2.5%, polydimethyl siloxane fluid 3%, 16/18 alcohol 1.5%；Water phase components：Deionized water 72.7%, glycerine 5%, butanediol 5%,
Water phase thickener 0.8%；Additive：Perfluorodecalin 5%, preservative 0.5%.
S102, by oil phase component：O/W types emulsifying agent 1.5%, isononyl isononanoate 2.5%, saualane 2.5%, poly- diformazan
Base silicone oil 3%, 16/18 alcohol 1.5%；Sequentially add heating stirring in oil phase pot and be dissolved to 85 DEG C；
S103, water phase components：Deionized water 72.7%, glycerine 5%, butanediol 5%, water phase thickener 0.8%；Successively plus
Enter heating stirring in aqueous phase pot and be dissolved to 85 DEG C；
S104, the water phase components in the oil phase component in oil phase pot and aqueous phase pot are added in emulsification pot, and stir homogeneous
5-8min is well mixed to oil phase component and water phase components；
S105, continue stirring and be cooled to 45 DEG C, add perfluorodecalin 5%, preservative 0.5% and quick (speed 4000-
6000rpm) stir.
S106, standing are filling after 2 hours.
Embodiment 2
A kind of Wrinkle removing eye cream containing perfluorodecalin of embodiment 2, it includes each raw material components of following percentage by weight：
Oil phase component：O/W types emulsifying agent 2%, isononyl isononanoate 4%, saualane 4%, polydimethyl siloxane fluid 4%, 16/
18 alcohol 2%；
Water phase components：Deionized water 62%, glycerine 8%, butanediol 8%, water phase thickener 0.5%；
Additive：Perfluorodecalin 5%, preservative 0.5%.
The step of preparing above-mentioned Wrinkle removing eye cream is as follows：
S101, prepare recipe ingredient：Oil phase component：O/W types emulsifying agent 2%, isononyl isononanoate 4%, saualane 4%,
Polydimethyl siloxane fluid 4%, 16/18 alcohol 2%；Water phase components：Deionized water 62%, glycerine 8%, butanediol 8%, water phase thickener
0.5%；Additive：Perfluorodecalin 5%, preservative 0.5%.
S102, by oil phase component：O/W types emulsifying agent 2%, isononyl isononanoate 4%, saualane 4%, polydimethyl siloxane fluid
4%, 16/18 alcohol 2%；Sequentially add heating stirring in oil phase pot and be dissolved to 85 DEG C；
S103, water phase components：Deionized water 62%, glycerine 8%, butanediol 8%, water phase thickener 0.5%；Sequentially add
Heating stirring is dissolved to 85 DEG C in aqueous phase pot；
S104, the water phase components in the oil phase component in oil phase pot and aqueous phase pot are added in emulsification pot, and stir homogeneous
5-8min is well mixed to oil phase component and water phase components；
S105, continue stirring and be cooled to 45 DEG C, add perfluorodecalin 5%, preservative 0.5% and quick (speed 4000-
6000rpm) stir.
S106, standing are filling after 2 hours.
Embodiment 3
A kind of Wrinkle removing eye cream containing perfluorodecalin of embodiment 3, it includes each raw material components of following percentage by weight：
Oil phase component：O/W types emulsifying agent 2%, isononyl isononanoate 4%, saualane 4%, polydimethyl siloxane fluid 4%, 16/
18 alcohol 2%；
Water phase components：Deionized water 57%, glycerine 8%, butanediol 8%, water phase thickener 0.5%；
Additive：Perfluorodecalin 10%, preservative 0.5%.
The step of preparing above-mentioned Wrinkle removing eye cream is as follows：
S101, prepare recipe ingredient：Oil phase component：O/W types emulsifying agent 2%, isononyl isononanoate 4%, saualane 4%,
Polydimethyl siloxane fluid 4%, 16/18 alcohol 2%；Water phase components：Deionized water 57%, glycerine 8%, butanediol 8%, water phase thickener
0.5%；Additive：Perfluorodecalin 10%, preservative 0.5%.
S102, by oil phase component：O/W types emulsifying agent 2%, isononyl isononanoate 4%, saualane 4%, polydimethyl siloxane fluid
4%, 16/18 alcohol 2%；Sequentially add heating stirring in oil phase pot and be dissolved to 85 DEG C；
S103, water phase components：Deionized water 57%, glycerine 8%, butanediol 8%, water phase thickener 0.5%；Sequentially add
Heating stirring is dissolved to 85 DEG C in aqueous phase pot；
S104, the water phase components in the oil phase component in oil phase pot and aqueous phase pot are added in emulsification pot, and stir 5-
8min is well mixed to oil phase component and water phase components；
S105, continue stirring and be cooled to 45 DEG C, add perfluorodecalin 10%, preservative 0.5% and quick (speed 4000-
6000rpm) stir.
S106, standing are filling after 2 hours.
In addition, in the preparation process of the Wrinkle removing eye cream containing perfluorodecalin, production should clean up agitated kettle before feeding intake, match somebody with somebody
Charging basket and production apparatus, and sterilized with 75% alcohol, ultraviolet, sterilized.By job instruction dispensing, feed intake, eye cream half
Finished product, after laboratory inspection by sampling is qualified, it is filling to be sent to bottling department progress.The packaging material such as bottle, lid, distributor (pump head) and
Dispense between apparatus enters packing after ultraviolet, ozonization and use.Cleaning, sterilization packing machine and conveyer after, half-and-half into
Product carry out filling.Outward appearance and metering test are examined by Quality Inspector on duty, and finished product examines qualified finished product can by laboratory inspection by sampling
With storage.Packaged qualified finished product transports finished room storage.
1st, procedure for producing homogeneous controls：Control temperature carries out homogeneous at 85 DEG C, homogenizing time control 5~8 minutes it
Between, stir.
2nd, vacuum production, vacuum packaging are paid attention to.
3rd, filling quality controls：The packaging material such as bottle, lid, distributor (pump head) and packing apparatus must be through ultraviolets, smelly
It is allowed for access between dispensing and uses after oxygen sterilization.Bottle placer and pipeline must cleaned, sterilization (with 75% alcohol) after can carry out
It is canned.The regulation of canned amount is by Quality Inspector's inspection and supervision on duty；It can be carried out after canned FAA first article assurance normal canned.
By the Wrinkle removing eye cream containing perfluorodecalin that above-described embodiment 1-3 is obtained according to by multiple fingers such as stability, both effectiveness
Mark carries out Experimental Comparison, and it is as shown in the table for the test parameters of acquisition.
Table 1 is each Wrinkle removing eye cream testing inspection results containing perfluorodecalin of embodiment 1-3
Test method：After nursing in 28 days, use the product containing 5%, 10% perfluorodecalin 2 times a day, 20 women by
Survey person, the age is between 25-55 year.As can be drawn from Table 1, the Wrinkle removing eye cream containing perfluorodecalin that technical scheme provides
It disclosure satisfy that the purpose of wrinkle reduction.
The grease of Wrinkle removing eye cream provided by the invention containing perfluorodecalin is compounded by isononyl isononanoate, saualane, DC200
Combination, the dosage of oil mass are controlled in 1-15%；Meet that grease will clearly, easily absorb, do not cause the burden of eye part skin.Add complete
Fluoronaphthalene alkane helps the skin optimization breathing of circumference of eyes, CO2 that can be in purifying skin and improves oxygen level so as to reduce skin
Wrinkle.
Embodiments of the present invention are explained in detail above, but the invention is not restricted to described embodiment.It is right
For those skilled in the art, in the case where not departing from the principle of the invention and spirit, these embodiments are carried out more
Kind change, modification, replacement and modification, still fall within protection scope of the present invention.
Claims (6)
1. a kind of Wrinkle removing eye cream containing perfluorodecalin, it is characterised in that it includes each raw material components of following percentage by weight：
Oil phase component：
O/W type emulsifying agents 0.1-3%；
16/18 alcohol 0.1-3%；
Isononyl isononanoate 0.1-5%；
Saualane 0.1-5%；
Polydimethyl siloxane fluid 0.5-5%；
Water phase components：
Glycerine 0.1-10%；
Butanediol 0.1-10%；
Water phase thickener 0.1-2%；
Deionized water 50-80%；
Additive：
Perfluorodecalin 0.1-20%；
Preservative 0.5%.
A kind of 2. Wrinkle removing eye cream containing perfluorodecalin according to claim 1, it is characterised in that the O/W types emulsifying agent
It is the mixture of cetostearyl alcohol glucoside, stearine and PEG-100 stearates.
A kind of 3. Wrinkle removing eye cream containing perfluorodecalin according to claim 1, it is characterised in that the polydimethyl siloxane fluid
It is DC200 silicone oil.
4. a kind of Wrinkle removing eye cream containing perfluorodecalin according to claim 1, it is characterised in that the water phase thickener is
Hydroxy-ethyl acrylate and the Taurate Copolymer of acryloyl two.
5. a kind of Wrinkle removing eye cream containing perfluorodecalin according to claim 1, it is characterised in that the preservative is oxybenzene
Methyl esters, Nipasol, Sensiva SC50, the preservative of 4 kinds of component mixing of Phenoxyethanol.
A kind of 6. preparation method of the Wrinkle removing eye cream containing perfluorodecalin, for preparing as described in claim 1-5 any one
Wrinkle removing eye cream containing perfluorodecalin, it is characterised in that the described method comprises the following steps：
S101, prepare recipe ingredient：Oil phase component：O/W types emulsifying agent 0.1-3%, isononyl isononanoate 0.1-5%, saualane
0.1-5%, polydimethyl siloxane fluid 0.5-5%, 16/18 alcohol 0.1-3%；Water phase components：Deionized water 50-80%, glycerine 0.1-
10%, butanediol 0.1-10%, water phase thickener 0.1-2%；Additive：Perfluorodecalin 0.1-20%, preservative 0.5%.
S102, by oil phase component：O/W types emulsifying agent 0.1-3%, isononyl isononanoate 0.1-5%, saualane 0.1-5%, poly- two
Methyl-silicone oil 0.5-5%%, 16/18 alcohol 0.1-3%, sequentially add heating stirring in oil phase pot and are dissolved to 85 DEG C；
S103, water phase components：Deionized water 50-80%, glycerine 0.1-10%, butanediol 0.1-10%, water phase thickener 0.1-
2%, sequentially add heating stirring in aqueous phase pot and be dissolved to 85 DEG C；
S104, the water phase components in the oil phase component in oil phase pot and aqueous phase pot are added in emulsification pot, and stir homogeneous 5-
8min is well mixed to oil phase component and water phase components；
S105, continue stirring and be cooled to 45 DEG C, add perfluorodecalin 0.1-20%, preservative 0.5% and with rotating speed 4000-
6000rpm stirs.
S106, standing are filling after 2 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711115607.4A CN107661223A (en) | 2017-11-13 | 2017-11-13 | A kind of Wrinkle removing eye cream containing perfluorodecalin and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711115607.4A CN107661223A (en) | 2017-11-13 | 2017-11-13 | A kind of Wrinkle removing eye cream containing perfluorodecalin and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN107661223A true CN107661223A (en) | 2018-02-06 |
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ID=61144369
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711115607.4A Pending CN107661223A (en) | 2017-11-13 | 2017-11-13 | A kind of Wrinkle removing eye cream containing perfluorodecalin and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109674582A (en) * | 2019-02-19 | 2019-04-26 | 郑岩 | A kind of Oxygen Generator oxygen supply treats wound the method and consumptive material of healing |
| CN111000750A (en) * | 2020-01-13 | 2020-04-14 | 蝶柔化妆品(浙江)有限公司 | Eye cream for quickly removing wrinkles |
-
2017
- 2017-11-13 CN CN201711115607.4A patent/CN107661223A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109674582A (en) * | 2019-02-19 | 2019-04-26 | 郑岩 | A kind of Oxygen Generator oxygen supply treats wound the method and consumptive material of healing |
| CN111000750A (en) * | 2020-01-13 | 2020-04-14 | 蝶柔化妆品(浙江)有限公司 | Eye cream for quickly removing wrinkles |
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Application publication date: 20180206 |