CN107653109A - A kind of antimicrobial soap and preparation method thereof - Google Patents

A kind of antimicrobial soap and preparation method thereof Download PDF

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Publication number
CN107653109A
CN107653109A CN201710969643.0A CN201710969643A CN107653109A CN 107653109 A CN107653109 A CN 107653109A CN 201710969643 A CN201710969643 A CN 201710969643A CN 107653109 A CN107653109 A CN 107653109A
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CN
China
Prior art keywords
parts
soap
antimicrobial
antimicrobial soap
saponification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710969643.0A
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Chinese (zh)
Inventor
巢雨
韦高
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guilin Chuang Technology Co Ltd
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Guilin Chuang Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guilin Chuang Technology Co Ltd filed Critical Guilin Chuang Technology Co Ltd
Priority to CN201710969643.0A priority Critical patent/CN107653109A/en
Publication of CN107653109A publication Critical patent/CN107653109A/en
Withdrawn legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen
    • C11D9/265Organic compounds, e.g. vitamins containing oxygen containing glycerol
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of antimicrobial soap and preparation method thereof, is related to articles for daily use technical field.The antimicrobial soap, surface-active in itself that have using lignosulfonates, scattered adsorption characteristic, chelating properties, hard water resistance and synergic remove, add it in soap system, make it under the conditions of high-hardness water, there is good decontamination and sterilization double effects;A kind of preparation method of antimicrobial soap provided by the invention, it is simple with method, production cost is low, and the characteristics of large-scale production can be applied to and be widely popularized, and prepared antimicrobial soap is without any preservative and other chemical substances, it is nontoxic, there is the advantages that dirt-removing power is strong, good antimicrobial effect, moistening skin-care.

Description

A kind of antimicrobial soap and preparation method thereof
Technical field
The invention belongs to articles for daily use technical field, more particularly to a kind of antimicrobial soap and preparation method thereof.
Background technology
Soap primarily serves bactericidal cleaning effect as commonly used cleaning products in daily life.As articles for washing Its performance in soft water is very excellent, but due to being limited by solubility in cold water, is washed during cold washing Poor-performing.In addition, the main component of soap is soap, intolerant to hard water, calcium not soluble in water, magnesium are easily formed in hard water Soap scum silica frost.Therefore when designing soap formulation, " lime soap dispersant " is commonly incorporated into increase the resistance to hard water ability of soap.By cost and The limitation of production technology, commercialized lime soap dispersant are simultaneously few.Conventional has AEO9, AES, MES, AOS etc., adds in soap Dosage is higher, and the detergency lifting effect to product is not notable, and AES, MES etc. are also easy to hydrolyze in alkaline system, It is unfavorable for the holding of the stabilization and performance of product.
Current soap species is various, and has many soap with health care and therapeutic effect commercially to occur, wherein A kind of is the soap for having antibacterial bacteriostatic function.Antimicrobial soap huge number, but the removal of bacteria effect on clothing is not Substantially, and Conventional soaps contain the material being harmful to human body skin:Such as bleaching powder, mercury, cleaning agent, corrosive agent.Therefore, open Hair is containing natural antibacterial ingredient and has clean effect, and has great importance to the soap of human body fanout free region.
The content of the invention
In view of the shortcomings of the prior art, the present invention provides a kind of antimicrobial soap and preparation method thereof.
The present invention is that solve above-mentioned technical problem by the following technical solutions:A kind of antimicrobial soap, by following heavy The component of amount part is made:Lignosulfonates 5-12 parts, highly basic 5-15 parts, grease 15-55 parts, absolute ethyl alcohol 3-8 parts, glycerine 2- 5 parts, plant additive 3-8 parts, water 10-35 parts.
Further, the plant additive includes one kind in coffee grounds, dregs of beans, the wine dregs of rice, grape pip and sunflower seeds It is or a variety of.
Further, the highly basic is sodium hydroxide solution or potassium hydroxide solution.
Further, the grease includes palm oil, coconut oil, olive oil, evening primrose oil and stearic combination.
Further, a kind of preparation method of antimicrobial soap, comprises the following steps:
(1)Prepare soap lye:By the highly basic of 5-15 parts, the grease of 15-55 parts, the absolute ethyl alcohol of 3-8 parts, 2-5 parts glycerine and The water of 10-35 parts, by being mixed evenly, thick shape soap lye is made;
(2)Saponification:By the step(1)Obtained thick shape soap lye is heated to 35-60 DEG C of progress saponification certain time, saponification After the completion of reaction, add the lignosulfonates of 5-12 parts and the plant additive of 3-8 parts is configured to premixed liquid, then stirring is equal It is even, soap semi-finished product are made;
(3)It is cooled and shaped:By the step(2)Obtained soap semi-finished product are poured into mould, are then cooled and shaped, and adopt It is freeze-dried with vacuum freeze drier, that is, the antimicrobial soap is made.
Further, the step(1)In time of saponification be 5-8 hours.
Compared with prior art, antimicrobial soap provided by the present invention, the surface having in itself using lignosulfonates Activity, scattered adsorption characteristic, chelating properties, hard water resistance and synergic remove, are added it in soap system, make its Under the conditions of high-hardness water, there is good decontamination and sterilization double effects;A kind of preparation of antimicrobial soap provided by the invention Method, has that method is simple, and production cost is low, and can be applied to large-scale production and the characteristics of be widely popularized, Er Qiesuo The antimicrobial soap of preparation is nontoxic without any preservative and other chemical substances, has that dirt-removing power is strong, good antimicrobial effect, The advantages that moistening skin-care.
Embodiment
The technical scheme in the present invention is clearly and completely described below, it is clear that described embodiment is only Part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art The every other embodiment obtained on the premise of creative work is not made, belongs to the scope of protection of the invention.
A kind of antimicrobial soap provided by the present invention, is made up of the component of following parts by weight:Lignosulfonates 5-12 parts, Highly basic 5-15 parts, grease 15-55 parts, absolute ethyl alcohol 3-8 parts, glycerine 2-5 parts, plant additive 3-8 parts, water 10-35 parts.
Plant additive includes the one or more in coffee grounds, dregs of beans, the wine dregs of rice, grape pip and sunflower seeds.
Highly basic is sodium hydroxide solution or potassium hydroxide solution.Grease includes palm oil, coconut oil, olive oil, oenothera biennis Oily and stearic combination.
A kind of preparation method of antimicrobial soap, comprises the following steps:
(1)Prepare soap lye:By the highly basic of 5-15 parts, the grease of 15-55 parts, the absolute ethyl alcohol of 3-8 parts, 2-5 parts glycerine and The water of 10-35 parts, by being mixed evenly, thick shape soap lye is made;
(2)Saponification:By step(1)Obtained thick shape soap lye is heated to 35-60 DEG C of progress saponification certain time, saponification After the completion of, add the lignosulfonates of 5-12 parts and the plant additive of 3-8 parts be configured to premixed liquid, then stir, Soap semi-finished product are made;
(3)It is cooled and shaped:By step(2)Obtained soap semi-finished product are poured into mould, are then cooled and shaped, and using true Vacuum freecing-dry machine is freeze-dried, that is, antimicrobial soap is made.
Step(1)In time of saponification be 5-8 hours.
Embodiment 1
A kind of antimicrobial soap, it is made up of the component of following parts by weight:10 parts of lignosulfonates, 8 parts of highly basic, 28 parts of grease, nothing 8 parts of water-ethanol, 5 parts of glycerine, 3 parts of plant additive, 35 parts of water.
Plant additive includes coffee grounds, dregs of beans and grape pip.
Highly basic is sodium hydroxide solution.
Grease includes palm oil, coconut oil, olive oil, evening primrose oil and stearic combination.
A kind of preparation method of antimicrobial soap, comprises the following steps:
(1)Prepare soap lye:By 8 parts of highly basic, 28 parts of grease, 8 parts of absolute ethyl alcohol, 5 parts of glycerine and 35 parts of water, lead to Cross and be mixed evenly, thick shape soap lye is made;
(2)Saponification:By step(1)Obtained thick shape soap lye is heated to 45-55 DEG C and carries out saponification 5 hours, and saponification is complete Cheng Hou, the lignosulfonates and 3 parts of plant additive for adding 10 parts are configured to premixed liquid, then stirred, and fertilizer is made Soap semi-finished product;
(3)It is cooled and shaped:By step(2)Obtained soap semi-finished product are poured into mould, are then cooled and shaped, and using true Vacuum freecing-dry machine is freeze-dried, that is, antimicrobial soap is made.
Embodiment 2
A kind of antimicrobial soap, it is made up of the component of following parts by weight:12 parts of lignosulfonates, 5 parts of highly basic, 40 parts of grease, nothing 8 parts of water-ethanol, 5 parts of glycerine, 8 parts of plant additive, 35 parts of water.
Plant additive includes dregs of beans, the wine dregs of rice, sunflower seeds.Highly basic is potassium hydroxide solution.
Grease includes palm oil, coconut oil, olive oil, evening primrose oil and stearic combination.
A kind of preparation method of antimicrobial soap, comprises the following steps:
(1)Prepare soap lye:By 5 parts of highly basic, 40 parts of grease, 8 parts of absolute ethyl alcohol, 5 parts of glycerine and 35 parts of water, lead to Cross and be mixed evenly, thick shape soap lye is made;
(2)Saponification:By step(1)Obtained thick shape soap lye is heated to 35-45 DEG C and carries out saponification 8 hours, and saponification is complete Cheng Hou, the lignosulfonates and 8 parts of plant additive for adding 12 parts are configured to premixed liquid, then stirred, and fertilizer is made Soap semi-finished product;
(3)It is cooled and shaped:By step(2)Obtained soap semi-finished product are poured into mould, are then cooled and shaped, and using true Vacuum freecing-dry machine is freeze-dried, that is, antimicrobial soap is made.
Above disclosed is only the embodiment of the present invention, but protection scope of the present invention is not limited thereto, Any one skilled in the art the invention discloses technical scope in, can readily occur in change or modification, all It should be included within the scope of the present invention.

Claims (6)

  1. A kind of 1. antimicrobial soap, it is characterised in that:It is made up of the component of following parts by weight:Lignosulfonates 5-12 parts, highly basic 5-15 parts, grease 15-55 parts, absolute ethyl alcohol 3-8 parts, glycerine 2-5 parts, plant additive 3-8 parts, water 10-35 parts.
  2. 2. antimicrobial soap as claimed in claim 1, it is characterised in that:The plant additive includes coffee grounds, dregs of beans, wine One or more in the dregs of rice, grape pip and sunflower seeds.
  3. 3. antimicrobial soap as claimed in claim 1, it is characterised in that:The highly basic is that sodium hydroxide solution or potassium hydroxide are molten Liquid.
  4. 4. antimicrobial soap as claimed in claim 1, it is characterised in that:The grease include palm oil, coconut oil, olive oil, Evening primrose oil and stearic combination.
  5. 5. a kind of preparation method of antimicrobial soap, it is characterised in that comprise the following steps:
    (1)Prepare soap lye:By the highly basic of 5-15 parts, the grease of 15-55 parts, the absolute ethyl alcohol of 3-8 parts, 2-5 parts glycerine and The water of 10-35 parts, by being mixed evenly, thick shape soap lye is made;
    (2)Saponification:By the step(1)Obtained thick shape soap lye is heated to 35-60 DEG C of progress saponification certain time, saponification After the completion of reaction, add the lignosulfonates of 5-12 parts and the plant additive of 3-8 parts is configured to premixed liquid, then stirring is equal It is even, soap semi-finished product are made;
    (3)It is cooled and shaped:By the step(2)Obtained soap semi-finished product are poured into mould, are then cooled and shaped, and adopt It is freeze-dried with vacuum freeze drier, that is, the antimicrobial soap is made.
  6. 6. the preparation method of antimicrobial soap as claimed in claim 5, it is characterised in that:The step(1)In saponification Time be 5-8 hours.
CN201710969643.0A 2017-10-18 2017-10-18 A kind of antimicrobial soap and preparation method thereof Withdrawn CN107653109A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710969643.0A CN107653109A (en) 2017-10-18 2017-10-18 A kind of antimicrobial soap and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710969643.0A CN107653109A (en) 2017-10-18 2017-10-18 A kind of antimicrobial soap and preparation method thereof

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CN107653109A true CN107653109A (en) 2018-02-02

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109825391A (en) * 2019-03-06 2019-05-31 扬州鸿和达塑胶日化有限公司 A kind of soap and its circulation production process process

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106883957A (en) * 2017-04-17 2017-06-23 帝善圆农业科技(苏州)有限公司 A kind of soap and preparation method thereof
CN107012029A (en) * 2017-03-24 2017-08-04 广东医科大学 A kind of antimicrobial soap and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107012029A (en) * 2017-03-24 2017-08-04 广东医科大学 A kind of antimicrobial soap and preparation method thereof
CN106883957A (en) * 2017-04-17 2017-06-23 帝善圆农业科技(苏州)有限公司 A kind of soap and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109825391A (en) * 2019-03-06 2019-05-31 扬州鸿和达塑胶日化有限公司 A kind of soap and its circulation production process process

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Application publication date: 20180202

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