CN103937621A - Tea saponin-containing pesticide removal detergent and preparation method thereof - Google Patents
Tea saponin-containing pesticide removal detergent and preparation method thereof Download PDFInfo
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- CN103937621A CN103937621A CN201410141759.1A CN201410141759A CN103937621A CN 103937621 A CN103937621 A CN 103937621A CN 201410141759 A CN201410141759 A CN 201410141759A CN 103937621 A CN103937621 A CN 103937621A
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Abstract
The invention discloses a tea saponin-containing pesticide removal detergent and a preparation method thereof and relates to a pesticide detergent and a preparation method thereof. The preparation method comprises the following steps: heating the following components in a water bath at the temperature of 10 to 60 DEG C in parts by weight: 3-10 parts of alkyl glycoside, 1-7 parts of alpha-alkenyl sodium sulfonate, 1-8 parts of fatty alcohol-polyoxyethylene ether sodium sulfate and 1-8 parts of coco fatty acid diethanol amide, stirring and mixing, adding 0.1-2 parts of sodium ethylene diamine tetraacetic acid, 0.5-3 parts of wool fat, 0.5-3 parts of propylene glycol, the residual distilled water and 0.1-5 parts of tea saponin solution after the previous materials are uniformly mixed, stirring for 5-40 minutes, adding citric acid to regulate the pH value, adding 0.5-3 parts of refined salt, and regulating the viscosity characters of the detergent through a wiredrawing agent. The tea saponin and multiple surfactants such as the alkyl glycoside are compatible with one another, and a pesticide removal effect of the detergent is improved. The tea saponin and multiple surfactants such as the alkyl glycoside are compatible with one another, so that the pesticide residue removal efficiency of the detergent is greatly improved.
Description
Technical field
The present invention relates to a kind of agricultural chemicals washing composition and preparation method thereof, particularly relate to a kind of tea saponin that contains except agricultural chemicals washing composition and preparation method thereof.
Background technology
The personnel's of food Pesticide Residue and the relevant industries that contact with agricultural chemicals health problem is of common occurrence.Using washing composition clean is to solve the simplest and the most direct method of this pesticide residue problem.It is high that washing composition should meet scrubbing efficiency, and decontamination degerming speed is fast, with low cost, the features such as green low residue.The present invention is taking natural green tensio-active agent as raw material, main component: alkyl glycoside, α-sodium olefin sulfonate, polyoxyethylenated alcohol sodium sulfate, lauric acid amide of ethanol, tea saponin etc., with refined salt, ethylenediamine tetraacetic sodium oxalate, citric acid, wire drawing agent regulates washing composition proterties.
Summary of the invention
The object of the present invention is to provide a kind of tea saponin that contains except agricultural chemicals washing composition and preparation method thereof, the present invention, by adding the kinds of surface promoting agent compatibilities such as tea saponin and alkyl glycoside, improves washing composition and removes agricultural chemicals effect.By the kinds of surface such as tea saponin and alkyl glycoside promoting agent compatibility, greatly improve washing composition and remove pesticide residue efficiency.
The object of the invention is to be achieved through the following technical solutions:
Containing tea saponin, except agricultural chemicals washing composition, described washing composition is in weight part, and its proportioning is as follows:
Alkyl glycoside 10-3 part; α-sodium olefin sulfonate 7-1 part; Polyoxyethylenated alcohol sodium sulfate 8-1 part; Lauric acid amide of ethanol 8-1 part; Ethylenediamine tetraacetic sodium oxalate 2-0.1 part; Refined salt 3-0.5 part; Lanolin 3-0.5 part; Citric acid appropriate (regulating PH); Propylene glycol 3-0.5 part; 80 parts of distilled water; Tea saponin solution 5-0.1 part.
Described removes agricultural chemicals washing composition containing tea saponin, described tea saponin solution is that 1-3g crude product tea saponin is dissolved in 15-30ml ethanol, under 20~80 DEG C of water-baths, with 5~40ml hydrogen peroxide and the decolouring of 1~8ml sodium hydroxide, after decompress filter, obtain the tea saponin solution after refining.
The described preparation method except agricultural chemicals washing composition containing tea saponin, described method comprises following process: first, alkyl glycoside 10-3 part by weight, α-sodium olefin sulfonate 7-1 part, polyoxyethylenated alcohol sodium sulfate 8-1 part, lauric acid amide of ethanol 8-1 part, heating in water bath at 10~60 DEG C, be uniformly mixed, to be mixedly evenly add ethylenediamine tetraacetic sodium oxalate 2-0.1 part, lanolin 3-0.5 part, propylene glycol 3-0.5 part, distilled water surplus, tea saponin solution 5-0.1 part, stir 5~40 minutes, add citric acid and regulate PH, refined salt 3-0.5 part, wire drawing agent regulates washing composition Viscosity Traits.
Advantage of the present invention and effect are:
The present invention, by adding the kinds of surface promoting agent compatibilities such as tea saponin and alkyl glycoside, improves washing composition except agricultural chemicals effect.By the kinds of surface such as tea saponin and alkyl glycoside promoting agent compatibility, greatly improve washing composition and remove pesticide residue efficiency.Can be used as Liquid soap, also can be used for melon, fruit and vegetable cleaning agent.Quality product meets QB/T 2654-2013.
Embodiment
Below in conjunction with embodiment, the invention will be further described.
The tea saponin that contains of the present invention, except agricultural chemicals washing composition, is characterized in that: by weight, its formula is as follows:
Alkyl glycoside 10-3 part; α-sodium olefin sulfonate 7-1 part; Polyoxyethylenated alcohol sodium sulfate 8-1 part; Lauric acid amide of ethanol 8-1 part; Ethylenediamine tetraacetic sodium oxalate 2-0.1 part; Refined salt 3-0.5 part; Lanolin 3-0.5 part; Citric acid appropriate (regulating PH); Propylene glycol 3-0.5 part; 80 parts of distilled water; Tea saponin solution 5-0.1 part.
Raw material of the present invention can commercially availablely obtain.Its tea saponin: natural sugar glycoside compound is a kind of natural nonionogenic tenside, and chemical property gentleness, is easy to biological degradation, is all having good performance aspect the emulsification of dispersion, foaming, decontamination and O/W type.Crude product tea saponin color is darker, the processing of need to decolouring.
Polyoxyethylenated alcohol sodium sulfate: green anion surfactant, nontoxic, good water solubility, character gentleness, does not injure skin, moistening, foaminess is better.
α-sodium olefin sulfonate: green anion surfactant, its good combination property, water-soluble very high, foaming power is strong, and biological degradability is good, has good detersive power, also demonstrates especially the feature that detersive power does not reduce substantially in hard water.
Lauric acid amide of ethanol: nontoxic nonionogenic tenside, there is excellent thickening properties, the performances such as its foaming and steady bubble are also better, can composite high viscosity product.
Alkyl glycoside: the more comprehensive new non-ionic surfactants of performance, have the characteristic of common nonionic and anion surfactant concurrently, having high surface, good ecological security and intermiscibility, is internationally recognized first-selection " green " functional surface promoting agent.Its principal feature is: abundant fine and smooth, the foam stability of gentle non-stimulated, foam can be good, have stronger compatibleness, can with polytype surfactant compound, synergistic effect obviously, can greatly reduce the pungency of anion surfactant in formula, stronger broad spectrum antibiotic activity.
Embodiment 1:
The present invention by weight, alkyl glycoside 10-3 part, α-sodium olefin sulfonate 7-1 part, polyoxyethylenated alcohol sodium sulfate 8-1 part, lauric acid amide of ethanol 8-1 part is added to the water, heating in water bath 2-3 hour at 10~60 DEG C, after stirring to clarify, add ethylenediamine tetraacetic sodium oxalate 2-0.1 part, lanolin 3-0.5 part, propylene glycol 3-0.5 part, distilled water surplus, decolouring tea saponin solution 5-0.1 part, stirs 5~40 minutes, adds citric acid and regulates PH=5.8-6.5, refined salt 3-0.5 part, wire drawing agent regulates washing composition Viscosity Traits.At-5~45 DEG C 48 hours not stratified, not muddy, do not precipitate, do not solidify, obtain product.
Claims (3)
1. remove agricultural chemicals washing composition containing tea saponin, it is characterized in that, described washing composition is in weight part, and its proportioning is as follows:
Alkyl glycoside 10-3 part; α-sodium olefin sulfonate 7-1 part; Polyoxyethylenated alcohol sodium sulfate 8-1 part; Lauric acid amide of ethanol 8-1 part; Ethylenediamine tetraacetic sodium oxalate 2-0.1 part; Refined salt 3-0.5 part; Lanolin 3-0.5 part; Citric acid appropriate (regulating PH); Propylene glycol 3-0.5 part; 80 parts of distilled water; Tea saponin solution 5-0.1 part.
2. the tea saponin that contains according to claim 1 is except agricultural chemicals washing composition, it is characterized in that, described tea saponin solution is that 1-3g crude product tea saponin is dissolved in 15-30ml ethanol, under 20~80 DEG C of water-baths, with 5~40ml hydrogen peroxide and the decolouring of 1~8ml sodium hydroxide, after decompress filter, obtain the tea saponin solution after refining.
3. the preparation method who removes agricultural chemicals washing composition containing tea saponin according to claim 1, it is characterized in that, described method comprises following process: first, alkyl glycoside 10-3 part by weight, α-sodium olefin sulfonate 7-1 part, polyoxyethylenated alcohol sodium sulfate 8-1 part, lauric acid amide of ethanol 8-1 part, heating in water bath at 10~60 DEG C, be uniformly mixed, to be mixedly evenly add ethylenediamine tetraacetic sodium oxalate 2-0.1 part, lanolin 3-0.5 part, propylene glycol 3-0.5 part, distilled water surplus, tea saponin solution 5-0.1 part, stir 5~40 minutes, add citric acid and regulate PH, refined salt 3-0.5 part, wire drawing agent regulates washing composition Viscosity Traits.
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CN201410141759.1A CN103937621A (en) | 2014-04-10 | 2014-04-10 | Tea saponin-containing pesticide removal detergent and preparation method thereof |
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CN201410141759.1A CN103937621A (en) | 2014-04-10 | 2014-04-10 | Tea saponin-containing pesticide removal detergent and preparation method thereof |
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CN201410141759.1A Pending CN103937621A (en) | 2014-04-10 | 2014-04-10 | Tea saponin-containing pesticide removal detergent and preparation method thereof |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105039003A (en) * | 2015-05-28 | 2015-11-11 | 上海仕操洗涤有限公司 | Fabric washing and wastewater recycling detergent, preparation method and uses thereof |
CN107955738A (en) * | 2017-12-04 | 2018-04-24 | 湖南金昌生物技术有限公司 | A kind of Tea Saponin neutrality vegetables and fruits cleaning agent and preparation method thereof |
CN108060028A (en) * | 2017-12-05 | 2018-05-22 | 徐云丽 | Green fruit-vegetable detergent |
CN108085162A (en) * | 2017-12-05 | 2018-05-29 | 徐云丽 | Environmentally protective detergent |
Citations (3)
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CN1621504A (en) * | 2003-11-27 | 2005-06-01 | 上海白猫有限公司 | Cleaning agent for vegetable and fruit |
US20060286062A1 (en) * | 2005-06-06 | 2006-12-21 | Schep Raymond A | Completely natural plant based shampoo and body wash devoid of synthetic ingredients |
CN102010798A (en) * | 2010-11-27 | 2011-04-13 | 郴州邦尔泰苏仙油脂有限公司 | Detergent for washing tableware or vegetables and fruits by hands |
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2014
- 2014-04-10 CN CN201410141759.1A patent/CN103937621A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1621504A (en) * | 2003-11-27 | 2005-06-01 | 上海白猫有限公司 | Cleaning agent for vegetable and fruit |
US20060286062A1 (en) * | 2005-06-06 | 2006-12-21 | Schep Raymond A | Completely natural plant based shampoo and body wash devoid of synthetic ingredients |
CN102010798A (en) * | 2010-11-27 | 2011-04-13 | 郴州邦尔泰苏仙油脂有限公司 | Detergent for washing tableware or vegetables and fruits by hands |
Non-Patent Citations (1)
Title |
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詹益兴: "《现代化工小商品制法大全 第3集》", 31 August 1999, 湖南大学出版社 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105039003A (en) * | 2015-05-28 | 2015-11-11 | 上海仕操洗涤有限公司 | Fabric washing and wastewater recycling detergent, preparation method and uses thereof |
CN105039003B (en) * | 2015-05-28 | 2018-02-23 | 上海仕操洗涤有限公司 | A kind of fabric washing and waste water circulation reuse detergent and its production and use |
CN107955738A (en) * | 2017-12-04 | 2018-04-24 | 湖南金昌生物技术有限公司 | A kind of Tea Saponin neutrality vegetables and fruits cleaning agent and preparation method thereof |
CN108060028A (en) * | 2017-12-05 | 2018-05-22 | 徐云丽 | Green fruit-vegetable detergent |
CN108085162A (en) * | 2017-12-05 | 2018-05-29 | 徐云丽 | Environmentally protective detergent |
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