CN110511826A - It is a kind of to sterilize nontoxic machine dishwasher detergent and preparation method thereof - Google Patents
It is a kind of to sterilize nontoxic machine dishwasher detergent and preparation method thereof Download PDFInfo
- Publication number
- CN110511826A CN110511826A CN201910816898.2A CN201910816898A CN110511826A CN 110511826 A CN110511826 A CN 110511826A CN 201910816898 A CN201910816898 A CN 201910816898A CN 110511826 A CN110511826 A CN 110511826A
- Authority
- CN
- China
- Prior art keywords
- parts
- immersion liquid
- sodium
- nontoxic
- dishwasher detergent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/08—Silicates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/3427—Organic compounds containing sulfur containing thiol, mercapto or sulfide groups, e.g. thioethers or mercaptales
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3715—Polyesters or polycarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38618—Protease or amylase in liquid compositions only
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38636—Preparations containing enzymes, e.g. protease or amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase or reductase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of nontoxic machine dishwasher detergents of sterilization and preparation method thereof, more particularly to detergent technical field, including following component and its parts by weight: 40-60 parts of sodium metasilicate, 40-60 parts of sodium citrate, 10-20 parts of SODIUM PERCARBONATE, 20-30 parts of sodium carbonate, 1-5 parts of spaonin powder, 10-20 parts of soapberry pericarp immersion liquid, 1-5 parts of allyl sulfides, 10-20 parts of lemon eucalyptus leaf immersion liquid, 1-3 parts of brightener, 1-5 parts of nonionic surfactant, 4-10 parts of polycarboxylate, 4-10 parts of bleaching agent, 1-5 parts of enzyme preparation and 30-50 parts of deionized water.The present invention passes through the fungistatic effect using the immersion liquid of soapberry pericarp and lemon eucalyptus leaf immersion liquid, it goes to make up due to the active hypoxgia that SODIUM PERCARBONATE content is lower and occurs, lead to the unconspicuous problem of bactericidal effect, the SODIUM PERCARBONATE of lower content is in the course of work of dish-washing machine simultaneously, it is easily decomposes, there is no residue problem, thus achieved the purpose that dishwasher detergent is nontoxic and sterilization is good, it is environmentally protective.
Description
Technical field
The present invention relates to detergent technical fields, it is more particularly related to a kind of nontoxic machine dishwasher detergent of sterilization
And preparation method thereof.
Background technique
Dish-washing machine is the equipment of the tablewares such as automatic cleaning bowl, chopsticks, disk, dish, knife, fork.Tableware is washed using dish-washing machine, it can be big
Mitigate cumbersome hand labour greatly.Only the tableware that will be washed is needed to be put into dish-washing machine, opens tap, one presses a button, and can put to the greatest extent
Heart does other things, because waiting in washing process without someone, can be automatically performed operation.
The working principle of dish-washing machine is that water pump smokes the liquid for being accumulated in lower part, then washes away tableware in spurting, then plus
The booster action of upper detergent can be realized tableware deep clean.Dishwasher detergent used in dish-washing machine is mostly the dishwasher detergent of profession,
Spot is decomposed by enzyme.But in existing dishwasher detergent, the content of SODIUM PERCARBONATE is higher, although SODIUM PERCARBONATE is in the mistake used
It is able to carry out decomposition, and the product good water solubility after decomposition in journey, but still suffers from some residuals, prevent dishwasher detergent is from reaching
To while sterilization and again nontoxic effect.
Summary of the invention
In order to overcome the drawbacks described above of the prior art, the embodiment of the present invention provide a kind of nontoxic machine dishwasher detergent of sterilization and
Preparation method obtains the immersion liquid of soapberry pericarp by impregnating after crushing soapberry pericarp and lemon eucalyptus leaf through deionized water
With lemon eucalyptus leaf immersion liquid, the raw materials such as sodium metasilicate, sodium citrate, SODIUM PERCARBONATE, sodium carbonate are combined with, in the process for preparing dishwasher detergent
In, it can reduce the content of SODIUM PERCARBONATE in raw material, using the fungistatic effect of the immersion liquid of soapberry pericarp and lemon eucalyptus leaf immersion liquid, go
It makes up due to the active hypoxgia that SODIUM PERCARBONATE content is lower and occurs, leads to the unconspicuous problem of bactericidal effect, while lower
The SODIUM PERCARBONATE of content can decompose generation active oxygen in the course of work of dish-washing machine, since active oxygen is too active, very
It is easy to oxidize, it is water-soluble fabulous, without residue problem, thus achieved the purpose that dishwasher detergent is nontoxic and sterilization is good, it is environmentally protective.
To achieve the above object, the invention provides the following technical scheme: a kind of sterilize nontoxic machine dishwasher detergent, including it is following
Ingredient and its parts by weight: 40-60 parts of sodium metasilicate, 40-60 parts of sodium citrate, 10-20 parts of SODIUM PERCARBONATE, 20-30 parts of sodium carbonate, soap
Powder 1-5 parts of angle, 10-20 parts of soapberry pericarp immersion liquid, 1-5 parts of allyl sulfides, 10-20 parts of lemon eucalyptus leaf immersion liquid, brightener 1-3
Part, 1-5 parts of nonionic surfactant, 4-10 parts of polycarboxylate, 4-10 parts of bleaching agent, 1-5 parts of enzyme preparation and deionized water 30-
50 parts；
The soapberry pericarp immersion liquid after crushed, impregnates 3-5 using the deionized water of 1:1 equal portions ratio by soapberry pericarp
Hour is made；
The lemon eucalyptus leaf immersion liquid after crushed, is impregnated 3-5 hours by lemon eucalyptus leaf using the deionized water of 1:1 equal portions ratio
It is made.
In a preferred embodiment, including following component and its parts by weight: 45-55 parts of sodium metasilicate, sodium citrate
45-55 parts, 12-18 parts of SODIUM PERCARBONATE, 22-28 parts of sodium carbonate, 2-4 parts of spaonin powder, 12-18 parts of soapberry pericarp immersion liquid, vulcanization
2-4 parts of propylene, 12-18 parts of lemon eucalyptus leaf immersion liquid, 1.5-2.5 parts of brightener, 2-4 parts of nonionic surfactant, polycarboxylate
6-8 parts, 6-8 parts of bleaching agent, 2-4 parts of enzyme preparation and 35-45 parts of deionized water.
In a preferred embodiment, including following component and its parts by weight: 50 parts of sodium metasilicate, sodium citrate 50
Part, 15 parts of SODIUM PERCARBONATE, 25 parts of sodium carbonate, 3 parts of spaonin powder, 15 parts of soapberry pericarp immersion liquid, 3 parts of allyl sulfides, lemon eucalyptus leaf
15 parts of immersion liquid, 2 parts of brightener, 3 parts of nonionic surfactant, 7 parts of polycarboxylate, 7 parts of bleaching agent, 3 parts of enzyme preparation and go from
40 parts of sub- water.
In a preferred embodiment, the enzyme preparation is specially the mixture of protease, amylase and phytase,
The protease, amylase and phytase mixed proportion are 1:1:3.
In a preferred embodiment, the particle mesh number of the spaonin powder is 300-500 mesh.
A kind of preparation method for sterilizing nontoxic machine dishwasher detergent, specifically comprises the following steps:
Step 1, by 15 parts of soapberry pericarp immersion liquid, 15 parts of lemon eucalyptus leaf immersion liquid and 3 parts of spaonin powder investments to reaction kettle
It is interior, 3 hours are kept the temperature after being warming up to 60 degrees Celsius, then it is stirred 10-15 minutes, after mixing them thoroughly, A is obtained
Phase；
40 parts of deionized water are poured into ingredients pot by step 2, to it inside successively add 50 parts of sodium metasilicate, citric acid
50 parts of sodium, 15 parts of SODIUM PERCARBONATE and 25 parts of sodium carbonate, using blender with revolving speed stirring 5-10 minutes of 120 revs/min, then
2 parts and 3 parts of nonionic surfactant of brightener are added while stirring, makes it after completely dissolution, obtains B phase；
Step 3 pours into B phase inside sealable container, and A phase is added in B phase, and adds 3 parts of allyl sulfides,
After stirring 3 minutes using blender with 120 revs/min of revolving speed, remove the dross and impurity of solution surface, then by container into
Row sealing, is placed under normal temperature environment after standing 6-8 hours, obtains C phase；
Step 4 is successively added 7 parts of polycarboxylate, 7 parts of bleaching agent and 3 parts of enzyme preparation into C phase, and is risen to container
Temperature, after the solution in container is warming up to 50 degrees Celsius, to the solution in container be stirred neutralize pH to 7-8 after, obtain at
Product sterilize nontoxic machine dishwasher detergent.
In a preferred embodiment, in the step 1, the speed of agitator of reaction kettle is 60 revs/min.
In a preferred embodiment, in the step 3, the temperature of standing is 10-20 degrees Celsius, the step
Speed of agitator in four is 80 revs/min.
Technical effect and advantage of the invention:
1, by will soapberry pericarp and lemon eucalyptus leaf crush after impregnate through deionized water, obtain the immersion liquid of soapberry pericarp and
Lemon eucalyptus leaf immersion liquid is combined with the raw materials such as sodium metasilicate, sodium citrate, SODIUM PERCARBONATE, sodium carbonate, in the process for preparing dishwasher detergent
In, it can reduce the content of SODIUM PERCARBONATE in raw material, using the fungistatic effect of the immersion liquid of soapberry pericarp and lemon eucalyptus leaf immersion liquid, go
It makes up due to the active hypoxgia that SODIUM PERCARBONATE content is lower and occurs, leads to the unconspicuous problem of bactericidal effect, while lower
The SODIUM PERCARBONATE of content can decompose generation active oxygen in the course of work of dish-washing machine, since active oxygen is too active, very
It is easy to oxidize, it is water-soluble fabulous, without residue problem, thus achieved the purpose that dishwasher detergent is nontoxic and sterilization is good, it is environmentally protective；
2, it after by being mixed soapberry pericarp immersion liquid with spaonin powder, is heated up and is kept the temperature, stirred evenly simultaneously,
It dilute the effective component in soapberry pericarp solution and spaonin powder can sufficiently, the soapberry contained using soapberry pericarp
The triterpenoid saponins such as saponin(e are cleaned, and serve as surfactant using spaonin powder, with the nonionic surfactant in raw material
It is used cooperatively, has the effects that wetting, emulsification, dispersion, so that dirt be removed, improve the cleaning ability to grease stain, and pure day
It is so nuisanceless；
3, the immersion liquid of soapberry pericarp and lemon eucalyptus leaf immersion liquid is cooperated to carry out assisting sterilisation by addition allyl sulfides, further
Compensate for the sterilization problem as brought by active hypoxgia, and allyl sulfides high volatility, noresidue, green non-poisonous
Under the premise of, it ensure that the bactericidal effect of dishwasher detergent, present invention process is simple, and equipment requirement is low, strong operability, has good
Society generalization application.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Embodiment 1:
A kind of nontoxic machine dishwasher detergent of sterilization, including following component and its parts by weight: sodium metasilicate, sodium citrate, percarbonic acid
Sodium, sodium carbonate, spaonin powder, the immersion liquid of soapberry pericarp, allyl sulfides, lemon eucalyptus leaf immersion liquid, brightener, non-ionic surface active
Agent, polycarboxylate, bleaching agent, enzyme preparation and deionized water；
Wherein, the soapberry pericarp immersion liquid by soapberry pericarp after crushed, utilize the deionization water logging of 1:1 equal portions ratio
Bubble is made for 4 hours；
The lemon eucalyptus leaf immersion liquid after crushed, is impregnated 4 hours using the deionized water of 1:1 equal portions ratio and is made by lemon eucalyptus leaf
At；
And specific in the present embodiment, specifically: 50 parts of sodium metasilicate, 50 parts of sodium citrate, 15 parts of SODIUM PERCARBONATE, sodium carbonate
25 parts, 3 parts of spaonin powder, 15 parts of soapberry pericarp immersion liquid, 3 parts of allyl sulfides, 15 parts of lemon eucalyptus leaf immersion liquid, 2 parts of brightener, it is non-from
3 parts of sub- surfactant, 7 parts of polycarboxylate, 7 parts of bleaching agent, 3 parts of enzyme preparation and 40 parts of deionized water；
Further, in mentioned component, the enzyme preparation is specially the mixture of protease, amylase and phytase, institute
Stating protease, amylase and phytase mixed proportion is 1:1:3, and the particle mesh number of the spaonin powder is 400 mesh；
On the basis of above-mentioned, a kind of preparation method for sterilizing nontoxic machine dishwasher detergent specifically comprises the following steps:
Step 1, by 15 parts of soapberry pericarp immersion liquid, 15 parts of lemon eucalyptus leaf immersion liquid and 3 parts of spaonin powder investments to reaction kettle
It is interior, 3 hours are kept the temperature after being warming up to 60 degrees Celsius, then it is carried out to stir 13 minutes with 60 revs/min of speed, makes it sufficiently
After mixing, A phase is obtained；
40 parts of deionized water are poured into ingredients pot by step 2, to it inside successively add 50 parts of sodium metasilicate, citric acid
50 parts of sodium, 15 parts of SODIUM PERCARBONATE and 25 parts of sodium carbonate are stirred 8 minutes with 120 revs/min of revolving speed using blender, are then existed
2 parts and 3 parts of nonionic surfactant of brightener are added in the state of stirring, makes it after completely dissolution, obtains B phase；
Step 3 pours into B phase inside sealable container, and A phase is added in B phase, and adds 3 parts of allyl sulfides,
After stirring 3 minutes using blender with 120 revs/min of revolving speed, remove the dross and impurity of solution surface, then by container into
Row sealing after being placed in indoor standing 7 hours of 15 degrees Celsius, obtains C phase；
Step 4 is successively added 7 parts of polycarboxylate, 7 parts of bleaching agent and 3 parts of enzyme preparation into C phase, and is risen to container
Temperature after the solution in container is warming up to 50 degrees Celsius, neutralizes pH to the solution in container with 80 revs/min of revolving speed stirring and arrives
After 7, finished product is obtained, that is, sterilizes nontoxic machine dishwasher detergent.
Embodiment 2:
A kind of nontoxic machine dishwasher detergent of sterilization, including following component and its parts by weight: sodium metasilicate, sodium citrate, percarbonic acid
Sodium, sodium carbonate, spaonin powder, the immersion liquid of soapberry pericarp, allyl sulfides, lemon eucalyptus leaf immersion liquid, brightener, non-ionic surface active
Agent, polycarboxylate, bleaching agent, enzyme preparation and deionized water；
Wherein, the soapberry pericarp immersion liquid by soapberry pericarp after crushed, utilize the deionization water logging of 1:1 equal portions ratio
Bubble is made for 3 hours；
The lemon eucalyptus leaf immersion liquid after crushed, is impregnated 3 hours using the deionized water of 1:1 equal portions ratio and is made by lemon eucalyptus leaf
At；
And specific in the present embodiment, specifically: 45 parts of sodium metasilicate, 45 parts of sodium citrate, 12 parts of SODIUM PERCARBONATE, sodium carbonate
22 parts, it is 2 parts of spaonin powder, 12 parts of soapberry pericarp immersion liquid, 2 parts of allyl sulfides, 12 parts of lemon eucalyptus leaf immersion liquid, 1.5 parts of brightener, non-
2 parts of ionic surface active agent, 6 parts of polycarboxylate, 6 parts of bleaching agent, 2 parts of enzyme preparation and 35 parts of deionized water；
Further, in mentioned component, the enzyme preparation is specially the mixture of protease, amylase and phytase, institute
Stating protease, amylase and phytase mixed proportion is 1:1:3, and the particle mesh number of the spaonin powder is 300-500 mesh；
On the basis of above-mentioned, a kind of preparation method for sterilizing nontoxic machine dishwasher detergent specifically comprises the following steps:
Step 1, by 12 parts of soapberry pericarp immersion liquid, 12 parts of lemon eucalyptus leaf immersion liquid and 2 parts of spaonin powder investments to reaction kettle
It is interior, 3 hours are kept the temperature after being warming up to 60 degrees Celsius, then it is carried out to stir 10- minutes with 60 revs/min of speed, fills it
After dividing mixing, A phase is obtained；
35 parts of deionized water are poured into ingredients pot by step 2, to it inside successively add 45 parts of sodium metasilicate, citric acid
45 parts of sodium, 12 parts of SODIUM PERCARBONATE and 22 parts of sodium carbonate are stirred 8 minutes with 120 revs/min of revolving speed using blender, are then existed
1.5 parts and 2 parts of nonionic surfactant of brightener are added in the state of stirring, makes it after completely dissolution, obtains B phase；
Step 3 pours into B phase inside sealable container, and A phase is added in B phase, and adds 2 parts of allyl sulfides,
After stirring 3 minutes using blender with 120 revs/min of revolving speed, remove the dross and impurity of solution surface, then by container into
Row sealing after being placed in indoor standing 6 hours of 10 degrees Celsius, obtains C phase；
Step 4 is successively added 6 parts of polycarboxylate, 6 parts of bleaching agent and 2 parts of enzyme preparation into C phase, and is risen to container
Temperature after the solution in container is warming up to 50 degrees Celsius, neutralizes pH to the solution in container with 80 revs/min of revolving speed stirring and arrives
After 8, finished product is obtained, that is, sterilizes nontoxic machine dishwasher detergent.
Embodiment 3:
A kind of nontoxic machine dishwasher detergent of sterilization, including following component and its parts by weight: sodium metasilicate, sodium citrate, percarbonic acid
Sodium, sodium carbonate, spaonin powder, the immersion liquid of soapberry pericarp, allyl sulfides, lemon eucalyptus leaf immersion liquid, brightener, non-ionic surface active
Agent, polycarboxylate, bleaching agent, enzyme preparation and deionized water；
Wherein, the soapberry pericarp immersion liquid by soapberry pericarp after crushed, utilize the deionization water logging of 1:1 equal portions ratio
Bubble is made for 5 hours；
The lemon eucalyptus leaf immersion liquid after crushed, is impregnated 5 hours using the deionized water of 1:1 equal portions ratio and is made by lemon eucalyptus leaf
At；
And specific in the present embodiment, specifically: 55 parts of sodium metasilicate, 55 parts of sodium citrate, 18 parts of SODIUM PERCARBONATE, sodium carbonate
28 parts, it is 4 parts of spaonin powder, 18 parts of soapberry pericarp immersion liquid, 4 parts of allyl sulfides, 18 parts of lemon eucalyptus leaf immersion liquid, 2.5 parts of brightener, non-
4 parts of ionic surface active agent, 8 parts of polycarboxylate, 8 parts of bleaching agent, 4 parts of enzyme preparation and 45 parts of deionized water；
Further, in mentioned component, the enzyme preparation is specially the mixture of protease, amylase and phytase, institute
Stating protease, amylase and phytase mixed proportion is 1:1:3, and the particle mesh number of the spaonin powder is 500 mesh；
On the basis of above-mentioned, a kind of preparation method for sterilizing nontoxic machine dishwasher detergent specifically comprises the following steps:
Step 1, by 18 parts of soapberry pericarp immersion liquid, 18 parts of lemon eucalyptus leaf immersion liquid and 4 parts of spaonin powder investments to reaction kettle
It is interior, 3 hours are kept the temperature after being warming up to 60 degrees Celsius, then it is carried out to stir 15 minutes with 60 revs/min of speed, makes it sufficiently
After mixing, A phase is obtained；
45 parts of deionized water are poured into ingredients pot by step 2, to it inside successively add 55 parts of sodium metasilicate, citric acid
55 parts of sodium, 18 parts of SODIUM PERCARBONATE and 28 parts of sodium carbonate are stirred 10 minutes with 120 revs/min of revolving speed using blender, are then existed
2.5 parts and 4 parts of nonionic surfactant of brightener are added in the state of stirring, makes it after completely dissolution, obtains B phase；
Step 3 pours into B phase inside sealable container, and A phase is added in B phase, and adds 4 parts of allyl sulfides,
After stirring 3 minutes using blender with 120 revs/min of revolving speed, remove the dross and impurity of solution surface, then by container into
Row sealing after being placed in indoor standing 8 hours of 20 degrees Celsius, obtains C phase；
Step 4 is successively added 8 parts of polycarboxylate, 8 parts of bleaching agent and 4 parts of enzyme preparation into C phase, and is risen to container
Temperature after the solution in container is warming up to 50 degrees Celsius, neutralizes pH to the solution in container with 80 revs/min of revolving speed stirring and arrives
After 8, finished product is obtained, that is, sterilizes nontoxic machine dishwasher detergent.
By the nontoxic machine dishwasher detergent of the available three kinds of sterilizations of above three groups of embodiments, these three are sterilized into nontoxic machine and is used
Dishwasher detergent is tested for the property respectively, then is made a service test with commercially available common dishwasher detergent, is as a result obtained in three groups of embodiments
The performance of the nontoxic machine dishwasher detergent of sterilization have different promotions, the property of nontoxic machine dishwasher detergent is wherein sterilized in embodiment 1
Highest preferably can be worth, wherein during performance test, every underlying parameter statistics is such as three groups of embodiments and commercial product
Following table:
It is compared by above-mentioned data, it can be seen that, product of the invention is substantially better than commercially available product, by soapberry fruit
Skin and lemon eucalyptus leaf impregnate after crushing through deionized water, obtain the immersion liquid of soapberry pericarp and lemon eucalyptus leaf immersion liquid, are combined with silicic acid
The raw materials such as sodium, sodium citrate, SODIUM PERCARBONATE, sodium carbonate can reduce SODIUM PERCARBONATE in raw material during preparing dishwasher detergent
Content go to make up since SODIUM PERCARBONATE content is lower using the fungistatic effect of the immersion liquid of soapberry pericarp and lemon eucalyptus leaf immersion liquid
And the active hypoxgia occurred, lead to the unconspicuous problem of bactericidal effect, while the SODIUM PERCARBONATE of lower content is in dish-washing machine
In the course of work, generation active oxygen can be decomposed, since active oxygen is too active, it is easy to it aoxidizes, it is water-soluble fabulous, do not have
Residue problem；
After being mixed soapberry pericarp immersion liquid with spaonin powder, is heated up and kept the temperature, stirred evenly simultaneously, made
Effective component in soapberry pericarp solution and spaonin powder can sufficiently dilute, the soapberry soap contained using soapberry pericarp
The triterpenoid saponins such as glycosides are cleaned, and serve as surfactant using spaonin powder, are matched with the nonionic surfactant in raw material
It closes and uses, have the effects that wetting, emulsification, dispersion, so that dirt be removed, improve the cleaning ability to grease stain, and pure natural
It is nuisanceless.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features,
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (8)
1. a kind of nontoxic machine dishwasher detergent of sterilization, which is characterized in that including following component and its parts by weight: 40-60 parts of sodium metasilicate,
40-60 parts of sodium citrate, 10-20 parts of SODIUM PERCARBONATE, 20-30 parts of sodium carbonate, 1-5 parts of spaonin powder, soapberry pericarp immersion liquid 10-20
Part, 1-5 parts of allyl sulfides, 10-20 parts of lemon eucalyptus leaf immersion liquid, 1-3 parts of brightener, 1-5 parts of nonionic surfactant, polycarboxylic acids
4-10 parts of ester, 4-10 parts of bleaching agent, 1-5 parts of enzyme preparation and 30-50 parts of deionized water；
The soapberry pericarp immersion liquid after crushed, is impregnated 3-5 hours by soapberry pericarp using the deionized water of 1:1 equal portions ratio
It is made；
The lemon eucalyptus leaf immersion liquid after crushed, is impregnated 3-5 hours using the deionized water of 1:1 equal portions ratio and is made by lemon eucalyptus leaf
At.
2. a kind of nontoxic machine dishwasher detergent of sterilization according to claim 1, which is characterized in that including following component and its again
Measure part: 45-55 parts of sodium metasilicate, 45-55 parts of sodium citrate, 12-18 parts of SODIUM PERCARBONATE, 22-28 parts of sodium carbonate, 2-4 parts of spaonin powder,
12-18 parts of soapberry pericarp immersion liquid, 2-4 parts of allyl sulfides, 12-18 parts of lemon eucalyptus leaf immersion liquid, 1.5-2.5 parts of brightener, it is non-from
Sub- surfactant 2-4 parts, 6-8 parts of polycarboxylate, 6-8 parts of bleaching agent, 2-4 parts of enzyme preparation and 35-45 parts of deionized water.
3. a kind of nontoxic machine dishwasher detergent of sterilization according to claim 1, which is characterized in that including following component and its again
Measure part: 50 parts of sodium metasilicate, 50 parts of sodium citrate, 15 parts of SODIUM PERCARBONATE, 25 parts of sodium carbonate, 3 parts of spaonin powder, soapberry pericarp immersion liquid
15 parts, 3 parts of allyl sulfides, 15 parts of lemon eucalyptus leaf immersion liquid, 2 parts of brightener, 3 parts of nonionic surfactant, 7 parts of polycarboxylate,
7 parts of bleaching agent, 3 parts of enzyme preparation and 40 parts of deionized water.
4. a kind of nontoxic machine dishwasher detergent of sterilization according to claim 1, it is characterised in that: the enzyme preparation is specially egg
The mixture of white enzyme, amylase and phytase, the protease, amylase and phytase mixed proportion are 1:1:3.
5. a kind of nontoxic machine dishwasher detergent of sterilization according to claim 1, it is characterised in that: the particle mesh of the spaonin powder
Number is 300-500 mesh.
6. a kind of preparation method using the nontoxic machine dishwasher detergent of sterilization described in claim 1-3 any one, feature exist
In specifically comprising the following steps:
Step 1 rises in 15 parts of soapberry pericarp immersion liquid, 15 parts of lemon eucalyptus leaf immersion liquid and 3 parts of spaonin powder investment to reaction kettles
Then temperature is stirred it 10-15 minutes, after mixing them thoroughly to keeping the temperature 3 hours after 60 degrees Celsius, obtain A phase；
40 parts of deionized water are poured into ingredients pot by step 2, to it inside successively add 50 parts of sodium metasilicate, sodium citrate 50
Part, 15 parts of SODIUM PERCARBONATE and 25 parts of sodium carbonate are stirred 5-10 minutes with 120 revs/min of revolving speed using blender, are then being stirred
2 parts and 3 parts of nonionic surfactant of brightener are added in the state of mixing, makes it after completely dissolution, obtains B phase；
Step 3 pours into B phase inside sealable container, and A phase is added in B phase, and adds 3 parts of allyl sulfides, utilizes
After blender is stirred 3 minutes with 120 revs/min of revolving speed, the dross and impurity of solution surface are removed, is then carried out container close
Envelope, is placed under normal temperature environment after standing 6-8 hours, obtains C phase；
Step 4 successively adds 7 parts of polycarboxylate, 7 parts of bleaching agent and 3 parts of enzyme preparation into C phase, and heats up to container,
After solution in container is warming up to 50 degrees Celsius, the solution in container is stirred after neutralizing pH to 7-8, obtains finished product,
Sterilize nontoxic machine dishwasher detergent.
7. a kind of preparation method for sterilizing nontoxic machine dishwasher detergent according to claim 6, it is characterised in that: the step
In one, the speed of agitator of reaction kettle is 60 revs/min.
8. a kind of preparation method for sterilizing nontoxic machine dishwasher detergent according to claim 6, it is characterised in that: the step
In three, the temperature of standing is 10-20 degrees Celsius, and the speed of agitator in the step 4 is 80 revs/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910816898.2A CN110511826A (en) | 2019-08-30 | 2019-08-30 | It is a kind of to sterilize nontoxic machine dishwasher detergent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910816898.2A CN110511826A (en) | 2019-08-30 | 2019-08-30 | It is a kind of to sterilize nontoxic machine dishwasher detergent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110511826A true CN110511826A (en) | 2019-11-29 |
Family
ID=68630010
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910816898.2A Pending CN110511826A (en) | 2019-08-30 | 2019-08-30 | It is a kind of to sterilize nontoxic machine dishwasher detergent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110511826A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112143584A (en) * | 2020-10-21 | 2020-12-29 | 湖南澳美佳健康科技有限公司 | Production process of sodium bicarbonate detergent with long shelf life |
| CN112143576A (en) * | 2020-10-21 | 2020-12-29 | 湖南澳美佳健康科技有限公司 | Production process of sodium bicarbonate cleanser without damaging skin |
| CN114525178A (en) * | 2022-01-26 | 2022-05-24 | 晋江市佐净日用品有限责任公司 | Oxygen-increasing phosphorus-free concentrated cleaning solution and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102115692A (en) * | 2010-07-27 | 2011-07-06 | 黄艳香 | Threeleaf-assembled abluent and preparation technology thereof |
| CN103320244A (en) * | 2013-07-04 | 2013-09-25 | 余姚市德派日用品有限公司 | Environment-friendly household clothes/dish washing bag |
| CN107267303A (en) * | 2017-06-08 | 2017-10-20 | 湖北大学 | Special dishwashing detergent pulvis of a kind of dish-washing machine and preparation method thereof |
-
2019
- 2019-08-30 CN CN201910816898.2A patent/CN110511826A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102115692A (en) * | 2010-07-27 | 2011-07-06 | 黄艳香 | Threeleaf-assembled abluent and preparation technology thereof |
| CN103320244A (en) * | 2013-07-04 | 2013-09-25 | 余姚市德派日用品有限公司 | Environment-friendly household clothes/dish washing bag |
| CN107267303A (en) * | 2017-06-08 | 2017-10-20 | 湖北大学 | Special dishwashing detergent pulvis of a kind of dish-washing machine and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112143584A (en) * | 2020-10-21 | 2020-12-29 | 湖南澳美佳健康科技有限公司 | Production process of sodium bicarbonate detergent with long shelf life |
| CN112143576A (en) * | 2020-10-21 | 2020-12-29 | 湖南澳美佳健康科技有限公司 | Production process of sodium bicarbonate cleanser without damaging skin |
| CN114525178A (en) * | 2022-01-26 | 2022-05-24 | 晋江市佐净日用品有限责任公司 | Oxygen-increasing phosphorus-free concentrated cleaning solution and preparation method thereof |
| CN114525178B (en) * | 2022-01-26 | 2024-06-07 | 晋江市佐净日用品有限责任公司 | Preparation method of oxygen-enriched phosphorus-free concentrated washing liquid |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110511826A (en) | It is a kind of to sterilize nontoxic machine dishwasher detergent and preparation method thereof | |
| EP0268064B1 (en) | Aqueous composition for the pretreatment of dishes | |
| CN105255601A (en) | Coconut oil fruit and vegetable cleaning agent | |
| CN106929190A (en) | Cloth grass bio-enzyme cleaning agent and its preparation method and application | |
| WO2001066682A1 (en) | Cleaning solution, and method and apparatus for cleaning using the same | |
| CN104818156B (en) | A kind of tableware immersion compound powder improving low temperature greasy dirt cleaning effect | |
| CN107312658A (en) | A kind of hand clothes washing soap powder easily rinsed | |
| JP4773997B2 (en) | Fermented Makuwa Multipurpose Detergent and Method for Producing the Same | |
| CN113943611A (en) | Fragrant floor scrubber effervescent cleaning tablet with sterilization effect | |
| KR20110019118A (en) | Liquid detergent composition | |
| CN109181899A (en) | A kind of carpet height bubble and defoaming sterilization cleaning combination agent and preparation method thereof | |
| CN105543001B (en) | A kind of duck hatching egg cleaning agent and its preparation method and application | |
| JPH05117695A (en) | Cleaning composition for nursing bottle and tableware | |
| CN113462485A (en) | Baijie milk formula and preparation process thereof | |
| JP4147135B2 (en) | Cleaning method for noodle cooking equipment | |
| CN106701373A (en) | Tea set bio-enzyme degerming cleaner and preparation method and application thereof | |
| CN105820888A (en) | Decontaminating bactericidal clothing detergent | |
| CN109266465A (en) | A kind of powdery dish washing liquid formula | |
| JPH05140590A (en) | Cleanser composition having color-developing and decoloring function | |
| CN104630802A (en) | Metal product cleaning and brightening agent | |
| CN108048240A (en) | A kind of production method of feature of environmental protection Green detergent | |
| CN109112009A (en) | A kind of detergent and preparation method thereof | |
| CN117264701A (en) | Food-grade spray detergent for degerming, decontaminating and removing pesticide residues of fruits, vegetables and tableware and preparation process thereof | |
| CN107384610A (en) | A kind of plant skin-care detergent and preparation method thereof | |
| CN114891579A (en) | Fragrant laundry detergent |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20191129 |
|
| RJ01 | Rejection of invention patent application after publication |