CN107603790A - A kind of tea oil soap powder and preparation method thereof - Google Patents
A kind of tea oil soap powder and preparation method thereof Download PDFInfo
- Publication number
- CN107603790A CN107603790A CN201710879842.2A CN201710879842A CN107603790A CN 107603790 A CN107603790 A CN 107603790A CN 201710879842 A CN201710879842 A CN 201710879842A CN 107603790 A CN107603790 A CN 107603790A
- Authority
- CN
- China
- Prior art keywords
- sodium
- tea oil
- soap powder
- powder
- oil soap
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
The invention discloses a kind of tea oil soap powder and preparation method thereof, include each component of following parts by weight, tea oil gleditsia sinensis：Sodium hydroxide：Sodium chloride：Compound=100：(1‑3)：100：110, the compound is the mixture of sodium carbonate, Sodium Polyacrylate, sodium sulfate of polyethenoxy ether of fatty alcohol, talcum powder, sodium citrate, ethylenediamine tetra-acetic acid, neopelex and essence, and wherein the weight proportion of sodium carbonate, Sodium Polyacrylate, sodium sulfate of polyethenoxy ether of fatty alcohol, talcum powder, sodium citrate, ethylenediamine tetra-acetic acid and neopelex is 6：1：0.5：2：0.5：0.5：0.5, the addition of essence is the 0.1 ‰ of tea oil soap powder gross weight；The tea oil soap powder has obvious dirt-removing power, for carbon ink class, protide and grease type spot, shows excellent clean result；Easily rinsing, small to skin irritatin, environment protecting is good, and cost is low.
Description
Technical field
The invention belongs to detergent and its manufacture field, and in particular to a kind of tea oil soap powder and preparation method thereof.
Background technology
The advantages that soap powder has low bubble environmental protection, and easily rinsing, dirt-removing power is strong, and chemistry addition is few, to skin safe, and protects
Fabric, the problems such as washing rear fabric " incrustation ", " precipitation ", " hardening " in the absence of synthetic detergent powder, it is the first-elected production of current cleaning supplies
Product.Soap powder in the market is mainly cocounut oil class soap powder, and soap powder price is generally higher than 3~5 times of washing powder.
The patent of invention of Application No. 99105917.4 disclose a kind of natural green soap powder cold process preparation technology and its
Finished product, the present invention are cold process preparation technology of natural green soap powder and products thereof.This technique is included under normal temperature, normal pressure, in raw material
Alkanolamide is added in oil foot waste material, sodium metasilicate is sequentially added under conditions of stirring and sodium hydroxide solution carries out saponification, is added
Enter sodium carbonate supplement saponification, hydrogen peroxide is slowly added to after stirring and carries out bleaching, then sequentially adds glycine betaine, nothing
Machine sodium salt and starch, finished product is can obtain through drying, screening after being sufficiently mixed uniformly.Though the natural green soap powder of the disclosure of the invention
So there is certain dirt-removing power, but be directed to some grease type spots, clean result is not so good, needs further to be improved.
The content of the invention
It is low that the technical problems to be solved by the invention are to provide a kind of cost, simple production process, and clean result is good
Tea oil soap powder and preparation method thereof.
In order to solve the above-mentioned technical problem, tea oil soap powder provided by the invention, each component of following parts by weight, tea oil are included
Soap stock：Sodium hydroxide：Sodium chloride：Compound=100：(1-3)：100：110, the compound be sodium carbonate, Sodium Polyacrylate,
Sodium sulfate of polyethenoxy ether of fatty alcohol, talcum powder, sodium citrate, ethylenediamine tetra-acetic acid, neopelex and essence
Mixture, wherein sodium carbonate, Sodium Polyacrylate, sodium sulfate of polyethenoxy ether of fatty alcohol, talcum powder, sodium citrate, ethylenediamine tetraacetic
The weight proportion of acetic acid and neopelex is 6：1：0.5：2：0.5：0.5：0.5, the addition of essence is tea oil soap
The 0.1 ‰ of powder gross weight.
Tea oil soap powder gross weight is the gross weight of the mixture of tea oil soap stock, sodium hydroxide, sodium chloride and compound.
Preferably, the tea oil gleditsia sinensis：Sodium hydroxide：Sodium chloride：The weight proportion of compound is 100：2：100：110.
Preferably, the tea oil gleditsia sinensis is the tea oil gleditsia sinensis that oleic acid content is high after physics cold pressing is squeezed
The present invention also provides a kind of preparation method of tea oil soap powder, comprises the following steps：
(1) saponification：Tea oil soap stock is weighed, is dissolved in water, stirs, be heated to 90-95 DEG C, it is completely molten to tea oil soap stock
Solution, adds sodium hydroxide solution in three times under stirring afterwards, per minor tick 20-25min, while tests pH value, makes pH
Value saponification time 2-3h, obtains soap base between 9-11；
(2) saltout：Under stirring, 4-5 addition sodium chloride is divided into above-mentioned soap base, adds water, temperature control exists
75-85 DEG C, until water is transparent, stratification, the clean soap base in upper strata is taken, carry out dispensing, obtain compound tea oil soap powder；
(3) just match somebody with somebody：Water is added in the compound tea oil soap powder that above-mentioned steps (2) obtain, is dissolved by heating, is added under stirring
Enter sodium carbonate and Sodium Polyacrylate, dissolve, be completely dissolved to sodium carbonate, be cooled to less than 60 DEG C afterwards, obtain just matching somebody with somebody soap powder；
(4) it will just match somebody with somebody made from step (3) and sodium sulfate of polyethenoxy ether of fatty alcohol, talcum powder, citric acid added in soap powder
Sodium, ethylenediamine tetra-acetic acid, neopelex and essence, after being sufficiently stirred, spontaneously dry, crush afterwards, obtain tea oil
Soap powder.
The beneficial effects of the invention are as follows：
(1) raw material of the waste soap stock as soap powder, oleic acid caused by production refining link contain after using physical squeezing tea oil
Amount is high, and environment protecting is good, and cost is low.
(2) the camellia oil soap powder prepared has obvious dirt-removing power, for carbon ink class, protide and grease type spot,
Show excellent clean result.
(3) the camellia oil soap powder obtained by easily rinses, to skin irritatin unobvious.
Brief description of the drawings
Fig. 1 is for the front and rear comparison diagram of the commercially available soap powder washing of carbon ink spot.
Fig. 2 is for the front and rear comparison diagram of the present invention washing of carbon ink spot.
Fig. 3 is for the front and rear comparison diagram of the commercially available soap powder washing of protide spot.
Fig. 4 is for the front and rear comparison diagram of the present invention washing of protide spot.
Fig. 5 is for the front and rear comparison diagram of the soap powder washing of the comparative example 2 of greasy soils.
Fig. 6 is for the front and rear comparison diagram of the present invention washing of greasy soils.
Fig. 7 is comparison diagram before and after rinsing of the soap powder of comparative example 2 in the test of easy rinsing performance.
Fig. 8 is comparison diagram before and after rinsing of the tea oil soap powder of the present invention in the test of easy rinsing performance.
Embodiment
Illustrate the embodiment of the present invention with reference to embodiment：
Embodiment 1
The tea oil refining soap stock after 100 parts by weight physics cold press is weighed first, is added in container, and adds water, is heated
To 90-95 DEG C, it is stirred continuously, is dissolved completely to soap stock, adds 2 part of 40% sodium hydroxide solution every 25min afterwards, in three times
Complete, pH value determination to 11, react 2-3h, generate soap base, soap base color at this moment is deeper, and few with glossy.
Add 100 parts of sodium chloride to divide 4-5 time and is added in above-mentioned soap base, addition water, temperature control at 85 DEG C, during not
Disconnected stirring, makes soap base be separated with water, the color of water from deep to shallow, until substantially transparent, stratification, goes water to take upper strata material.
Above-mentioned upper strata material is added in allocates container, adds suitable quantity of water, is dissolved by heating, is stirred continuously 60 parts of carbon of lower addition
Sour sodium and 10 parts of Sodium Polyacrylates, dissolve 10min, are completely dissolved to sodium carbonate and Sodium Polyacrylate is evenly distributed, cooled afterwards
To less than 60 DEG C, obtain just matching somebody with somebody soap powder.
To it is above-mentioned just match somebody with somebody soap powder in add 5 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 20 parts of talcum powder, 5 parts of sodium citrates,
5 parts of ethylenediamine tetra-acetic acids, 5 parts of neopelexes and the essence for accounting for tea oil soap powder gross weight 0.1 ‰, after being sufficiently stirred certainly
So it is dried, crushes after placement 4-5h, obtains tea oil soap powder.
Embodiment 2
The tea oil refining soap stock after 100 parts by weight physics cold press is weighed first, is added in container, and adds water, is heated
To 90-95 DEG C, it is stirred continuously, is dissolved completely to soap stock, adds 1 part of 30% sodium hydroxide solution (weighing body every 25min afterwards
Product ratio), complete in three times, pH value determination to 9, react 2-3h, generate soap base, soap base color at this moment is deeper, and carries light less
Pool.
Add 100 parts of sodium chloride to divide 4-5 time and is added in above-mentioned soap base, addition water, temperature control at 75 DEG C, during not
Disconnected stirring, makes soap base be separated with water, the color of water from deep to shallow, until substantially transparent, stratification, goes water to take upper strata material.
Above-mentioned upper strata material is added in allocates container, adds suitable quantity of water, is dissolved by heating, is stirred continuously 60 parts of carbon of lower addition
Sour sodium and 10 parts of Sodium Polyacrylates, dissolve 20min, are completely dissolved to sodium carbonate and Sodium Polyacrylate is evenly distributed, cooled afterwards
To less than 60 DEG C, obtain just matching somebody with somebody soap powder.
To it is above-mentioned just match somebody with somebody soap powder in add 5 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 20 parts of talcum powder, 5 parts of sodium citrates,
5 parts of ethylenediamine tetra-acetic acids, 5 parts of neopelexes and the essence for accounting for tea oil soap powder gross weight 0.1 ‰, after being sufficiently stirred certainly
So it is dried, crushes after placement 4-5h, obtains tea oil soap powder.
Comparative example 1
Commercially available soap powder.
Comparative example 2
The soap powder prepared using method disclosed in the patent of invention of Application No. 99105917.4.
Method of testing：
1. according to professional standard《QB/T2387-2008 laundry powdered soaps》Routine inspection, knot are carried out to the tea oil soap powder of preparation
Fruit is shown in Table 1.
Table 1
2. according to the method for daily laundry, the clean result of carbon ink spot, protein stain, greasy soils is tested,
Observe by the naked eye to obtain result, specific experiment is as follows.
(1) carbon ink spot clean result is tested：
By the concentration that the ink dilution printed calligraphy is 1/50, prepare the suitable calico of two block sizes, every piece of calico drop
Ink after 10 drop dilutions, naturally dry.
The 0.2% natural aqueous solution of the 1 commercially available soap powder of tea oil soap powder and comparative example of equivalent embodiment 1 is respectively configured, by dirt
Cloth is placed wherein, and same people washes 5min taking-ups by rubbing with the hands, compares the clean result of the two.As depicted in figs. 1 and 2, before washing is in left side
Pieces of cloth, right side is the pieces of cloth after washing, by comparative analysis, finds the washing effect of the more commercially available soap powder of clean result of the present invention
Fruit is good.
(2) protide spot (blood) clean result is tested
Prepare the suitable calico of two block sizes, be infected with suitable chicken blood, naturally dry.
The tea oil soap powder and the commercially available 0.2% natural aqueous solution of soap powder of comparative example 1 of equivalent embodiment 1 is respectively configured, by soiled cotton
Place wherein, same people washes 5min taking-ups by rubbing with the hands, compares the clean result of the two, and as shown in Figure 3-4, left side is the cloth before washing
Piece, right side is the pieces of cloth after washing, by comparative analysis, finds the clean result of the more commercially available soap powder of clean result of the present invention
It is good.
(3) greasy soils clean result is tested
Prepare the suitable calico of two block sizes, the wiping device in milling shop equipment, naturally dry.
The tea oil soap powder of equivalent embodiment 1 and the soap powder of comparative example 2 is respectively configured, soiled cotton is placed wherein, same people rubs with the hands
5min taking-ups are washed, compare the clean result of the two, as seen in figs. 5-6, left side is the pieces of cloth before washing, and right side is the cloth after washing
Piece, by comparative analysis, it is found that the clean result of the present invention is good compared with the clean result of the soap powder of comparative example 2.
(4) easily rinsing performance test
Take 2 identical clothes, be separately added into 2 washing tubs 2.5g embodiments 1 camellia oil soap powder and 2.5g pairs
The soap powder of ratio 2,1.5kg running water is added, after same people washes by rubbing with the hands, change 1.5kg running water and rinsed, compare the two
Foam and feel, as Figure 7-8, left side are the clothing photo before rinsing, and right side is the foam after rinsing, by score
Analysis, it is found that the clean result of the present invention is good compared with the wash effect of the soap powder of comparative example 2.
Tested more than, draw following result and conclusion：
1. camellia oil soap powder quality disclosed by the invention meets《QB/T2387-2008 laundry powdered soaps》Requirement；
2. for carbon ink class and protide spot, the dirt-removing power of tea oil soap powder prepared by the present invention and commercially available soap powder compared with
It is good；
3. for grease type spot, tea oil soap powder produced by the present invention can be cleaned completely, and the soap powder of comparative example 2 wash after according to
Old obvious yellow, therefore the clean result of the camellia oil soap powder of the present invention is substantially better than the soap powder of comparative example 2；
4. compared to the soap powder of comparative example 2, camellia oil soap powder disclosed by the invention is more easy to rinse, smaller to skin irritatin.
Claims (4)
1. a kind of tea oil soap powder, it is characterised in that include each component of following parts by weight, tea oil gleditsia sinensis：Sodium hydroxide：Chlorination
Sodium：Compound=100：(1-3)：100：110, the compound is sodium carbonate, Sodium Polyacrylate, AEO sulphur
Sour sodium, talcum powder, sodium citrate, ethylenediamine tetra-acetic acid, the mixture of neopelex and essence, wherein sodium carbonate,
Sodium Polyacrylate, sodium sulfate of polyethenoxy ether of fatty alcohol, talcum powder, sodium citrate, ethylenediamine tetra-acetic acid and detergent alkylate sulphur
The weight proportion of sour sodium is 6：1：0.5：2：0.5：0.5：0.5, the addition of essence is the 0.1 ‰ of tea oil soap powder gross weight.
2. tea oil soap powder as claimed in claim 1, it is characterised in that the tea oil gleditsia sinensis：Sodium hydroxide：Sodium chloride：Compounding
The weight proportion of thing is 100：2：100：110.
3. tea oil soap powder as claimed in claim 1 or 2, it is characterised in that the tea oil gleditsia sinensis is oleic acid after physics cold pressing is squeezed
The high tea oil gleditsia sinensis of content.
4. a kind of preparation method of tea oil soap powder as claimed in claim 1, it is characterised in that comprise the following steps：
(1) saponification：Tea oil soap stock is weighed, is dissolved in water, stirs, be heated to 90-95 DEG C, be completely dissolved to tea oil soap stock,
Sodium hydroxide solution is added in three times under stirring afterwards, per minor tick 20-25min, while is tested pH value, pH value is existed
Between 9-11, saponification time 2-3h, soap base is obtained；
(2) saltout：Under stirring, 4-5 addition sodium chloride is divided into above-mentioned soap base, adds water, temperature control is in 75-85
DEG C, until water is transparent, stratification, the clean soap base in upper strata is taken, obtain compound tea oil soap powder；
(3) just match somebody with somebody：Water is added in the compound tea oil soap powder that above-mentioned steps (2) obtain, is dissolved by heating, carbon is added under stirring
Sour sodium and Sodium Polyacrylate, dissolve, are completely dissolved to sodium carbonate, are cooled to less than 60 DEG C afterwards, obtain just matching somebody with somebody soap powder；
(4) it will just match somebody with somebody made from step (3) and sodium sulfate of polyethenoxy ether of fatty alcohol, talcum powder, sodium citrate, second added in soap powder
Ethylenediamine tetraacetic acid (EDTA), neopelex and essence, after being sufficiently stirred, spontaneously dry, crush afterwards, obtain tea oil soap powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710879842.2A CN107603790A (en) | 2017-09-26 | 2017-09-26 | A kind of tea oil soap powder and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710879842.2A CN107603790A (en) | 2017-09-26 | 2017-09-26 | A kind of tea oil soap powder and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107603790A true CN107603790A (en) | 2018-01-19 |
Family
ID=61058506
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710879842.2A Pending CN107603790A (en) | 2017-09-26 | 2017-09-26 | A kind of tea oil soap powder and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107603790A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110079404A (en) * | 2019-05-27 | 2019-08-02 | 李祝晟 | A kind of daily cleaning agent of environment-friendly type writing brush and its application method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1240227A (en) * | 1999-07-23 | 2000-01-05 | 李志军 | Multi-function washing powder and productive process |
| CN1603396A (en) * | 2004-08-31 | 2005-04-06 | 盛金英 | Method for producing high-efficiency washing soap powder by using sewer oil or swill oil |
| CN102296004A (en) * | 2011-07-26 | 2011-12-28 | 山东丽波日化股份有限公司 | Paste washing agent for cleaning hard surfaces in kitchen and preparation method thereof |
| CN102703266A (en) * | 2012-06-21 | 2012-10-03 | 南通顺阳化工有限公司 | Powder detergent for clothes |
| CN105441239A (en) * | 2014-09-22 | 2016-03-30 | 丰益油脂化学（上海）有限公司 | Laundry soap powder slurry and preparation method thereof |
-
2017
- 2017-09-26 CN CN201710879842.2A patent/CN107603790A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1240227A (en) * | 1999-07-23 | 2000-01-05 | 李志军 | Multi-function washing powder and productive process |
| CN1603396A (en) * | 2004-08-31 | 2005-04-06 | 盛金英 | Method for producing high-efficiency washing soap powder by using sewer oil or swill oil |
| CN102296004A (en) * | 2011-07-26 | 2011-12-28 | 山东丽波日化股份有限公司 | Paste washing agent for cleaning hard surfaces in kitchen and preparation method thereof |
| CN102703266A (en) * | 2012-06-21 | 2012-10-03 | 南通顺阳化工有限公司 | Powder detergent for clothes |
| CN105441239A (en) * | 2014-09-22 | 2016-03-30 | 丰益油脂化学（上海）有限公司 | Laundry soap powder slurry and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110079404A (en) * | 2019-05-27 | 2019-08-02 | 李祝晟 | A kind of daily cleaning agent of environment-friendly type writing brush and its application method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105062703B (en) | A kind of protease Superconcentrated washing liquid and preparation method thereof | |
| CN101798552B (en) | Fabric detergent with colour-preserving function and preparation method thereof | |
| CN102304437B (en) | High-efficiency liquid-phase washing agent with bleaching effect for colored fabric | |
| CN103525571A (en) | Strong degreasing detergent and production method thereof | |
| CN108130199A (en) | Efficient color protection liquid detergent and preparation method thereof | |
| CN106281756A (en) | The anti-liquid detergent and preparation method thereof that fades | |
| CN104152291A (en) | Dye-resistant laundry detergent and preparation method thereof | |
| CN106381234A (en) | Brightening laundry bead and preparation method thereof | |
| CN110157559A (en) | A kind of oxygen-containing Liquid laundry composition and its preparation method and application | |
| CN103710167B (en) | Liquid laundry detergent for infants and preparation method thereof | |
| CN109439474A (en) | A kind of cleansing soap of cation-containing copolymer and preparation method thereof | |
| CN107603790A (en) | A kind of tea oil soap powder and preparation method thereof | |
| CN114164054A (en) | Cleaning composition for removing protein stains | |
| CN110511832A (en) | A kind of antibacterial environment protection liquid detergent and preparation method thereof | |
| CN107446732A (en) | A kind of submissive whitening laundry soap composition and preparation method thereof | |
| CN106047526A (en) | Detergent sheet and preparation method thereof | |
| CN106350288A (en) | Cross-color-proof type laundry condensate bead and preparation method thereof | |
| CN106929194A (en) | Liquid detergent and preparation method thereof | |
| CN102888313A (en) | Infant laundry detergent | |
| CN104830561A (en) | Super-concentrated low-foam high-efficient laundry detergent | |
| CN102586039B (en) | Clothes washing rinsing synergist containing methyl sulfate-based quaternary ammonium salt | |
| CN103555481A (en) | Infant laundry detergent production method | |
| WO2009047468A1 (en) | Fabric dye | |
| CN107835877B (en) | Washing machine and washing method | |
| CN108659980A (en) | A kind of without phosphorus color protection liquid detergent |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180119 |