CN107556138A - A kind of amino acid fertilizer - Google Patents
A kind of amino acid fertilizer Download PDFInfo
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- CN107556138A CN107556138A CN201710846456.3A CN201710846456A CN107556138A CN 107556138 A CN107556138 A CN 107556138A CN 201710846456 A CN201710846456 A CN 201710846456A CN 107556138 A CN107556138 A CN 107556138A
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Abstract
The invention provides a kind of amino acid fertilizer, and it contains the raw material of following parts by weight：50~70 parts of fish-bone amino acid, 1~3 part of urea, 0.5~2 part of sylvite, 1~3 part of ammonium sulfate, 5~10 parts of plant ash, 1~5 part of trbasic zinc phosphate, 5~15 parts of people and animals' fecaluria, 3~8 parts of borax, the inorganic salts of one or more moderate-elements in silicon, calcium, magnesium, sulphur, boron, zinc, molybdenum, iron, manganese, copper, trace element composition, amount to and account for 1~3 part of mass parts.Present invention also offers the preparation method of the amino acid fertilizer.Nutrition of the present invention is comprehensive, can activating soil, increase the content of soil with organic matter, improved soil, improve soil function；Strengthen crop resistance, prevention droop, root rot, etc. soil-borne disease, so as to improve crop yield, improving quality.Amino acid fertilizer of the present invention is applied widely, is not limited by region, soil, crop varieties, can be applied to vegetables, fruit tree etc..
Description
Technical field
The present invention relates to fertilizer field, and in particular to a kind of amino acid fertilizer.
Background technology
In recent years, developing rapidly with China's mariculture industry, substantial amounts of fish-bone by discarded, and fish-bone contain it is abundant
Protein and the mineral nutrient such as calcium, iron, phosphorus improve fish accessory substance value, be allowed to turn waste into wealth.By discarded fish
Bone is processed, and has facilitation greatly to improving the overall economic benefit of fish and surcharge.Fish-bone can be through being hydrolyzed into
Fertilizer is re-dubbed after amino acid.Amino acid is the machine compound that one group of molecular weight differs in size, and is the base of synthetic protein
Our unit, amino acid can provide organic nitrogen source, the amino acid of plant available molecular state.Numerous studies prove that amino acid can carry
High crop yield and quality, enhancing crop resistance, improve the ecological environment, therefore develop a kind of new-type fertilizer tool containing amino acid
There is vast potential for future development.
The content of the invention
Based on this, it is an object of the invention to provide a kind of amino acid fertilizer, by fish bone collagen acid hydrolysis into amino acid
Afterwards, inorganic fertilizer is added, is prepared into amino acid fertilizer.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of amino acid fertilizer, the raw material containing following parts by weight：50~70 parts of fish-bone amino acid, 1~3 part of urea, sylvite
0.5~2 part, 1~3 part of ammonium sulfate, 5~10 parts of plant ash, 1~5 part of trbasic zinc phosphate, 5~15 parts of people and animals' fecaluria, 3~8 parts of borax.
Preferably, a kind of amino acid fertilizer, the raw material containing following parts by weight：55~65 parts of fish-bone amino acid, urea 1.3~
2.4 parts, 0.9~1.4 part of sylvite, 1.3~2.7 parts of ammonium sulfate, 6.8~8.7 parts of plant ash, 2.4~4.3 parts of trbasic zinc phosphate, people and animals
8~12 parts of fecaluria, 4~6 parts of borax.
Preferably, a kind of amino acid fertilizer, the raw material containing following parts by weight：61 parts of fish-bone amino acid, 2 parts of urea, sylvite
1.2 parts, 2.1 parts of ammonium sulfate, 7 parts of plant ash, 3 parts of trbasic zinc phosphate, 11 parts of people and animals' fecaluria, 5 parts of borax.
Described fish-bone amino acid is obtained fish-bone amino acid after fish bone collagen proteolysis.
A kind of amino acid fertilizer, foregoing formula also include one in silicon, calcium, magnesium, sulphur, boron, zinc, molybdenum, iron, manganese, copper
Kind or a variety of moderate-elements, the inorganic salts of trace element composition, amount to and account for 1~3 part of mass parts.
A kind of preparation method of amino acid fertilizer, is comprised the steps of：
(1) after fish bone collagen albumen being added into acid progress acidolysis, neutrality is washed to, is concentrated and dried, obtains fish-bone amino acid；
(2) plant ash, people and animals' fecaluria are well mixed, in installation for fermenting ferment at constant temperature, obtain organic fermentation fertilizer；
(3) the fish-bone amino acid obtained step (1) add urea, sylvite, ammonium sulfate, trbasic zinc phosphate, borax and other in
Amount, micro- inorganic salts are mixed evenly, and add organic fermentation fertilizer that step (2) obtains, finally thoroughly stir
Afterwards, gained is amino acid fertilizer of the present invention.
Acidolysis in the step (1) is operated specifically, using 0.5%H2SO4 soaks raw material half an hour.
Fermentation process in the step (2) is 40~50 DEG C of constant temperature, and batch (-type) carries out turning over throwing, continues 8~12 hours
After terminate.
It is the device have the advantages that as follows：Fertilizer nutrient of the present invention is comprehensive, contains organic matter, organic N P and K, ammonia
Trace element in base acid and calcium, magnesium, sulphur, zinc, iron, boron etc., can activating soil, increase the content of soil with organic matter, improvement
Soil, improve soil function；Strengthen crop resistance, prevention droop, root rot, etc. soil-borne disease, so as to improve crop yield,
Improving quality.Amino acid fertilizer of the present invention is applied widely, is not limited by region, soil, crop varieties, can be applied to vegetables,
Fruit tree etc..
Specific embodiment
For a better understanding of the present invention, with reference to embodiments, the present invention will be described in further detail.It should manage
Solution, the specific embodiments described herein are merely illustrative of the present invention, is not intended to limit the present invention.
The amino acid fertilizer embodiment 1~5 of the present invention is formulated, and is shown in Table 1.
Table 1
A kind of embodiment 1-5 amino acid fertilizer is prepared as follows：
(1) after fish bone collagen albumen being added into 0.5%H2SO4 immersion raw material half an hour progress acidolysis, neutrality is washed to, it is dense
Contracting drying, obtain fish-bone amino acid；
(2) plant ash, people and animals' fecaluria are well mixed, in 40~50 DEG C of fermentations of installation for fermenting constant temperature, and batch (-type) is carried out
Throwing is turned over, is terminated after continuing 8~12 hours, obtains organic fermentation fertilizer；
(3) the fish-bone amino acid that step (1) obtains is added into urea, sylvite, ammonium sulfate, trbasic zinc phosphate, borax, manganese chloride to mix
Conjunction stirs, and adds organic fermentation fertilizer that step (2) obtains, after finally thoroughly stirring, gained is of the present invention
Amino acid fertilizer.
Comparative example 1
The fertilizer of fish-bone amino acid is not added, includes the composition of following parts by weight：2 parts of urea, 1.2 parts of sylvite, ammonium sulfate
2.1 parts, 7 parts of plant ash, 3 parts of trbasic zinc phosphate, 11 parts of people and animals' fecaluria, 5 parts of borax, 2 parts of manganese chloride.
Preparation method is as follows：
(1) plant ash, people and animals' fecaluria are well mixed, in 40~50 DEG C of fermentations of installation for fermenting constant temperature, and batch (-type) is carried out
Throwing is turned over, is terminated after continuing 8~12 hours, obtains organic fermentation fertilizer；
(2) urea, sylvite, ammonium sulfate, trbasic zinc phosphate, borax and other Medium-microelements inorganic salts are added to mix
Uniformly, organic fermentation fertilizer that step (2) obtains is added, after finally thoroughly stirring, gained is amino acid of the present invention
Fertilizer.
Experimental example 1
The indices in above-described embodiment 1-5 and the amino acid fertilizer of comparative example 1 are detected, measurement result is shown in Table 2.
Table 2
Analysis：The amino acid fertilizer national standard for the GB/T 17419-1998 that the amino acid fertilizer of the present invention uses, embodiment 1-
The amino acid fertilizer prepared in 5 contains the more amino acid and total nutrient beneficial to crops, can give crops good battalion
Form point, improve the quality of crops；And embodiment does not add fish-bone amino acid, the nutrient of fertilizer is not up to standard, and what is contained has
Evil composition is exceeded, is underproof product；By the proportioning of repeatedly change weight of fertilizer part, present invention technology to be protected is obtained
Scheme.
Test example 2
Design experiment, influence of the amino acid fertilizer of the present invention to cucumber quality is verified, and it is as follows to do corresponding experiment registration
Test report：
For trying cucumber variety：Upper highland
Material to be tested：The soil of plastic tent cucumber plantation, basic physicochemical character are：It is pH6.8, organic matter 17.69g/kg, complete
It is 72.5mg/kg that nitrogen 2.12g/kg, full phosphorus 3.14g/kg, full potassium 16.5g/kg, soil, which crack nitrogen content, rapid available phosphorus
11.1mg/kg, available potassium 152.7mg/kg.Experimental design：3 groups of experiment point, (1) blank control group, i.e., does not apply any fertilizer；
(2) common fertilizer is applied；(3) amino acid fertilizer of the present invention is applied.Every group the seedling stage after field planting, initial bloom stage, harvesting are first respectively
Phase application fertilizer, dose 230g/m2, and mix Soil and Fertilizer.The Planting Row Distance of cucumber is 0.6m, and spacing in the rows is
0.5m, plot area 30m2, (every group 10 plants).
The measure of cucumber yield and quality record such as table 3 below.
Table 3
Cucumber of the invention through experimental cultivation detects that the content of nitrate is below national standard, below
It is 432mg.kg-1 and lower than the nitrate content of common fertilizer plantation；The soluble sugar of cucumber, the content of vitamin, yield
All applied fertilizer than control group and commonly high, plant growth can be promoted by illustrating the amino-acid compound fertilizer of the present invention, have crops good
Good quality and economic benefit.
2nd, it is as follows to the record of cucumber residues of pesticides and pest and disease damage：
A, cucumber pesticide residue determination is as follows：
(1) cucumber 20g samples are weighed, are accurate to 0.1g, are placed in 250mL tissue mashing cups, add 60mL acetone, vibration
40min, filtering, residue is washed with acetone.Filtrate is collected in 100mL volumetric flasks and constant volume is diluted with acetone；(2) it is accurate to move
L0mL extract solutions are taken, are placed in 50mL polypropylene centrifuge tubes, add about 1mL saturated nacl aqueous solutions, are mixed, with about 15mL acetone
+ n-hexane (1+3) extracts twice, each vortex mixing lmin, 3000r/min centrifugation 5min, merge upper organic phase, and lead to
Anhydrous sodium sulfate post is crossed with a small amount of normal hexane column scrubber.Rotary evaporation below 40 DEG C of the efflux of merging is concentrated into about 1mL to treat
Purification；(3) by ENVI-carb (6mL, 0.5g) pillar on solid-phase extraction device, 0.5g acidic oxidations are added in pillar
Aluminium, pillar is first eluted in advance with the normal hexane of 3mL acetone ten (1+3), extract solution is crossed into ENVI-carb pillars, l0mL acetone ten is just
Alkane (1+9) elutes.Eluent is placed in less than 40 DEG C nitrogen and is blown near dry, 1mL is settled to normal hexane, it is to be measured.
As a result such as table 4.
Table 4
Remarks：National Specification：DDVP≤0.2mg/kg, parathion-methyl≤0.01mg/kg, malathion≤
mg/kg。
B, pest and disease damage record such as table 5 in cucumber test.
Table 5
| Group | Strain number living | Dead strain number | Incidence of disease % | Control rate % |
| Blank control group | 7 | 3 | 51.2 | 3.7 |
| Common fertilising group | 8 | 2 | 36.5 | 32.4 |
| Amino acid fertilizer | 10 | 0 | 13.6 | 78.6 |
With reference to table 4 and table 5, because being applied with amino acid fertilizer has certain sterilization and disinsection effect, soil texture can be improved, made
Cucumber the incidence of disease it is relatively low, so apply agricultural chemicals it is also fewer than blank control group and common fertilising group, this is to cause agricultural chemicals residual
The low one of reason of allowance；In addition, amino acid fertilizer can also be absorbed on cucumber blade face, promote the metabolism of cell, promote
Enter its photosynthesis, reduce residues of pesticides；Although the common fertilizer of application can increase the nutrient absorption of cucumber, promote cucumber life
It is long, but effect is notable without the amino acid fertilizer of the present invention.
Above-described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.Tool described herein
Body embodiment is used only for the parsing present invention, is not intended to limit the present invention.It is common based on the embodiment in the present invention, this area
All other embodiment that technical staff is obtained on the premise of creative work is not made, belong to what the present invention protected
Scope.
Claims (8)
1. a kind of amino acid fertilizer, it is characterised in that the mass parts of the amino acid fertilizer formula are：50~70 parts of fish-bone amino acid,
1~3 part of urea, 0.5~2 part of sylvite, 1~3 part of ammonium sulfate, 5~10 parts of plant ash, 1~5 part of trbasic zinc phosphate, people and animals' fecaluria 5~15
Part, 3~8 parts of borax.
2. a kind of amino acid fertilizer according to claim 1, it is characterised in that the amino acid takes the mass parts being formulated and is：
55~65 parts of fish-bone amino acid, 1.3~2.4 parts of urea, 0.9~1.4 part of sylvite, 1.3~2.7 parts of ammonium sulfate, plant ash 6.8~
8.7 parts, 2.4~4.3 parts of trbasic zinc phosphate, 8~12 parts of people and animals' fecaluria, 4~6 parts of borax.
3. a kind of amino acid fertilizer according to claim 1, it is characterised in that the amino acid takes the mass parts being formulated and is：
61 parts of fish-bone amino acid, 2 parts of urea, 1.2 parts of sylvite, 2.1 parts of ammonium sulfate, 7 parts of plant ash, 3 parts of trbasic zinc phosphate, people and animals' fecaluria 11
Part, 5 parts of borax.
4. a kind of amino acid fertilizer according to any one of claims 1 to 3, it is characterised in that described fish-bone amino acid is
Obtained fish-bone amino acid after fish bone collagen proteolysis.
A kind of 5. amino acid fertilizer according to any one of Claims 1 to 4, it is characterised in that described formula also include silicon,
One or more moderate-elements, the inorganic salts of trace element composition in calcium, magnesium, sulphur, boron, zinc, molybdenum, iron, manganese, copper, amount to and account for 1
~3 parts of mass parts.
A kind of 6. method for preparing the amino acid fertilizer as described in 1~5 any one, it is characterised in that the preparation method bag of amino acid fertilizer
Containing following steps：
(1) after fish bone collagen albumen being added into acid progress acidolysis, neutrality is washed to, is concentrated and dried, obtains fish-bone amino acid；
(2) plant ash, people and animals' fecaluria are well mixed, in installation for fermenting ferment at constant temperature, obtain organic fermentation fertilizer；
(3) the fish-bone amino acid obtained step (1) adds urea, sylvite, ammonium sulfate, trbasic zinc phosphate, borax and amount in other, micro-
Secondary element inorganic salts are mixed evenly, and add organic fermentation fertilizer that step (2) obtains, after finally thoroughly stirring, institute
It must be amino acid fertilizer of the present invention.
7. preparation method according to claim 6, it is characterised in that in step (1), the acidolysis operation is specifically, make
Use 0.5%H2SO4 soaks raw material half an hour.
8. preparation method according to claim 6, it is characterised in that in step (2), the fermentation process is constant temperature 40
~50 DEG C, and batch (-type) carries out turning over throwing, terminates after continuing 8~12 hours.
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| CN201710846456.3A CN107556138A (en) | 2017-09-18 | 2017-09-18 | A kind of amino acid fertilizer |
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| CN201710846456.3A CN107556138A (en) | 2017-09-18 | 2017-09-18 | A kind of amino acid fertilizer |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101913947A (en) * | 2010-08-03 | 2010-12-15 | 云南云叶化肥股份有限公司 | Amino acid-containing organic-inorganic compound fertilizer and preparation method thereof |
| CN104291901A (en) * | 2014-09-18 | 2015-01-21 | 青岛点石文具用品有限公司 | Special fertilizer for honeysuckle and preparation method of special fertilizer |
| CN105523825A (en) * | 2014-09-29 | 2016-04-27 | 安庆华辉生物科技有限公司 | Compound type amino-acid water-soluble fertilizer and preparation method therefor |
| CN106348821A (en) * | 2016-08-31 | 2017-01-25 | 菱花集团有限公司 | Novel amino acid water-soluble fertilizer and preparation method thereof |
| CN106518264A (en) * | 2016-11-23 | 2017-03-22 | 深圳市华嘉名生物科技有限公司 | Multielement selenium-rich amino acid water-soluble fertilizer and manufacturing method thereof |
| CN106748220A (en) * | 2016-12-30 | 2017-05-31 | 武汉天度植物科技有限公司 | A kind of amino acid Water soluble fertilizer and preparation method thereof |
-
2017
- 2017-09-18 CN CN201710846456.3A patent/CN107556138A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101913947A (en) * | 2010-08-03 | 2010-12-15 | 云南云叶化肥股份有限公司 | Amino acid-containing organic-inorganic compound fertilizer and preparation method thereof |
| CN104291901A (en) * | 2014-09-18 | 2015-01-21 | 青岛点石文具用品有限公司 | Special fertilizer for honeysuckle and preparation method of special fertilizer |
| CN105523825A (en) * | 2014-09-29 | 2016-04-27 | 安庆华辉生物科技有限公司 | Compound type amino-acid water-soluble fertilizer and preparation method therefor |
| CN106348821A (en) * | 2016-08-31 | 2017-01-25 | 菱花集团有限公司 | Novel amino acid water-soluble fertilizer and preparation method thereof |
| CN106518264A (en) * | 2016-11-23 | 2017-03-22 | 深圳市华嘉名生物科技有限公司 | Multielement selenium-rich amino acid water-soluble fertilizer and manufacturing method thereof |
| CN106748220A (en) * | 2016-12-30 | 2017-05-31 | 武汉天度植物科技有限公司 | A kind of amino acid Water soluble fertilizer and preparation method thereof |
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