CN108623371A - A method of preparing fertilizer using yellow ginger hydrolyzate - Google Patents

A method of preparing fertilizer using yellow ginger hydrolyzate Download PDF

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Publication number
CN108623371A
CN108623371A CN201711034728.6A CN201711034728A CN108623371A CN 108623371 A CN108623371 A CN 108623371A CN 201711034728 A CN201711034728 A CN 201711034728A CN 108623371 A CN108623371 A CN 108623371A
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CN
China
Prior art keywords
fertilizer
hydrolyzate
yellow ginger
added
soluble
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Pending
Application number
CN201711034728.6A
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Chinese (zh)
Inventor
陈永宏
孙辉学
陈金钟
陈金平
晏乐
奚祥洲
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Shaanxi Yongchun Ecological Technology Co Ltd
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Shaanxi Yongchun Ecological Technology Co Ltd
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Priority to CN201711034728.6A priority Critical patent/CN108623371A/en
Publication of CN108623371A publication Critical patent/CN108623371A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C9/00Fertilisers containing urea or urea compounds
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/10Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12Granules or flakes
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers
    • C05G5/23Solutions

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Plant Pathology (AREA)
  • Fertilizers (AREA)

Abstract

A kind of method preparing fertilizer using yellow ginger hydrolyzate of the present invention, belongs to the processing method comprehensively utilized to yellow ginger processing enterprise, concretely relates to a kind of method preparing fertilizer using yellow ginger hydrolyzate.The present invention is using the method that yellow ginger hydrolyzate prepares fertilizer:By yellow ginger hydrolyzate, neutralization reaction tank is squeezed into pump, potassium hydroxide solution is added and adjusts hydrolyzate PH to 6.5 --- 7, then it is 10-320g/l, 0-380g/l of phosphorus element fertilizer, 10-20g/l of 0-300g/l of potassium fertilizer and trace-element fertilizer that nitrogen manure is added in a liquid, stirring or heating stirring obtain water-soluble fertilizer after cold filtration.The method that the present invention prepares fertilizer using yellow ginger hydrolyzate, functional water-soluble natural fertilizer of the scientific utilization yellow ginger production with comprehensive function, it not only can fully develop the value of yellow ginger hydrolyzate, and the pharmacological property ingredient that Chinese medicine can be utilized natural, the soil environment of plant growth is improved, the natural equilibrium of the various microbial bacterias of soil is adjusted.

Description

A method of preparing fertilizer using yellow ginger hydrolyzate
Technical field
The processing method that the invention belongs to be comprehensively utilized to yellow ginger processing enterprise, concretely relate to it is a kind of utilize yellow ginger The method that hydrolyzate prepares fertilizer.
Background technology
China starts from the 50's of last century to yellow ginger resources development and utilization, by development for many years, China's steroid hormone Medicine industry has begun to take shape, and national saponin, diene manufacturing enterprise have reached 200 or so, and large and medium-sized hormone pharmaceutical factory is up to 100 More families, have utilized Dioscin aglucon to synthesize more than 100 kinds of drug, and annual value of production accounts for the 4% of the medical industry gross output value, becomes Important component in China's medical industry system.But there is Heavy environmental pollution in production of saponin:In process of production A large amount of high concentrated organic wastewaters and waste residue are will produce, serious environmental pollution is caused.
Production of saponin enterprise major pollutants are the waste residues after waste hydrolyzed liquid and extraction, abandon it, result in waste of resources, also dirt Environment is contaminated, very unfortunately.
In view of the above-mentioned problems, we develop the method for utilizing and preparing fertilizer with yellow ginger hydrolyzate.Through retrieval, do not send out The identical technical solution of the existing present invention.
Invention content
The technical problem to be solved in the present invention is to provide the method for preparing fertilizer using yellow ginger hydrolyzate, what the present invention made The a large amount of active materials contained in fertilizer utilization yellow ginger hydrolyzate, are equipped with nitrogen, phosphorus, potassium and trace element, can effectively improve agriculture The yield of crop, the quality for improving agricultural product, improvement soil.
The present invention solve technical problem technical solution be:
It is to be prepared as follows fertilizer using yellow ginger hydrolyzate as raw material in the method that yellow ginger hydrolyzate prepares fertilizer:
By yellow ginger hydrolyzate, neutralization reaction tank is squeezed into pump, potassium hydroxide solution is added and adjusts hydrolyzate PH to 6.5 --- 7, so It is 10-320g/l, 0-380g/l of phosphorus element fertilizer, 0-300g/l of potassium fertilizer and micro that nitrogen manure is added in a liquid afterwards 10-20g/l of element fertilizer, stirring or heating stirring, obtain water-soluble fertilizer after cold filtration.
The method that yellow ginger hydrolyzate of the present invention prepares fertilizer, the stirring means are that nitrogen manure is added in a liquid For 10-320g/l, 0-380g/l of phosphorus element fertilizer, 10-20g/l of 0-300g/l of potassium fertilizer and trace-element fertilizer, stirring 2.5 --- 5 hours.
The method that yellow ginger hydrolyzate of the present invention prepares fertilizer, the heating stirring method are that nitrogen is added in a liquid Fertilizer be 10-320g/l, 0-380g/l of phosphorus element fertilizer, 10-20g/l of 0-300g/l of potassium fertilizer and trace-element fertilizer, It is heated to 80 --- 100 DEG C, it is carried out at the same time mixing time 1--2 hours.
The method that the present invention prepares fertilizer with yellow ginger hydrolyzate, is further improved, and water-soluble fertilizer input spray drying is made Solid-state water-soluble fertilizer is made in grain machine, concentrate drying.
The beneficial effects of the invention are as follows:
(1)The method that the present invention prepares fertilizer with yellow ginger hydrolyzate, it is that raw material prepares fertilizer, measurement result to choose yellow ginger hydrolyzate Show to reach as many as 236 kinds containing a large amount of bioactive ingredients in yellow ginger hydrolyzate, wherein from the point of view of the effect of traditional Chinese medicine, There are 14 kinds of clearing heat and detoxicating substance, 9 kinds of desinsection, pest-resistant substance, antibacterial to sterilize 10 kinds of substance, 8 kinds of anti-inflammatory substance resists 6 kinds of cancer substance, 5 kinds of antitumorigenic substance are used for 10 kinds of hypertensive substances, 6 kinds of analgesic matter, and 4 kinds of alkaloid is used for heart and brain blood disease 15 kinds of the ingredient of disease is used for 4 kinds of the ingredient of asthma;In addition there are 3 kinds of the substance with preservative, 16 kinds of the substance of intermediate, For 12 kinds of the substance of scientific research, other act on 48 kinds of unknown substance, small peptide substance amino acid class 19 to sort out 47 kinds of substance Kind, also as being rich in fulvic acid potassium in yellow ginger, fulvic acid potassium is a kind of short carbon chain molecule extracted from natural humic acid Structural material.It has high load amount and physiological activity.It is that plant utilizes that chelating constant and trace nutrient, which make it preferably,; Controlling plant diseases enhance Flood resistance;Excite plant microbiological activity;Improve chemical fertilizer and pesticide utilizes;Nutrition is improved to inhale It receives, promotes plant germination and growth;Accelerate precipitation to decompose, improves soil texture.Using so many yellow ginger hydrolyzate active material, Completely new water-soluble compoiste fertilizer can be produced.Therefore, the fertilizer that the present invention makes, which has, promotes plant cell division, increases Chlorophyll improves photosynthesis of plant efficiency, and biological enzyme in activated plant makes crop yield improve.
(2)The method that the present invention prepares fertilizer with yellow ginger hydrolyzate, with contain in yellow ginger hydrolyzate it is a large amount of activity at Point, these active constituents have more than 10 kinds of different function.Some of substances have relatively more clear in agricultural production Function, such as pyrethrin, cinerin, cantharidin etc. be the natural active material with insecticidal action.3- hydroxyl first The antibiotic such as oxygen benzyl Aminometradine, ampicillin, mupirocin, chloramphenicol alcohol have certain preventive and therapeutic effect to bacterium class disease. Hydroxyecdysone has insect growth regulator, IGR effect.Small peptide substance amino acid class is the origin of amino acid of natural plant.By In the fertilizer for preparing of the present invention contain desinsection, pest-resistant substance mebendazole metabolin, pyrethrin II, cinerin and antibacterial, The substances such as substance DL-2- aminocaprylic acids, 3- hydroxyl methoxybenzyl aminopyrimidines are sterilized, therefore, the fertilizer that the present invention makes, which has, to be made The disease-resistant function of object reduces Pesticide use amount.
(3)The method that the present invention prepares fertilizer with yellow ginger hydrolyzate adds nitrogen, phosphorus, potassium and micro in yellow ginger hydrolyzate Element is prepared as compoiste fertilizer, due to having big element fertilizer in fertilizer, also has trace element, which can be used to make The base fertilizer of object can be used for crop top dressing, also has and improves crop products and quality, improves and fertilizing soil acts on.
The effect example of Fertilizer application prepared by the present invention
Enforcement place:Jingbian County agricultural science and technology Demonstration Garden
Potato yield increases production 48-52% than pure fertilizer rational application of fertilizers, increases production 96-114% than habits fertilization, N P and K halves processing Than pure fertilizer N P and K full dose processing volume increase 8-12%;Significantly inhibit continuous cropping disease.Demonstrate organic total nutrient fertilizing treatment continuous cropping barrier The effect hindered.
(4)The method that the present invention prepares fertilizer with yellow ginger hydrolyzate prepares fertilizer with yellow ginger hydrolyzate, solves with yellow ginger When hydrolyzate extracts saponin the problem of hydrolyzate exhaust emission, Zero discharge can be reached, the pollution problem not only solved, also Raw material availability is improved, the added value of manufacturing enterprise is increased.Therefore, the method that the present invention prepares fertilizer with yellow ginger hydrolyzate, It is the beneficial way of yellow ginger comprehensive utilization, not only there is prodigious economic benefit, also good social benefit.
In conclusion the method that the present invention prepares fertilizer with yellow ginger hydrolyzate, the production of scientific utilization yellow ginger has comprehensive make Functional water-soluble natural fertilizer not only can fully develop the value of yellow ginger hydrolyzate, and can utilize Chinese medicine Natural pharmacological property ingredient, improves the soil environment of plant growth, rationally utilizes natural resource, adjusts the various microbial bacterias of soil Natural equilibrium, subtract medicine, and then produce natural organic safety food.
Described in synthesis, compared with prior art, the present invention technology is easy to implement.
Specific implementation mode
For that can further appreciate that the invention content of the present invention, following embodiment is hereby enumerated, detailed description are as follows:
Embodiment 1
With 1000 kilograms of yellow ginger hydrolyzates, fertilizer is prepared with following steps
Yellow ginger hydrolyzate is pumped into neutralization reaction tank, potassium hydroxide is added and carries out neutralization reaction, adjusts PH to 6.5 --- 7, enter 400 kilograms of urea is added in material-compound tank, and 20 kilograms of 200 kilograms of monoammonium phosphate, 50 kilograms of potassium sulfate and trace element are heated to 80 DEG C It is carried out at the same time stirring 2 hours, liquid obtains 2670 kilograms of liquid water-soluble fertilizer after cooling.
Make solid-state water-soluble fertilizer:2670 kilograms of liquid water-soluble fertilizers are inputted into spray drying granulation machine, are concentrated and dried system At 1017 kilograms of solid-state water-soluble fertilizer.
Embodiment 2
With 1000 kilograms of yellow ginger hydrolyzates, fertilizer is prepared with following steps
Yellow ginger hydrolyzate is pumped into neutralization reaction tank, potassium hydroxide is added and carries out neutralization reaction, adjusts PH to 6.5 --- 7, enter 20 kilograms of 500 kilograms of urea, 250 kilograms of potassium sulfate and trace element is added in material-compound tank, is heated to 100 DEG C and is carried out at the same time stirring 1 Hour, liquid obtains 3320 kilograms of liquid water-soluble fertilizer after cooling.
Make solid-state water-soluble fertilizer:3320 kilograms of liquid water-soluble fertilizers are inputted into spray drying granulation machine, are concentrated and dried system At 1188 kilograms of solid-state water-soluble fertilizer.
Embodiment 3
With 1000 kilograms of yellow ginger hydrolyzates, fertilizer is prepared with following steps
Yellow ginger hydrolyzate is pumped into neutralization reaction tank, potassium hydroxide is added and carries out neutralization reaction, adjusts PH to 6.5 --- 7, enter 400 kilograms of urea is added in material-compound tank, and 200 kilograms of monoammonium phosphate, 20 kilograms of trace element are stirred 2.5 hours, liquid is through cold But 2864 kilograms of liquid water-soluble fertilizer is obtained afterwards.
Make solid-state water-soluble fertilizer:2864 kilograms of liquid water-soluble fertilizers are inputted into spray drying granulation machine, are concentrated and dried system At 998 kilograms of solid-state water-soluble fertilizer.
Embodiment 4
With 1000 kilograms of yellow ginger hydrolyzates, fertilizer is prepared with following steps
Yellow ginger hydrolyzate is pumped into neutralization reaction tank, potassium hydroxide is added and carries out neutralization reaction, adjusts PH to 6.5 --- 7, enter 300 kilograms of urea is added in material-compound tank, and it is small to stir 5 for 60 kilograms of 200 kilograms of monoammonium phosphate, 200 kilograms of potassium sulfate and trace element When, obtain 3249 kilograms of liquid water-soluble fertilizer.
Make solid-state water-soluble fertilizer:3249 kilograms of liquid water-soluble fertilizers are inputted into spray drying granulation machine, are concentrated and dried system At 1187 kilograms of solid-state water-soluble fertilizer.

Claims (4)

1. a kind of method preparing fertilizer using yellow ginger hydrolyzate, it is characterized in that:The method for preparing fertilizer using yellow ginger hydrolyzate It is
By yellow ginger hydrolyzate, neutralization reaction tank is squeezed into pump, potassium hydroxide solution is added and adjusts hydrolyzate PH to 6.5 --- 7, so It is 10-320g/l, 0-380g/l of phosphorus element fertilizer, 0-300g/l of potassium fertilizer and micro that nitrogen manure is added in a liquid afterwards 10-20g/l of element fertilizer, stirring or heating stirring, obtain water-soluble fertilizer after cold filtration.
2. according to the method described in claim 1, it is characterized in that:The stirring means are that nitrogen manure is added in a liquid For 10-320g/l, 0-380g/l of phosphorus element fertilizer, 10-20g/l of 0-300g/l of potassium fertilizer and trace-element fertilizer, stirring 2.5 --- 5 hours.
3. according to the method described in claim 1, it is characterized in that:The heating stirring method is that nitrogen is added in a liquid Fertilizer be 10-320g/l, 0-380g/l of phosphorus element fertilizer, 10-20g/l of 0-300g/l of potassium fertilizer and trace-element fertilizer, It is heated to 80 --- 100 DEG C, it is carried out at the same time mixing time 1--2 hours.
4. according to the method described in claim 1, it is characterized in that:Water-soluble fertilizer is inputted into spray drying granulation machine, is concentrated and dried Solid-state water-soluble fertilizer is made.
CN201711034728.6A 2017-10-28 2017-10-28 A method of preparing fertilizer using yellow ginger hydrolyzate Pending CN108623371A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109776139A (en) * 2019-04-01 2019-05-21 陕西科技大学 Using production Chinese yam saponin slubbing waste water preparation apple foliage fertilizer, and preparation method thereof and fertilizing method
CN112624845A (en) * 2020-12-23 2021-04-09 竹山县鑫源皂素有限责任公司 Process method for producing water-soluble fertilizer by using turmeric wastewater
CN113526997A (en) * 2021-07-12 2021-10-22 湖北佰特克生物工程有限公司 Method for producing selenium-rich quick-acting fertilizer by using turmeric wastewater

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1488581A (en) * 2003-08-14 2004-04-14 华中师范大学 Yellow giner saponin industrial sewage treating method and comprehensive utilization
CN103848882A (en) * 2013-12-20 2014-06-11 西北农林科技大学 Turmeric saponin extraction method without waste emission
CN105734085A (en) * 2016-01-22 2016-07-06 竹山县鑫源皂素有限责任公司 After-treatment method of yellow ginger hydrolysate
CN107162724A (en) * 2017-05-19 2017-09-15 姚罗 A kind of preparation method using peltate yam waste slag as the compoiste fertilizer of raw material

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1488581A (en) * 2003-08-14 2004-04-14 华中师范大学 Yellow giner saponin industrial sewage treating method and comprehensive utilization
CN103848882A (en) * 2013-12-20 2014-06-11 西北农林科技大学 Turmeric saponin extraction method without waste emission
CN105734085A (en) * 2016-01-22 2016-07-06 竹山县鑫源皂素有限责任公司 After-treatment method of yellow ginger hydrolysate
CN107162724A (en) * 2017-05-19 2017-09-15 姚罗 A kind of preparation method using peltate yam waste slag as the compoiste fertilizer of raw material

Non-Patent Citations (1)

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马新爱: "黄姜皂素废水预处理与废渣资源化利用的研究", 《西北农林科技大学硕士学位论文》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109776139A (en) * 2019-04-01 2019-05-21 陕西科技大学 Using production Chinese yam saponin slubbing waste water preparation apple foliage fertilizer, and preparation method thereof and fertilizing method
CN112624845A (en) * 2020-12-23 2021-04-09 竹山县鑫源皂素有限责任公司 Process method for producing water-soluble fertilizer by using turmeric wastewater
CN113526997A (en) * 2021-07-12 2021-10-22 湖北佰特克生物工程有限公司 Method for producing selenium-rich quick-acting fertilizer by using turmeric wastewater

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Application publication date: 20181009