CN106748220A - A kind of amino acid Water soluble fertilizer and preparation method thereof - Google Patents
A kind of amino acid Water soluble fertilizer and preparation method thereof Download PDFInfo
- Publication number
- CN106748220A CN106748220A CN201611256472.9A CN201611256472A CN106748220A CN 106748220 A CN106748220 A CN 106748220A CN 201611256472 A CN201611256472 A CN 201611256472A CN 106748220 A CN106748220 A CN 106748220A
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- Prior art keywords
- amino acid
- water soluble
- soluble fertilizer
- acid water
- chelating agent
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The invention provides a kind of amino acid Water soluble fertilizer and preparation method thereof, mainly it is made up of the raw material of following weight percents：Compound amino acid 20 25%, middle micro- 10 15%, organic carbon 15 20%, potassium sulfate 5 10%, potassium dihydrogen phosphate 10 15%, chelating agent 8 15%, urea 20 30%, plant surface activating agent 3 6%.Amino acid Water soluble fertilizer of the invention is nutritious, is absorbed beneficial to crop, and the improvement of volume increase and quality to crop has obviously effect, and can improve soil quality, improves utilization rate of fertilizer, cost-effective.
Description
Technical field
The present invention relates to agricultural fertilizer manufacturing technology field, more particularly to a kind of amino acid Water soluble fertilizer and preparation method thereof.
Background technology
The Water soluble fertilizer of agricultural is a kind of water-soluble polyelement composite fertilizer, is a kind of new fertilizer of rising in recent years
Material, it can rapidly be dissolved in the water, it is easier to be absorbed by crops, and absorption rate is of a relatively high, more crucial
It is that it can apply to be sprayed the industrialized agricultures such as filling, realizes water-fertilizer integral, reaches the effect that water-saving saves fertile saving of labor.It is agriculture at present
Water-soluble fertilizer mainly has the macroelement fertilizer and single or various trace elements mixing blade face based on nitrogenous, phosphorus, potassium
Fertilizer, crop only plays a part of to supplement respective element after, there is certain effect of increasing production to crop, but existing market water
Although molten fertilizer dissolubility is good, the absorptivity of crop is relatively low, therefore the utilization rate of fertilizer is not high, cause the loss of fertilizer compared with
Greatly, it is relatively costly；On the other hand, current Water soluble fertilizer is not played fundamentally improves soil quality, alleviates China's soil
The effect of the problems such as content of organic matter decline, soil hardening, is unfavorable for the sustainable development of China's agricultural, therefore, improve fertilizer
Utilization rate, raising soil quality and crop product quantity are still the focus that China's agricultural sustainable development needs to solve at present
Problem.
The content of the invention
For the drawbacks described above and problem of prior art, the purpose of the embodiment of the present invention is to provide a kind of amino acid Water soluble fertilizer
And preparation method thereof, the amino acid Water soluble fertilizer is not only nutritious, and the improvement of volume increase and quality to crop is with very bright
Aobvious effect, for green non-pollution, organic products provide fertilizer, and can improve soil quality, improve utilization rate of fertilizer, solution
Existing Water soluble fertilizer utilization rate of having determined is relatively low, high cost, and is unfavorable for improving soil quality, and then improves the skill of crop yield in itself
Art problem.
In order to achieve the above object, the present invention provides following technical scheme：
A kind of amino acid Water soluble fertilizer of the invention, is mainly made up of the raw material of following weight percents：Compound amino acid 20-
25%, middle micro- 10-15%, organic carbon 15-20%, potassium sulfate 5-10%, potassium dihydrogen phosphate 10-15%, chelating agent 8-
15%, urea 20-30%, plant surface activating agent 3-6%.
Further, the chelating agent is the adjacent sodium of ethylenediamine two, polyepoxysuccinic acid salt, amino carboxylic acid, poly-
One or more in bright olefin(e) acid sodium；Wherein, the ratio of the chelating agent and compound amino acid is 2-5:4-6.
Further, the ratio of the chelating agent and compound amino acid is 2:5.
Further, mainly it is made up of the raw material of following weight percents：Compound amino acid 20-22%, middle trace element
10-12%, organic carbon 15-18%, potassium sulfate 5-6%, potassium dihydrogen phosphate 10-12%, chelating agent 8-10%, urea 20-25%,
Plant surface activating agent 3-4%.
Further, the plant surface activating agent is the sodium salt or sylvite of alkyl benzene sulphonate.
Further, the middle trace element includes calcium, magnesium, iron, zinc, boron and molybdenum；Wherein, the Han Liang of calcium≤10g/L, magnesium
Han Liang≤10g/L, the Han Liang≤5g/L of iron, the Han Liang≤5g/L of zinc, the Han Liang≤5g/L of boron, the Han Liang≤5g/L of molybdenum.
Further, the compound amino acid exists with free amino acid and small active peptides form.
Present invention also offers a kind of preparation method of amino acid Water soluble fertilizer, comprise the following steps：
Step one, by the compound amino acid of formula ratio and it is middle trace element mixing, add chelating agent and a certain amount of water
Stirring chelating 4-6 hours, chelates temperature is 60-80 DEG C；
Step 2, to reacting organic carbon, potassium sulfate, biphosphate that formula ratio is added in the product that obtains in step one
The mixing of potassium, urea and plant surface activating agent, stirring reaction 1-2 hours, reaction temperature was 50-70 DEG C；
Step 3, the mixed liquor that will be obtained in step 2 homogeneous refinement in high pressure homogenizer；Wherein, the homogeneous time be
30-40min, temperature is 60-80 DEG C, and homogenizer pressure is 100-150MPa；
Step 4, will be homogeneous after mixture condensing crystallizing, dry packing.
Further, in step one, the compound amino acid of formula ratio and middle trace element are mixed in reactor, then add
Enter chelating agent and the stirring of a certain amount of water is chelated 4 hours, chelates temperature is 80 DEG C；In step 2, stirring reaction 1 hour, reaction
Temperature is 60 DEG C；In step 3, the homogeneous time is 30min, and temperature is 60 DEG C, and homogenizer pressure is 150MPa.
A kind of amino acid Water soluble fertilizer that the present invention is provided and preparation method thereof, it is micro- by using compound amino acid and chelating agent
Secondary element is chelated to trace element in Chelating state, crop can be induced to produce the substantial amounts of basic element of cell division and promote chlorophyll to close
Into, raising photosynthetic rate and intensity of photosynthesis, and then lift plant life vigor.Plant surface activating agent rationally is added,
Make the dispersiveness of fertilizer more preferable with dissolubility；Meanwhile, it is more easy to be absorbed and used by plants, so as to help plant preferably to absorb support
Point, absorptivity of the crop to fertilizer is greatly enhanced, the loss of fertilizer is reduced, save cost.
Meanwhile, Water soluble fertilizer of the invention is not only nutritious, and the improvement of volume increase and quality to crop is with very bright
Aobvious effect, for green non-pollution, organic products provide fertilizer.On this basis, this Water soluble fertilizer can also improve soil quality,
The retain water and nutrients ability of soil is improved, environmental pollution is reduced, the development of organic food, pollution-free food can be significantly improved
Space.
Specific embodiment
Below in conjunction with embodiments of the invention, technical scheme is clearly and completely described, it is clear that
Described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based on the implementation in the present invention
Example, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made is belonged to
The scope of protection of the invention.
In the embodiment of the present invention, compound amino acid is hydrolyzed by animal protein, filtered, is concentrated to give.
Embodiment 1
The amino acid Water soluble fertilizer of the embodiment of the present invention 1, is mainly made up of the raw material of following weight percents：Compound amino acid
20%, middle micro- 15%, organic carbon 15%, potassium sulfate 5%, potassium dihydrogen phosphate 10%, chelating agent 10%, urea 20%,
Plant surface activating agent 3%.
The preparation method of the amino acid Water soluble fertilizer of the present embodiment 1, specially：By above-mentioned formula ratio by compound amino acid and in
Trace element is mixed in reactor, adds chelating agent and the stirring of a certain amount of water is chelated 4 hours, and chelates temperature is 80 DEG C；
The sodium salt for adding organic carbon, potassium sulfate, potassium dihydrogen phosphate, urea and alkyl benzene sulphonate is mixed, stirring reaction 1 hour,
Reaction temperature is 60 DEG C；The mixture that will be obtained again homogeneous refinement in high pressure homogenizer；Wherein, the homogeneous time is 30min, temperature
It is 60 DEG C to spend, and homogenizer pressure is 150MPa；Finally by mixed liquor condensing crystallizing, packaging obtains final product the present embodiment after spray drying
Amino acid Water soluble fertilizer.
Embodiment 2
The amino acid Water soluble fertilizer of the embodiment of the present invention 2, is mainly made up of the raw material of following weight percents：Compound amino acid
22%, middle micro- 10%, organic carbon 16%, potassium sulfate 5%, potassium dihydrogen phosphate 12%, chelating agent 10%, urea 20%,
Plant surface activating agent 4%.
The amino acid Water soluble fertilizer preparation method of the present embodiment 2 is with embodiment 1.
Embodiment 3
The amino acid Water soluble fertilizer of the embodiment of the present invention 3, is mainly made up of the raw material of following weight percents：Compound amino acid
25%, middle micro- 10%, organic carbon 15%, potassium sulfate 8%, potassium dihydrogen phosphate 10%, chelating agent 8%, urea 20% is planted
Thing surfactant 4%.
The amino acid Water soluble fertilizer preparation method of the present embodiment 3 is with embodiment 1.
Test case
1st, the amino acid Water soluble fertilizer for taking the present embodiment 2 is tested in the apple production that kind is Fuji apple.
2nd, for examination soil to fly bubble sandy soil, organic matter 15.35g/kg, pH5.8, full nitrogen 0.70g/kg, available phosphorus
15.45mg/mg, available potassium 75.38mg/kg, pH8.1.
Experimental design
This experiment sets 3 treatment, 3 repetitions, random alignment, and plot area is 4 apple tree 96m2, other agronomy of field
Measure is consistent.
Treatment a, Routine control.Base is topdressed by local routine service condition, and foliar fertilizer and conditioning agent are not used.
Treatment b, clear water control.Every mu every time so that with period foliage-sprays such as 3 equivalent clear water for the treatment of, other measures of fertilizer are same
Treatment a.
Treatment c, the amino acid Water soluble fertilizer using the present embodiment 2.Every mu of fertilizer sprayed every time after being watered 800 times of dilution
100ml starts to spray one inferior to fruit, the leaf and soil of growth at interval of 10 days in blade face after apple is thanked and spent, and 4 are sprayed altogether
Secondary, other measures of fertilizer are same to process a.
Experiment field management
This is tested and base manure is applied mid-March, May tillage and weeding, sprays 4 agricultural chemicals 4-7 months, and October 25 harvested,
Do field record during whole fertility well.
Interpretation of result
Specifically it is shown in Table 1, table 2.
Table 1 applies influence of the amino acid Water soluble fertilizer of the present embodiment 2 to apple biological character
The comparing of the different disposal apple production of table 2
Result of the test shows：Apple on the basis of conventional fertilizer application, after spraying the amino acid Water soluble fertilizer of the present embodiment 2, with
Conventional, clear water control is compared, and increased that the plant height of apple, stem be thick and Weight per plant, so as to improve yield, than Routine control mu
249.8kg/ mus of volume increase, rate of growth 10.6% increases production 185.6kg/ mus, rate of growth 7.9% than clear water control mu.
The above, specific embodiment only of the invention, but protection scope of the present invention is not limited thereto, and it is any
Those familiar with the art the invention discloses technical scope in, change or replacement can be readily occurred in, should all contain
Cover within protection scope of the present invention.Therefore, protection scope of the present invention described should be defined by scope of the claims.
Claims (9)
1. a kind of amino acid Water soluble fertilizer, it is characterised in that：Mainly it is made up of the raw material of following weight percents：Compound amino acid
20-25%, middle micro- 10-15%, organic carbon 15-20%, potassium sulfate 5-10%, potassium dihydrogen phosphate 10-15%, chelating agent
8-15%, urea 20-30%, plant surface activating agent 3-6%.
2. a kind of amino acid Water soluble fertilizer according to claim 1, it is characterised in that：The chelating agent is the adjacent benzene of ethylenediamine two
A kind of or wherein several mixture in guanidine-acetic acid sodium, polyepoxysuccinic acid salt, amino carboxylic acid, polypropylene acid sodium；Wherein,
The ratio of the chelating agent and compound amino acid is 2-5:4-6.
3. a kind of amino acid Water soluble fertilizer according to claim 2, it is characterised in that：The chelating agent and compound amino acid
Ratio is 2:5.
4. a kind of amino acid Water soluble fertilizer according to claim 1,2 or 3, it is characterised in that：Mainly by following weight percent
The raw material of ratio is made：Compound amino acid 20-22%, middle micro- 10-12%, organic carbon 15-18%, potassium sulfate 5-6%, phosphorus
Acid dihydride potassium 10-12%, chelating agent 8-10%, urea 20-25%, plant surface activating agent 3-4%.
5. a kind of amino acid Water soluble fertilizer according to claim 1,2 or 3, it is characterised in that：The plant surface activating agent
It is the sodium salt or sylvite of alkyl benzene sulphonate.
6. a kind of amino acid Water soluble fertilizer according to claim 1,2 or 3, it is characterised in that：The middle trace element includes
Calcium, magnesium, iron, zinc, boron and molybdenum；Wherein, the Han Liang≤10g/L of calcium, the Han Liang≤10g/L of magnesium, the Han Liang≤5g/L of iron, zinc contain
Liang≤5g/L, the Han Liang≤5g/L of boron, the Han Liang≤5g/L of molybdenum.
7. a kind of amino acid Water soluble fertilizer according to claim 1,2 or 3, it is characterised in that：The compound amino acid is swimming
Isolated amino acid and small active peptides form are present.
8. the preparation method of a kind of amino acid Water soluble fertilizer as any one of claim 1 to 7, it is characterised in that：Including
Following steps：
Step one, by the compound amino acid of formula ratio and it is middle trace element mixing, add chelating agent and a certain amount of water stirring
Chelating 4-6 hours, chelates temperature is 60-80 DEG C；
Step 2, to reacting organic carbon, potassium sulfate, potassium dihydrogen phosphate, urine that formula ratio is added in the product that obtains in step one
Element and the mixing of plant surface activating agent, stirring reaction 1-2 hours, reaction temperature was 50-70 DEG C；
Step 3, the mixed liquor that will be obtained in step 2 homogeneous refinement in high pressure homogenizer；Wherein, the homogeneous time is 30-
40min, temperature is 60-80 DEG C, and homogenizer pressure is 100-150MPa；
Step 4, will be homogeneous after mixture condensing crystallizing, dry packing.
9. the preparation method of a kind of amino acid Water soluble fertilizer according to claim 8, it is characterised in that：In step one, will match somebody with somebody
The compound amino acid of side's amount and middle trace element mix in reactor, add chelating agent and a certain amount of water stirring chelating 4
Hour, chelates temperature is 80 DEG C；In step 2, stirring reaction 1 hour, reaction temperature is 60 DEG C；In step 3, the homogeneous time is
30min, temperature is 60 DEG C, and homogenizer pressure is 150MPa.
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| CN201611256472.9A CN106748220A (en) | 2016-12-30 | 2016-12-30 | A kind of amino acid Water soluble fertilizer and preparation method thereof |
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| CN201611256472.9A CN106748220A (en) | 2016-12-30 | 2016-12-30 | A kind of amino acid Water soluble fertilizer and preparation method thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107285927A (en) * | 2017-08-15 | 2017-10-24 | 清远市美村生物技术有限公司 | A kind of composite fertilizer with trace elements and preparation method thereof |
| CN107434744A (en) * | 2017-08-22 | 2017-12-05 | 清远市美村生物技术有限公司 | A kind of Particles dispersed secondary and micro-element fertilizers and preparation method thereof |
| CN107540470A (en) * | 2017-10-30 | 2018-01-05 | 成都云图控股股份有限公司 | A kind of water-soluble fertilizer containing fulvic acid and preparation method thereof |
| CN107556138A (en) * | 2017-09-18 | 2018-01-09 | 佛山实瑞先导材料研究院（普通合伙） | A kind of amino acid fertilizer |
| CN107573157A (en) * | 2017-09-21 | 2018-01-12 | 阿米巴南京生物技术有限责任公司 | A kind of preparation method of the water-soluble fertilizer of element type containing amino acid calcium |
| CN107573153A (en) * | 2017-09-21 | 2018-01-12 | 阿米巴南京生物技术有限责任公司 | A kind of preparation method of the water-soluble fertilizer of element type containing amino-acid zinc |
| CN107573156A (en) * | 2017-09-21 | 2018-01-12 | 阿米巴南京生物技术有限责任公司 | A kind of preparation method of the water-soluble fertilizer containing amino acid |
| CN107698334A (en) * | 2017-11-06 | 2018-02-16 | 王友福 | A kind of novel solid nutrient solution Water soluble fertilizer of full nutritive element and preparation method thereof |
| CN111440023A (en) * | 2020-03-17 | 2020-07-24 | 浙江丰瑜生态科技股份有限公司 | Slow-release water-soluble fertilizer containing humic acid |
| CN111499449A (en) * | 2020-03-25 | 2020-08-07 | 浙江丰瑜生态科技股份有限公司 | Slow-release water-soluble fertilizer suitable for planting in sandy soil and application thereof |
| CN112225619A (en) * | 2020-10-28 | 2021-01-15 | 沈阳师范大学 | Amino acid-containing water-soluble fertilizer for lawn rejuvenation |
| CN112679278A (en) * | 2020-12-29 | 2021-04-20 | 北京世纪阿姆斯生物工程有限公司 | Amino acid water-soluble fertilizer with function of enhancing low-temperature resistance of crops and preparation method thereof |
| CN113651647A (en) * | 2021-08-17 | 2021-11-16 | 广东凯米瑞特肥科技有限公司 | Preparation method of amino acid water-soluble fertilizer |
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| CN104326817A (en) * | 2014-10-18 | 2015-02-04 | 郑州在田农业科学技术研究院 | Special foliage spray water-soluble fertilizer for apples |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107285927A (en) * | 2017-08-15 | 2017-10-24 | 清远市美村生物技术有限公司 | A kind of composite fertilizer with trace elements and preparation method thereof |
| CN107434744A (en) * | 2017-08-22 | 2017-12-05 | 清远市美村生物技术有限公司 | A kind of Particles dispersed secondary and micro-element fertilizers and preparation method thereof |
| CN107556138A (en) * | 2017-09-18 | 2018-01-09 | 佛山实瑞先导材料研究院（普通合伙） | A kind of amino acid fertilizer |
| CN107573156A (en) * | 2017-09-21 | 2018-01-12 | 阿米巴南京生物技术有限责任公司 | A kind of preparation method of the water-soluble fertilizer containing amino acid |
| CN107573157A (en) * | 2017-09-21 | 2018-01-12 | 阿米巴南京生物技术有限责任公司 | A kind of preparation method of the water-soluble fertilizer of element type containing amino acid calcium |
| CN107573153A (en) * | 2017-09-21 | 2018-01-12 | 阿米巴南京生物技术有限责任公司 | A kind of preparation method of the water-soluble fertilizer of element type containing amino-acid zinc |
| CN107540470A (en) * | 2017-10-30 | 2018-01-05 | 成都云图控股股份有限公司 | A kind of water-soluble fertilizer containing fulvic acid and preparation method thereof |
| CN107698334A (en) * | 2017-11-06 | 2018-02-16 | 王友福 | A kind of novel solid nutrient solution Water soluble fertilizer of full nutritive element and preparation method thereof |
| CN111440023A (en) * | 2020-03-17 | 2020-07-24 | 浙江丰瑜生态科技股份有限公司 | Slow-release water-soluble fertilizer containing humic acid |
| CN111499449A (en) * | 2020-03-25 | 2020-08-07 | 浙江丰瑜生态科技股份有限公司 | Slow-release water-soluble fertilizer suitable for planting in sandy soil and application thereof |
| CN111499449B (en) * | 2020-03-25 | 2021-11-16 | 浙江丰瑜生态科技股份有限公司 | Slow-release water-soluble fertilizer suitable for planting in sandy soil and application thereof |
| CN112225619A (en) * | 2020-10-28 | 2021-01-15 | 沈阳师范大学 | Amino acid-containing water-soluble fertilizer for lawn rejuvenation |
| CN112679278A (en) * | 2020-12-29 | 2021-04-20 | 北京世纪阿姆斯生物工程有限公司 | Amino acid water-soluble fertilizer with function of enhancing low-temperature resistance of crops and preparation method thereof |
| CN113651647A (en) * | 2021-08-17 | 2021-11-16 | 广东凯米瑞特肥科技有限公司 | Preparation method of amino acid water-soluble fertilizer |
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