CN107362108A - A kind of Golden flower facial mask and preparation method thereof - Google Patents

A kind of Golden flower facial mask and preparation method thereof Download PDF

Info

Publication number
CN107362108A
CN107362108A CN201710882890.7A CN201710882890A CN107362108A CN 107362108 A CN107362108 A CN 107362108A CN 201710882890 A CN201710882890 A CN 201710882890A CN 107362108 A CN107362108 A CN 107362108A
Authority
CN
China
Prior art keywords
golden flower
facial mask
extract
hibiscus esculentus
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710882890.7A
Other languages
Chinese (zh)
Inventor
李方源
李彩艳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen Juyuan Baoding Agricultural Biotechnology Industry Development Co Ltd
Original Assignee
Shenzhen Juyuan Baoding Agricultural Biotechnology Industry Development Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shenzhen Juyuan Baoding Agricultural Biotechnology Industry Development Co Ltd filed Critical Shenzhen Juyuan Baoding Agricultural Biotechnology Industry Development Co Ltd
Priority to CN201710882890.7A priority Critical patent/CN107362108A/en
Publication of CN107362108A publication Critical patent/CN107362108A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/673Vitamin B group
    • A61K8/675Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/737Galactomannans, e.g. guar; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/004Aftersun preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/524Preservatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention discloses a kind of Golden flower facial mask and preparation method thereof, and the composition of raw materials of the Golden flower facial mask is as follows:80 ~ 90 parts of water, 0.2 ~ 0.5 part of Hibiscus esculentus L. extract, 0.3 ~ 0.5 part of niacinamide, 0.02 ~ 0.06 part of allantoin, 7 ~ 10 parts of NMF, 0.03 ~ 0.1 part of preservative, 0.6 ~ 1.0 part of film forming agent, 0.3 ~ 0.6 part of antioxidant, 0.2 ~ 0.4 part of emulsifying agent, 0.01 ~ 0.03 part of essence.The facial mask is under the synergy of tara gum and xanthans, whole system has stable property, so that Hibiscus esculentus L. extract does not go bad, Hibiscus esculentus L. extract has very strong antiinflammation to face acne, acne, reparation sunburn, serve effective skin effect, Hibiscus esculentus L. extract property is gentle simultaneously, to skin natural no stimulation.

Description

A kind of Golden flower facial mask and preparation method thereof
Technical field
The present invention relates to skin protection cosmetics field, more particularly to a kind of Golden flower facial mask and preparation method thereof.
Background technology
Facial mask is the skin care item commonly used in daily life, has the function that to make one to loosen while skin of face is maintained, Meanwhile the active material of the facial mask of existing market appearance is mostly chemical composition, has certain side effect, day to human body skin The facial mask of right plant is into new focus.
Golden flower is to originate in a kind of plant of south China, is recorded according to Compendium of Materia Medica, and there is Golden flower the clear sore of anti-inflammatory to make With to face acne, acne, repairing sunburn there is very strong antiinflammation, modern experimental is studied and draws following result;Plant gold Tree mallow is to repair appearance inflammation and acne most natural plants.The active ingredient of Golden flower is applied in facial mask, inherently obtained Gratifying skin effect.
In the prior art, there has been no the case for applying to Golden flower in facial mask, meanwhile, keeping Hibiscus esculentus L. extract While active ingredient activity, it is ensured that the stability of entire surface film system, and technological difficulties.
Therefore, prior art has yet to be improved and developed.
The content of the invention
In view of above-mentioned the deficiencies in the prior art, it is an object of the invention to provide a kind of Golden flower facial mask and its preparation side Method, it is intended to solve the problems, such as to there is no Hibiscus esculentus L. extract facial mask in the prior art.
Technical scheme is as follows:
A kind of Golden flower facial mask, wherein, in parts by weight, its composition of raw materials composition is:
80 ~ 90 parts of water, 0.2 ~ 0.5 part of Hibiscus esculentus L. extract, 0.3 ~ 0.5 part of niacinamide, 0.02 ~ 0.06 part of allantoin, NMF 7 ~ 10 parts, 0.03 ~ 0.1 part of preservative, 0.6 ~ 1.0 part of film forming agent, 0.3 ~ 0.6 part of antioxidant, 0.2 ~ 0.4 part of emulsifying agent, essence 0.01 ~ 0.03 part.
Described Golden flower facial mask, wherein, the NMF is glycerine, butanediol, glycine betaine, propane diols, hyaluronic acid One or more in sodium.
Described Golden flower facial mask, wherein, the preservative is methyl hydroxybenzoate, iodine propilolic alcohol butyl mephenesin Carbamate, double(Hydroxyl Methyl)One or more in imidazolidinyl urea.
Described Golden flower facial mask, wherein, the film forming agent is tara gum.
Described Golden flower facial mask, wherein, the antioxidant is silk glue protein.
Described Golden flower facial mask, wherein, the emulsifying agent is xanthans.
A kind of preparation method of Golden flower facial mask as described above, wherein, comprise the following steps:
Hibiscus esculentus L. extract is obtained by extraction;
Water, Hibiscus esculentus L. extract, niacinamide, allantoin, NMF, preservative, film forming agent, anti-is separately added into according to aforementioned proportion Oxidant, emulsifying agent and essence, facial mask liquid is obtained after mixing;
The facial mask liquid is heated to 90 ~ 120 DEG C emulsifying liquid, holding is cooled to 30 ~ 50 DEG C after 30 ~ 40 minutes, Obtain facial mask gel;
Facial mask gel tiling is pulled into the consistent uniform film of thickness using film balance, obtains gel mould;
The gel mould is placed on one layer of nylon mesh, Golden flower facial mask is made.
The preparation method of described Golden flower facial mask, wherein, described the step of Hibiscus esculentus L. extract is obtained by extraction, specifically wraps Include:
Golden flower raw material is put into emulsification machine equipment to addition deionized water after smashing refinement and obtains Golden flower suspension;
Supercritical CO is carried out to the Golden flower suspension2Extraction, obtains Golden flower extract;
The Golden flower extract is filtered, obtains Hibiscus esculentus L. extract.
The preparation method of described Golden flower facial mask, wherein, in the Golden flower suspension, deionized water is former with Golden flower The weight ratio of material is 50:1.
The preparation method of described Golden flower facial mask, wherein, the filtration step is specially:Golden flower is extracted using gauze Liquid is taken to be filtered, in triplicate.
Beneficial effect:Golden flower facial mask provided by the present invention, there is advantages below:1st, natural Hibiscus esculentus L. extract, property Matter is gently non-stimulated to skin, does not produce side effect;2nd, Golden flower has the effect of repairing appearance inflammation and acne so that golden flower Certain herbaceous plants with big flowers facial mask has preferably maintenance effect;3rd, tara gum has preferably compatible effect with entire surface film system, it is ensured that each The stability of individual component so that facial mask property is unlikely to deteriorate.
Embodiment
The present invention provides a kind of Golden flower facial mask and preparation method thereof, to make the purpose of the present invention, technical scheme and effect Clearer, clear and definite, the present invention is described in more detail below.It should be appreciated that specific embodiment described herein is only To explain the present invention, it is not intended to limit the present invention.
A kind of Golden flower facial mask that the embodiment of the present invention is provided, wherein, in parts by weight, its composition of raw materials composition For:
80 ~ 90 parts of water, 0.2 ~ 0.5 part of Hibiscus esculentus L. extract, 0.3 ~ 0.5 part of niacinamide, 0.02 ~ 0.06 part of allantoin, NMF 7 ~ 10 parts, 0.03 ~ 0.1 part of preservative, 0.6 ~ 1.0 part of film forming agent, 0.3 ~ 0.6 part of antioxidant, 0.2 ~ 0.4 part of emulsifying agent, essence 0.01 ~ 0.03 part.
Wherein, water dissolves all compositions, specifically, the water is deionized water, and Hibiscus esculentus L. extract is made as solvent For active component, as astringent and antiphlogistic, there is the effect of repairing appearance inflammation and acne, niacinamide is vitamin B3 A kind of derivative, and the skin anti-aging composition that cosmetic dermatology field is generally acknowledged, are used as whitening anti-freckle agent in body series Use, allantoin is a kind of amphoteric compound, can combine many kinds of substance formed double salt, have lucifuge, sterilization and anticorrosion, analgesic, resist Oxidation, skin can be made to keep moisture content, moisten and soft, used in body series as antiinflammatory, NMF is using During ensure moisture-keeping function of the facial mask to skin of face;Mentioned component dissolves forming face in a solvent by the effect of emulsifying agent Film liquid, while add preservative and antioxidant in facial mask liquid and prevent ingredient spoilage, in the presence of film forming agent, facial mask liquid is cold But it is changed into gel afterwards, addition of the essence in system can be fragrant during the use of product, lifts the use of user Impression.
Further, described Golden flower facial mask, wherein, the NMF be glycerine, butanediol, glycine betaine, propane diols, One or more in Sodium Hyaluronate.
Wherein, glycerine also has the effect of dissolving niacinamide concurrently, butanediol is in cosmetics in addition to being used as NMF Often do NMF and solvent uses, in terms of moisturizing, because butanediol is small molecule moisturizing composition, so water ratio very little is grabbed, Also there is certain bacteriostasis simultaneously, glycine betaine is a kind of alkaloid, has strong moisture pick-up properties, soluble in water, in moisturizing While with certain cleaning action, while glycine betaine indifferent equilibrium does not injure skin, also had in whole system certain Bactericidal antiphlogistic effect, propane diols and glycerine coordinates and is used as wetting agent, solid material can be made to be more easy to be soaked in water, by reducing it Surface tension or interfacial tension, allow the water to be deployed on solid material surface, or penetrate its surface, and solid material is soaked, Ensure the moistening degree of entire surface film system, Sodium Hyaluronate is one of composition of human body skin in itself, is distributed most in human body The acid glutinous sugar of wide one kind, is present in the matrix of connective tissue, adds as NMF in facial mask, have to user's skin Good moisture-keeping function.
Further, described Golden flower facial mask, wherein, the preservative is methyl hydroxybenzoate, iodine propilolic alcohol butyl ammonia first It is acid esters, double(Methylol)One or more in imidazolidinyl urea.
Wherein, methyl hydroxybenzoate has broad spectrum antibiotic activity, can suppress Gram-negative, positive bacteria, to saccharomycete and mould Bacterium has stronger inhibitory action, with traditional aseptic production (such as:Sodium benzoate) compare, have concentration low, wide spectrum is high The advantages of effect, and safety economy, grown using the effect phase;Iodine propilolic alcohol butyl mephenesin Carbamate(IPBC it is) that a kind of novel cosmetic is used Preservative, there is good fungistatic effect, and have preferable dissolubility in surfactant, emulsifying agent, polar solvent;It is double (Methylol)Imidazolidinyl urea has good dissolubility, can with all component interworkings in facial mask system, with methyl hydroxybenzoate, iodine third Alkynol butyl mephenesin Carbamate interworking, improve the antiseptic property of whole system.
Further, described Golden flower facial mask, wherein, the film forming agent is tara gum.
Wherein, the property of tara gum is between locust bean gum and guar gum, and tasteless albumen is refined more Sugar, mainly contains mannose and gala is warded off, and character of use is gently nonirritant in facial mask, and its most important feature is it and body Xanthans in system has a certain degree of gel cooperative effect, can make it is compound after dosage level it is very low and improve gel tissue Structure.Tara gum is only partly dissolved in cold water, is heated to 85 degree and is kept more than the 10 minutes abundant aquations of ability, with system Other interior components are dissolved each other, and peak viscosity is reached after cooling, form gelatinous material.
Further, described Golden flower facial mask, wherein, the antioxidant is silk glue protein.
Wherein, the amino acid in silk glue protein can suppress the activity of tyrosinase in skin, anti-oxidant so as to play Effect, effectively help the pollution of user skin against external, keep skin ph value balance, strengthen skin immunity.
Further, described Golden flower facial mask, wherein, the emulsifying agent is xanthans.
Xanthans is a kind of to integrate thickening, suspend, emulsify, being stable at superior performances as a kind of natural materials Biogum, xanthans can be used as food additives in itself, therefore use is to no skin irritation in facial mask, while as breast Agent uses, and promotes the dissolving of each component in a solvent, while is cooperateed with tara gum and play gel cooperative effect, reduces compound Dosage afterwards is horizontal and improves gel tissue's structure, it is ensured that the gel mould for processing to obtain is in most stable of state.
The present invention also provides a kind of preparation method of Golden flower facial mask as described above, wherein, comprise the following steps:
Hibiscus esculentus L. extract is obtained by extraction;
Water, Hibiscus esculentus L. extract, niacinamide, allantoin, NMF, preservative, film forming agent, anti-is separately added into according to aforementioned proportion Oxidant, emulsifying agent and essence, facial mask liquid is obtained after mixing;
The facial mask liquid is heated to 90 ~ 120 DEG C emulsifying liquid, holding is cooled to 30 ~ 50 DEG C after 30 ~ 40 minutes, Obtain facial mask gel;
Facial mask gel tiling is pulled into the consistent uniform film of thickness using film balance, obtains gel mould;
The gel mould is placed on one layer of nylon mesh, Golden flower facial mask is made.
Wherein, technical thought of the invention is facial mask system being prepared into gel mould, and gel mould is placed on into nylon yarn After net, be made Golden flower facial mask, user using when the Golden flower facial mask applied throwing off the nylon mesh afterwards on the face, i.e., Face mask film can be started;During facial mask liquid is made, using xanthans as emulsifying agent, each component is mixed, 2 hours afterwards Within facial mask liquid is heated to 90 ~ 120 DEG C, wherein, when temperature reaches more than 85 DEG C, the tara gum as film forming agent starts Generation aquation simultaneously mixes with solvent, and due to having other components in system, therefore the heating-up temperature of whole facial mask liquid is minimum 90 DEG C, if heating-up temperature is too high, high temperature can cause Hibiscus esculentus L. extract to lose activity, and therefore, the maximum temperature of heating is 120 DEG C, heat the too fast material that can cause near heating sources and be denatured, it is therefore desirable to slowly heat, speed is 2 hours;
Facial mask liquid need to be kept 30 ~ 40 minutes at 90 ~ 120 DEG C, wherein, tara gum need to keep under the temperature range in itself to Few more than the ten minutes abundant aquations of ability, because tara gum also needs to mutually act synergistically with xanthans, and each component In the well mixed reaction time, at least need to keep the time of 30 minutes, just can guarantee that reaction is complete, entire surface at 90 ~ 120 DEG C Film liquid is fully emulsified;Heat time is long, then can cause the in one's duty active matter of group while wasting the energy, reducing production efficiency Matter is lost activity, and therefore, the heat time was controlled at 30 ~ 40 minutes.
30 ~ 50 DEG C are cooled to, whole facial mask liquid cooling, tara gum is condensed into gel, is evened up and cut out using film balance Afterwards, gel mould is obtained.
Further, the preparation method of described Golden flower facial mask, wherein, the step that Hibiscus esculentus L. extract is obtained by extraction Suddenly specifically include:
Golden flower raw material is put into emulsification machine equipment to addition deionized water after smashing refinement and obtains Golden flower suspension;
Supercritical CO is carried out to the Golden flower suspension2Extraction, obtains Golden flower extract;
The Golden flower extract is filtered, obtains Hibiscus esculentus L. extract.
Wherein, the extraction to Hibiscus esculentus L. extract is divided into pretreatment, extracts and filter three steps,
In preprocessing process, the equipment using emulsification machine equipment as grinding Golden flower raw material is smashed, Golden flower raw material is emulsifying High-speed motion in gap between the multi-layer rotor and stator of machine equipment, forms strong aquashear and turbulent flow, dispersed material, Centrifugation is produced simultaneously and the comprehensive function power such as extrudes, mill, colliding, and material is sufficiently mixed, stirred, is refined and reach ideal and grind Mill requires, after adding deionized water, forms Golden flower suspension;
In extraction process, supercritical carbon dioxide has special dissolubility to plants essential oil, its dissolubility and density Correlation, and density can be adjusted by temperature and pressure, so as to which Hibiscus esculentus L. extract be separated out.Detailed process is:Utilize spy Fixed equipment makes carbon dioxide reach supercriticality(More than 32 DEG C of temperature, more than 7.2 MPas of pressure), by the golden flower in material Certain herbaceous plants with big flowers extract extracts, then separates Hibiscus esculentus L. extract by alternating temperature transformation.
Filtration step removes the solid impurity remained in extraction process, so as to obtain pure Hibiscus esculentus L. extract.
Further, the preparation method of described Golden flower facial mask, wherein, in the Golden flower suspension, deionized water Weight ratio with Golden flower raw material is 50:1.
The ratio of Golden flower raw material and deionized water determines the concentration of Hibiscus esculentus L. extract, and concentration is too small to cause extraction Thing is too dilute, it is impossible to reaches the skin effect of anticipation;Excessive concentration can then cause Skin Cell dehydration, skin ambustion, therefore, go from The control of the ratio of sub- water and Golden flower raw material is 50:1.
Further, the preparation method of described Golden flower facial mask, wherein, the filtration step is specially:Use gauze Golden flower extract is filtered, in triplicate.
Because during emulsifier device cutting and grinding Golden flower raw material, Golden flower raw material is ground into thinner powder End, solid matter residual is had after extraction is completed, it is therefore desirable to pass through filtration step, it is ensured that the degree of purity of extract;Its In, the gauze is specially medical sterile gauze, by filtering three times, it is ensured that filters out the solid impurity filter in Golden flower extract Except clean.
In order to more describe the preparation method of the present invention in detail, embodiment further description is exemplified below.
Embodiment 1
A kind of factory formula of Golden flower facial mask:90 parts of water, 5 parts of glycerine, 2 parts of butanediol, 0.8 part of tara gum, silk gum egg White 0.5 part, 0.3 part of glycine betaine, 0.3 part of Hibiscus esculentus L. extract, 0.4 part of niacinamide, 0.5 part of propane diols, 0.05 part of allantoin, It is 0.3 part of xanthans, 0.2 part of Sodium Hyaluronate, 0.02 part of methyl hydroxybenzoate, 0.02 part of iodine propilolic alcohol butyl mephenesin Carbamate, double(Hydroxyl first Base)0.01 part of imidazolidinyl urea, 0.01 part of essence.
Preparation technology:Golden flower raw material is put into after smashing refinement in emulsification machine equipment, by 50:1 ratio add go from Sub- water obtains Golden flower suspension;Supercritical CO is carried out to the Golden flower suspension2Extraction, obtains Golden flower extract;Make The Golden flower extract is filtered three times with gauze, obtains Hibiscus esculentus L. extract.
By 90 parts of water, 5 parts of glycerine, 2 parts of butanediol, 0.8 part of tara gum, 0.5 part of silk glue protein, glycine betaine 0.3 Part, 0.3 part of Hibiscus esculentus L. extract, 0.4 part of niacinamide, 0.5 part of propane diols, 0.05 part of allantoin, 0.3 part of xanthans, hyalomitome It is sour 0.2 part of sodium, 0.02 part of methyl hydroxybenzoate, 0.02 part of iodine propilolic alcohol butyl mephenesin Carbamate, double(Methylol)Imidazolidinyl urea 0.01 Part, 0.01 part of essence are well mixed and obtain facial mask liquid.
The facial mask liquid is heated into 100 DEG C in 2 hours to emulsify facial mask liquid, it is after being kept for 35 minutes that facial mask liquid is cold But to 40 DEG C, facial mask gel is obtained, facial mask gel tiling is pulled into the consistent uniform film of thickness using film balance, obtained Gel mould;The gel mould is placed on one layer of nylon mesh, Golden flower facial mask is made.
Obtained facial mask, under the synergy of tara gum and xanthans, whole system has stable property, makes Obtain Hibiscus esculentus L. extract not go bad, Hibiscus esculentus L. extract makees face acne, acne, reparation sunburn with very strong anti-inflammatory With serving effective skin effect.
Beneficial effect:Golden flower facial mask provided by the present invention, there is advantages below:1st, natural Hibiscus esculentus L. extract, property Matter is gently non-stimulated to skin, does not produce side effect;2nd, Golden flower has the effect of repairing appearance inflammation and acne so that golden flower Certain herbaceous plants with big flowers facial mask has preferably maintenance effect;3rd, tara gum has preferably compatible effect with entire surface film system, it is ensured that each The stability of individual component so that facial mask property is unlikely to deteriorate.Obtained facial mask indices are as shown in table 1, by the detection of table 1 As a result visible in, high using the Golden flower facial mask of the present invention, hardness, dimensionally stable, property is gentle, to skin natural no stimulation Property.
Inspection project Unit Standard requirement Assay Single item evaluation
Outward appearance —— The fiber pad pasting of infiltration or gluey shaping pad pasting Light yellow gel is attached on non-woven fabrics It is qualified
PH(25℃) —— 3.5~8.5 5.0 It is qualified
Methanol mg/kg ≤2000 Do not detect It is qualified
Lead mg/kg ≤10 < 1.0 It is qualified
Arsenic mg/kg ≤2 < 0.5 It is qualified
Mercury mg/kg ≤1 < 0.1 It is qualified
Cadmium mg/kg ≤5 < 0.59 It is qualified
Yeast and mold sum CFU/ml ≤100 < 10 It is qualified
Heat-resisting coliform /ml It must not detect Do not detect It is qualified
Staphylococcus aureus group /ml It must not detect Do not detect It is qualified
Pseudomonas aeruginosa /ml It must not detect Do not detect It is qualified
It should be appreciated that the application of the present invention is not limited to above-mentioned citing, for those of ordinary skills, can To be improved or converted according to the above description, all these modifications and variations should all belong to the guarantor of appended claims of the present invention Protect scope.

Claims (10)

1. a kind of Golden flower facial mask, it is characterised in that in parts by weight, its composition of raw materials composition is:
80 ~ 90 parts of water, 0.2 ~ 0.5 part of Hibiscus esculentus L. extract, 0.3 ~ 0.5 part of niacinamide, 0.02 ~ 0.06 part of allantoin, NMF 7 ~ 10 parts, 0.03 ~ 0.1 part of preservative, 0.6 ~ 1.0 part of film forming agent, 0.3 ~ 0.6 part of antioxidant, 0.2 ~ 0.4 part of emulsifying agent, essence 0.01 ~ 0.03 part.
2. Golden flower facial mask according to claim 1, it is characterised in that the NMF is glycerine, butanediol, beet One or more in alkali, propane diols, Sodium Hyaluronate.
3. Golden flower facial mask according to claim 1, it is characterised in that the preservative is methyl hydroxybenzoate, iodine propilolic alcohol It is butyl mephenesin Carbamate, double(Methylol)One or more in imidazolidinyl urea.
4. Golden flower facial mask according to claim 1, it is characterised in that the film forming agent is tara gum.
5. Golden flower facial mask according to claim 1, it is characterised in that the antioxidant is silk glue protein.
6. Golden flower facial mask according to claim 1, it is characterised in that the emulsifying agent is xanthans.
7. the preparation method of a kind of Golden flower facial mask as described in claim 1 ~ 6 is any, it is characterised in that including following step Suddenly:
Hibiscus esculentus L. extract is obtained by extraction;
Water, Hibiscus esculentus L. extract, niacinamide, allantoin, NMF, preservative, film forming agent, anti-is separately added into according to aforementioned proportion Oxidant, emulsifying agent and essence, facial mask liquid is obtained after mixing;
The facial mask liquid is heated to 90 ~ 120 DEG C, 30 ~ 50 DEG C is cooled to after being kept for 30 ~ 40 minutes, obtains facial mask and coagulate Glue;
The facial mask gel is laid into the consistent uniform film of thickness, obtains gel mould;
The gel mould is placed on nylon mesh, Golden flower facial mask is made.
8. the preparation method of Golden flower facial mask according to claim 7, it is characterised in that the Golden flower that is obtained by extraction carries The step of taking thing specifically includes:
Addition deionized water obtains Golden flower suspension after Golden flower raw material is smashed into refinement;
Supercritical CO is carried out to the Golden flower suspension2Extraction, obtains Golden flower extract;
The Golden flower extract is filtered, obtains Hibiscus esculentus L. extract.
9. the preparation method of Golden flower facial mask according to claim 8, it is characterised in that in the Golden flower suspension, The weight ratio of deionized water and Golden flower raw material is 50:1.
10. the preparation method of Golden flower facial mask according to claim 8, it is characterised in that the filtration step is specially: Golden flower extract is filtered using gauze, and in triplicate.
CN201710882890.7A 2017-09-26 2017-09-26 A kind of Golden flower facial mask and preparation method thereof Pending CN107362108A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710882890.7A CN107362108A (en) 2017-09-26 2017-09-26 A kind of Golden flower facial mask and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710882890.7A CN107362108A (en) 2017-09-26 2017-09-26 A kind of Golden flower facial mask and preparation method thereof

Publications (1)

Publication Number Publication Date
CN107362108A true CN107362108A (en) 2017-11-21

Family

ID=60302575

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710882890.7A Pending CN107362108A (en) 2017-09-26 2017-09-26 A kind of Golden flower facial mask and preparation method thereof

Country Status (1)

Country Link
CN (1) CN107362108A (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108524406A (en) * 2018-07-21 2018-09-14 河南中立宝花茶有限公司 A kind of Golden flower facial mask and preparation method thereof
CN110063923A (en) * 2019-06-10 2019-07-30 广州禾安化工有限公司 A kind of anti-inflammatory Shu Min repair latex containing Golden flower
CN110870841A (en) * 2019-12-09 2020-03-10 内蒙古自治区生物技术研究院 Abelmoschus manihot facial mask and preparation method thereof
CN111135129A (en) * 2020-02-24 2020-05-12 林淑娴 After-sun repair composition, preparation method thereof and cosmetic
CN111150696A (en) * 2020-02-24 2020-05-15 林淑娴 After-sun repair emulsion and preparation method thereof
CN113181093A (en) * 2021-04-26 2021-07-30 于长海 Method for preparing and storing fruit and vegetable facial mask
JP7535562B2 (en) 2022-08-24 2024-08-16 オール イン オン カンパニー リミテッド Method for producing cosmetic composition containing extract of Aloesia japonica

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105168038A (en) * 2015-08-14 2015-12-23 武汉狼堡科技有限公司 Aurea helianthus flower mud facial mask and preparation method therefor
CN105853287A (en) * 2016-05-03 2016-08-17 广州暨南生物医药研究开发基地有限公司 Hibiseu Smanihot L. moisturizing essence and preparation method thereof
CN106074238A (en) * 2016-06-14 2016-11-09 广州暨南生物医药研究开发基地有限公司 A kind of golden flower certain herbaceous plants with big flowers whitening and spot eliminating cream and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105168038A (en) * 2015-08-14 2015-12-23 武汉狼堡科技有限公司 Aurea helianthus flower mud facial mask and preparation method therefor
CN105853287A (en) * 2016-05-03 2016-08-17 广州暨南生物医药研究开发基地有限公司 Hibiseu Smanihot L. moisturizing essence and preparation method thereof
CN106074238A (en) * 2016-06-14 2016-11-09 广州暨南生物医药研究开发基地有限公司 A kind of golden flower certain herbaceous plants with big flowers whitening and spot eliminating cream and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
广州市薏莉雅生物技术开发有限公司: "金花葵植物面膜", 《国产非特殊用途化妆品备案服务平台》 *
张建: "金花葵花总黄酮解热抗炎作用的实验研究", 《中国医科大学学报》 *
詹益兴: "《绿色精细化工-天然产品制造法.第3集》", 31 January 2008, 科学技术文献出版社 *

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108524406A (en) * 2018-07-21 2018-09-14 河南中立宝花茶有限公司 A kind of Golden flower facial mask and preparation method thereof
CN110063923A (en) * 2019-06-10 2019-07-30 广州禾安化工有限公司 A kind of anti-inflammatory Shu Min repair latex containing Golden flower
CN110063923B (en) * 2019-06-10 2022-03-11 广州嘉瑜生物科技有限公司 Abelmoschus manihot-containing anti-inflammatory and allergy-relieving repair emulsion
CN110870841A (en) * 2019-12-09 2020-03-10 内蒙古自治区生物技术研究院 Abelmoschus manihot facial mask and preparation method thereof
CN111135129A (en) * 2020-02-24 2020-05-12 林淑娴 After-sun repair composition, preparation method thereof and cosmetic
CN111150696A (en) * 2020-02-24 2020-05-15 林淑娴 After-sun repair emulsion and preparation method thereof
CN111135129B (en) * 2020-02-24 2021-02-05 江苏雪豹日化有限公司 After-sun repair composition, preparation method thereof and cosmetic
CN113181093A (en) * 2021-04-26 2021-07-30 于长海 Method for preparing and storing fruit and vegetable facial mask
JP7535562B2 (en) 2022-08-24 2024-08-16 オール イン オン カンパニー リミテッド Method for producing cosmetic composition containing extract of Aloesia japonica

Similar Documents

Publication Publication Date Title
CN107362108A (en) A kind of Golden flower facial mask and preparation method thereof
KR102057022B1 (en) Cosmetic composition and manufacturing method for the same
KR101562560B1 (en) Natural extract fermentation-maturity composition for preventing skin aging and improving skin wrinkle, Natural cosmetics containing that and Manufacturing method thereof
WO2014117316A1 (en) Multi-function aloe gel and preparation method thereof
CN107496195A (en) A kind of recombined human hyaluronic acid compositions and its application in cosmetics
CN104306262A (en) Beauty mask
KR20140072680A (en) Natural shampoo bar for preventing and treating of scalp and hair, and manufacturing method thereof
CN1682690A (en) Bathing liquid composition and its preparing method
KR101780863B1 (en) Cosmetic Composion for Acne Improvement Containing Butanol Fraction of Red Ginseng Ethanol Extract
CN107684530A (en) Acne-removing composition and preparation method thereof
CN104042529A (en) Anti-allergic cosmetic composition and preparation method thereof
CN106109264B (en) A kind of facial treatment mask and preparation method thereof with anti-bacteria wet keeping function
CN110559229A (en) Night cream containing cannabidiol CBD nano-emulsion and preparation method thereof
CN111973481A (en) Blue ketone peptide repair essence and preparation method thereof
KR101050427B1 (en) Protective and cleansing composition of the scalp and hair including herbal extracts and nutrient capsules
CN105534869A (en) Preparation method for anti-ultraviolet silk fibroin
CN107519118A (en) A kind of snake gall eye mask and preparation method thereof
CN115154343B (en) Composition and preparation for improving eye relaxation and black eye, preparation method and application
KR101736478B1 (en) Method for manufacturing lotions with effective in treating acne
CN111973544A (en) Carnosine firming lifting mask and preparation method thereof
CN108309840A (en) A kind of profession repair membrane facial mask liquid and preparation method thereof
KR100807842B1 (en) Anti-fungal composition for deodorization
CN107397712A (en) A kind of snake gall facial mask and preparation method thereof
CN107569417A (en) Antipruritic emulsion of the elderly's skin care and preparation method thereof
KR102062822B1 (en) Functional soap containing a composition to prevent hair loss and manufacturing method of the same

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20171121