CN105853287A - Hibiseu Smanihot L. moisturizing essence and preparation method thereof - Google Patents

Hibiseu Smanihot L. moisturizing essence and preparation method thereof Download PDF

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CN105853287A
CN105853287A CN201610289216.3A CN201610289216A CN105853287A CN 105853287 A CN105853287 A CN 105853287A CN 201610289216 A CN201610289216 A CN 201610289216A CN 105853287 A CN105853287 A CN 105853287A
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extract
parts
hibiscus
flos osmanthi
osmanthi fragrantis
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CN105853287B (en
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王飞
王一飞
王林涛
王闯
马婧
王巧利
任哲
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Guangzhou Jinan Biomedicine Research and Development Base Co Ltd
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Guangzhou Jinan Biomedicine Research and Development Base Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

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Abstract

The invention belongs to the technical field of cosmetics and particularly relates to Hibiseu Smanihot L. moisturizing essence and a preparation method thereof. The moisturizing essence is prepared from 6-8 parts of Hibiseu Smanihot L. extracts, 1-3 parts of sweet osmanthus extracts, 0.5-1 part of terminalia ferdinandiana extracts, 4-8 parts of butanediol, 0.1-0.3 part of carbomer, 1-4 part of propylene glycol, 0.1-0.2 part of sodium hyaluronate, 1-2 parts of xylitol, 1-2 parts of milk protein, 0.1-0.3 part of triethanolamine, 0.3-0.5 part of phenoxyethanol and 70-90 parts of water. The moisturizing essence is easy to absorb, safe, free of irritation and good in moisturizing and moisture retention effect.

Description

A kind of Hibiscus manihot L. moisturizing essence and preparation method thereof
Technical field
The invention belongs to cosmetic technical field, be specifically related to a kind of Hibiscus manihot L. moisturizing essence and preparation method thereof.
Background technology
Hibiscus manihot L. (formal name used at school: Hibiseu Smanihot L.), has another name called vegetable Furong, and the wildest Hibisci Mutabilis, is annual Draft Malvaceae Abelmoschus plant.Flower of Hibiscus manihot L dietotherapeutic, Compendium of Material Medica records the medicinal valency of Abelmoschus manihot (L.) Medic Value, energy heat clearing away, removing heat from blood, removing toxic substances, it spends nontoxic, has effect of eliminating damp-heat, anti-inflammatory analgesic, for oral administration main Controlling five types of stranguria, edema, external curing soup is scalded.Modern medicine study shows, the total flavones of Hibiscus manihot L. have analgesia, Anti-cerebral ischemia and the treatment effect such as oral ulcer, complete protein contained by it, high polysaccharide glue, dietary fiber, micro- Secondary element selenium, zinc, multiple non-saponifiable matter etc., have and significantly regulate human endocrine, immunity, increases human body Drag, improves cardiovascular and cerebrovascular vessel and microcirculation function, enhancing body oxidation resistance, anti-cardiac-cerebral ischemia, anoxia, Antiinflammatory, town pain, resisting fatigue, defying age, anticancer, anti-cancer, blood fat reducing function.Hibiscus manihot L. has well guarantor Strong effect, so Hibiscus manihot L. uses mainly as health product at present, such as golden flower sunflower health tea, Abelmoschus manihot health care mouth Take liquid, capsule etc..
But in terms of eating and be medicinal, use Hibiscus manihot L. the most merely, greatly limit its use value.Gold In tree mallow, active component is numerous, can be applicable in cosmetics.As Chinese patent application CN 105168038A is public Opened a kind of Hibiscus manihot L. flower clay mask, its contain Hibiscus manihot L. flower, Fructus Luffae flower, propylene glycol, carbomer, Triethanolamine, citral etc., it has maintenance elasticity of skin, antioxidation and whitening effect, but it uses Hibiscus manihot L. flower, Fructus Luffae flower can not fully disengage effect as functional raw material, the effective ingredient in Hibiscus manihot L., Skin effect is the best.Through retrieval, rarely has Hibiscus manihot L. application in moisturizing class cosmetics.
To sum up, it is necessary to a kind of Hibiscus manihot L. moisturizing essence of research and development, the abundantest Hibiscus manihot L. application and Its use value, on the other hand also meets the demand of people, provides a kind of new, effective replenishing water and preserving moisture for people Essence.
Summary of the invention
In order to overcome the deficiencies in the prior art, it is an object of the invention to provide a kind of Hibiscus manihot L. moisturizing essence, Its gentle pro-skin, easily absorbs, and safe and non-stimulating, replenishing water and preserving moisture effect is good.
To achieve these goals, technical scheme is as follows:
A kind of Hibiscus manihot L. moisturizing essence, including the component of following weight portion: Hibiscus esculentus L. extract 6~8 parts, osmanthus Flower extract 1~3 parts, method ground Terminalia catappa berry extract 0.5~1 part, butanediol 4~8 parts, carbomer 0.1~0.3 Part, propylene glycol 1~4 parts, hyaluronate sodium 0.1~0.2 part, xylitol 1~2 parts, milk protein 1~2 parts, Triethanolamine 0.1~0.3 part, phenoxyethanol 0.3~0.5 part and water 70~90 parts.
Further, described Hibiscus esculentus L. extract is prepared by following methods: takes dry Hibiscus manihot L., adds it heavy The water of amount 4~6 times amount, heating and refluxing extraction 2~3 hours, to filter, filtrate is at vacuum-concentrcted to 60 DEG C Lower relative density is the extractum of 1.10~1.25, obtains Hibiscus esculentus L. extract.
Further, described Flos Osmanthi Fragrantis extract is prepared by following methods: take dry Flos Osmanthi Fragrantis, adds its weight The water of 4~6 times amount, heating and refluxing extraction 2~3 hours, to filter, filtrate is phase at vacuum-concentrcted to 60 DEG C To the extractum that density is 1.10~1.25, obtain Flos Osmanthi Fragrantis extract.
As the preferred embodiment of the present invention, described Hibiscus manihot L. moisturizing essence is by the component group of following weight portion Become: Hibiscus esculentus L. extract 8 parts, Flos Osmanthi Fragrantis extract 2 parts, method ground Terminalia catappa berry extract 1 part, butanediol 6 Part, carbomer 0.1 part, propylene glycol 2 parts, hyaluronate sodium 0.1 part, xylitol 2 parts, milk protein 1 Part, triethanolamine 0.1 part, phenoxyethanol 0.4 part and 77.3 parts of water.
Accordingly, present invention also offers the preparation method of above-mentioned Hibiscus manihot L. moisturizing essence, specifically include following Step:
S1, the preparation of Hibiscus esculentus L. extract: take dry Hibiscus manihot L., add the water of its weight 4~6 times amount, add Circumfluence distillation 2~3 hours, filter, and filtrate relative density at vacuum-concentrcted to 60 DEG C is 1.10~1.25 Extractum, obtain Hibiscus esculentus L. extract;
S2, the preparation of Flos Osmanthi Fragrantis extract: take dry Flos Osmanthi Fragrantis, add the water of its weight 4~6 times amount, heat back Stream extracts 2~3 hours, filters, and filtrate relative density at vacuum-concentrcted to 60 DEG C is 1.10~1.25 Extractum, obtains Flos Osmanthi Fragrantis extract;
S3, weighing the butanediol of formula ratio, carbomer, propylene glycol, hyaluronate sodium and water, mixing, while stir Mix limit and be heated to 40~45 DEG C, be incubated 10 minutes, obtain mixture;
S4, in described mixture, add the xylitol of formula ratio, Hibiscus esculentus L. extract, Flos Osmanthi Fragrantis extract, method Ground Terminalia catappa berry extract, milk protein, phenoxyethanol and triethanolamine, stir, get final product discharging, prepares Hibiscus manihot L. moisturizing essence.
In the inventive solutions, under certain condition, prepared Hibiscus esculentus L. extract is extracted as main work With composition, it is effectively skin replenishing water and preserving moisture, improves dry, coarse skin condition;Again with under certain condition extract The Flos Osmanthi Fragrantis extract prepared and existing method ground Terminalia catappa berry extract compound, and further promote replenishing water and preserving moisture Effect, and degree of depth lock water, long-acting moisturizing;In conjunction with milk protein, butanediol, carbomer, propylene glycol, The adjuvant such as hyaluronate sodium, xylitol so that Hibiscus manihot L. moisturizing essence of the present invention is easily absorbed by the skin, and makes Clearly do not stick greasy with rear, make skin beauty water profit smooth.
Therefore, compared with prior art, present invention have an advantage that
(1) Hibiscus manihot L. moisturizing essence of the present invention contains Hibiscus esculentus L. extract, Flos Osmanthi Fragrantis extract, method ground Terminalia catappa Deng abundant plant extraction composition, skin bottom can be goed deep into and keeps the skin wet quickly by skin overall absorption and lock simultaneously Water, hence it is evident that improve and be dried coarse skin condition, replenishing water and preserving moisture effect is obvious, makes skin water tender smooth, is rich in elastic force.
(2) each component of Hibiscus manihot L. moisturizing essence of the present invention is worked in coordination with, and replenishing water and preserving moisture is effective, and safety is stingless Swashing, stable system, the preparation method of Hibiscus manihot L. moisturizing essence the most of the present invention is simple, process stabilizing, it is simple to Implement, can industrialized production, beneficially popularization and application.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following example. Within the scope of the invention or without departing from present disclosure, spirit and scope, to gold of the present invention Tree mallow moisturizing essence carries out being suitably modified, replacing the component that effect is identical, to those skilled in the art Being apparent from, they are considered as being included within the scope of the present invention.
The ground of method described in embodiment of the present invention Terminalia catappa berry extract is purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd, goods Number it is PW1331PG0247.
Described milk protein is purchased from You Ran bio tech ltd, Guangzhou, and article No. is Y15728.
Embodiment 1, Hibiscus manihot L. moisturizing essence of the present invention
Formula: Hibiscus esculentus L. extract 6kg, Flos Osmanthi Fragrantis extract 1kg, method ground Terminalia catappa berry extract 1kg, fourth two Alcohol 4kg, carbomer 0.3kg, propylene glycol 4kg, hyaluronate sodium 0.1kg, xylitol 1kg, milk protein 2kg, triethanolamine 0.1kg, phenoxyethanol 0.3kg and water 80.2kg.
Described Hibiscus esculentus L. extract is prepared by following methods: take dry Hibiscus manihot L., adds its weight 4 times amount Water, heating and refluxing extraction 3 hours, filter, filtrate relative density at vacuum-concentrcted to 60 DEG C is 1.10 Extractum, obtain Hibiscus esculentus L. extract.
Described Flos Osmanthi Fragrantis extract is prepared by following methods: take dry Flos Osmanthi Fragrantis, adds the water of its weight 4 times amount, Heating and refluxing extraction 3 hours, filters, and filtrate relative density at vacuum-concentrcted to 60 DEG C is 1.10 Extractum, obtains Flos Osmanthi Fragrantis extract.
Preparation method:
S1, the preparation of Hibiscus esculentus L. extract: take dry Hibiscus manihot L., add the water of its weight 4 times amount, heating Reflux, extract, 3 hours, filters, and filtrate relative density at vacuum-concentrcted to 60 DEG C is the extractum of 1.10, Obtain Hibiscus esculentus L. extract;
S2, the preparation of Flos Osmanthi Fragrantis extract: take dry Flos Osmanthi Fragrantis, add the water of its weight 4 times amount, be heated to reflux Extracting 3 hours, filter, filtrate relative density at vacuum-concentrcted to 60 DEG C is the extractum of 1.10, To Flos Osmanthi Fragrantis extract;
S3, weighing the butanediol of formula ratio, carbomer, propylene glycol, hyaluronate sodium and water, mixing, while stir Mix limit and be heated to 40 DEG C, be incubated 10 minutes, obtain mixture;
S4, in described mixture, add the xylitol of formula ratio, Hibiscus esculentus L. extract, Flos Osmanthi Fragrantis extract, method Ground Terminalia catappa berry extract, milk protein, phenoxyethanol and triethanolamine, stir, get final product discharging, prepares Hibiscus manihot L. moisturizing essence.
Embodiment 2, Hibiscus manihot L. moisturizing essence of the present invention
Formula: Hibiscus esculentus L. extract 7kg, Flos Osmanthi Fragrantis extract 3kg, method ground Terminalia catappa berry extract 0.5kg, fourth two Alcohol 8kg, carbomer 0.1kg, propylene glycol 1kg, hyaluronate sodium 0.2kg, xylitol 2kg, milk protein 1kg, triethanolamine 0.3kg, phenoxyethanol 0.5kg and water 76.4kg.
Described Hibiscus esculentus L. extract is prepared by following methods: take dry Hibiscus manihot L., adds its weight 6 times amount Water, heating and refluxing extraction 2 hours, filter, filtrate relative density at vacuum-concentrcted to 60 DEG C is 1.25 Extractum, obtain Hibiscus esculentus L. extract.
Described Flos Osmanthi Fragrantis extract is prepared by following methods: take dry Flos Osmanthi Fragrantis, adds the water of its weight 6 times amount, Heating and refluxing extraction 2 hours, filters, and filtrate relative density at vacuum-concentrcted to 60 DEG C is 1.25 Extractum, obtains Flos Osmanthi Fragrantis extract.
Preparation method:
S1, the preparation of Hibiscus esculentus L. extract: take dry Hibiscus manihot L., add the water of its weight 6 times amount, heating Reflux, extract, 2 hours, filters, and filtrate relative density at vacuum-concentrcted to 60 DEG C is the extractum of 1.25, Obtain Hibiscus esculentus L. extract;
S2, the preparation of Flos Osmanthi Fragrantis extract: take dry Flos Osmanthi Fragrantis, add the water of its weight 6 times amount, be heated to reflux Extracting 2 hours, filter, filtrate relative density at vacuum-concentrcted to 60 DEG C is the extractum of 1.25, To Flos Osmanthi Fragrantis extract;
S3, weighing the butanediol of formula ratio, carbomer, propylene glycol, hyaluronate sodium and water, mixing, while stir Mix limit and be heated to 45 DEG C, be incubated 10 minutes, obtain mixture;
S4, in described mixture, add the xylitol of formula ratio, Hibiscus esculentus L. extract, Flos Osmanthi Fragrantis extract, method Ground Terminalia catappa berry extract, milk protein, phenoxyethanol and triethanolamine, stir, get final product discharging, prepares Hibiscus manihot L. moisturizing essence.
Embodiment 3, Hibiscus manihot L. moisturizing essence of the present invention
Formula: Hibiscus esculentus L. extract 8kg, Flos Osmanthi Fragrantis extract 2kg, method ground Terminalia catappa berry extract 1kg, fourth two Alcohol 6kg, carbomer 0.1kg, propylene glycol 2kg, hyaluronate sodium 0.1kg, xylitol 2kg, milk protein 1kg, triethanolamine 0.1kg, phenoxyethanol 0.4kg and water 77.3kg.
Described Hibiscus esculentus L. extract is prepared by following methods: take dry Hibiscus manihot L., adds its weight 5 times amount Water, heating and refluxing extraction 2.5 hours, filter, filtrate relative density at vacuum-concentrcted to 60 DEG C is The extractum of 1.20, obtains Hibiscus esculentus L. extract.
Described Flos Osmanthi Fragrantis extract is prepared by following methods: take dry Flos Osmanthi Fragrantis, adds the water of its weight 5 times amount, Heating and refluxing extraction 2.5 hours, filters, and filtrate relative density at vacuum-concentrcted to 60 DEG C is 1.20 Extractum, obtain Flos Osmanthi Fragrantis extract.
Preparation method:
S1, the preparation of Hibiscus esculentus L. extract: take dry Hibiscus manihot L., add the water of its weight 5 times amount, heating Reflux, extract, 2.5 hours, filters, and filtrate relative density at vacuum-concentrcted to 60 DEG C is the leaching of 1.20 Cream, obtains Hibiscus esculentus L. extract;
S2, the preparation of Flos Osmanthi Fragrantis extract: take dry Flos Osmanthi Fragrantis, add the water of its weight 5 times amount, be heated to reflux Extracting 2.5 hours, filter, filtrate relative density at vacuum-concentrcted to 60 DEG C is the extractum of 1.20, Obtain Flos Osmanthi Fragrantis extract;
S3, weighing the butanediol of formula ratio, carbomer, propylene glycol, hyaluronate sodium and water, mixing, while stir Mix limit and be heated to 40 DEG C, be incubated 10 minutes, obtain mixture;
S4, in described mixture, add the xylitol of formula ratio, Hibiscus esculentus L. extract, Flos Osmanthi Fragrantis extract, method Ground Terminalia catappa berry extract, milk protein, phenoxyethanol and triethanolamine, stir, get final product discharging, prepares Hibiscus manihot L. moisturizing essence.
The Hibiscus manihot L. moisturizing essence of embodiment 1~3 is done testing performance index, and its test result is as follows:
1, outward appearance: semi-transparent flowing
2, pH value: 5.5~6.5
3, viscosity: 2,#12 1500~2500mpa
4, heat-resistant stability investigates (48 DEG C × 24h): qualified
5, cold-resistant study on the stability (-15 DEG C × 24h): qualified
Comparative example 1,
Compared with Example 3, the difference of this comparative example is: without Flos Osmanthi Fragrantis extract and method ground Terminalia catappa fruit Extract, the consumption of Hibiscus esculentus L. extract is 11kg.Preparation method reference example 3.
Comparative example 2,
Compared with Example 3, the formula of this comparative example is: Hibiscus esculentus L. extract 8kg, Flos Osmanthi Fragrantis extract 2kg, Method ground Terminalia catappa berry extract 1kg, butanediol 6kg, carbomer 1.1kg, propylene glycol 2kg, hyaluronate sodium 1.1kg, Triethanolamine 1.1kg, phenoxyethanol 0.4kg and water 77.3kg.Preparation method reference example 3.
Comparative example 3,
The formula of this comparative example is same as in Example 3, except for the difference that step S1 in the preparation method of this comparative example, The preparation of Hibiscus esculentus L. extract: take dry Hibiscus manihot L., the volume fraction adding its weight 5 times amount is 70% Ethanol, heating and refluxing extraction 2.5 hours, filter, filtrate is relative density at vacuum-concentrcted to 60 DEG C It is the extractum of 1.20, obtains Hibiscus esculentus L. extract;Step S2~S4 reference example 3.
Test example, product effect assessment
Part I:
One, trial target: the moisturizing essence that embodiment 1~3, comparative example 1~3 prepare
Two, tested crowd
Sex number: female, 60 people
Age: between 20~50 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Packet: be divided into 6 groups, often organize 10 people.
Three, method of testing: often group experimenter tries out above-mentioned trial target 2 days respectively, the most each use is once.The One day use before use Fes Kai Er SK-III skin moisture detector test respectively forehead, left face, right face and under The moisture of bar skin, and take arithmetic mean of instantaneous value;The 3rd day morning in the case of not using essence, then Test forehead, left face, right face and the skin moisture content of chin same location with skin moisture tester, and take Arithmetic mean of instantaneous value.Often the result tested is taken arithmetic mean of instantaneous value by 10 experimenters of group.
Four, test result such as table 1 below:
Table 1 skin moisture content test result table
From upper table 1:
(1) the moisturizing effect of the embodiment of the present invention 1~3 Hibiscus manihot L. moisturizing essence is notable, 2 days on probation, is subject to Examination person's skin moisture content increases, and uses skin average moisture difference > 5% before and after essence, is also superior to comparative example 1~3, wherein with the moisturizing best results of embodiment 3, before and after using essence, skin average moisture difference reaches 6.3%.
(2) comparative example 1 is without Flos Osmanthi Fragrantis extract and method ground Terminalia catappa berry extract, and comparative example 2 is without xylitol And milk protein, comparative example 3 uses ethanol solution to extract the Hibiscus esculentus L. extract obtained, its replenishing water and preserving moisture effect All not as embodiment 1~3.
Part II:
One, trial target: the moisturizing essence that embodiment 1~3, comparative example 1~3 prepare
Two, tested crowd
Sex number: female, 180 people
Age: between 20~50 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Packet: be divided into 6 groups, often organizes 30 people, often 34 ± 1 years old mean age of group.
Three, method of testing: often group experimenter tries out above-mentioned trial target two weeks respectively, the most each use is once.
Four, result of the test: test assessment result is as follows:
(two weeks) on probation feedback conclusive table of table 2 embodiment 1 Hibiscus manihot L. moisturizing essence
(two weeks) on probation feedback conclusive table of table 3 embodiment 2 Hibiscus manihot L. moisturizing essence
(two weeks) on probation feedback conclusive table of table 4 embodiment 3 Hibiscus manihot L. moisturizing essence
(two weeks) on probation feedback conclusive table of table 5 comparative example 1 essence
(two weeks) on probation feedback conclusive table of table 6 comparative example 2 essence
(two weeks) on probation feedback conclusive table of table 7 comparative example 3 essence
From upper table 2~7, the degree of recognition of the Hibiscus manihot L. moisturizing essence of the embodiment of the present invention 1~3 is high, wherein The degree of recognition of embodiment 3 Hibiscus manihot L. moisturizing essence is the highest.Experimenter all represents, Hibiscus manihot L. moisturizing of the present invention essence China's liquid, easily by percutaneous absorption, does not clearly stick greasy after using, replenishing water and preserving moisture is effective, substantially feels after using two weeks Feel that skin becomes water tender smooth, significantly improve scaly dry skin, the situation such as coarse, obscure.Experimenter simultaneously Questionnaire there is not people the bad phenomenon such as allergy, red swelling of the skin occurs.
Comparative example 1 is without Flos Osmanthi Fragrantis extract and method ground Terminalia catappa berry extract, and comparative example 2 is without xylitol and milk Albumen, comparative example 3 uses ethanol solution to extract the Hibiscus esculentus L. extract obtained, and its using effect is all not as good as implementing Example 1~3.
The principle of above-described embodiment only illustrative present invention and effect thereof, not for limiting the present invention.Appoint Above-described embodiment all can be repaiied by what those skilled in the art under the spirit and the scope of the present invention Decorations or change.Therefore, art has usually intellectual such as without departing from disclosed All equivalences completed under spirit and technological thought are modified or change, and must be contained by the claim of the present invention Lid.

Claims (5)

1. a Hibiscus manihot L. moisturizing essence, it is characterised in that include the component of following weight portion: Hibiscus manihot L. Extract 6~8 parts, Flos Osmanthi Fragrantis extract 1~3 parts, method ground Terminalia catappa berry extract 0.5~1 part, butanediol 4~8 parts, Carbomer 0.1~0.3 part, propylene glycol 1~4 parts, hyaluronate sodium 0.1~0.2 part, xylitol 1~2 parts, cattle Milk proem 1~2 parts, triethanolamine 0.1~0.3 part, phenoxyethanol 0.3~0.5 part and water 70~90 parts.
2. Hibiscus manihot L. moisturizing essence as claimed in claim 1, it is characterised in that described Hibiscus esculentus L. extract Prepared by following methods: take dry Hibiscus manihot L., add the water of its weight 4~6 times amount, heating and refluxing extraction 2~3 hours, filtering, filtrate relative density at vacuum-concentrcted to 60 DEG C is the extractum of 1.10~1.25, Obtain Hibiscus esculentus L. extract.
3. as claimed in claim 1 Hibiscus manihot L. moisturizing essence, it is characterised in that described Flos Osmanthi Fragrantis extract by Following methods prepares: takes dry Flos Osmanthi Fragrantis, adds the water of its weight 4~6 times amount, heating and refluxing extraction 2~3 Hour, filtering, filtrate relative density at vacuum-concentrcted to 60 DEG C is the extractum of 1.10~1.25, obtains Flos Osmanthi Fragrantis extract.
4. Hibiscus manihot L. moisturizing essence as claimed in claim 1, it is characterised in that by the group of following weight portion It is grouped into: Hibiscus esculentus L. extract 8 parts, Flos Osmanthi Fragrantis extract 2 parts, method ground Terminalia catappa berry extract 1 part, butanediol 6 parts, carbomer 0.1 part, propylene glycol 2 parts, hyaluronate sodium 0.1 part, xylitol 2 parts, milk protein 1 Part, triethanolamine 0.1 part, phenoxyethanol 0.4 part and 77.3 parts of water.
5. preparing a method for Hibiscus manihot L. moisturizing essence as described in Claims 1 to 4 is arbitrary, its feature exists In, comprise the following steps:
S1, the preparation of Hibiscus esculentus L. extract: take dry Hibiscus manihot L., add the water of its weight 4~6 times amount, add Circumfluence distillation 2~3 hours, filter, and filtrate relative density at vacuum-concentrcted to 60 DEG C is 1.10~1.25 Extractum, obtain Hibiscus esculentus L. extract;
S2, the preparation of Flos Osmanthi Fragrantis extract: take dry Flos Osmanthi Fragrantis, add the water of its weight 4~6 times amount, heat back Stream extracts 2~3 hours, filters, and filtrate relative density at vacuum-concentrcted to 60 DEG C is 1.10~1.25 Extractum, obtains Flos Osmanthi Fragrantis extract;
S3, weighing the butanediol of formula ratio, carbomer, propylene glycol, hyaluronate sodium and water, mixing, while stir Mix limit and be heated to 40~45 DEG C, be incubated 10 minutes, obtain mixture;
S4, in described mixture, add the xylitol of formula ratio, Hibiscus esculentus L. extract, Flos Osmanthi Fragrantis extract, method Ground Terminalia catappa berry extract, milk protein, phenoxyethanol and triethanolamine, stir, get final product discharging, prepares Hibiscus manihot L. moisturizing essence.
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CN107550800A (en) * 2017-10-24 2018-01-09 广东芭薇生物科技股份有限公司 A kind of multi-faceted lightening compositions and its application
CN108478486A (en) * 2018-05-08 2018-09-04 紫阳县硒资源开发研究所 A kind of Golden flower active material extraction process
CN115517304A (en) * 2021-06-24 2022-12-27 杭州同界茶叶有限公司 Preparation method of osmanthus fragrans black tea
CN117442534A (en) * 2023-12-14 2024-01-26 广州嘉瑜生物科技有限公司 Abelmoschus manihot extract, preparation method thereof and application thereof in preparing skin care product
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