CN105168038B - Golden flower flower clay mask and preparation method thereof - Google Patents
Golden flower flower clay mask and preparation method thereof Download PDFInfo
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- CN105168038B CN105168038B CN201510501229.8A CN201510501229A CN105168038B CN 105168038 B CN105168038 B CN 105168038B CN 201510501229 A CN201510501229 A CN 201510501229A CN 105168038 B CN105168038 B CN 105168038B
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Abstract
The invention discloses a kind of Golden flower flower clay mask, each component raw material percentage composition is as follows：Golden flower flower：20~30%, sponge gourd flower：20~30%, propylene glycol：5~8%, carbomer：0.3~0.7%, triethanolamine：1.0~1.5%, EUXYL K300：0.05~0.1%, citral：0.002~0.005%, surplus grows water for luffa vine.The preparation method of the facial mask includes the following steps：1) luffa vine grows water sterilization, filtering for use；2) flower crushing, stirring is for use into muddy；3) carbomer luffa vine is grown water-swellable；4) carbomer gel matrix is prepared；5) it after citral being dissolved in propylene glycol, adds in luffa vine and grows water, obtain solution I；6) solution I and flower slurries are added in gel-type vehicle, add EUXYL K300, be uniformly mixed and both obtain Golden flower flower clay mask.The facial mask has whitening, moisture-keeping efficacy, and without side-effects.
Description
Technical field
The invention belongs to a kind of plant clay mask of cosmetic technical field, more particularly to a kind of Golden flower flower mud face
Film and preparation method thereof.
Background technology
Facial mask is pasted on to external therapy of the way derived from drug of face, is one of common cosmetic skin care methods.It uses
After facial mask, skin seems salubrious smooth, pure white delicacy, this is because facial mask can generate affinity with skin, with face after coating
The gradual drying of film, face temperature raising, blood circulation are accelerated, and skin-tightening and tension are strengthened, the sebum of skin secretion
With moisture reverse osmosis in cuticula, unfold epidermal cell softness, pore instinct is opened, and the active ingredient in facial mask penetrates into skin quilt
It is absorbed.Again since facial mask can be tightly affixed with skin, when understanding facial mask, deep layer is dirty in the aging cutin, pore on skin
Dirt is stripped under band, makes skin pure and fresh clean.At present, it is more using the facial mask of minerals as facial mask mud excipient in the market, but
Have no by the use of the slurries of Golden flower flower and sponge gourd flower as excipient and manufactured using luffa vine taste water as preparation solvent
Facial mask.
Golden flower is once in Ming Dynasty constitution ancestor between change year《Shuande mansion will》Described in be Shuande mansion specialty plant.1984
Year, extinction plant is confirmed as by living nature when not finding Golden flower during National Agricultural resource investigation.In August, 2003, Chinese agriculture
Ke Yuan research institutes find Golden flower for the first time in Qiu Xian in Hebei, because of its peculiar biological effect, at home and abroad flowers, food rapidly
The markets such as product, medicine, health products and chemical circles cause strong repercussion.Golden Golden flower also known as vegetable Furong, golden lotus, are annual
Herbaceous plant is Malvaceae, is belonged to sunset abelmoschus root.Its taste trembles with fear, is sweet, is nontoxic, and the general florescence, every plant bloomed 30~60 in 7~September
Piece, for flower as large as bowl, corolla is golden yellow.Flower of JINHUAKUI dietotherapeutic,《Compendium of Materia Medica》Record its energy heat-clearing, cool blood, removing toxic substances, nothing itself
Poison.For oral administration to cure mainly five leaching, oedema, external application can control soup scald.《It is good to help book on Chinese herbal medicine》All malignant sores can be controlled by recording it.
Modern technologies are analyzed, and glycosides displayed, complete protein, high glycan glue, dietary fiber, micro is contained in Golden flower flower
Elemental selenium, zinc, a variety of unsaponifiable matter etc..Have it is demonstrated experimentally that natural flavone content is contour more tens of than ginkgo, soybean in flower of JINHUAKUI
Times, with heat-clearing, dampness removing, anti-inflammatory, removing toxic substances, analgesia and other effects；The Proteinaceous knot of vitamin E energy stabilizing cell membrane contained by it
Structure promotes the normal development of muscle and keeps the elasticity of skin, and vitamin E directly can help skin to fight after entering Skin Cell
The infringement of free radical, ultraviolet light and pollutant prevents skin because some are chronic or when stealthy injury follows the string until aging.
Some document reports, the total flavone glucoside extract of Golden flower have tyrosinase activity apparent inhibiting effect, and tyrosinase is
A kind of main enzyme during melanin generates, when its activity inhibited, the ability that melanocyte generates melanin will be corresponding
It reduces, that is, achievees the effect that whitening.
In conclusion with the facial mask that raw material is wanted based on Golden flower flower to make, have and maintain elasticity of skin, skin is helped to resist
The skin-care effects such as oxidation, anti-aging and promotion whitening.
Luffa cucurbitaceous plant, sweet in flavor mild-natured, sponge gourd flower contains there are many amino acid, and there is clearing heat and detoxicating, anti-inflammatory to rush down
Fire, only sore-throat disappear tired the effects that quenching the thirst.Contain β-paddy Zi alcohol, oleanolic acid and Luffa saponin in its male flower.Oleanolic acid has
There is whitening function, Luffa saponin has acquisition, consolidation and the reproduction effect promoted longevity, promote memory, can moisturizing, treatment
Scald etc..β-paddy Zi alcohol is other than it can reduce the total cholesterol level in blood, also with anti-inflammatory, inhibition tumour, inhibition mammary gland
The effects that hyperplasia and adjusting immune system.
In conclusion it is that the facial mask that primary raw material makes has the anti-inflammatory of help skin, the fat anti-acne that disappears, suppression with sponge gourd flower flower
The effects that skin neoplasin processed and whitening.
Luffa vine grows water also known as loofah bleeding sap, day Luo Shui etc., and luffa vine, which is grown, to be contained natural moisturizing factor, lets out root in water
Acid, catalase, superoxide dismutase, multiple-microorganism and trace element can supplement moisture of skin, remove extra freedom
Base, inhibiting bacteria and diminishing inflammation, the activity etc. for inhibiting tyrosinase help to moisturize the skin, whitening and anti-oxidant.Luffa vine is grown water and is contained
98.7~99.3% moisture.Result of study shows that luffa vine grows water and has the excellent skin-care effects such as moisturizing, whitening.In addition, its
Have enough moisture, it can be as the solvent for preparing facial mask.
General Chinese herbal medicine facial mask is mostly powder face pack, i.e., Chinese herbal medicine is pulverized and sieved packing, faces the used time and is tuned into water
Pulpous state is coated on face.Such facial mask usually easily blocks pore, is not easy to clean completely.In addition, some in Chinese herbal medicine have
Effect ingredient cannot dissolve dispersion when without emulsification treatment well, therefore cannot play its due skin care effect.
Invention content
Present invention aim to overcome above-mentioned the shortcomings of the prior art, a kind of Golden flower flower clay mask is provided
And preparation method thereof, have and maintain elasticity of skin, help anti-oxidant skin, anti-aging and promote the skin-care effects such as whitening.
To achieve the above object, the technical proposal of the invention is realized in this way：A kind of Golden flower flower clay mask, it leads
It to be prepared by the raw material of following weight percent, the weight percent of wherein each component raw material is as follows：
Golden flower flower：20~30%, sponge gourd flower：20~30%, propylene glycol：5~8%, carbomer：0.3~
0.7%th, triethanolamine：1.0~1.5%, EUXYL K300：0.05~0.1%, citral：0.002~0.005%, surplus is
Luffa vine grows water.
Preferably, the facial mask is mainly prepared by the raw material of following weight percent, and wherein each component is former
The weight percent of material is as follows：
Golden flower flower：22~25%, sponge gourd flower：22~25%, propylene glycol：5~8%, carbomer：0.3~
0.5%th, triethanolamine：1.0~1.5%, EUXYL K300：0.05~0.1%, citral：0.002~0.005%, surplus is
Luffa vine grows water.
Scheme more preferably, the facial mask are mainly prepared by the raw material of following weight percent, wherein each component
The weight percent of raw material is as follows：
Golden flower flower：22.5%th, sponge gourd flower：22.5%th, propylene glycol：5%th, carbomer：0.5%th, triethanolamine：
1.5%th, EUXYL K300：0.05%th, citral：0.004%, surplus grows water for luffa vine.
Preferably, the carbomer is carbomer U20.Carbomer U20 is acrylate and alkyl acrylate
Cross-linked copolymer, have the function of thickening, suspension, stable emulsion system, regulation and control water and active material release etc., it can increase
The consistency of flower slurries makes facial mask show ideal figuration effect, and coated on face when is unlikely to drip, flow etc. existing
As；Flower of JINHUAKUI, sponge gourd flower can be grown the active ingredient rapid dispersion in water around luffa vine and be suspended in gel-type vehicle by it,
Face is uniformly distributed in everywhere, so as to generate the slim and graceful organoleptic properties for sprawling sense and salubrious sense, effectively improving facial mask.
The preparation method of above-mentioned Golden flower flower clay mask, includes the following steps：
1) it after luffa vine being grown water by ultraviolet ray sterilizer disinfection and filter filtering, is placed in disinfecting container for use；
2) by Golden flower flower and sponge gourd flower crushing, stirring into muddy, for use；
3) carbomer is grown water with step 1) treated luffa vine to be fully swollen, stands overnight；
4) triethanolamine is added in the carbomer solution of swelling that step 3) obtains, stirs to get clear gel base
Matter；
5) it after citral being dissolved in propylene glycol, adds in step 1) treated luffa vine and grows in water, obtain solution I；
6) flower slurries made from solution I made from step 5) and step 2) are added to gel-type vehicle made from step 4)
In, then lower addition EUXYL K300 are being stirred continuously, it is uniformly mixed and both obtains Golden flower flower clay mask.
Preferably, the filter core precision of the filter used in the step 1) is 0.2 μm.
Preferably, luffa vine taste water is previously heated to 50~60 DEG C used in the step 3)
The present invention selects triethanolamine that carbomer resin molecule is made to obtain significant expansion stretching, extension, so as to increase the thick of system
Degree, while facial mask is made to keep faintly acid pH=6.3~6.8, ensure the skin effect of facial mask.
The present invention selects propylene glycol, and propylene glycol is efficient moisture-retention agent, emulsifier, stabilizer and dermal osmosis accelerator, it
It can make during a variety of volatile oil in Golden flower flower and sponge gourd flower are preferably soluble in the aqueous phase；It can delay flower and luffa vine
Some ingredients hydrolysis in water is grown, increases its stability；Propylene glycol also has moisture-keeping function, and facial mask can be made to be protected in long-term storage
Not drying shrinkage is held, there is good infiltration function, the active constituent that flower and luffa vine are grown in water can be guided and penetrate into skin in a larger amount
Among skin, enhance skin-protecting function.
The citral system fruit type food flavor that the present invention selects can have product of the present invention and make us salubrious suitable sense
Official's effect.
The EUXYL K300 systems compounding component preservative that the present invention selects.EUXYL K300 by Phenoxyethanol, methyl hydroxybenzoate,
Several in butyl hydroxybenzoate, ethyl hydroxy benzoate, Nipasol, oxybenzene isobutyl ester compound, commercially available.Do not discharge first
Aldehyde has effects that broad-spectrum sterilization to bacterium, saccharomycete and mould, and applicable PH ranges are big, mild non-stimulated, suitable sun-proof, often
For special cosmetics such as eye and child care products.
Flower of JINHUAKUI, sponge gourd flower used in the present invention and luffa vine grow water be Wuhan Lang Bao Science and Technology Ltd.s in
Wuhan City Caidian District Hong Beiyuan planting bases produce.
The present invention has the following advantages：
(1) present invention grows water as main function raw material using Golden flower flower, sponge gourd flower and luffa vine, can protrude
Golden flower flower, sponge gourd flower and luffa vine grow the natural organic characteristic of water etc., give full play to its moisturizing, whitening, anti-inflammatory, anti-mistake
It is quick, promote skin blood cycle and the skin-protecting functions such as anti-aging；
(2) present invention mainly is organized to form by plant in itself, but because it has used thickening, suspension, emulsification etc. are modern to make
Technology enables the active ingredient that Golden flower flower, sponge gourd flower and luffa vine grow water etc. to be evenly dispersed in system；Transdermal
Under the guiding of accelerating agent, skin performance skin care effect can be infiltered in time and dust particles are stranded in pore；
(3) raw material used in the present invention is nontoxic, without side-effects, safe and feasible, meets cosmetics manufacture requirement.
Description of the drawings
Fig. 1：Golden flower flower clay mask performance of keeping humidity test chart；
Fig. 2：Golden flower flower clay mask inhibits tyrosinase activity comparison diagram.
Specific embodiment
With reference to specific embodiment, the present invention is described in further detail.
Embodiment 1
1) Golden flower flower is weighed：22.5%th, sponge gourd flower：22.5%th, propylene glycol：5%th, carbomer：0.5%th, three second
Hydramine：1.5%th, EUXYL K300：0.05%th, citral：0.002%, surplus grows water for luffa vine；
2) by luffa vine taste water sterilized with 1200mL/h rates by ultraviolet ray sterilizer, then by filter core precision be 0.2 μ
The filter filtering of m, is placed in disinfecting container for use；
3) fresh Golden flower flower and sponge gourd flower are picked, cleans and drains, removes stem branch, crushing, stirring is into muddy；
4) will sterilize, filtering after luffa vine grow water be previously heated to 55 DEG C, by carbomer with luffa vine grow water in fully
Swelling, stands overnight；
5) triethanolamine is added in the carbomer solution of swelling, stirs to get clear gel matrix；
6) citral is dissolved in propylene glycol, is added to luffa vine and grows in water, obtain solution I；
7) solution I and flower mud are slowly added into gel-type vehicle, then are being stirred continuously lower addition EUXYL K300,
It is uniformly mixed and both obtains Golden flower flower clay mask.
Embodiment 2
1) Golden flower flower is weighed：25%th, sponge gourd flower：25%th, propylene glycol：8%th, carbomer：0.7%th, triethanolamine：
1.5%th, EUXYL K300：0.08%th, citral：0.004%, surplus grows water for luffa vine；
2) by luffa vine taste water sterilized with 1200mL/h rates by ultraviolet ray sterilizer, then by filter core precision be 0.2 μ
The filter filtering of m, is placed in disinfecting container for use；
3) fresh Golden flower flower and sponge gourd flower are picked, cleans and drains, removes stem branch, crushing, stirring is into muddy；
4) will sterilize, filtering after luffa vine grow water be previously heated to 55 DEG C, by carbomer with luffa vine grow water in fully
Swelling, stands overnight；
5) triethanolamine is added in the carbomer solution of swelling, stirs to get clear gel matrix；
6) citral is dissolved in propylene glycol, is added to luffa vine and grows in water, obtain solution I；
7) solution I and flower mud are slowly added into gel-type vehicle, then are being stirred continuously lower addition EUXYL K300,
It is uniformly mixed and both obtains Golden flower flower clay mask.
Embodiment 3
1) Golden flower flower is weighed：20%th, sponge gourd flower：20%th, propylene glycol：6%th, carbomer：0.3%th, triethanolamine：
1.0%th, EUXYL K300：0.1%th, citral：0.005%, surplus grows water for luffa vine；
2) by luffa vine taste water sterilized with 1200mL/h rates by ultraviolet ray sterilizer, then by filter core precision be 0.2 μ
The filter filtering of m, is placed in disinfecting container for use；
3) fresh Golden flower flower and sponge gourd flower are picked, cleans and drains, removes stem branch, crushing, stirring is into muddy；
4) will sterilize, filtering after luffa vine grow water be previously heated to 50 DEG C, by carbomer with luffa vine grow water in fully
Swelling, stands overnight；
5) triethanolamine is added in the carbomer solution of swelling, stirs to get clear gel matrix；
6) citral is dissolved in propylene glycol, is added to luffa vine and grows in water, obtain solution I；
7) solution I and flower mud are slowly added into gel-type vehicle, then are being stirred continuously lower addition EUXYL K300,
It is uniformly mixed and both obtains Golden flower flower clay mask.
Embodiment 4
1) Golden flower flower is weighed：30%th, sponge gourd flower：30%th, propylene glycol：8%th, carbomer：0.5%th, triethanolamine：
1.3%th, EUXYL K300：0.08%th, citral：0.005%, surplus grows water for luffa vine；
2) by luffa vine taste water sterilized with 1200mL/h rates by ultraviolet ray sterilizer, then by filter core precision be 0.2 μ
The filter filtering of m, is placed in disinfecting container for use；
3) fresh Golden flower flower and sponge gourd flower are picked, cleans and drains, removes stem branch, crushing, stirring is into muddy；
4) will sterilize, filtering after luffa vine grow water be previously heated to 60 DEG C, by carbomer with luffa vine grow water in fully
Swelling, stands overnight；
5) triethanolamine is added in the carbomer solution of swelling, stirs to get clear gel matrix；
6) citral is dissolved in propylene glycol, is added to luffa vine and grows in water, obtain solution I；
7) solution I and flower mud are slowly added into gel-type vehicle, then are being stirred continuously lower addition EUXYL K300,
It is uniformly mixed and both obtains Golden flower flower clay mask.
1st, cutaneous safety is tested：
According to《Safety evaluation of cosmetics program and method》(GB7919-87) relevant regulations carry out skin to the present invention
Stimulate the reaction is tested.
The healthy men and women experimenter 70 of random selection, experimenter is to alcohol and medical proof fabric without allergies.
It wipes dry from first being cleaned ancon 4cm at clear water on the inside of left forearm to volunteer, then takes facial mask of the invention in skin
2.5 × 2.5cm squares, thickness about 0.5cm are divided on skin.Then it is gently applied with gauze piece, then is covered with one layer of oilpaper,
It is pasted and fixed with medical proof fabric.Gauze is opened after 1h, observes change of skin, is carried out according to 1 skin wound repair evaluation criterion of table
Analysis.
1 skin wound repair evaluation criterion of table
2 Golden flower flower clay mask skin wound repair test result of table
Above-mentioned result of the test shows in the experimenter that visible erythema, the visible erythema of 1 people, positive rate are only only 3 people reluctantly
5.7%；In the experimenter, visible oedema, positive rate are only 2.9% to only 2 people reluctantly, and the present invention is excellent to the safety of skin.
2nd, the measure of performance of keeping humidity
The moisture content of skin is kept, skin elasticity can be increased, makes skin eubolism, reduces the life of wrinkle and color spot
Into.In general, the water content normal value at people's different skin position is as follows：
| Skin part | Cheek portion | Forehead | Eyelid | The palm of the hand | The back of the hand | Wrist |
| Water content | 30~50% | 30~50% | 40~50% | 40~55% | 30~50% | 35~40% |
This experiment uses the digital skin water tester (Skin that Ai Beimei Science and Technology Ltd.s of Shenzhen produce
Detector SD) skin part is specified to test subject, SD systems use the high-precision skin of Bioelectrical impedance analysis technology
Skin water tester.By test probe flicking after the tested person skin part several seconds, LCD display shows that skin is instant
Water content percentage.
Moisturizing test volunteer 60 is selected, the age between 20-45 Sui, is randomly divided into three groups.Subject is in room temperature 25
DEG C or so, in the environment of relative humidity 50%, first cleaned on the inside of left finesse with clean water, difference then treated that test agent is equal respectively
It is even that divide into 3 × 3cm rectangular.First group is applied physiological saline gauze in specified skin part；Second group is applied in specified skin part
With the matrix facial mask that water is grown without flower mud and luffa vine；Third group is in specified skin part application facial mask of the present invention.30min
Afterwards, each determinand is removed.In 0,30,60,90, carry out respectively at the periods cutaneous applications of the SD to three groups of subjects such as 120min
Test obtains skin moisture content, surveys number average value to each group and compare and analyze.Test result is shown in Fig. 1.
Test result shows that without moisture-keeping function, the matrix facial mask for growing water without flower mud and rattan has centainly physiological saline
Moisture-keeping function, but moisture-keeping function is not lasting；Facial mask of the present invention has significant moisturizing efficiency, and the skin water after 120min
Part content is still within ideal value.
3rd, whitening function is tested
The primary raw material for manufacturing the black pigment of skin is tyrosine, and tyrosinase is the main speed limit that tyrosine is changed into melanocyte
Enzyme, when tyrosinase activity is suppressed, melanocyte, which produces Melanogenic ability, accordingly to be declined.In other words, inhibit tyrosine
Enzymatic activity can play the role of skin whitening.
It is as follows to the whitening function testing procedure of facial mask of the present invention：
Prepare tyrosine enzyme solution：Fresh intact potato is taken to clean to be pre-chilled 4 hours or so after 4 DEG C, peeling is cut into about
1.3cm2Fourth shape in -20 DEG C of freeze overnights, presses 1 after taking-up:The ratio of 1 (W/V) adds in phosphate buffer, uses tissue mashing machine
Homogenate is made, with 3 layers of filtered through gauze, filtrate centrifuges 10min then at 4000r/min, and supernatant is that the tyrosinase of gained is thick
Enzyme solution in 4 DEG C of preservations, is finished in 2 hours.
Test solution is treated in preparation：Facial mask 40mg of the present invention is accurately weighed, is sufficiently stirred with 100ml deionized waters, centrifugal filtration takes
Supernatant obtains 0.4mg/ml and treats test solution.
Prepare positive control solution：Ascorbic acid (Vc) 40mg accurately is weighed, with sodium phosphate buffer (PH6.8,0.1mol/
L it) dissolves, is configured to the solution of 0.4mg/ml.
Prepare l-tyrosine reagent：It is accurate to weigh l-tyrosine 90.595mg, few drops of concentrated hydrochloric acids are added in, low-grade fever is completely dissolved
Afterwards, add water number 10ml, be neutralized to neutrality with sodium hydroxide, be settled to 100ml, it is 5mol/L to make l-tyrosine solution concentration.
This experiment is using deionized water as negative control, and using 0.4mg/mlVc solution as positive control, total reaction volume is
2ml, wherein tyrosinase crude extract 0.5ml, 0.1mol/L phosphate buffers (PH6.8) 0.5ml, in blank tube plus deionized water
1.0ml；It treats to treat test solution 0.5ml in test solution pipe.L-tyrosine solution 0.5ml；Vc solution 0.5ml, L- junket ammonia in positive control pipe
Acid solution 0.5ml.
Specific test process：First by l-tyrosine solution and phosphate buffer mixing, 30 DEG C of warm bath 10min are added and are treated
Survey liquid and tyrosinase crude extract.Continue to distinguish warm bath 30min, 60min, 120min in 30 DEG C of water-baths.Then with blank tube
For reference, absorbance value of each tube reaction liquid under spectrophotometer 475mm wavelength is measured.Using negative control group as reference,
The mean of three parallel samples is taken, is calculated respectively with following equation and treats the inhibiting rate of test solution and Vc solution to tyrosinase activity,
And it maps and compares and analyzes.
Inhibitory activity against tyrosinase %=[(A-B)/A] × 100
Wherein：A：The absorbance value of negative control group, B：The absorbance value of experimental group.Inhibiting rate height shows to tyrosinase
The inhibition strength of activity is high.
Inhibiting tyrosinase activity, experimental result is shown in Fig. 2.Originally the experimental results showed that, Vc extends at any time, inhibits junket ammonia
The function of phytase activity gradually lowers, and it is first to increase that the facial mask of the present invention, which inhibits the function of tyrosinase activity, then gradually
It reduces.Generally speaking, Vc and all great effect for inhibiting tyrosinase activity of the facial mask of the present invention.
4th, quality control standards (QCS)
(1) reference《Pharmacopoeia of People's Republic of China》It is surveyed in (version in 2012) I about total flavone glucoside content assaying method
The content of total flavone glucoside in fixed facial mask of the present invention, measurement result are labelled amount ± 5%.
(2) physical behavior is examined：Product colour of the present invention is yellow green, and translucent plant pureed is homogeneous, is had slight
Golden flower and the fragrant of sponge gourd mixing.Spreading property is good, non-stimulated coated on skin；It removes within 15~20 minutes, skin seems
Water is tender, fine and smooth, smooth.
(3) health chemical testing：Lead, mercury, arsenic are no more than what the Ministry of Public Health issued《Cosmetics health specification》Required standard.
(4) microorganism detection：Total plate count, excrement colibacillus group, Pseudomonas aeruginosa, staphylococcus aureus, saccharomycete, mould
Clump counts is waited to be no more than what the Ministry of Public Health issued《Cosmetics health specification》Required standard.
(5) toxicology test：Multiple Skin Irritation Test, acute ocular irritation test meet national standard；
(6) packing instructions：Meet country about《Cosmetics inspection rule (QB/T 1684)》、《Cosmetic product packaging is outer
See requirement (QB/T 1685)》With《Metrolgy Inspection of Products in Prepackages rule (JJF 1070-2000)》It is advised Deng correlation
It is fixed, be in direct contact product packaging material accomplish it is nontoxic, it is sterile.
Claims (4)
1. a kind of Golden flower flower clay mask, it is characterised in that：It is prepared by the raw material of following weight percent, wherein respectively
The weight percent of component raw material is as follows：
Golden flower flower：22.5%th, sponge gourd flower 22.5%, propylene glycol：5%th, carbomer：0.5%th, triethanolamine：1.5%th,
EUXYL K300：0.05%th, citral：0.004%, surplus grows water for luffa vine；The carbomer is carbomer U20.
2. the preparation method of Golden flower flower clay mask described in a kind of claim 1, which is characterized in that this method includes following step
Suddenly：
1) it after luffa vine being grown water by ultraviolet ray sterilizer disinfection and filter filtering, is placed in disinfecting container for use；
2) by Golden flower flower and sponge gourd flower crushing, stirring into muddy, for use；
3) carbomer is grown water with step 1) treated luffa vine to be fully swollen, stands overnight；
4) triethanolamine is added in the carbomer solution of swelling that step 3) obtains, stirs to get clear gel matrix；
5) it after citral being dissolved in propylene glycol, adds in step 1) treated luffa vine and grows in water, obtain solution I；
6) flower slurries made from solution I made from step 5) and step 2) are added in gel-type vehicle made from step 4),
Lower addition EUXYL K300 are being stirred continuously, is being uniformly mixed and both obtains Golden flower flower clay mask.
3. the preparation method of Golden flower flower clay mask according to claim 2, it is characterised in that：It is used in the step 1)
Filter filter core precision be 0.2 μm.
4. the preparation method of Golden flower flower clay mask according to claim 2, it is characterised in that：It is used in the step 3)
Luffa vine grow water be previously heated to 50~60 DEG C.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105853287B (en) * | 2016-05-03 | 2018-08-28 | 广州暨南生物医药研究开发基地有限公司 | A kind of Golden flower moisturizing essence and preparation method thereof |
| CN106074238B (en) * | 2016-06-14 | 2019-01-18 | 广州暨南生物医药研究开发基地有限公司 | A kind of Golden flower whitening and spot eliminating cream and preparation method thereof |
| CN106109369B (en) * | 2016-06-21 | 2018-12-11 | 广州暨南生物医药研究开发基地有限公司 | A kind of anti-wrinkle composition and its anti-wrinkle cream containing Golden flower |
| KR101857528B1 (en) * | 2016-07-01 | 2018-05-15 | 에스케이바이오랜드 주식회사 | Cosmetic composition with the extract of Aurea Helianthus for skin-whitening |
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