CN107334647A - A kind of colorful anti-wrinkle face mask of painting type and preparation method thereof - Google Patents
A kind of colorful anti-wrinkle face mask of painting type and preparation method thereof Download PDFInfo
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- CN107334647A CN107334647A CN201710539175.3A CN201710539175A CN107334647A CN 107334647 A CN107334647 A CN 107334647A CN 201710539175 A CN201710539175 A CN 201710539175A CN 107334647 A CN107334647 A CN 107334647A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
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Abstract
The invention discloses colorful anti-wrinkle face mask of a kind of painting type and preparation method thereof.The present invention the colorful anti-wrinkle face mask of painting type according to weight than each group be divided into：Toning base-material：400 500 parts, interleaving agent：200 300 parts, continuous phase：300 400 parts.The colorful anti-wrinkle face mask color of painting type of the present invention appears, pleasing, gives the enjoyment of U.S.；The facial mask uses green raw material, will not have a negative impact to human body and environment；The mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good, and anti-wrinkle effect is notable；The mature preparation process of the facial mask, adapt to industrialized production.
Description
Technical field
The invention belongs to field of fine chemical, and in particular to a kind of colorful anti-wrinkle face mask of painting type and preparation method thereof.
Background technology
Nowadays, as the raising of people's quality of the life and the pursuit to U.S., more and more people's selections are maintained using facial mask
Skin.Anti-wrinkle face mask is a kind of carrier of face beautifying health keeping product, and sufficient moisture and nutriment can be provided to skin, is had anti-
Wrinkle, firm skin and other effects, are loved by people.Anti-wrinkle face mask on the market is mostly sticking type facial mask now.Attach
Formula facial mask is to use non-woven fabrics etc. to be used as matrix, infiltration Essence etc. to spread on skin.Subject matter existing for this mode is
Due to individual difference, facial mask can not be bonded completely with skin.Daubing-type facial mask solves this problem.In use, by paste face
Film is uniformly applied on skin, is treated that Essence absorbs and is finished, can tear in flakes.The crease-resistant face of the painting type of all kinds of brands on the market
Film is a feast for the eyes.In order to win the market, manufacturers, which try one's best, makes miscellaneous product.They are formulated health environment-friendly,
Attractive packages is generous.By contrast, the visual effect of the content that consumer more takes notice of in itself, which but has no characteristic, to be sayed.Now,
Daubing-type facial mask on the market is transparent or monochromatic lotion.Product colour is single, can not meet pursuit of the consumer to U.S..
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of colorful anti-wrinkle face mask of painting type and its preparation
Method.The colorful anti-wrinkle face mask color of the painting type appears, pleasing, gives the enjoyment of U.S.；And using green
Raw material, will not have a negative impact to human body and environment；Patch skin is good during use, and adhesion is moderate, and film forming is fast, pliability
It is good, crease-resistant, firm skin significant effect；Mature preparation process, adapt to industrialized production.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of colorful anti-wrinkle face mask of painting type, is made up of the raw material of following parts by weight：Toning base-material 400-500 parts, interleaving agent
200-300 parts and continuous phase 300-400 parts.
Described interleaving agent is made up of the raw material of following parts by weight：Deionized water 850-950 parts, insulating powder 50-150 parts,
Preservative 1-3 parts.
Described insulating powder is lithium magnesium silicate, aluminium-magnesium silicate, S482 one or more of compositions；Described preservative
For Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
The preparation process of described interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 400-500 revs/min of rotating speed；
2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring 30-40 minutes to dissolving；
3）Surplus insulating powder is put into reactor, 30-40 minutes are stirred under same rotational speed.
The continuous phase is made up of the raw material of following parts by weight：Deionized water 600-750 parts, water-base resin 200-400 parts,
Anti wrinkling agent 10-20 parts, NMF 10-30 parts, thickener 3-15 parts, preservative 3-5 parts, pH adjusting agent 0-5 parts, complexing agent 0.2-
1 part.
In continuous phase, described water-base resin is one or both of Carfil 9221 or Carfil 9220；
Described anti wrinkling agent is Sodium Hyaluronate, Argireline, one or more of compositions in Wushengtai；The NMF is 1,2-
Propane diols, glycerine, ethylene glycol, sorbierite, one or more of compositions in butanediol；Described thickener is Guar
Glue, carbomer, sodium carboxymethylcellulose, hydroxyethyl cellulose, one or more of compositions in hydroxypropyl cellulose；It is described
PH adjusting agent be diethanol amine, triethanolamine, one or more of compositions in AMP-95；Described complexing agent is second two
Amine tetraacethyl disodium, one kind in the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is Kathon CG, Phenoxyethanol, nipalgin
Methyl esters, one or more of compositions in propylben.
The preparation process of the continuous phase is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, is resisted
Wrinkle agent, complexing agent and preservative, stirs 30-40 minutes；
2）Water-base resin is added, stirs 15-20 minutes；
3）Thickener is slowly added to, stirs 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces continuous phase.
Described toning base-material is made up of the raw material of following parts by weight：Base-material 980-1000 parts, dyestuff 0-20 parts；It is described
Base-material be made up of the raw material of following parts by weight：Deionized water 350-550 parts, water-base resin 300-500 parts, interleaving agent 50-
150 parts, anti wrinkling agent 10-20 parts, NMF 10-30 parts；Thickener 20-80 parts, pH adjusting agent 0-50 parts, preservative 3-5 parts, network
Mixture 0.2-1 parts；The dyestuff is assorted food-grade or cosmetics-stage transparency dye.
In base-material, described water-base resin is one or both of Carfil 9221 or Carfil 9220；Institute
The anti wrinkling agent stated is Sodium Hyaluronate, Argireline, one or more of compositions in Wushengtai；The NMF is 1,2- third
Glycol, glycerine, ethylene glycol, sorbierite, one or more of compositions in butanediol；Described thickener is Aculyn
One or more of compositions in 33, Vesmody A901, Vesmody A406；Described pH adjusting agent is diethanol
Amine, triethanolamine, one or more of compositions in AMP-95；Described complexing agent is disodium ethylene diamine tetraacetate, diethyl
One kind in alkene Pentetate Pentasodium；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, in propylben
One or more of compositions.
The preparation process of described base-material is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, is resisted
Wrinkle agent, complexing agent and preservative, stirs 30-40 minutes；
2）Water-base resin is added, stirs 15-20 minutes；
3）Thickener and interleaving agent are slowly added to, stirs 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces base-material；
The preparation process of described toning base-material is：
1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；
2）The dyestuff of formula ratio is separately added into, 20-30 minutes is stirred, produces toning base-material.
A kind of method for preparing the colorful anti-wrinkle face mask of painting type as described above, including step as described below：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；
2）The toning base-material of formula ratio is directly added into interleaving agent by comminutor, gained particle, granulation continues to stir after terminating
Mix 10-15 minutes；
3）Continuous phase is slowly added to reactor, 20-30 minutes are stirred with 100-150 revs/min of speed.It is more to produce painting type
Color anti-wrinkle face mask.
The beneficial effects of the present invention are：
1）Mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good, and anti-wrinkle effect is notable；Due to skin temperature compared with
Height, after colorful anti-wrinkle face mask is coated on skin, interleaving agent fails rapidly, promotes the elite thing in toning base-material and continuous phase
Release, while water-base resin formed diaphragm structure, in favor of maintenance terminate after depart from skin；
2）The colorful anti-wrinkle face mask color of painting type appears, pleasing, gives the enjoyment of U.S.；And use green original
Material is made, and will not have a negative impact to human body and environment；
3）The mature preparation process of facial mask, adapt to industrialized production.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described.
Obviously, described embodiment is only the part of the present invention, and based on the embodiment in the present invention, those skilled in the art exist
The every other embodiment obtained under the premise of creative work is not made, belongs to the scope of protection of the invention.
Embodiment 1
A kind of colorful anti-wrinkle face mask of painting type is made up of the raw material of following parts by weight：400 parts of base-material of toning, 250 parts of interleaving agent, even
Continuous 350 parts of phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：452 parts of deionized water, 9,221 350 parts of Carfil, silicic acid
100 parts of the magnesium lithium aqueous solution, 25 parts of 1,2-PD, 4 parts of Argireline, 33 35 parts of Aculyn, 30 parts of triethanolamine, Phenoxyethanol
3.2 parts, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
Grey and the compound method of white basic material are identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and are configured to
Grey base-material, 99.8 parts of base-materials add 0.2 part of white dye and are configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, controls 800 revs/min of rotating speed, sequentially adds 1,2-PD, six
Win peptide, disodium ethylene diamine tetraacetate, Phenoxyethanol, stir 30 minutes；
2）Carfil 9221 and the lithium magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of lithium magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 500 revs/min of rotating speed；
2）The lithium magnesium silicate powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus lithium magnesium silicate powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：675 parts of deionized water, 9,221 280 parts of Carfil, third
25 parts of triol, 5 parts of Argireline, 1 part of 21 5 parts of carbomer Carbopol Ultrez, hydroxyethyl cellulose 250HBR, benzene oxygen second
3 parts of alcohol, 5 parts of AMP-95,1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds glycerine, six victory
Peptide, disodium ethylene diamine tetraacetate, Phenoxyethanol, stir 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and hydroxyethyl cellulose 250HBR are slowly added to, is stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful anti-wrinkle face mask of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）The toning base-material of formula ratio is directly added into the lithium magnesium silicate aqueous solution by comminutor, gained particle, granulation terminates
After continue stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.It is colorful crease-resistant to produce painting type
Facial mask 1.
Embodiment 2
A kind of colorful anti-wrinkle face mask of painting type is made up of the raw material of following parts by weight：500 parts of base-material of toning, 200 parts of interleaving agent, even
Continuous 400 parts of phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：482 parts of deionized water, 9,221 320 parts of Carfil, silicic acid
The magnalium aqueous solution（Interleaving agent）100 parts, 25 parts of 1,2-PD, 3 parts of Argireline, 1 part of Wushengtai, Vesmody A901 35
Part, 30 parts of triethanolamine, 3 parts of propylben, 1 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, blueness, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of grey, blueness and white basic material is identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and matched somebody with somebody
Grey base-material is made, 99.8 parts of base-materials add 0.2 part of blue dyes and prepare au bleu base-material, and 99.8 parts of base-materials add 0.2 part in vain
Color dyestuff is configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, controls 800 revs/min of rotating speed, sequentially adds 1,2-PD, six
Win peptide, Wushengtai, disodium ethylene diamine tetraacetate, Phenoxyethanol, stir 30 minutes；
2）Carfil 9221 and the aluminium-magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of aluminium-magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 500 revs/min of rotating speed；
2）The magnesium silicate aluminium powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus magnesium silicate aluminium powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：675 parts of deionized water, 9,221 280 parts of Carfil, third
25 parts of triol, 3 parts of Argireline, 2 parts of Wushengtai, 1 part of 21 5 parts of Carbopol Ultrez, 250HBR, 3 parts of propylben,
5 parts of AMP-95,1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds glycerine, six victory
Peptide, Wushengtai, disodium ethylene diamine tetraacetate, propylben, stir 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful anti-wrinkle face mask of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）The toning base-material of formula ratio is directly added into the aluminium-magnesium silicate aqueous solution by comminutor, gained particle, granulation terminates
After continue stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.It is colorful crease-resistant to produce painting type
Facial mask 2.
Embodiment 3
A kind of colorful anti-wrinkle face mask of painting type is made up of the raw material of following parts by weight：450 parts of base-material of toning, 300 parts of interleaving agent, even
Continuous 300 parts of phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：457 parts of deionized water, 9,220 350 parts of Carfil, S-
482 solution（Interleaving agent）100 parts, 20 parts of 1,2-PD, 5 parts of glycerine, 8 parts of Sodium Hyaluronate, Vesmody A901 30
Part, 26 parts of triethanolamine, 3.2 parts of methyl hydroxybenzoate, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, red, blue food-grade transparency dye.
Toning base-material preparation process be：
1）100 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.2 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of red and blue base-material is identical with yellow base-material, and 199.6 parts of base-materials add 0.4 part of orchil and are configured to
Red base-material, 149.7 parts of base-materials add 0.3 part of gray dyes and prepare grey base-material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, controls 800 revs/min of rotating speed, sequentially adds 1,2-PD, third
Triol, Sodium Hyaluronate, disodium ethylene diamine tetraacetate, Phenoxyethanol, stir 30 minutes；
2）Carfil 9221 and S-482 solution are sequentially added, is stirred 30 minutes；
3）Vesmody A901 are added, are stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of S-482 powder, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 500 revs/min of rotating speed；
2）The S-482 powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus S-482 powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：666 parts of deionized water, 9,221 280 parts of Carfil, 1,
25 parts of 2- propane diols, 5 parts of glycerine, 9 parts of Sodium Hyaluronate, 1 part of 21 5 parts of Carbopol Ultrez, 250HBR, nipalgin
3 parts of methyl esters, 5 parts of AMP-95,1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, controls 800 revs/min of rotating speed, sequentially adds 1,2-PD, third
Triol, Sodium Hyaluronate, disodium ethylene diamine tetraacetate and methyl hydroxybenzoate, stir 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful anti-wrinkle face mask of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）The toning base-material of formula ratio is directly added into the S482 aqueous solution by comminutor, gained particle, it is follow-up to be granulated end
Continuous stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.It is colorful crease-resistant to produce painting type
Facial mask 3.
Use feeling and crease-resistant efficacy assessments, specific test side are carried out to the embodiment 1-3 colorful anti-wrinkle face mask of painting type
Method is as follows：
Each test group chooses 20 female volunteers, and age 35-55 year, skin health, there is certain degree microgroove in face, tested
When health it is good, 60 people altogether.Application method：After volunteer cleans face, tested facial mask is homogeneously applied to left face
As test section, right face is without test, as a comparison area.Facial mask is thrown off after 15 minutes.Experiment facial mask uses every other day, continues 3
After individual month, use feeling investigation is carried out to volunteer, evaluation is divided into 5 grades：More than 90% subject is satisfied with, and comments 5 points；80%-
90% subject is satisfied with, and comments 4 points；70%-80% subject is satisfied with, and comments 3 points；60-70% subject is satisfied with, and comments 2 points；Less than 60% by
Examination person is satisfied with, and comments 1 point.Evaluation result is classified as table 1.
The use feeling evaluation of the colorful anti-wrinkle face masks of embodiment 1-3 of table 1.
For contrast table 1 as can be seen that the made colorful anti-wrinkle face mask anti-wrinkle effects of embodiment 1-3 are good, firm skin significant effect is ventilative
Property it is good, it is small to skin irritation, complete skin care after easily torn off from face.
It is described above, be only presently preferred embodiments of the present invention, any formal limitation not done to the present invention, therefore it is all not
Depart from the content of technical solution of the present invention, according to the present invention technical spirit to any simple modification made for any of the above embodiments,
Equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (9)
- A kind of 1. colorful anti-wrinkle face mask of painting type, it is characterised in that：It is made up of the raw material of following parts by weight：Mix colours base-material 400- 500 parts, interleaving agent 200-300 parts and continuous phase 300-400 parts；Described interleaving agent is made up of the raw material of following parts by weight：Go Ionized water 850-950 parts, insulating powder 50-150 parts, preservative 1-3 parts；The continuous phase is made up of the raw material of following parts by weight： Deionized water 600-750 parts, water-base resin 200-400 parts, anti wrinkling agent 10-20 parts, NMF 10-30 parts, thickener 3-15 parts, Preservative 3-5 parts, pH adjusting agent 0-5 parts, complexing agent 0.2-1 parts.
- 2. the colorful anti-wrinkle face mask of painting type according to claim 1, it is characterised in that：Described insulating powder is magnesium silicate One or more of compositions in lithium, aluminium-magnesium silicate, S482；Described preservative is Kathon CG, Phenoxyethanol, Metagin Ester, one or more of compositions in propylben.
- 3. the colorful anti-wrinkle face mask of painting type according to claim 1 or 2, it is characterised in that：The preparation of described interleaving agent Process is：1）The deionized water of formula ratio is put into reactor, controls 400-500 revs/min of rotating speed；2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring 30-40 minutes to dissolving；3）Surplus insulating powder is put into reactor, 30-40 minutes are stirred under same rotational speed, interleaving agent is made.
- 4. the colorful anti-wrinkle face mask of painting type according to claim 1 or 2, it is characterised in that：Described water-base resin is One or both of Carfil 9221 or Carfil 9220；Described anti wrinkling agent is Sodium Hyaluronate, Argireline, five Win one or more of compositions in peptide；The NMF is 1,2-PD, glycerine, ethylene glycol, sorbierite, butanediol In one or more of compositions；Described thickener is guar gum, carbomer, sodium carboxymethylcellulose, hydroxy ethyl fiber Element, one or more of compositions in hydroxypropyl cellulose；Described pH adjusting agent is diethanol amine, triethanolamine, AMP- One or more of compositions in 95；Described complexing agent is disodium ethylene diamine tetraacetate, the sodium of diethylene triamine pentacetic acid (DTPA) five In one kind；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of groups in propylben Compound.
- 5. the colorful anti-wrinkle face mask of painting type according to claim 1 or 2, it is characterised in that：The preparation step of the continuous phase Suddenly it is：1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, is resisted Wrinkle agent, complexing agent and preservative, stirs 30-40 minutes；2）Water-base resin is added, stirs 15-20 minutes；3）Thickener is slowly added to, stirs 30-40 minutes；4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces continuous phase.
- 6. the colorful anti-wrinkle face mask of painting type according to claim 1 or 2, it is characterised in that：The toning base-material is by following The raw material composition of parts by weight：Base-material 980-1000 parts, dyestuff 0-20 parts；Described base-material by following parts by weight raw material group Into：Deionized water 350-550 parts, water-base resin 300-500 parts, interleaving agent 50-150 parts, anti wrinkling agent 10-20 parts, NMF 10- 30 parts, thickener 20-80 parts, pH adjusting agent 0-50 parts, preservative 3-5 parts, complexing agent 0.2-1 parts；The dyestuff is eaten to be assorted Grade or cosmetics-stage transparency dye.
- 7. the colorful anti-wrinkle face mask of painting type according to claim 6, it is characterised in that：In base-material, described water-base resin For one or both of Carfil 9221 or Carfil 9220；Described anti wrinkling agent is Sodium Hyaluronate, Argireline, One or more of compositions in Wushengtai；The NMF is 1,2-PD, glycerine, ethylene glycol, sorbierite, fourth two One or more of compositions in alcohol；Described thickener is Aculyn 33, Vesmody A901, Vesmody One or more of compositions in A406；Described pH adjusting agent is diethanol amine, triethanolamine, one kind in AMP-95 or Several compositions；Described complexing agent is disodium ethylene diamine tetraacetate, one kind in the sodium of diethylene triamine pentacetic acid (DTPA) five；It is described Preservative be Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
- 8. the colorful anti-wrinkle face mask of painting type according to claim 6, it is characterised in that：The preparation process of described base-material For：1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, is resisted Wrinkle agent, complexing agent and preservative, stirs 30-40 minutes；2）Water-base resin is added, stirs 15-20 minutes；3）Thickener and interleaving agent are slowly added to, stirs 30-40 minutes；4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces base-material；The preparation process of described toning base-material is：1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；2）The dyestuff of formula ratio is separately added into, 20-30 minutes is stirred, produces toning base-material.
- A kind of 9. method of the colorful anti-wrinkle face mask of painting type prepared as described in claim 1-2, it is characterised in that：Including as follows The step：1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；2）The toning base-material of formula ratio is directly added into interleaving agent by comminutor, gained particle, granulation continues to stir after terminating Mix 10-15 minutes；3）Continuous phase is slowly added to reactor, 20-30 minutes are stirred with 100-150 revs/min of speed.It is more to produce painting type Color anti-wrinkle face mask.
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| CN201710539175.3A CN107334647A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful anti-wrinkle face mask of painting type and preparation method thereof |
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| CN201710539175.3A CN107334647A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful anti-wrinkle face mask of painting type and preparation method thereof |
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