CN107334657A - A kind of colorful deep clean facial mask of painting type and preparation method thereof - Google Patents
A kind of colorful deep clean facial mask of painting type and preparation method thereof Download PDFInfo
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- CN107334657A CN107334657A CN201710538655.8A CN201710538655A CN107334657A CN 107334657 A CN107334657 A CN 107334657A CN 201710538655 A CN201710538655 A CN 201710538655A CN 107334657 A CN107334657 A CN 107334657A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/87—Polyurethanes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses colorful deep clean facial mask of a kind of painting type and preparation method thereof.The present invention the colorful deep clean facial mask of painting type according to weight than each group be divided into：Toning base-material：400 500 parts, interleaving agent：200 300 parts, continuous phase：300 400 parts.The colorful deep clean facial mask color of painting type of the present invention appears, pleasing, gives the enjoyment of U.S.；The facial mask uses green raw material, will not have a negative impact to human body and environment；The mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good, can remove blackhead, pore refining, the significant effect of deep clean skin；The mature preparation process of the facial mask, adapt to industrialized production.
Description
Technical field
The invention belongs to field of fine chemical, and in particular to a kind of colorful deep clean facial mask of painting type and its preparation side
Method.
Background technology
Nowadays, as the raising of people's quality of the life and the pursuit to U.S., more and more people's selections are maintained using facial mask
Skin.Deep clean facial mask is a kind of carrier of face beautifying health keeping product, can remove blackhead, pore refining, there is deep clean skin
And other effects, it is loved by people.Deep clean facial mask on the market is mostly sticking type facial mask now.Sticking type facial mask is
Using non-woven fabrics etc. as matrix, infiltration Essence etc. is spread on skin.Subject matter existing for this mode is due to individual
Difference, facial mask can not be bonded completely with skin.Daubing-type facial mask solves this problem.In use, cream pack is uniformly applied
Smear on skin, treat Essence absorb finish, can tear in flakes.The painting type deep clean facial mask beautiful jade of all kinds of brands on the market
Thinkling sound meets the eye on every side.In order to win the market, manufacturers, which try one's best, makes miscellaneous product.They are formulated health environment-friendly, packaging
It is elegant in appearance.By contrast, the visual effect of the content that consumer more takes notice of in itself, which but has no characteristic, to be sayed.Now, market
On painting type deep clean facial mask be transparent or monochromatic lotion.Product colour is single, can not meet that consumer chases after to U.S.A
Ask.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of colorful deep clean facial mask of painting type and its
Preparation method.The colorful deep clean facial mask color of the painting type appears, pleasing, gives the enjoyment of U.S.；And use
Green raw material, will not have a negative impact to human body and environment；Patch skin is good during use, and adhesion is moderate, and film forming is fast,
Pliability is good, can remove blackhead, pore refining, the significant effect of deep clean skin；Mature preparation process, adapt to industrialization
Production.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of colorful deep clean facial mask of painting type, is made up of the raw material of following parts by weight：Toning base-material 400-500 parts, isolation
Agent 200-300 parts and continuous phase 300-400 parts.
Described interleaving agent is made up of the raw material of following parts by weight：Deionized water 850-950 parts, insulating powder 50-150 parts,
Preservative 1-3 parts.
Described insulating powder is lithium magnesium silicate, aluminium-magnesium silicate, S482 one or more of compositions；Described preservative
For Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
The preparation process of described interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 400-500 revs/min of rotating speed；
2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring 30-40 minutes to dissolving；
3）Surplus insulating powder is put into reactor, 30-40 minutes are stirred under same rotational speed.
The continuous phase is made up of the raw material of following parts by weight：Deionized water 600-750 parts, water-base resin 200-400 parts,
Cleaning agent 2-10 parts, pore astringent 5-20 parts, NMF 10-30 parts, thickener 3-15 parts, preservative 3-5 parts, pH adjusting agent
0-5 parts, complexing agent 0.2-1 parts.
In continuous phase, described water-base resin is one or both of Carfil 9221 or Carfil 9220；
Described cleaning agent is the composition of one or both of salicylic acid and tartaric acid；The pore astringent is Sodium Hyaluronate,
Vitamin K, one or more of compositions in medical collagen；The NMF is 1,2-PD, glycerine, second two
Alcohol, sorbierite, one or more of compositions in butanediol；Described thickener is guar gum, carbomer, carboxymethyl cellulose
Plain sodium, hydroxyethyl cellulose, one or more of compositions in hydroxypropyl cellulose；Described pH adjusting agent is diethanol
Amine, triethanolamine, one or more of compositions in AMP-95；Described complexing agent is disodium ethylene diamine tetraacetate, diethyl
One kind in alkene Pentetate Pentasodium；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, in propylben
One or more of compositions.
The preparation process of the continuous phase is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, clearly
Clean dose, pore astringent, complexing agent and preservative, stir 30-40 minutes；
2）Water-base resin is added, stirs 15-20 minutes；
3）Thickener is slowly added to, stirs 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces continuous phase.
Described toning base-material is made up of the raw material of following parts by weight：Base-material 980-1000 parts, dyestuff 0-20 parts；It is described
Base-material be made up of the raw material of following parts by weight：Deionized water 350-550 parts, water-base resin 300-500 parts, interleaving agent 50-
150 parts, cleaning agent 2-10 parts, pore astringent 5-20 parts, NMF 10-30 parts；Thickener 20-80 parts, pH adjusting agent 0-50
Part, preservative 3-5 parts, complexing agent 0.2-1 parts；The dyestuff is assorted food-grade or cosmetics-stage transparency dye.
In base-material, described water-base resin is one or both of Carfil 9221 or Carfil 9220；Institute
The cleaning agent stated is the composition of one or both of salicylic acid and tartaric acid；The pore astringent is Sodium Hyaluronate, dimension
Raw plain K, one or more of compositions in medical collagen；The NMF is 1,2-PD, glycerine, second two
Alcohol, sorbierite, one or more of compositions in butanediol；Described thickener is Aculyn 33, Vesmody
One or more of compositions in A901, Vesmody A406；Described pH adjusting agent is diethanol amine, triethanolamine,
One or more of compositions in AMP-95；Described complexing agent is disodium ethylene diamine tetraacetate, diethylene triamine pentacetic acid (DTPA)
One kind in five sodium；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, the one or more in propylben
Composition.
The preparation process of described base-material is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, clearly
Clean dose, pore astringent, complexing agent and preservative, stir 30-40 minutes；
2）Water-base resin is added, stirs 15-20 minutes；
3）Thickener and interleaving agent are slowly added to, stirs 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces base-material；
The preparation process of described toning base-material is：
1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；
2）The dyestuff of formula ratio is separately added into, 20-30 minutes is stirred, produces toning base-material.
A kind of method for preparing the colorful deep clean facial mask of painting type as described above, including step as described below：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；
2）The toning base-material of formula ratio is directly added into interleaving agent by comminutor, gained particle, granulation continues to stir after terminating
Mix 10-15 minutes；
3）Continuous phase is slowly added to reactor, 20-30 minutes are stirred with 100-150 revs/min of speed.It is more to produce painting type
Color deep clean facial mask.
The beneficial effects of the present invention are：
1）Mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good, can remove blackhead, pore refining, deep clean
The significant effect of skin；Because the temperature of skin is higher, after colorful deep clean facial mask is coated on skin, interleaving agent is rapid
Failure, promote the release of toning base-material and the elite thing in continuous phase, while water-base resin forms diaphragm structure, in favor of maintenance
Depart from skin after end；
2）The colorful deep clean facial mask color of painting type appears, pleasing, gives the enjoyment of U.S.；And use green ring
Protect raw material to be made, will not have a negative impact to human body and environment；
3）The mature preparation process of facial mask, adapt to industrialized production.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described.
Obviously, described embodiment is only the part of the present invention, and based on the embodiment in the present invention, those skilled in the art exist
The every other embodiment obtained under the premise of creative work is not made, belongs to the scope of protection of the invention.
Embodiment 1
A kind of colorful deep clean facial mask of painting type is made up of the raw material of following parts by weight：400 parts of base-material of toning, interleaving agent 250
Part, 350 parts of continuous phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：442 parts of deionized water, 9,221 350 parts of Carfil, silicic acid
100 parts of the magnesium lithium aqueous solution, 25 parts of 1,2-PD, 4 parts of salicylic acid, 10 parts of Sodium Hyaluronate, 33 35 parts of Aculyn, three ethanol
30 parts of amine, 3.2 parts of Phenoxyethanol, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
Grey and the compound method of white basic material are identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and are configured to
Grey base-material, 99.8 parts of base-materials add 0.2 part of white dye and are configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,2-PD, water
Poplar acid, Sodium Hyaluronate, disodium ethylene diamine tetraacetate, Phenoxyethanol, is stirred 30 minutes；
2）Carfil 9221 and the lithium magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of lithium magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 500 revs/min of rotating speed；
2）The lithium magnesium silicate powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus lithium magnesium silicate powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：663 parts of deionized water, 9,221 280 parts of Carfil, third
25 parts of triol, 5 parts of salicylic acid, 12 parts of Sodium Hyaluronate, 21 5 parts of carbomer Carbopol Ultrez, hydroxyethyl cellulose
1 part of 250HBR, 3 parts of Phenoxyethanol, 5 parts of AMP-95,1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds glycerine, bigcatkin willow
Acid, Sodium Hyaluronate, disodium ethylene diamine tetraacetate, Phenoxyethanol, stir 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful deep clean facial mask of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）The toning base-material of formula ratio is directly added into the lithium magnesium silicate aqueous solution by comminutor, gained particle, granulation terminates
After continue stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful depth of painting type
Cleaning pack 1.
Embodiment 2
A kind of colorful deep clean facial mask of painting type is made up of the raw material of following parts by weight：500 parts of base-material of toning, interleaving agent 200
Part, 400 parts of continuous phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：461 parts of deionized water, 9,221 320 parts of Carfil, silicic acid
The magnalium aqueous solution（Interleaving agent）100 parts, 25 parts of 1,2-PD, 5 parts of tartaric acid, 20 parts of vitamin K, Vesmody A901 35
Part, 30 parts of triethanolamine, 3 parts of propylben, 1 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, blueness, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of grey, blueness and white basic material is identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and matched somebody with somebody
Grey base-material is made, 99.8 parts of base-materials add 0.2 part of blue dyes and prepare au bleu base-material, and 99.8 parts of base-materials add 0.2 part in vain
Color dyestuff is configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,2-PD, fruit
Acid, vitamin K, disodium ethylene diamine tetraacetate, Phenoxyethanol, stir 30 minutes；
2）Carfil 9221 and the aluminium-magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of aluminium-magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 500 revs/min of rotating speed；
2）The magnesium silicate aluminium powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus magnesium silicate aluminium powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：675 parts of deionized water, 9,221 280 parts of Carfil, third
25 parts of triol, 5 parts of tartaric acid, 20 parts of vitamin K, 1 part of 21 5 parts of Carbopol Ultrez, 250HBR, propylben 3
Part, 5 parts of AMP-95,1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, controls 800 revs/min of rotating speed, sequentially adds glycerine, tartaric acid,
Vitamin, disodium ethylene diamine tetraacetate, propylben, stir 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful deep clean facial mask of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）The toning base-material of formula ratio is directly added into the aluminium-magnesium silicate aqueous solution by comminutor, gained particle, granulation terminates
After continue stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful depth of painting type
Cleaning pack 2.
Embodiment 3
A kind of colorful deep clean facial mask of painting type is made up of the raw material of following parts by weight：450 parts of base-material of toning, interleaving agent 300
Part, 300 parts of continuous phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：457 parts of deionized water, 9,220 350 parts of Carfil, S-
482 solution（Interleaving agent）100 parts, 20 parts of 1,2-PD, 5 parts of glycerine, 4 parts of salicylic acid, 15 parts of medical collagen,
30 parts of Vesmody A901,26 parts of triethanolamine, 3.2 parts of methyl hydroxybenzoate, 0.8 part of five sodium of diethylene triamine pentacetic acid (DTPA).
The dyestuff is yellow, red, blue food-grade transparency dye.
Toning base-material preparation process be：
1）100 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.2 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of red and blue base-material is identical with yellow base-material, and 199.6 parts of base-materials add 0.4 part of orchil and are configured to
Red base-material, 149.7 parts of base-materials add 0.3 part of gray dyes and prepare grey base-material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, controls 800 revs/min of rotating speed, sequentially adds 1,2-PD, third
Triol, salicylic acid, medical collagen, the sodium of diethylene triamine pentacetic acid (DTPA) five, Phenoxyethanol, stir 30 minutes；
2）Carfil 9221 and S-482 solution are sequentially added, is stirred 30 minutes；
3）Vesmody A901 are added, are stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of S-482 powder, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 500 revs/min of rotating speed；
2）The S-482 powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus S-482 powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：666 parts of deionized water, 9,221 280 parts of Carfil, 1,
25 parts of 2- propane diols, 5 parts of glycerine, 4 parts of salicylic acid, 15 parts of medical collagen, 21 5 parts of Carbopol Ultrez,
1 part of 250HBR, 3 parts of methyl hydroxybenzoate, 5 parts of AMP-95,1 part of five sodium of diethylene triamine pentacetic acid (DTPA).
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, controls 800 revs/min of rotating speed, sequentially adds 1,2-PD, third
Triol, salicylic acid, medical collagen, the sodium of diethylene triamine pentacetic acid (DTPA) five and methyl hydroxybenzoate, stir 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful deep clean facial mask of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）The toning base-material of formula ratio is directly added into the S482 aqueous solution by comminutor, gained particle, it is follow-up to be granulated end
Continuous stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful depth of painting type
Cleaning pack 3.
Use feeling and deep clean efficacy assessments, tool are carried out to the embodiment 1-3 colorful deep clean facial mask of painting type
Body examination method for testing is as follows：
Each test group chooses 20 female volunteers, age 20-40 year, face, and nose has a certain degree blackhead, and pore is thick
Greatly, health is good when tested, altogether 60 people.Application method：After volunteer cleans face, tested facial mask is evenly coated with
In left face as test section, right face is without test, area as a comparison.Facial mask is thrown off after 20 minutes.Experiment facial mask uses every other day,
After continuing 3 months, use feeling investigation is carried out to volunteer, evaluation is divided into 5 grades：More than 90% subject is satisfied with, and comments 5 points；
80%-90% subject is satisfied with, and comments 4 points；70%-80% subject is satisfied with, and comments 3 points；60-70% subject is satisfied with, and comments 2 points；It is less than
60% subject is satisfied with, and comments 1 point.Evaluation result is classified as table 1.
The use feeling evaluation of the colorful deep clean facial masks of the embodiment 1-3 of table 1.
As it can be seen from table 1 the made colorful deep clean facial masks of embodiment 1-3 can effectively remove blackhead, pore refining, depth is clear
Clean skin effects are notable, and good permeability is small to skin irritation, easily torn off after completing skin care from face.
It is described above, be only presently preferred embodiments of the present invention, any formal limitation not done to the present invention, therefore it is all not
Depart from the content of technical solution of the present invention, according to the present invention technical spirit to any simple modification made for any of the above embodiments,
Equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (9)
- A kind of 1. colorful deep clean facial mask of painting type, it is characterised in that：It is made up of the raw material of following parts by weight：Toning base-material 400-500 parts, interleaving agent 200-300 parts and continuous phase 300-400 parts；Described interleaving agent by following parts by weight raw material group Into：Deionized water 850-950 parts, insulating powder 50-150 parts, preservative 1-3 parts；The continuous phase by following parts by weight raw material Composition：Deionized water 600-750 parts, water-base resin 200-400 parts, cleaning agent 2-10 parts, pore astringent 5-20 parts, NMF 10-30 parts, thickener 3-15 parts, preservative 3-5 parts, pH adjusting agent 0-5 parts, complexing agent 0.2-1 parts.
- 2. the colorful deep clean facial mask of painting type according to claim 1, it is characterised in that：Described insulating powder is silicic acid One or more of compositions in magnesium lithium, aluminium-magnesium silicate, S482；Described preservative is Kathon CG, Phenoxyethanol, Metagin Ester, one or more of compositions in propylben.
- 3. the colorful deep clean facial mask of painting type according to claim 1 or 2, it is characterised in that：Described interleaving agent Preparation process is：1）The deionized water of formula ratio is put into reactor, controls 400-500 revs/min of rotating speed；2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring 30-40 minutes to dissolving；3）Surplus insulating powder is put into reactor, 30-40 minutes are stirred under same rotational speed, interleaving agent is made.
- 4. the colorful deep clean facial mask of painting type according to claim 1 or 2, it is characterised in that：Described water-base resin For one or both of Carfil 9221 or Carfil 9220；Described cleaning agent is one in salicylic acid and tartaric acid Kind or two kinds of composition；The pore astringent is Sodium Hyaluronate, vitamin K, one kind or several in medical collagen The composition of kind；The NMF is 1,2-PD, glycerine, ethylene glycol, sorbierite, one or more of in butanediol Composition；Described thickener is guar gum, carbomer, sodium carboxymethylcellulose, hydroxyethyl cellulose, in hydroxypropyl cellulose One or more of compositions；Described pH adjusting agent is diethanol amine, triethanolamine, one or more of in AMP-95 Composition；Described complexing agent is disodium ethylene diamine tetraacetate, one kind in the sodium of diethylene triamine pentacetic acid (DTPA) five；Described anti-corrosion Agent is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
- 5. the colorful deep clean facial mask of painting type according to claim 1 or 2, it is characterised in that：The system of the continuous phase It is for step：1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, clearly Clean dose, pore astringent, complexing agent and preservative, stir 30-40 minutes；2）Water-base resin is added, stirs 15-20 minutes；3）Thickener is slowly added to, stirs 30-40 minutes；4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces continuous phase.
- 6. the colorful deep clean facial mask of painting type according to claim 1 or 2, it is characterised in that：It is described toning base-material by The raw material composition of following parts by weight：Base-material 980-1000 parts, dyestuff 0-20 parts；Described base-material by following parts by weight original Material composition：Deionized water 350-550 parts, water-base resin 300-500 parts, interleaving agent 50-150 parts, cleaning agent 2-10 parts, pore are received Hold back agent 5-20 parts, NMF 10-30 parts, thickener 20-80 parts, pH adjusting agent 0-50 parts, preservative 3-5 parts, complexing agent 0.2-1 Part；The dyestuff is assorted food-grade or cosmetics-stage transparency dye.
- 7. the colorful deep clean facial mask of painting type according to claim 6, it is characterised in that：In base-material, described is water-based Resin is one or both of Carfil 9221 or Carfil 9220；Described cleaning agent is in salicylic acid and tartaric acid One or two kinds of compositions；The pore astringent is Sodium Hyaluronate, vitamin K, one kind in medical collagen Or several composition；The NMF is 1,2-PD, glycerine, ethylene glycol, sorbierite, one kind or several in butanediol The composition of kind；Described thickener is Aculyn 33, one kind or several in Vesmody A901, Vesmody A406 The composition of kind；Described pH adjusting agent is diethanol amine, triethanolamine, one or more of compositions in AMP-95；Institute The complexing agent stated is disodium ethylene diamine tetraacetate, one kind in the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
- 8. the colorful deep clean facial mask of painting type according to claim 6, it is characterised in that：The preparation of described base-material Cheng Wei：1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, clearly Clean dose, pore astringent, complexing agent and preservative, stir 30-40 minutes；2）Water-base resin is added, stirs 15-20 minutes；3）Thickener and interleaving agent are slowly added to, stirs 30-40 minutes；4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces base-material；The preparation process of described toning base-material is：1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；2）The dyestuff of formula ratio is separately added into, 20-30 minutes is stirred, produces toning base-material.
- A kind of 9. method of the colorful deep clean facial mask of painting type prepared as described in claim 1-2, it is characterised in that：Including Step as described below：1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；2）The toning base-material of formula ratio is directly added into interleaving agent by comminutor, gained particle, granulation continues to stir after terminating Mix 10-15 minutes；3）Continuous phase is slowly added to reactor, 20-30 minutes are stirred with 100-150 revs/min of speed.It is more to produce painting type Color deep clean facial mask.
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| CN201710538655.8A CN107334657A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful deep clean facial mask of painting type and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710538655.8A CN107334657A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful deep clean facial mask of painting type and preparation method thereof |
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| CN107334657A true CN107334657A (en) | 2017-11-10 |
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| CN201710538655.8A Pending CN107334657A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful deep clean facial mask of painting type and preparation method thereof |
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| EP1608330A1 (en) * | 2003-04-01 | 2005-12-28 | MGP Ingredients Inc | Skin-tightening preparations containing gliadin |
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Address after: 350100 first and second floors of No.1 Workshop, No.1 East Road, phase I, Minhou economic and Technological Development Zone, Jingxi Town, Minhou County, Fuzhou City, Fujian Province Applicant after: FUJIAN HUAXIALAN NEW MATERIAL TECHNOLOGY CO., LTD. Address before: Near East Taihe square in Jinan District of Fuzhou city in Fujian province 350011 SOHO office building No. 3 room 308-313 Applicant before: FUJIAN HUAXIALAN NEW MATERIAL TECHNOLOGY CO., LTD. |
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