CN107213034A - A kind of colorful moisture saver mask of painting type and preparation method thereof - Google Patents
A kind of colorful moisture saver mask of painting type and preparation method thereof Download PDFInfo
- Publication number
- CN107213034A CN107213034A CN201710376562.XA CN201710376562A CN107213034A CN 107213034 A CN107213034 A CN 107213034A CN 201710376562 A CN201710376562 A CN 201710376562A CN 107213034 A CN107213034 A CN 107213034A
- Authority
- CN
- China
- Prior art keywords
- parts
- minutes
- base
- colorful
- added
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/87—Polyurethanes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses colorful moisture saver mask of a kind of painting type and preparation method thereof.The present invention the colorful moisture saver mask of painting type according to weight than each group be divided into：Toning base-material：400 500 parts, interleaving agent：200 300 parts, continuous phase：300 400 parts.The colorful moisture saver mask color of painting type of the present invention appears, pleasing, gives the enjoyment of U.S.；The facial mask uses the raw material of environmental protection, will not have a negative impact to human body and environment；The mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good；The mature preparation process of the facial mask, adapts to industrialized production.
Description
Technical field
The invention belongs to field of fine chemical, and in particular to a kind of colorful moisture saver mask of painting type and preparation method thereof.
Background technology
Nowadays, with the raising of people's quality of the life and to beautiful pursuit, more and more people's selections are maintained using facial mask
Skin.Facial mask is a kind of carrier of face beautifying health keeping product, and sufficient moisture and nutriment can be provided to skin, can be skin
The effects such as moisturizing is brightened, is loved by people.Now facial mask on the market at most be sticking type facial mask.Sticking type facial mask is to make
With non-woven fabrics etc. as matrix, infiltrate Essence etc. and spread on skin.The subject matter that this mode is present is due to individual difference
Different, facial mask can not completely fit with skin.Daubing-type facial mask solves this problem.In use, cream pack is uniformly smeared
Finish, can tear in flakes on skin, treating that Essence absorbs.The daubing-type facial mask of all kinds of brands is a feast for the eyes on the market.In order to
Win the market, manufacturers, which try one's best, makes miscellaneous product.They are formulated health environment-friendly, effect different properties, bag
Fill elegant in appearance.By contrast, the state of the content that consumer more takes notice of in itself, which but has no characteristic, to be sayed.Now, on the market
Daubing-type facial mask be transparent or monochromatic lotion.The homogeneity of product appearance allows consumer to have no way of selecting.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of colorful moisture saver mask of painting type and its preparation
Method.The colorful moisture saver mask color of the painting type appears, pleasing, gives the enjoyment of U.S.；And use environmental protection
Raw material, will not have a negative impact to human body and environment；Patch skin is good when using, and adhesion is moderate, and film forming is fast, pliability
It is good；Mature preparation process, adapts to industrialized production.
To achieve the above object, the present invention is adopted the following technical scheme that：
A kind of colorful moisture saver mask of painting type, is made up of the raw material of following parts by weight：400-500 parts of base-material of toning, interleaving agent
200-300 parts and 300-400 parts of continuous phase.
Described interleaving agent is made up of the raw material of following parts by weight：850-950 parts of deionized water, 50-150 parts of insulating powder,
1-3 parts of preservative.
Described insulating powder is lithium magnesium silicate, aluminium-magnesium silicate, S482 one or more of compositions；Described preservative
For Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
The preparation process of described interleaving agent is：
1）The deionized water of formula ratio is put into reactor, 400-500 revs/min of rotating speed is controlled；
2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring is extremely dissolved for 30-40 minutes；
3）Surplus insulating powder is put into reactor, is stirred 30-40 minutes under same rotational speed.
The continuous phase is made up of the raw material of following parts by weight：600-750 parts of deionized water, 200-400 parts of water-base resin,
20-50 parts of NMF, 3-15 parts of thickener, 3-5 parts of preservative, 0-5 parts of pH adjusting agent, 0.2-1 parts of complexing agent.
In continuous phase, described water-base resin is one or both of Carfil 9221 or Carfil 9220；
Described NMF is 1,3-PD, glycerine, ethylene glycol, sorbierite, one or more of compositions in butanediol；Institute
The thickener stated is guar gum, carbomer, sodium carboxymethylcellulose, hydroxyethyl cellulose, one kind in hydroxypropyl cellulose or
Several compositions；Described pH adjusting agent is diethanol amine, and triethanolamine, CP-950 is one or more of in AMP-95
Composition；Described complexing agent is one kind in disodium ethylene diamine tetraacetate, the sodium of diethylene triamine pentacetic acid (DTPA) five；Described anti-corrosion
Agent is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
The preparation process of the continuous phase is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, network
Mixture and preservative, are stirred 30-40 minutes；
2）Water-base resin is added, is stirred 15-20 minutes；
3）Thickener is slowly added to, is stirred 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7, stirs 20-30 minutes, produces continuous phase.
Described toning base-material is made up of the raw material of following parts by weight：980-1000 parts of base-material, 0-20 parts of dyestuff；It is described
Base-material be made up of the raw material of following parts by weight：350-550 parts of deionized water, 300-500 parts of water-base resin, interleaving agent 50-
150 parts, 20-50 parts of NMF, 20-80 parts of thickener, 0-50 parts of pH adjusting agent, 3-5 parts of preservative, 0.2-1 parts of complexing agent；Institute
It is assorted food-grade or cosmetics-stage transparency dye to state dyestuff.
In base-material, described water-base resin is one or both of Carfil 9221 or Carfil 9220；Institute
The NMF stated is 1,3-PD, glycerine, ethylene glycol, sorbierite, one or more of compositions in butanediol；It is described
Thickener be Aculyn 33, one or more of compositions in Vesmody A901, Vesmody A406；It is described
PH adjusting agent be diethanol amine, triethanolamine, CP-950, one or more of compositions in AMP-95；Described complexing
Agent is one kind in disodium ethylene diamine tetraacetate, the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is Kathon CG, benzene oxygen second
One or more of compositions in alcohol, methyl hydroxybenzoate, propylben.
The preparation process of described base-material is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, network
Mixture and preservative, are stirred 30-40 minutes；
2）Water-base resin is added, is stirred 15-20 minutes；
3）Thickener and interleaving agent are slowly added to, is stirred 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7, stirs 20-30 minutes, produces base-material；
The preparation process of described toning base-material is：
1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；
2）The dyestuff of formula ratio is separately added into, stirs 20-30 minutes, produces toning base-material.
A kind of method for preparing the colorful moisture saver mask of painting type as described above, including step as described below：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into interleaving agent, and granulation continues to stir after terminating
Mix 10-15 minutes；
3）Continuous phase is slowly added to reactor, stirred 20-30 minutes with 100-150 revs/min of speed.Produce painting type many
Color moisture saver mask.
The beneficial effects of the present invention are：
1）Mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good；Because the temperature of skin is higher, colorful moisture saver mask
After being coated on skin, interleaving agent fails rapidly, promotes the release of toning base-material and the elite thing in continuous phase, while aqueous
Resin formation diaphragm structure, departs from skin after terminating in favor of maintenance；
2）The colorful moisture saver mask color of painting type appears, pleasing, gives the enjoyment of U.S.；And it is former using environmental protection
Material is made, and will not have a negative impact to human body and environment；
3）The mature preparation process of facial mask, adapts to industrialized production.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described.
Obviously, described embodiment is only the part of the present invention, and based on the embodiment in the present invention, those skilled in the art exist
The every other embodiment obtained under the premise of creative work is not made, the scope of protection of the invention is belonged to.
Embodiment 1
A kind of colorful moisture saver mask of painting type is made up of the raw material of following parts by weight：400 parts of base-material of toning, 250 parts of interleaving agent, even
Continuous 350 parts of phase.
Base-material is specifically made up of the raw material of following parts by weight：450 parts of deionized water, 9,221 350 parts of Carfil, silicic acid
The magnesium lithium aqueous solution（Interleaving agent）100 parts, 25 parts of 1,3-PD, 6 parts of glycerine, 33 35 parts of Aculyn, 30 parts of triethanolamine,
3.2 parts of Phenoxyethanol, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
Grey and the compound method of white basic material are identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and are configured to
Grey base-material, 99.8 parts of base-materials add 0.2 part of white dye and are configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,3-PD, third
Triol, disodium ethylene diamine tetraacetate, Phenoxyethanol is stirred 30 minutes；
2）Carfil 9221 and the lithium magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of lithium magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, 500 revs/min of rotating speed is controlled；
2）The lithium magnesium silicate powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus lithium magnesium silicate powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：670 parts of deionized water, 9,221 280 parts of Carfil, 1,
30 parts of ammediol（NMF）, 5 parts of glycerine（NMF）, 21 5 parts of carbomer Carbopol Ultrez, ethoxy fibre
Tie up 1 part of element 250HBR, 3 parts of Phenoxyethanol（Preservative）, 5 parts of AMP-95（PH adjusting agent）, 1 part of disodium ethylene diamine tetraacetate
（Complexing agent）.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,3-PD, third
Triol, disodium ethylene diamine tetraacetate, Phenoxyethanol is stirred 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful moisture saver mask of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into the lithium magnesium silicate aqueous solution, and granulation terminates
Continue to stir 10 minutes afterwards；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful moisturizing of painting type
Facial mask 1.
Embodiment 2
A kind of colorful moisture saver mask of painting type is made up of the raw material of following parts by weight：500 parts of base-material of toning, 200 parts of interleaving agent, even
Continuous 400 parts of phase.
Base-material is specifically made up of the raw material of following parts by weight：450 parts of deionized water, 9,221 320 parts of Carfil, silicic acid
The magnalium aqueous solution（Interleaving agent）100 parts, 30 parts of 1,3-PD, 5 parts of glycerine, 35 parts of Vesmody A901, triethanolamine
30 parts, 3 parts of propylben, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, blueness, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of grey, blueness and white basic material is identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and matched somebody with somebody
Grey base-material is made, 99.8 parts of base-materials add 0.2 part of blue dyes and prepare au bleu base-material, and 99.8 parts of base-materials add 0.2 part in vain
Color dyestuff is configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,3-PD, third
Triol, disodium ethylene diamine tetraacetate, Phenoxyethanol is stirred 30 minutes；
2）Carfil 9221 and the aluminium-magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of aluminium-magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, 500 revs/min of rotating speed is controlled；
2）The magnesium silicate aluminium powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus magnesium silicate aluminium powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：670 parts of deionized water, 9,221 280 parts of Carfil, 1,
30 parts of ammediol, 5 parts of glycerine, 21 5 parts of Carbopol Ultrez, 1 part of 250HBR, 3 parts of propylben, AMP-95
5 parts, 1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,3-PD, third
Triol, disodium ethylene diamine tetraacetate, propylben is stirred 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful moisture saver mask of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into the aluminium-magnesium silicate aqueous solution, and granulation terminates
Continue to stir 10 minutes afterwards；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful moisturizing of painting type
Facial mask 2.
Embodiment 3
A kind of colorful moisture saver mask of painting type is made up of the raw material of following parts by weight：450 parts of base-material of toning, 300 parts of interleaving agent, even
Continuous 300 parts of phase.
Base-material is specifically made up of the raw material of following parts by weight：450 parts of deionized water, 9,220 350 parts of Carfil, S-
482 solution（Interleaving agent）100 parts, 25 parts of 1,3-PD, 6 parts of glycerine, 30 parts of Vesmody A901, triethanolamine 26
Part, 3.2 parts of methyl hydroxybenzoate, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, red, blue food-grade transparency dye.
Toning base-material preparation process be：
1）100 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.2 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of red and blue base-material is identical with yellow base-material, and 199.6 parts of base-materials add 0.4 part of orchil and are configured to
Red base-material, 149.7 parts of base-materials add 0.3 part of gray dyes and prepare grey base-material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,3-PD, third
Triol, disodium ethylene diamine tetraacetate, Phenoxyethanol is stirred 30 minutes；
2）Carfil 9221 and S-482 solution are sequentially added, is stirred 30 minutes；
3）Vesmody A901 are added, are stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of S-482 powder, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, 500 revs/min of rotating speed is controlled；
2）The S-482 powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus S-482 powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：670 parts of deionized water, 9,221 280 parts of Carfil, 1,
30 parts of ammediol, 5 parts of glycerine, 21 5 parts of Carbopol Ultrez, 1 part of 250HBR, 3 parts of methyl hydroxybenzoate, AMP-95
5 parts, 1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,3-PD, third
Triol, disodium ethylene diamine tetraacetate and methyl hydroxybenzoate, are stirred 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful moisture saver mask of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into the S482 aqueous solution, and granulation terminates follow-up
Continuous stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful moisturizing of painting type
Facial mask 3.
Use feeling and moisture-keeping efficacy evaluation, specific test side are carried out to the embodiment 1-3 colorful moisture saver mask of painting type
Method is as follows：
Each test group chooses 20 female volunteers, age 20-35 Sui, skin health, and health is good when tested, amounts to
60 people.Application method：Volunteer is cleaned after face, tested facial mask is homogeneously applied to left face as test section, right face conduct
Contrast district, facial mask is thrown off after 15 minutes, using moisture of skin tester, carries out left face and right face skin respectively at regular intervals
Water content is tested, and using each cell mean as test result, is classified as table 1.And use feeling investigation is carried out to volunteer, evaluate and divide
For 5 grades：More than 90% subject is satisfied with, and comments 5 points；80%-90% subject is satisfied with, and comments 4 points；70%-80% subject is satisfied with,
Comment 3 points；60-70% subject is satisfied with, and comments 2 points；Less than 60% subject satisfaction, 1 point is commented.Evaluation result is classified as table 2.
The moisture content of skin evaluation of the colorful moisture saver mask of embodiment 1-3 of table 1.
The colorful moisture saver mask use feelings of the embodiment 1-3 of table 2. are evaluated
The test section and contrast district of contrast table 1, all test facial masks have obvious moistening effect.
From table 2 it can be seen that the made colorful moisture saver mask good permeabilities of embodiment 1-3, small to skin irritation, skin is completed
Easily torn off after skin maintenance from face, reach the purpose cleaned rapidly.
It is described above, be only presently preferred embodiments of the present invention, any formal limitation not done to the present invention, therefore it is all not
Depart from technical solution of the present invention content, according to the present invention technical spirit to it is made for any of the above embodiments it is any it is simple modification,
Equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (10)
1. a kind of colorful moisture saver mask of painting type, it is characterised in that：It is made up of the raw material of following parts by weight：Mix colours base-material 400-
500 parts, 300-400 parts of 200-300 parts of interleaving agent and continuous phase；Described interleaving agent is made up of the raw material of following parts by weight：Go
850-950 parts of ionized water, 50-150 parts of insulating powder, 1-3 parts of preservative.
2. the colorful moisture saver mask of painting type according to claim 1, it is characterised in that：Described insulating powder is magnesium silicate
One or more of compositions in lithium, aluminium-magnesium silicate, S482；Described preservative is Kathon CG, Phenoxyethanol, Metagin
One or more of compositions in ester, propylben.
3. the colorful moisture saver mask of painting type according to claim 1 or 2, it is characterised in that：The preparation of described interleaving agent
Process is：
1）The deionized water of formula ratio is put into reactor, 400-500 revs/min of rotating speed is controlled；
2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring is extremely dissolved for 30-40 minutes；
3）Surplus insulating powder is put into reactor, is stirred 30-40 minutes under same rotational speed, interleaving agent is made.
4. the colorful moisture saver mask of painting type according to claim 1 or 2, it is characterised in that：The continuous phase is by following heavy
Measure the raw material composition of part：600-750 parts of deionized water, 200-400 parts of water-base resin, 20-50 parts of NMF, thickener 3-15
Part, 3-5 parts of preservative, 0-5 parts of pH adjusting agent, 0.2-1 parts of complexing agent.
5. the colorful moisture saver mask of painting type according to claim 4, it is characterised in that：Described water-base resin is Carfil
One or both of 9221 or Carfil 9220；Described NMF be 1,3-PD, glycerine, ethylene glycol,
One or more of compositions in sorbierite, butanediol；Described thickener is guar gum, carbomer, carboxymethyl cellulose
One or more of compositions in sodium, hydroxyethyl cellulose, hydroxypropyl cellulose；Described pH adjusting agent is diethanol amine,
One or more of compositions in triethanolamine, CP-950, AMP-95；Described complexing agent is disodium ethylene diamine tetraacetate,
One kind in the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, nipalgin third
One or more of compositions in ester.
6. the colorful moisture saver mask of painting type according to claim 4, it is characterised in that：The preparation process of the continuous phase
For：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, network
Mixture and preservative, are stirred 30-40 minutes；
2）Water-base resin is added, is stirred 15-20 minutes；
3）Thickener is slowly added to, is stirred 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7, stirs 20-30 minutes, produces continuous phase.
7. the colorful moisture saver mask of painting type according to claim 1 or 2, it is characterised in that：The toning base-material is by following
The raw material composition of parts by weight：980-1000 parts of base-material, 0-20 parts of dyestuff；Described base-material by following parts by weight raw material group
Into：350-550 parts of deionized water, 300-500 parts of water-base resin, 50-150 parts of interleaving agent, 20-50 parts of NMF, thickener 20-
80 parts, 0-50 parts of pH adjusting agent, 3-5 parts of preservative, 0.2-1 parts of complexing agent；The dyestuff is assorted food-grade or cosmetics-stage
Transparency dye.
8. the colorful moisture saver mask of painting type according to claim 7, it is characterised in that：In base-material, described water-base resin
For one or both of Carfil 9221 or Carfil 9220；Described NMF be 1,3-PD, glycerine,
One or more of compositions in ethylene glycol, sorbierite, butanediol；Described thickener is Aculyn 33, Vesmody
One or more of compositions in A901, Vesmody A406；Described pH adjusting agent be diethanol amine, triethanolamine,
One or more of compositions in CP-950, AMP-95；Described complexing agent is disodium ethylene diamine tetraacetate, diethylenetriamine
One kind in the sodium of pentaacetic acid five；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one kind in propylben
Or several compositions.
9. the colorful moisture saver mask of painting type according to claim 7, it is characterised in that：The preparation process of described base-material
For：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, network
Mixture and preservative, are stirred 30-40 minutes；
2）Water-base resin is added, is stirred 15-20 minutes；
3）Thickener and interleaving agent are slowly added to, is stirred 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7, stirs 20-30 minutes, produces base-material；
The preparation process of described toning base-material is：
1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；
2）The dyestuff of formula ratio is separately added into, stirs 20-30 minutes, produces toning base-material.
10. a kind of method of the colorful moisture saver mask of the painting type prepared as described in claim 1-2, it is characterised in that：Including such as
Under the step：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into interleaving agent, and granulation continues to stir after terminating
Mix 10-15 minutes；
3）Continuous phase is slowly added to reactor, stirred 20-30 minutes with 100-150 revs/min of speed.Produce painting type many
Color moisture saver mask.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710376562.XA CN107213034A (en) | 2017-05-25 | 2017-05-25 | A kind of colorful moisture saver mask of painting type and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710376562.XA CN107213034A (en) | 2017-05-25 | 2017-05-25 | A kind of colorful moisture saver mask of painting type and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107213034A true CN107213034A (en) | 2017-09-29 |
Family
ID=59944559
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710376562.XA Pending CN107213034A (en) | 2017-05-25 | 2017-05-25 | A kind of colorful moisture saver mask of painting type and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107213034A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1608330A1 (en) * | 2003-04-01 | 2005-12-28 | MGP Ingredients Inc | Skin-tightening preparations containing gliadin |
| CN102772345A (en) * | 2012-06-29 | 2012-11-14 | 安徽省王巢食品有限公司 | All-natural bee pollen facial mask paste and production method thereof |
| CN103181861A (en) * | 2011-12-30 | 2013-07-03 | 广东雅威生物科技有限公司 | Bubble facial mask and preparation process thereof |
| CN104688621A (en) * | 2015-03-02 | 2015-06-10 | 上海卡卡化妆品有限公司 | Self-foaming cosmetic composition and preparation method thereof |
| CN105168054A (en) * | 2015-09-17 | 2015-12-23 | 长沙九超生物科技有限公司 | Mask capable of supplementing water, whitening and removing wrinkles and preparation method of mask |
-
2017
- 2017-05-25 CN CN201710376562.XA patent/CN107213034A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1608330A1 (en) * | 2003-04-01 | 2005-12-28 | MGP Ingredients Inc | Skin-tightening preparations containing gliadin |
| CN103181861A (en) * | 2011-12-30 | 2013-07-03 | 广东雅威生物科技有限公司 | Bubble facial mask and preparation process thereof |
| CN102772345A (en) * | 2012-06-29 | 2012-11-14 | 安徽省王巢食品有限公司 | All-natural bee pollen facial mask paste and production method thereof |
| CN104688621A (en) * | 2015-03-02 | 2015-06-10 | 上海卡卡化妆品有限公司 | Self-foaming cosmetic composition and preparation method thereof |
| CN105168054A (en) * | 2015-09-17 | 2015-12-23 | 长沙九超生物科技有限公司 | Mask capable of supplementing water, whitening and removing wrinkles and preparation method of mask |
Non-Patent Citations (2)
| Title |
|---|
| 化工百科全书编委会: "《化工百科全书 第7卷 核能技术-计算机技术》", 30 September 1994, 化学工业出版社 * |
| 董艳: "《化学与健康消费》", 31 August 2008, 中国石油大学出版社 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108030704B (en) | Plant hair dye with graphene oxide as dyeing assistant and preparation method thereof | |
| CN1201718C (en) | Hair dyeing composition | |
| CN108451780A (en) | A kind of washable hair dye and preparation method thereof | |
| US20150366763A1 (en) | Eyeliner Decal Composition and Method of Use | |
| CN107541160B (en) | Low-temperature quick-drying high-adhesion high-speed cigarette lap adhesive and preparation process thereof | |
| CN105176170B (en) | A kind of aqueous acrylamide drawing pigment and preparation method thereof | |
| CN102952431A (en) | Cigarette tipping paper water-based ink and preparation method | |
| CN107496187A (en) | A kind of cosmetic pigment powder for pasting the fabulous hydrophobic oleophobic of skin and its preparation method and application | |
| CN107286745A (en) | A kind of environmentally friendly fast-drying aqueous ink | |
| CN101864210A (en) | Alcohol-soluble printing ink and preparation method thereof | |
| CN104194004A (en) | A green synthesis method of a nanometer silver-sodium alginate composition | |
| CN104861778A (en) | Water-based ink for grainy paper printing and preparation method thereof | |
| CN101869536B (en) | Gallic acid hair dyes and preparation method and application thereof | |
| CN107982072A (en) | The water-based eye-liner and preparation method of a kind of graphene-containing | |
| CN107213034A (en) | A kind of colorful moisture saver mask of painting type and preparation method thereof | |
| CN102286223B (en) | Pigment composition for drawing of children and preparation method thereof | |
| CN106349811A (en) | Six-color full-color soft printing ink and preparation method thereof | |
| CN101935486A (en) | PVC (polyvinyl chloride) artificial leather pigment color paste | |
| JP3074443B2 (en) | Mashike coloring hair dye | |
| CN1600983A (en) | Printing paste and preparation method | |
| CN107137240A (en) | A kind of colorful cleawhite pack of painting type and preparation method thereof | |
| CN102492373B (en) | Starch gum and preparation method and application thereof | |
| CN102048670B (en) | Natural plant hair dye | |
| CN107334647A (en) | A kind of colorful anti-wrinkle face mask of painting type and preparation method thereof | |
| CN107334657A (en) | A kind of colorful deep clean facial mask of painting type and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information | ||
| CB02 | Change of applicant information |
Address after: 350100 first and second floors of No.1 Workshop, No.1 East Road, phase I, Minhou economic and Technological Development Zone, Jingxi Town, Minhou County, Fuzhou City, Fujian Province Applicant after: FUJIAN HUAXIALAN NEW MATERIAL TECHNOLOGY CO., LTD. Address before: Near East Taihe square in Jinan District of Fuzhou city in Fujian province 350011 SOHO office building No. 3 room 308-313 Applicant before: FUJIAN HUAXIALAN NEW MATERIAL TECHNOLOGY CO., LTD. |
|
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170929 |