CN107334646A - A kind of colorful Deacne pack of painting type and preparation method thereof - Google Patents
A kind of colorful Deacne pack of painting type and preparation method thereof Download PDFInfo
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- CN107334646A CN107334646A CN201710538086.7A CN201710538086A CN107334646A CN 107334646 A CN107334646 A CN 107334646A CN 201710538086 A CN201710538086 A CN 201710538086A CN 107334646 A CN107334646 A CN 107334646A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/671—Vitamin A; Derivatives thereof, e.g. ester of vitamin A acid, ester of retinol, retinol, retinal
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
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Abstract
The invention discloses colorful Deacne pack of a kind of painting type and preparation method thereof.The present invention the colorful Deacne pack of painting type according to weight than each group be divided into：Toning base-material：400 500 parts, interleaving agent：200 300 parts, continuous phase：300 400 parts.The colorful Deacne pack color of painting type of the present invention appears, pleasing, gives the enjoyment of U.S.；The facial mask uses green raw material, will not have a negative impact to human body and environment；The mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good, small to skin irritation, and anti-acne effect is notable；The mature preparation process of the facial mask, adapt to industrialized production.
Description
Technical field
The invention belongs to field of fine chemical, and in particular to a kind of colorful Deacne pack of painting type and preparation method thereof.
Background technology
Nowadays, as the raising of people's quality of the life and the pursuit to U.S., more and more people's selections are maintained using facial mask
Skin.Deacne pack is a kind of carrier of face beautifying health keeping product, and sufficient moisture and nutriment can be provided to skin, there is anti-acne
Many effects such as skin lightening, are loved by people.Deacne pack on the market is mostly sticking type facial mask now.Sticking type face
Film is to use non-woven fabrics etc. to be used as matrix, infiltration Essence etc. to spread on skin.Subject matter existing for this mode is due to
Individual difference, facial mask can not be bonded completely with skin.Daubing-type facial mask solves this problem.It is in use, cream pack is equal
It is even to be applied on skin, treat that Essence absorbs and finish, can tear in flakes.The painting type Deacne pack beautiful jade of all kinds of brands on the market
Thinkling sound meets the eye on every side.In order to win the market, manufacturers, which try one's best, makes miscellaneous product.They are formulated health environment-friendly, packaging
It is elegant in appearance.By contrast, the visual effect of the content that consumer more takes notice of in itself, which but has no characteristic, to be sayed.Now, market
On daubing-type facial mask be transparent or monochromatic lotion.Product colour is single, can not meet pursuit of the consumer to U.S..
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of colorful Deacne pack of painting type and its preparation
Method.The colorful Deacne pack color of the painting type appears, pleasing, gives the enjoyment of U.S.；And using green
Raw material, will not have a negative impact to human body and environment；Patch skin is good during use, and adhesion is moderate, and film forming is fast, pliability
Good, small to skin irritation, anti-acne effect is notable；Mature preparation process, adapt to industrialized production.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of colorful Deacne pack of painting type, is made up of the raw material of following parts by weight：Toning base-material 400-500 parts, interleaving agent
200-300 parts and continuous phase 300-400 parts.
Described interleaving agent is made up of the raw material of following parts by weight：Deionized water 850-950 parts, insulating powder 50-150 parts,
Preservative 1-3 parts.
Described insulating powder is lithium magnesium silicate, aluminium-magnesium silicate, S482 one or more of compositions；Described preservative
For Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
The preparation process of described interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 400-500 revs/min of rotating speed；
2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring 30-40 minutes to dissolving；
3）Surplus insulating powder is put into reactor, 30-40 minutes are stirred under same rotational speed.
The continuous phase is made up of the raw material of following parts by weight：Deionized water 600-750 parts, water-base resin 200-400 parts,
Acne removing agent 1-5 parts, anti-freckle agent 10-30 parts, thickener 3-15 parts, preservative 3-5 parts, pH adjusting agent 0-5 parts, complexing agent 0.2-1
Part.
In continuous phase, described water-base resin is one or both of Carfil 9221 or Carfil 9220；
Described acne removing agent is all-trans retinoic acid, one or more of compositions in azelaic acid and salicylic acid；The anti-freckle agent is urine
The composition of one or both of Bursin, medical collagen；Described thickener is guar gum, carbomer, and carboxymethyl is fine
Tie up plain sodium, hydroxyethyl cellulose, one or more of compositions in hydroxypropyl cellulose；Described pH adjusting agent is diethanol
Amine, triethanolamine, one or more of compositions in CP-950, AMP-95；Described complexing agent is ethylenediamine tetra-acetic acid two
Sodium, one kind in the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, nipalgin
One or more of compositions in propyl ester.
The preparation process of the continuous phase is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds acne removing agent, dispel
Spot agent, complexing agent and preservative, stir 30-40 minutes；
2）Water-base resin is added, stirs 15-20 minutes；
3）Thickener is slowly added to, stirs 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces continuous phase.
Described toning base-material is made up of the raw material of following parts by weight：Base-material 980-1000 parts, dyestuff 0-20 parts；It is described
Base-material be made up of the raw material of following parts by weight：Deionized water 350-550 parts, water-base resin 300-500 parts, interleaving agent 50-
150 parts, acne removing agent 1-5 parts, anti-freckle agent 10-30 parts, thickener 20-80 parts, pH adjusting agent 0-50 parts, preservative 3-5 parts, complexing
Agent 0.2-1 parts；The dyestuff is assorted food-grade or cosmetics-stage transparency dye.
In base-material, described water-base resin is one or both of Carfil 9221 or Carfil 9220；Institute
The acne removing agent stated is all-trans retinoic acid, one or more of compositions in azelaic acid and salicylic acid；The anti-freckle agent is allantois
The composition of one or both of element, medical collagen；Described thickener is Aculyn 33, Vesmody A901,
One or more of compositions in Vesmody A406；Described pH adjusting agent is diethanol amine, triethanolamine, CP-
One or more of compositions in 950, AMP-95；Described complexing agent is disodium ethylene diamine tetraacetate, diethylenetriamine five
One kind in the sodium of acetic acid five；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one kind in propylben or
Several compositions.
The preparation process of described base-material is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds acne removing agent, dispel
Spot agent, complexing agent and preservative, stir 30-40 minutes；
2）Water-base resin is added, stirs 15-20 minutes；
3）Thickener and interleaving agent are slowly added to, stirs 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces base-material；
The preparation process of described toning base-material is：
1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；
2）The dyestuff of formula ratio is separately added into, 20-30 minutes is stirred, produces toning base-material.
A kind of method for preparing the colorful Deacne pack of painting type as described above, including step as described below：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；
2）The toning base-material of formula ratio is directly added into interleaving agent by comminutor, gained particle, granulation continues to stir after terminating
Mix 10-15 minutes；
3）Continuous phase is slowly added to reactor, 20-30 minutes are stirred with 100-150 revs/min of speed.It is more to produce painting type
Color Deacne pack.
The beneficial effects of the present invention are：
1）Mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good, small to skin irritation, and anti-acne effect is notable；By
Higher in the temperature of skin, after colorful Deacne pack is coated on skin, interleaving agent fails rapidly, promotes toning base-material and company
The release of elite thing in continuous phase, while water-base resin forms diaphragm structure, departs from skin after terminating in favor of maintenance；
2）The colorful Deacne pack color of painting type appears, pleasing, gives the enjoyment of U.S.；And use green original
Material is made, and will not have a negative impact to human body and environment；
3）The mature preparation process of facial mask, adapt to industrialized production.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described.
Obviously, described embodiment is only the part of the present invention, and based on the embodiment in the present invention, those skilled in the art exist
The every other embodiment obtained under the premise of creative work is not made, belongs to the scope of protection of the invention.
Embodiment 1
A kind of colorful Deacne pack of painting type is made up of the raw material of following parts by weight：400 parts of base-material of toning, 250 parts of interleaving agent, even
Continuous 350 parts of phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：447 parts of deionized water, 9,221 350 parts of Carfil, silicic acid
100 parts of the magnesium lithium aqueous solution, 3 parts of all-trans retinoic acid, 15 parts of allantoin, 15 parts of medical collagen, 33 35 parts of Aculyn, three
30 parts of monoethanolamine, 3.2 parts of Phenoxyethanol, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
Grey and the compound method of white basic material are identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and are configured to
Grey base-material, 99.8 parts of base-materials add 0.2 part of white dye and are configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds all-trans retinoic acid,
Allantoin, medical collagen, disodium ethylene diamine tetraacetate, Phenoxyethanol, stir 30 minutes；
2）Carfil 9221 and the lithium magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of lithium magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 500 revs/min of rotating speed；
2）The lithium magnesium silicate powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus lithium magnesium silicate powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：660 parts of deionized water, 9,221 280 parts of Carfil, entirely
3 parts of transretinoic acid, 15 parts of allantoin, 15 parts of medical collagen, 21 5 parts of carbomer Carbopol Ultrez, ethoxy
1 part of cellulose 250HBR, 3 parts of Phenoxyethanol, 5 parts of AMP-95,1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds all-trans retinoic acid,
Allantoin, medical collagen, disodium ethylene diamine tetraacetate and Phenoxyethanol, stir 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful Deacne pack of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）The toning base-material of formula ratio is directly added into the lithium magnesium silicate aqueous solution by comminutor, gained particle, granulation terminates
After continue stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful anti-acne of painting type
Facial mask 1.
Embodiment 2
A kind of colorful Deacne pack of painting type is made up of the raw material of following parts by weight：500 parts of base-material of toning, 200 parts of interleaving agent, even
Continuous 400 parts of phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：466 parts of deionized water, 9,221 320 parts of Carfil, silicic acid
The magnalium aqueous solution（Interleaving agent）100 parts, 2 parts of azelaic acid, 30 parts of medical collagen, 35 parts of Vesmody A901, three ethanol
30 parts of amine, 3 parts of propylben, 1 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, blueness, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of grey, blueness and white basic material is identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and matched somebody with somebody
Grey base-material is made, 99.8 parts of base-materials add 0.2 part of blue dyes and prepare au bleu base-material, and 99.8 parts of base-materials add 0.2 part in vain
Color dyestuff is configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds azelaic acid, medical adhesive
Former albumen, disodium ethylene diamine tetraacetate, Phenoxyethanol, stir 30 minutes；
2）Carfil 9221 and the aluminium-magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of aluminium-magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 500 revs/min of rotating speed；
2）The magnesium silicate aluminium powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus magnesium silicate aluminium powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：660 parts of deionized water, 9,221 280 parts of Carfil, nonyl
2 parts of diacid, 30 parts of medical collagen, 1 part of 21 5 parts of Carbopol Ultrez, 250HBR, 3 parts of propylben, AMP-
95 5 parts, 1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds azelaic acid, medical adhesive
Former albumen, disodium ethylene diamine tetraacetate, propylben, stir 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful Deacne pack of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）The toning base-material of formula ratio is directly added into the aluminium-magnesium silicate aqueous solution by comminutor, gained particle, granulation terminates
After continue stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful anti-acne of painting type
Facial mask 2.
Embodiment 3
A kind of colorful Deacne pack of painting type is made up of the raw material of following parts by weight：450 parts of base-material of toning, 300 parts of interleaving agent, even
Continuous 300 parts of phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：450 parts of deionized water, 9,220 350 parts of Carfil, S-
482 solution（Interleaving agent）100 parts, 2 parts of salicylic acid, 25 parts of allantoin, 30 parts of Vesmody A901,26 parts of triethanolamine, Buddhist nun
Moor 3.2 parts of tortoise beetle ester, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, red, blue food-grade transparency dye.
Toning base-material preparation process be：
1）100 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.2 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of red and blue base-material is identical with yellow base-material, and 199.6 parts of base-materials add 0.4 part of orchil and are configured to
Red base-material, 149.7 parts of base-materials add 0.3 part of gray dyes and prepare grey base-material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds salicylic acid, allantois
Element, disodium ethylene diamine tetraacetate, Phenoxyethanol, stir 30 minutes；
2）Carfil 9221 and S-482 solution are sequentially added, is stirred 30 minutes；
3）Vesmody A901 are added, are stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of S-482 powder, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, controls 500 revs/min of rotating speed；
2）The S-482 powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus S-482 powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：658 parts of deionized water, 9,221 280 parts of Carfil, water
2 parts of poplar acid, 30 parts of allantoin, 1 part of 21 5 parts of Carbopol Ultrez, 250HBR, 3 parts of methyl hydroxybenzoate, AMP-95 5
Part, 1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds salicylic acid, allantois
Element, disodium ethylene diamine tetraacetate and methyl hydroxybenzoate, stir 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful Deacne pack of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）The toning base-material of formula ratio is directly added into the S482 aqueous solution by comminutor, gained particle, it is follow-up to be granulated end
Continuous stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful anti-acne of painting type
Facial mask 3.
Use feeling and acne-removing evaluation, specific test side are carried out to the embodiment 1-3 colorful Deacne pack of painting type
Method is as follows：
Each test group chooses 20 female volunteers, age 18-35 year, and with moderate whelk, health is good for face,
60 people altogether.Application method：After volunteer cleans face, tested facial mask is homogeneously applied to left face as test section, right face
Without test, as a comparison area.Facial mask is thrown off after 15 minutes.Experiment facial mask uses every other day, after continuing 2 months, to volunteer
Use feeling investigation is carried out, evaluation is divided into 5 grades：More than 90% subject is satisfied with, and comments 5 points；80%-90% subject is satisfied with, and comments
4 points；70%-80% subject is satisfied with, and comments 3 points；60-70% subject is satisfied with, and comments 2 points；It is satisfied with less than 60% subject, comments 1 point.Comment
Valency result is classified as table 1.
The use feeling evaluation of the colorful Deacne packs of embodiment 1-3 of table 1.
Contrast table 1 as can be seen that the made colorful Deacne pack anti-acne effects of embodiment 1-3 it is notable, good permeability, to skin irritatin
Property it is slighter, complete skin care after easily torn off from face.
It is described above, be only presently preferred embodiments of the present invention, any formal limitation not done to the present invention, therefore it is all not
Depart from the content of technical solution of the present invention, according to the present invention technical spirit to any simple modification made for any of the above embodiments,
Equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (9)
- A kind of 1. colorful Deacne pack of painting type, it is characterised in that：It is made up of the raw material of following parts by weight：Mix colours base-material 400- 500 parts, interleaving agent 200-300 parts and continuous phase 300-400 parts；Described interleaving agent is made up of the raw material of following parts by weight：Go Ionized water 850-950 parts, insulating powder 50-150 parts, preservative 1-3 parts；The continuous phase is made up of the raw material of following parts by weight： Deionized water 600-750 parts, water-base resin 200-400 parts, acne removing agent 1-5 parts, anti-freckle agent 10-30 parts, thickener 3-15 parts, prevent Rotten agent 3-5 parts, pH adjusting agent 0-5 parts, complexing agent 0.2-1 parts.
- 2. the colorful Deacne pack of painting type according to claim 1, it is characterised in that：Described insulating powder is magnesium silicate One or more of compositions in lithium, aluminium-magnesium silicate, S482；Described preservative is Kathon CG, Phenoxyethanol, Metagin Ester, one or more of compositions in propylben.
- 3. the colorful Deacne pack of painting type according to claim 1 or 2, it is characterised in that：The preparation of described interleaving agent Process is：1）The deionized water of formula ratio is put into reactor, controls 400-500 revs/min of rotating speed；2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring 30-40 minutes to dissolving；3）Surplus insulating powder is put into reactor, 30-40 minutes are stirred under same rotational speed, interleaving agent is made.
- 4. the colorful Deacne pack of painting type according to claim 1 or 2, it is characterised in that：Described water-base resin is One or both of Carfil 9221 or Carfil 9220；Described acne removing agent is all-trans retinoic acid, azelaic acid and One or more of compositions in salicylic acid；The anti-freckle agent is one or both of allantoin, medical collagen Composition；Described thickener is guar gum, carbomer, sodium carboxymethylcellulose, hydroxyethyl cellulose, in hydroxypropyl cellulose One or more of compositions；Described pH adjusting agent is diethanol amine, triethanolamine, one kind in CP-950, AMP-95 Or several composition；Described complexing agent is disodium ethylene diamine tetraacetate, one kind in the sodium of diethylene triamine pentacetic acid (DTPA) five；Institute The preservative stated is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
- 5. the colorful Deacne pack of painting type according to claim 1 or 2, it is characterised in that：The preparation step of the continuous phase Suddenly it is：1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds acne removing agent, dispel Spot agent, complexing agent and preservative, stir 30-40 minutes；2）Water-base resin is added, stirs 15-20 minutes；3）Thickener is slowly added to, stirs 30-40 minutes；4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces continuous phase.
- 6. the colorful Deacne pack of painting type according to claim 1 or 2, it is characterised in that：The toning base-material is by following The raw material composition of parts by weight：Base-material 980-1000 parts, dyestuff 0-20 parts；Described base-material by following parts by weight raw material group Into：Deionized water 350-550 parts, water-base resin 300-500 parts, interleaving agent 50-150 parts, acne removing agent 1-5 parts, anti-freckle agent 10-30 Part, thickener 20-80 parts, pH adjusting agent 0-50 parts, preservative 3-5 parts, complexing agent 0.2-1 parts；The dyestuff is assorted food Level or cosmetics-stage transparency dye.
- 7. the colorful Deacne pack of painting type according to claim 6, it is characterised in that：In base-material, described water-base resin For one or both of Carfil 9221 or Carfil 9220；Described acne removing agent is all-trans retinoic acid, azelaic acid With one or more of compositions in salicylic acid；The anti-freckle agent is one or both of allantoin, medical collagen Composition；Described thickener is Aculyn 33, the one or more in Vesmody A901, Vesmody A406 Composition；Described pH adjusting agent is diethanol amine, triethanolamine, one or more of combinations in CP-950, AMP-95 Thing；Described complexing agent is disodium ethylene diamine tetraacetate, one kind in the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
- 8. the colorful Deacne pack of painting type according to claim 6, it is characterised in that：The preparation process of described base-material For：1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds acne removing agent, dispel Spot agent, complexing agent and preservative, stir 30-40 minutes；2）Water-base resin is added, stirs 15-20 minutes；3）Thickener and interleaving agent are slowly added to, stirs 30-40 minutes；4）PH adjusting agent is added, makes system pH=7,20-30 minutes is stirred, produces base-material；The preparation process of described toning base-material is：1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；2）The dyestuff of formula ratio is separately added into, 20-30 minutes is stirred, produces toning base-material.
- A kind of 9. method of the colorful Deacne pack of painting type prepared as described in claim 1-2, it is characterised in that：Including as follows The step：1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；2）The toning base-material of formula ratio is directly added into interleaving agent by comminutor, gained particle, granulation continues to stir after terminating Mix 10-15 minutes；3）Continuous phase is slowly added to reactor, 20-30 minutes are stirred with 100-150 revs/min of speed.It is more to produce painting type Color Deacne pack.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710538086.7A CN107334646A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful Deacne pack of painting type and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710538086.7A CN107334646A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful Deacne pack of painting type and preparation method thereof |
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| CN107334646A true CN107334646A (en) | 2017-11-10 |
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| CN201710538086.7A Pending CN107334646A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful Deacne pack of painting type and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1608330A1 (en) * | 2003-04-01 | 2005-12-28 | MGP Ingredients Inc | Skin-tightening preparations containing gliadin |
| CN102772345A (en) * | 2012-06-29 | 2012-11-14 | 安徽省王巢食品有限公司 | All-natural bee pollen facial mask paste and production method thereof |
| CN103181861A (en) * | 2011-12-30 | 2013-07-03 | 广东雅威生物科技有限公司 | Bubble facial mask and preparation process thereof |
| CN104688621A (en) * | 2015-03-02 | 2015-06-10 | 上海卡卡化妆品有限公司 | Self-foaming cosmetic composition and preparation method thereof |
| CN105168054A (en) * | 2015-09-17 | 2015-12-23 | 长沙九超生物科技有限公司 | Mask capable of supplementing water, whitening and removing wrinkles and preparation method of mask |
-
2017
- 2017-07-04 CN CN201710538086.7A patent/CN107334646A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1608330A1 (en) * | 2003-04-01 | 2005-12-28 | MGP Ingredients Inc | Skin-tightening preparations containing gliadin |
| CN103181861A (en) * | 2011-12-30 | 2013-07-03 | 广东雅威生物科技有限公司 | Bubble facial mask and preparation process thereof |
| CN102772345A (en) * | 2012-06-29 | 2012-11-14 | 安徽省王巢食品有限公司 | All-natural bee pollen facial mask paste and production method thereof |
| CN104688621A (en) * | 2015-03-02 | 2015-06-10 | 上海卡卡化妆品有限公司 | Self-foaming cosmetic composition and preparation method thereof |
| CN105168054A (en) * | 2015-09-17 | 2015-12-23 | 长沙九超生物科技有限公司 | Mask capable of supplementing water, whitening and removing wrinkles and preparation method of mask |
Non-Patent Citations (2)
| Title |
|---|
| 《化工百科全书》编委会》: "《化工百科全书》", 30 September 1994, 化学工业出版社 * |
| 董艳编著: "《化学与健康消费》", 31 August 2008, 中国石油大学出版社 * |
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Address after: 350100 first and second floors of No.1 Workshop, No.1 East Road, phase I, Minhou economic and Technological Development Zone, Jingxi Town, Minhou County, Fuzhou City, Fujian Province Applicant after: FUJIAN HUAXIALAN NEW MATERIAL TECHNOLOGY CO., LTD. Address before: Near East Taihe square in Jinan District of Fuzhou city in Fujian province 350011 SOHO office building No. 3 room 308-313 Applicant before: FUJIAN HUAXIALAN NEW MATERIAL TECHNOLOGY CO., LTD. |
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Application publication date: 20171110 |
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