CN107313270B - A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing - Google Patents
A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing Download PDFInfo
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/67341—Salts or hydroxides of elements different from the alkaline or alkaline-earth metals or with anions containing those elements
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67383—Inorganic compounds containing silicon
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
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- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
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- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
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- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/20—Physical treatments affecting dyeing, e.g. ultrasonic or electric
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- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/20—Physical treatments affecting dyeing, e.g. ultrasonic or electric
- D06P5/2011—Application of vibrations, pulses or waves for non-thermic purposes
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The present invention relates to historical relic's protection fields, disclose a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, comprising: A) the kiginu system of beating；B) Jiao Fanshui is prepared；C) gluing；D) print draws pigment solution preparation；E calcium hydroxide aqueous solution) is gradually added in Xiang Yinhui pigment solution until solution ph is neutral or alkalescent；F) paint, gluing；G) aging.The present invention not only can effectively simulate ancient times classical Chinese painting on silk; sample is provided for ancient times classical Chinese painting on silk historical relic ageing research and protection work; there is very important realistic meaning to protection China's preciousness traditional culture resource, and fixation treatment is carried out to this, make it with more durable firm characteristic.
Description
Technical field
The present invention relates to historical relic's protection field more particularly to a kind of durable fixation classical Chinese painting on silk preparations based on archaistic colored drawing
Method.
Background technique
Chinese silk goods are originating from the Neolithic Age before more than 5,000 years, in the paper uncreated very long years, silk
Fabric is always the carrier painted.Its middle ancient times classical Chinese painting on silk belongs to the higher class of researching value in silk fabric cultural relics, and classical Chinese painting on silk is also named
Painting on silk, the unearthed Warring states in finding material object such as Changsha, Western Han Dynastry's painting on silk book copied on silk.But since spun silk is mainly made of silk, silk fibroin
The attribute of dimension determines " tender constitution, rapid wear are difficult to ensure and deposit " of textile, at the same be extremely easy by environmental factor as it is moist, damp and hot,
The influence that improper ventilation, animals and plants disease corrode, the silk furthermore mainly formed as thin,tough silk are especially quick to light, acid, alkali, salt etc.
Sense.And the pigment of ancient times classical Chinese painting on silk, then based on mineral pigment, phyteral pigment, pigment in humid conditions, can change in classical Chinese painting on silk
Acid-base property of the silk scroll at this, can accelerate the ager process of classical Chinese painting on silk.Unearthed classical Chinese painting on silk due to being imbedded in underground for a long time simultaneously, by each
The effect of kind factor, fiber have occurred and that different degrees of aging, and after being unearthed, the effect of light and other each factors can accelerate it
Aging finally makes silk weaving historical relic change so much that one loses one's identity, some even serious embrittlements, dusting, touching powder, a large amount of cause
The presence for making the factor of classical Chinese painting on silk historical relic aging, protection and research to classical Chinese painting on silk bring very big difficulty.Therefore, for classical Chinese painting on silk
Protect extremely urgent, to this status, the research for carrying out its aging phenomenon is great to the Protection significance after it.Meanwhile ancient times draw
Drawing skill and technique makes pigment form one layer of membranoid substance on silk fabrics surface, this layer of membranoid substance can completely cut off the contact of thin,tough silk with light, mould,
So that thin,tough silk slows down the ager process of classical Chinese painting on silk from its destruction.
Preciousness witness in kind due to unearthed classical Chinese painting on silk historical relic rare numbers and as Chinese nation's successive dynasties civilized history is very
Preciousness, cannot be used for historical relic's protection research work easily, thus effectively simulate ancient times classical Chinese painting on silk study its agine mechaism and its
Protection has extremely important effect to ancient times classical Chinese painting on silk historical relic's protection.
Summary of the invention
The durable fixation classical Chinese painting on silk system that in order to solve the above-mentioned technical problems, the present invention provides a kind of based on archaistic colored drawing
Preparation Method.The raw material that natural or ancient times use are all made of in the method for the present invention, it being capable of more accurate simulation ancient times classical Chinese painting on silk
The preparation of historical relic.
The specific technical proposal of the invention is: a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, packet
Include following steps:
A) the kiginu system of beating: the alcoholic solution to white kiginu concentration less than 15wt% is cleaned, then natural air drying beats 8
~ 12 minutes.
The silicone oil in kiginu fabric can be cleaned with ethyl alcohol, ethanol water never excessive concentration, in order to avoid in cleaning process
In the protein in silk fiber is caused to damage.The silk fiber system of beating is flat, visually it can be observed that compared to before beating system,
Cloth gap becomes smaller, but cannot make fibrous fracture, and fabric tightness type is more preferably conducive to fixation when dye after processing.
B) Jiao Fanshui is prepared: measuring gelatin, alum and deionized water respectively according to 2 ~ 4:1 of mass ratio ~ 2:100 ~ 200, so
Gelatin is mixed with water afterwards, and stirs to moisture and is completely immersed in glue, expansion is placed on completely carries out in 65-75 DEG C of water-bath
Heating stirring, after heating, gelatin melts completely, is cooled to 50 DEG C hereinafter, alum is added in solution, stirring to solution
Be completely dissolved to alum, be made Jiao Fanshui, be subsequently placed in 25-35 DEG C of water-bath keep the temperature it is spare.
C) gluing: will beat the kiginu made and fixed with picture frame, carry out water spray processing to kiginu, Jiao Fanshui is uniformly brushed in
On kiginu cloth, after having brushed one side, after cloth it is micro- it is dry after brush the second face after two sides is brushed cloth be placed in ventilation
Locate natural air drying, ripe thin,tough silk is made.
Water spray is sprayed water using watering can, to guarantee that the water sprayed in watering can is fog-like during water spray and the amount sprayed water can not mistake
It is more.After carrying out Jiao Fanshui brushing to kiginu, it is easier to paint.
D) print draws pigment solution preparation: mixing mineral pigments and attapulgite by the mass ratio of 1.5-2.5:1 and goes forward side by side
Row oscillation, then stands 5-7 hours, obtains pigment mixture；Then air bladder denaturation extract is added by the mass ratio of 1:5-7
It into water, is sufficiently stirred, then adds pigment mixture, be placed in 65-75 DEG C of water-bath and keep the temperature, it is spare.
The present invention is mixed using attapulgite with pigment, and advantage is the hybrid pigment of attapulgite preparation compared with other clays
Stability is prominent for mineral.The main component of air bladder extract is collagen, and viscosity is very big, is highly suitable for making
Standby natural pigment adhesive.The adhesive derives from natural products, compared with organic synthesis adhesive, is free of formaldehyde, safe nothing
It poisons, it being capable of more accurate simulation ancient times classical Chinese painting on silk historical relic.
E calcium hydroxide aqueous solution) is gradually added in Xiang Yinhui pigment solution until solution ph is neutral or alkalescent.
The present invention adjusts pH to neutrality using calcium hydroxide aqueous solution, and it is excellent durable that advantage is to make in this way pigment to have
Solid color.
F the print modulated) is drawn pigment solution painting to be plotted on ripe thin,tough silk, until paint region pigment is substantially uniform, from
So air-dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, is brushed without repeating, complete
At rear natural air drying, classical Chinese painting on silk is made.
In paint, never there is not molten pigment little particle.
Since the aging of ancient times ripe classical Chinese painting on silk is the comprehensive functions such as thin,tough silk, glue alum and environment as a result, thus must be to simulation
Classical Chinese painting on silk carry out sizing alum processing, while herein simulate on the basis of durable fixation treatment is carried out to it, allow color it is stronger and
For a long time.
G it) by the classical Chinese painting on silk after paint, being put into ultraviolet deterioration with moisture combined test chamber and carries out aging, setting humidity is 75-85%,
Temperature is 40-50 DEG C；Aging period, classical Chinese painting on silk need daily turn-over primary, and ageing time is 3-4 weeks.
Preferably, step D) in, the mineral pigments is ochre, malachite green, orpiment, indigo.
Preferably, step D) in, air bladder denaturation extract the preparation method is as follows: fresh air bladder is taken to clean, will
It is immersed in water mesohigh boiling 1-2h, and taking-up removes moisture removal, is placed in container and stirs 0.5-1.5h, then add it to dense
It is digested in the basic protein enzyme aqueous solution that degree is 0.05-0.15wt%, the enzyme deactivation at 110-130 DEG C after enzymatic hydrolysis, filtering is dense
Air bladder extract is made after contracting, drying, air bladder extract is finally impregnated into 0.5-1.5h in acetone soln, is made after taking out drying
It obtains air bladder and is denaturalized extract.
The present invention is extracted using hot water and enzymatic isolation method extracts the collagen in air bladder, fish made from above-mentioned specific process
Fish glue extract viscosity is especially good.In order to further increase the stickiness of albumen, when enzyme deactivation, uses high temperature, makes protein denaturation, then
It is soaked in acetone again, further increases the stickiness of albumen.
Preferably, pH value of solution is 7.5-9, hydrolysis temperature is 30-40 DEG C, enzymolysis time 2-4h.
In order to further increase the stickiness of albumen, alkaline environment is specially used in enzymatic hydrolysis, makes protein denaturation, improves it
Stickiness.
Preferably, step E) in, pH value of solution is adjusted to 7-8.5.
It is compared with the prior art, the beneficial effects of the present invention are:
1, it can generally simulate through the invention and draw ancient times classical Chinese painting on silk with mineral pigment, be the historical relic aging of ancient times classical Chinese painting on silk
Research and protection work provide sample, have very important realistic meaning to protection China's preciousness traditional culture resource.
2, the chemistry and physics and ancient times classical Chinese painting on silk that the classical Chinese painting on silk prepared through the invention contains are almost the same, by right
It, which carries out deterioration research, can effectively inquire into out the degradation mechanism of ancient times classical Chinese painting on silk, and carrying out ageing research on this basis can obtain
To more accurate as a result, having great importance to ancient records and relics protection.
3, it develops through the invention with the durable color-fixing method drawn in mineral pigment on ancient times classical Chinese painting on silk, for from now on
The durable fixation of colored drawing classical Chinese painting on silk provides a good method.
Specific embodiment
The present invention will be further described with reference to the examples below.
Embodiment 1
A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, comprising the following steps:
A) the kiginu system of beating: the alcoholic solution of white kiginu concentration 10wt% is cleaned, then natural air drying beats 10 points
Clock.
B) Jiao Fanshui is prepared: gelatin, alum and deionized water are measured respectively according to mass ratio 3:1.5:150, it then will be bright
Glue is mixed with water, and is stirred to moisture and be completely immersed in glue, and expansion, which is placed in 70 DEG C of water-bath, completely carries out heating stirring,
After heating, gelatin melts completely, is cooled to 50 DEG C hereinafter, alum is added in solution to solution, stirring is complete to alum
Fully dissolved, be made Jiao Fanshui, be subsequently placed in 30 DEG C of water-bath keep the temperature it is spare.
C) gluing: will beat the kiginu made and fixed with picture frame, carry out water spray processing to kiginu, Jiao Fanshui is uniformly brushed in
On kiginu cloth, after having brushed one side, after cloth it is micro- it is dry after brush the second face after two sides is brushed cloth be placed in ventilation
Locate natural air drying, ripe thin,tough silk is made.
D) print draws pigment solution preparation: mixing mineral pigments (ochre) and attapulgite by the mass ratio of 2:1 and goes forward side by side
Row oscillation, then stands 6 hours, obtains pigment mixture；Then air bladder denaturation extract is added to water by the mass ratio of 1:6
In, it is sufficiently stirred, then adds pigment mixture, be placed in 70 DEG C of water-baths and keep the temperature, it is spare.
Air bladder denaturation extract the preparation method is as follows: fresh air bladder is taken to clean, be immersed in the steaming of water mesohigh
1.5h is boiled, taking-up removes moisture removal, is placed in container and stirs 1h, then adds it to the alkali protease water that concentration is 0.1wt%
It is digested in solution, pH value of solution 8, hydrolysis temperature is 35 DEG C, enzymolysis time 3h.The enzyme deactivation at 120 DEG C, mistake after enzymatic hydrolysis
Air bladder extract is made after concentration, drying in filter, finally air bladder extract is impregnated 1h in acetone soln, made after taking-up is dry
It obtains air bladder and is denaturalized extract.
E calcium hydroxide aqueous solution) is gradually added in Xiang Yinhui pigment solution until solution ph is 7.5.
F the print modulated) is drawn pigment solution painting to be plotted on ripe thin,tough silk, until paint region pigment is substantially uniform, from
So air-dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, is brushed without repeating, complete
At rear natural air drying, classical Chinese painting on silk is made.
G it) by the classical Chinese painting on silk after paint, is put into ultraviolet deterioration with moisture combined test chamber and carries out aging, setting humidity is 80%, temperature
Degree is 45 DEG C；Aging period, classical Chinese painting on silk need daily turn-over primary, and ageing time is 25 days.
Embodiment 2
A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, comprising the following steps:
A) the kiginu system of beating: the alcoholic solution of white kiginu concentration 12wt% is cleaned, then natural air drying beats 8 points
Clock.
B) Jiao Fanshui is prepared: gelatin, alum and deionized water is measured respectively according to mass ratio 2:1:100, then by gelatin
It is mixed with water, and stirs to moisture and be completely immersed in glue, expansion, which is placed in 65 DEG C of water-bath, completely carries out heating stirring, adds
After heat, gelatin melts completely, is cooled to 50 DEG C hereinafter, alum is added in solution to solution, stirring is complete to alum
Dissolution, be made Jiao Fanshui, be subsequently placed in 25 DEG C of water-bath keep the temperature it is spare.
C) gluing: will beat the kiginu made and fixed with picture frame, carry out water spray processing to kiginu, Jiao Fanshui is uniformly brushed in
On kiginu cloth, after having brushed one side, after cloth it is micro- it is dry after brush the second face after two sides is brushed cloth be placed in ventilation
Locate natural air drying, ripe thin,tough silk is made.
D) print draws pigment solution preparation: mixing mineral pigments (malachite green) and attapulgite simultaneously by the mass ratio of 1.5:1
It is vibrated, then stands 5 hours, obtain pigment mixture；Then air bladder denaturation extract is added to by the mass ratio of 1:5
It in water, is sufficiently stirred, then adds pigment mixture, be placed in 65 DEG C of water-baths and keep the temperature, it is spare.
Air bladder denaturation extract the preparation method is as follows: fresh air bladder is taken to clean, be immersed in the steaming of water mesohigh
1h is boiled, taking-up removes moisture removal, is placed in container and stirs 0.5h, then adds it to the alkali protease that concentration is 0.05wt%
It is digested in aqueous solution, pH value of solution 7.5, hydrolysis temperature is 30 DEG C, enzymolysis time 4h.The enzyme deactivation at 110 DEG C after enzymatic hydrolysis,
Filtering is made air bladder extract after concentration, drying, air bladder extract is finally impregnated 0.5h in acetone soln, takes out drying
Air bladder is made afterwards and is denaturalized extract.
E calcium hydroxide aqueous solution) is gradually added in Xiang Yinhui pigment solution until solution ph is 7.
F the print modulated) is drawn pigment solution painting to be plotted on ripe thin,tough silk, until paint region pigment is substantially uniform, from
So air-dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, is brushed without repeating, complete
At rear natural air drying, classical Chinese painting on silk is made.
G it) by the classical Chinese painting on silk after paint, is put into ultraviolet deterioration with moisture combined test chamber and carries out aging, setting humidity is 75%, temperature
Degree is 40 DEG C；Aging period, classical Chinese painting on silk need daily turn-over primary, and ageing time is 3 weeks.
Embodiment 3
A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, comprising the following steps:
A) the kiginu system of beating: the alcoholic solution of white kiginu concentration 14wt% is cleaned, then natural air drying beats 12 points
Clock.
B) Jiao Fanshui is prepared: gelatin, alum and deionized water is measured respectively according to mass ratio 4:2:200, then by gelatin
It is mixed with water, and stirs to moisture and be completely immersed in glue, expansion, which is placed in 75 DEG C of water-bath, completely carries out heating stirring, adds
After heat, gelatin melts completely, is cooled to 50 DEG C hereinafter, alum is added in solution to solution, stirring is complete to alum
Dissolution, be made Jiao Fanshui, be subsequently placed in 35 DEG C of water-bath keep the temperature it is spare.
C) gluing: will beat the kiginu made and fixed with picture frame, carry out water spray processing to kiginu, Jiao Fanshui is uniformly brushed in
On kiginu cloth, after having brushed one side, after cloth it is micro- it is dry after brush the second face after two sides is brushed cloth be placed in ventilation
Locate natural air drying, ripe thin,tough silk is made.
D) print draws pigment solution preparation: mixing mineral pigments (orpiment, indigo) and attapulgite by the mass ratio of 2.5:1
Merging is vibrated, and is then stood 7 hours, is obtained pigment mixture；Then air bladder denaturation extract is added by the mass ratio of 1:7
It adds in water, is sufficiently stirred, then add pigment mixture, be placed in 75 DEG C of water-baths and keep the temperature, it is spare.
Air bladder denaturation extract the preparation method is as follows: fresh air bladder is taken to clean, be immersed in the steaming of water mesohigh
2h is boiled, taking-up removes moisture removal, is placed in container and stirs 1.5h, then adds it to the alkali protease that concentration is 0.15wt%
It is digested in aqueous solution, pH value of solution 9, hydrolysis temperature is 40 DEG C, enzymolysis time 4h.The enzyme deactivation at 130 DEG C, mistake after enzymatic hydrolysis
Air bladder extract is made after concentration, drying in filter, air bladder extract is finally impregnated 1.5h in acetone soln, after taking-up is dry
Air bladder is made and is denaturalized extract.
E calcium hydroxide aqueous solution) is gradually added in Xiang Yinhui pigment solution until solution ph is 8.5.
F the print modulated) is drawn pigment solution painting to be plotted on ripe thin,tough silk, until paint region pigment is substantially uniform, from
So air-dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, is brushed without repeating, complete
At rear natural air drying, classical Chinese painting on silk is made.
G it) by the classical Chinese painting on silk after paint, is put into ultraviolet deterioration with moisture combined test chamber and carries out aging, setting humidity is 85%, temperature
Degree is 50 DEG C；Aging period, classical Chinese painting on silk need daily turn-over primary, and ageing time is 4 weeks.
Raw materials used in the present invention, equipment is unless otherwise noted the common raw material, equipment of this field；In the present invention
Method therefor is unless otherwise noted the conventional method of this field.
The above is only presently preferred embodiments of the present invention, is not intended to limit the invention in any way, it is all according to the present invention
Technical spirit any simple modification, change and equivalent transformation to the above embodiments, still fall within the technology of the present invention side
The protection scope of case.
Claims (4)
1. a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, it is characterised in that the following steps are included:
A) the kiginu system of beating: the alcoholic solution to white kiginu concentration less than 15wt% is cleaned, natural air drying, then beat 8~
12 minutes；
B) Jiao Fanshui is prepared: measuring gelatin, alum and deionized water respectively according to mass ratio 2~4: 1~2: 100~200, then
Gelatin is mixed with water, and stirs to moisture and is completely immersed in glue, expansion is placed on completely is added in 65-75 DEG C of water-bath
Thermal agitation, after heating, gelatin melts completely, is cooled to 50 DEG C hereinafter, alum is added in solution to solution, stirring is extremely
Alum is completely dissolved, be made Jiao Fanshui, be subsequently placed in 25-35 DEG C of water-bath keep the temperature it is spare；
C) gluing: the kiginu made will be beaten and fixed with picture frame, water spray processing is carried out to kiginu, Jiao Fanshui is uniformly brushed in kiginu
On cloth, after having brushed one side, after cloth it is micro- it is dry after brush the second face, after two sides is brushed, by cloth be placed in ventilation from
It so air-dries, ripe thin,tough silk is made；
D) print draws pigment solution preparation: mineral pigments and attapulgite being mixed and shaken by 1.5-2.5: 1 mass ratio
It swings, then stands 5-7 hours, obtain pigment mixture；Then air bladder denaturation extract is added to water by 1: 5-7 mass ratio
In, it is sufficiently stirred, then adds pigment mixture, be placed in 65-75 DEG C of water-bath and keep the temperature, it is spare；
Air bladder denaturation extract the preparation method is as follows: fresh air bladder is taken to clean, be immersed in water mesohigh boiling 1-
2h, taking-up remove moisture removal, are placed in container and stir 0.5-1.5h, then add it to the alkali that concentration is 0.05-0.15wt%
Property aqueous solution of protease in digested, the enzyme deactivation at 110-130 DEG C after enzymatic hydrolysis, filtering, concentration, it is dry after air bladder be made extract
Air bladder extract is finally impregnated 0.5-1.5h by object in acetone soln, and air bladder denaturation extract is made after taking out drying；
E calcium hydroxide aqueous solution) is gradually added in Xiang Yinhui pigment solution until solution ph is neutral or alkalescent；
F the print modulated) is drawn pigment solution painting to be plotted on ripe thin,tough silk, until paint region pigment is substantially uniform, natural wind
It is dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, is brushed without repeating, after the completion
Classical Chinese painting on silk is made in natural air drying；
G it) by the classical Chinese painting on silk after paint, is put into ultraviolet deterioration with moisture combined test chamber and carries out aging, setting humidity is 75-85%, temperature
Degree is 40-50 DEG C；Aging period, classical Chinese painting on silk need daily turn-over primary, and ageing time is 3-4 weeks.
2. a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing as described in claim 1, which is characterized in that
Step D) in, the mineral pigments is ochre, malachite green, orpiment, indigo.
3. a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing as described in claim 1, which is characterized in that
PH value of solution is 7.5-9, and hydrolysis temperature is 30-40 DEG C, enzymolysis time 2-4h.
4. a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing as described in claim 1, which is characterized in that
Step E) in, pH value of solution is adjusted to 7-8.5.
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| CN102277743A (en) * | 2011-07-08 | 2011-12-14 | 雷加木 | Blocker for silk painting |
| CN104313102A (en) * | 2014-11-06 | 2015-01-28 | 伍曾利 | Method of preparing collagen |
| CN104372611A (en) * | 2014-10-30 | 2015-02-25 | 浙江理工大学 | Preparation process for imitating ancient silk painting antique |
| CN105297394A (en) * | 2015-10-30 | 2016-02-03 | 浙江理工大学 | Preparation method for simulating ancient silk painting |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102277743A (en) * | 2011-07-08 | 2011-12-14 | 雷加木 | Blocker for silk painting |
| CN104372611A (en) * | 2014-10-30 | 2015-02-25 | 浙江理工大学 | Preparation process for imitating ancient silk painting antique |
| CN104313102A (en) * | 2014-11-06 | 2015-01-28 | 伍曾利 | Method of preparing collagen |
| CN105297394A (en) * | 2015-10-30 | 2016-02-03 | 浙江理工大学 | Preparation method for simulating ancient silk painting |
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