CN107044058A - Resist agent and preparation method, batik and batik method - Google Patents
Resist agent and preparation method, batik and batik method Download PDFInfo
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- CN107044058A CN107044058A CN201710361621.6A CN201710361621A CN107044058A CN 107044058 A CN107044058 A CN 107044058A CN 201710361621 A CN201710361621 A CN 201710361621A CN 107044058 A CN107044058 A CN 107044058A
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- batik
- parts
- resist agent
- cloth
- wax
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/12—Reserving parts of the material before dyeing or printing ; Locally decreasing dye affinity by chemical means
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/06—Material containing basic nitrogen containing amide groups using acid dyes
Abstract
A kind of resist agent and preparation method, batik and batik method, belong to field of printing and dyeing.Preparing the raw material of resist agent includes the following components of peace parts by weight meter：60~80 parts of emulsified wax, 1~5 part of triethanolamine, 1~3 part of modified organic silicon, 1~5 part of alkyl-modified organosiloxane, 3~7 parts of Tissuemat E, 10~16 parts of neopelex.The resist agent that the present invention is provided can become apparent from the pattern contour of the cloth of batik.
Description
Technical field
The present invention relates to field of printing and dyeing, in particular to a kind of resist agent and preparation method, batik and batik side
Method.
Background technology
Batik is race of China folk tradition textile printing and dyeing handicraft, and Gu claims wax, with twisting figured silk fabrics (tie dyeing), folder figured silk fabrics (hollow out stamp)
And the referred to as big stamp skill of Ancient Times in China three.Batik is good at by the nationalitys such as Guizhou, Yunnan Miao ethnic group, the Bouyei.Batik is dipped in wax spatula
Dewaxing is painted after Hua Yubu is contaminated with indigo, both contaminates wax, cloth cover take on blue bottom spend in vain or white background indigo plant flower multiple patterns, together
When, in dip-dye, as the wax exposure cracking of resist agent, make cloth cover that special " ice line " is presented, have glamour especially.Due to batik figure
Case is enriched, and tone is plain, unique style, for making dress and personal adornment and various life utilities, it appears simple generous, pure and fresh happy
Mesh, rich in national characters.But, current wax-dyeing process is all that, using rosin as raw material, it has the disadvantage, not only cost is high, and shape
Into line it is coarse, do not reach the effect of hair batik.
The content of the invention
In the first aspect of the present invention there is provided a kind of resist agent, can improve the profile after the batik of cloth become apparent from,
Feel is more preferable.
In the second aspect of the present invention, there is provided a kind of method for preparing resist agent.The preparation method technique is simple, make
Cycle is short, can reduce it and prepare cost.
In the third aspect of the present invention batik method is prepared there is provided one kind.Carrying out batik using foregoing resist agent can be with
Batik effect is improved, batikses quality is improved.
In the fourth aspect of the present invention, there is provided a kind of batik.Batik Color is good, and color is dense, wheel is cleaned up
It is clear.
What the present invention was realized in：
A kind of resist agent.Preparing the raw material of resist agent includes the following components of peace parts by weight meter：Emulsified wax 60~80
Part, 1~5 part of triethanolamine, 1~3 part of modified organic silicon, 1~5 part of alkyl-modified organosiloxane, 3~7 parts of Tissuemat E, ten
10~16 parts of dialkyl benzene sulfonic acids sodium.A kind of preparation method of above-mentioned resist agent, including raw material is mixed.
A kind of batik method, for being dyed to weaving cotton cloth, batik is carried out using above-mentioned resist agent.Batik method includes：
Progress of weaving cotton cloth is pre-processed and obtains fresh cloth；Fresh cloth being attached to according to target pattern in the resist agent of fluid state and obtaining waxing treat
Dye cloth；It will wax after being soaked in wait dying cloth and being dyed the coloring agent obtained by plant extract, pull out and dry and obtain siccative；
Remove the resist agent on siccative.
A kind of batik prepared by above-mentioned batik method.
The beneficial effect of the embodiment of the present invention：The resist printing effect of resist agent provided in an embodiment of the present invention is good, can be effective
The problem of avoiding the unintelligible or soft edge of batik pattern.Resist agent viscosity is big, thus can firmly be adhered with cloth.Resist agent
Pliability it is good, after being supported on, the effect such as larger extruding, curling in the external world can be born, so as to keep preferably outside
Shape, it is to avoid inadvertently fall off, and cause the diffusion of pigmented section.
Embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the present invention.It is unreceipted specific in embodiment
Condition person, the condition advised according to normal condition or manufacturer is carried out.Agents useful for same or the unreceipted production firm person of instrument, be
The conventional products that can be obtained by commercially available purchase.
It is specifically described below for the resist agent and preparation method, batik and batik method of the embodiment of the present invention：
A kind of resist agent.Preparing the raw material of resist agent includes the following components of peace parts by weight meter：Emulsified wax 60~80
Part, 1~5 part of triethanolamine, 1~3 part of modified organic silicon, 1~5 part of alkyl-modified organosiloxane, 3~7 parts of Tissuemat E, ten
10~16 parts of dialkyl benzene sulfonic acids sodium.
Wherein, emulsified wax is canescence homogeneous translucent liquid.Under usual conditions, emulsified wax is used as waterproofing agent.Breast
The characteristics of fossil waxes have chemical property stabilization, are difficult layering.Sealing place shady place can deposit 2 years it is not stratified, do not break
Breast, do not lump.Emulsified wax also has antiacid, alkali resistant, resistance to hard water, a water-soluble strong, emulsion-stabilizing, the dilution of arbitrary proportion water regardless of
Layer, be not demulsified, do not lump, the performance characteristics such as long shelf-life, solid content height, good dispersion.
In the present invention, used using emulsified wax in batik, the compliance of batik cloth can be improved, improve anti-tensile strong
Degree.In addition, emulsified wax has relatively good dissolubility, and its film forming is uniform, spreadability is good, therefore, in the batik system of progress
When making cloth, clear-cut pattern is more likely formed.
Triethanolamine can produce chemical reaction with dyestuff, especially reactive dye, so that dyestuff loses and fiber
Binding ability, so as to avoid the problem of unexpected pigmented section is colored.Triethanolamine is combined with emulsified wax, so as to enter
Avoid to one step the problem of dyestuff is combined with unexpected pigmented section fiber, at the same the cloth in the region that makes to be unstained more it is bright simultaneously
Improve compliant characteristic.
Modified organic silicon and alkyl-modified organosiloxane can improve the compliance of fiber, and texture, and can improve
Weave cotton cloth yellowing the problem of.It is particularly suitable for use in super soft undercoat suede, PV pile fabrics etc..In addition, modified organic silicon and alkyl-modified having
Organic siloxane also helps the workability of resist agent, improves film forming, so as to improve resist agent in the attachment stability of cloth.
Tissuemat E has the characteristics such as cold resistance, heat resistance, chemical resistance and wearability, can improve resist agent and be attached to
Mechanical stability after cloth.Further, Tissuemat E is preferred to use OPE, its have a certain amount of carbonyl and
Hydroxyl, thus dyestuff combination is easier to, so that dyestuff is not easy to cloth bonding, keep preferably resist printing effect.
The mixing uniformity of each component in neopelex enhancing resist agent, so that the entirety of resist agent
Chemically and physically characteristic is more uniform, plays the non-staining color for making unexpected pigmented section keep more unified.
The resist agent that the present invention is provided is so that with preferable dispersed emulsified wax, mixing can be with dyestuff phase
Interaction and the active material for inactivating dyestuff, and by strengthening film forming and mechanical strength, it is achieved thereby that preferably
Resist printing effect.
The content of each component can make appropriate adjustment within the above range in resist agent, further to improve resist printing effect
Really.
In some instances, preparing the raw material of resist agent includes the following components of peace parts by weight meter：Emulsified wax 65~
70 parts, 2~4 parts of triethanolamine, 1~3 part of modified organic silicon, 2~4 parts of alkyl-modified organosiloxane, 4~7 parts of Tissuemat E,
12~14 parts of neopelex.Further, preparing the raw material of resist agent includes the following components of peace parts by weight meter：
It is 68~70 parts of emulsified wax, 2~4 parts of triethanolamine, 2~3 parts of modified organic silicon, 2~4 parts of alkyl-modified organosiloxane, poly-
5~7 parts of ethylene waxes, 13~14 parts of neopelex.
Further, preparing the raw material of resist agent includes the following components of peace parts by weight meter：69 parts of emulsified wax, three
3 parts of monoethanolamine, 2 parts of modified organic silicon, 2 parts of alkyl-modified organosiloxane, 6 parts of Tissuemat E, neopelex 10
Part.
In some other example, preparing the raw material of resist agent includes the following components of peace parts by weight meter：Emulsified wax
72 parts, 3 parts of triethanolamine, 2 parts of modified organic silicon, 4 parts of alkyl-modified organosiloxane, 5 parts of Tissuemat E, detergent alkylate sulphur
Sour 13 parts of sodium.The resist agent matched using aforementioned ratio has more resist printing effect.
The preparation method of above-mentioned resist agent can be raw material mixing.As preferred scheme, by emulsified wax, Tissuemat E
It is mixed and heated to molten condition and obtains the first batch mixing；Triethanolamine, modified organic silicon and alkyl-modified organosiloxane are mixed
Conjunction obtains the second batch mixing；Neopelex is added into the second batch mixing, and adds under conditions of stirring the first batch mixing.
By the way that different component is handled respectively, remix, the mixing uniformity of resist agent can be improved.By by breast
Fossil waxes and polyvinyl alcohol are heated to molten condition, can be that polyvinyl alcohol is preferably distributed in emulsified wax, and
With reference to dispersant (neopelex), then with liquid triethanolamine, modified organic silicon and alkyl-modified organic silica
Alkane is mixed, the problems such as improving caused by avoiding various material properties different with easily reduction, reunion, to keep the flowing of resist agent
Property, so as to improve the ease of use of resist agent.
Present invention also offers a kind of batik method for being dyed to weaving cotton cloth.Batik method utilizes foregoing resist printing
Agent carries out batik.
Specifically, batik method includes：
Progress of weaving cotton cloth is pre-processed and obtains fresh cloth.Obtained fresh cloth is attached to according to target pattern in the resist agent of fluid state
Wait to dye cloth to waxing.It will wax after being soaked in wait dying cloth and being dyed the coloring agent obtained by plant extract, pull out and dry
Obtain siccative.Remove the resist agent on siccative.
Wherein, the method that pretreatment is weaved cotton cloth has a variety of, for example clean, arrange etc..It is used as a kind of preferred scheme, this hair
In bright embodiment, the method pre-processed to weaving cotton cloth includes：Weaved cotton cloth 3~8 days using dipping by lye, cotton is used after being cleaned with clear water
Burlap material is kneaded.Weaved cotton cloth by using base extraction, on the one hand can remove the grease for being attached to and weaving cotton cloth, while can be with
So that woven fibrous is more roughened, so as to be easier to combine resist agent and dyeing.
Further, be preferably 60~90 DEG C for pre-processing the temperature of alkali lye weaved cotton cloth, with improve pretreatment efficiency and
Effect.
Dyestuff mentioned in the present invention is to provide obtained natural dye by plant, for example, acanthaceous indigo, madder, Asian puccoon carry
Take thing.The method that dyestuff is extracted is to smash plant complete stool to pieces, is mixed well with deionized water as paste.Preferably, add in coloring agent
Added with sodium alginate.It is thickener, stabilizer, emulsifying agent that sodium alginate, which can be used as, so that coloring agent is more easy to disperse, meanwhile, dye
Color molecule has certain binding characteristic with sodium alginate, can improve tinctorial yield, improves the finish of pigmented section.Sodium alginate
Intermediary is alternatively arranged as, dye molecule is transferred to cloth, and is more easy to spread in web surface.
More preferably, the viscosity of sodium alginate is in 1000~2000mpas, and acid number is more than 300, so as to reduce dye
The flaw of cloth formation.
The present invention also provides a kind of batik that system is contaminated by such scheme
Resist agent and preparation method, batik and batik method with reference to embodiments to the present invention makees further detailed
Thin description.
Embodiment 1
A kind of resist agent.Preparing the raw material of resist agent includes following components：60 kilograms of emulsified wax, 1 kilogram of triethanolamine,
1 kilogram of modified organic silicon, 1 kilogram of alkyl-modified organosiloxane, 3 kilograms of Tissuemat E, 10 kilograms of neopelex.
Preparing the method for resist agent includes：By emulsified wax, triethanolamine, modified organic silicon, alkyl-modified organic silica
Alkane, Tissuemat E, neopelex mixing, and stir.
Embodiment 2
A kind of resist agent.Preparing the raw material of resist agent includes following components：80 kilograms of emulsified wax, 5 kilograms of triethanolamine,
3 kilograms of modified organic silicon, 5 kilograms of alkyl-modified organosiloxane, 7 kilograms of Tissuemat E, 16 kilograms of neopelex.
Preparing the method for resist agent includes：By emulsified wax, triethanolamine, modified organic silicon, alkyl-modified organic silica
Alkane, Tissuemat E, neopelex mixing, and stir.
Embodiment 3
A kind of resist agent.Preparing the raw material of resist agent includes following components：65 kilograms of emulsified wax, 2 kilograms of triethanolamine,
1 kilogram of modified organic silicon, 2 kilograms of alkyl-modified organosiloxane, 4 kilograms of Tissuemat E, 12 kilograms of neopelex.
Preparing the method for resist agent includes：
Emulsified wax, Tissuemat E are mixed and heated to 90 DEG C and be incubated and obtains the first batch mixing within 10 minutes.By triethanolamine,
Stirring is mixed to get the second batch mixing under modified organic silicon and alkyl-modified organosiloxane production normal temperature.To temperature for 90 DEG C the
Neopelex is added in two batch mixings, and adds under conditions of stirring the first batch mixing.
Embodiment 4
A kind of resist agent.Preparing the raw material of resist agent includes following components：70 kilograms of emulsified wax, 4 kilograms of triethanolamine,
3 kilograms of modified organic silicon, 4 kilograms of alkyl-modified organosiloxane, 7 kilograms of Tissuemat E, 14 kilograms of neopelex.
Preparing the method for resist agent includes：
Emulsified wax, Tissuemat E are mixed and heated to 100 DEG C and be incubated and obtains the first batch mixing within 5 minutes.By triethanolamine,
Stirring is mixed to get the second batch mixing under modified organic silicon and alkyl-modified organosiloxane production normal temperature.To second in room temperature
Neopelex is added in batch mixing, and adds under conditions of stirring the first batch mixing.
Embodiment 5
A kind of resist agent.Preparing the raw material of resist agent includes following components：72 kilograms of emulsified wax, 3 kilograms of triethanolamine,
2 kilograms of modified organic silicon, 4 kilograms of alkyl-modified organosiloxane, 5 kilograms of Tissuemat E, 13 kilograms of neopelex.
Preparing the method for resist agent includes：By emulsified wax, triethanolamine, modified organic silicon, alkyl-modified organic silica
Alkane, Tissuemat E, neopelex mixing, and stir.
Embodiment 6
A kind of resist agent.Preparing the raw material of resist agent includes following components：67 kilograms of emulsified wax, 1 kilogram of triethanolamine,
4 kilograms of modified organic silicon, 5 kilograms of alkyl-modified organosiloxane, 6 kilograms of Tissuemat E, 11 kilograms of neopelex.
Preparing the method for resist agent includes：By emulsified wax, triethanolamine, modified organic silicon, alkyl-modified organic silica
Alkane, Tissuemat E, neopelex mixing, and stir.
Embodiment 7
A kind of batik.Batik is to be formed by weaving cotton cloth of working out of silk by batik.
Preparing the method for batik includes：
Cleaned to weaving cotton cloth with clear water, fresh cloth is obtained after drying.
Resist agent prepared by heating embodiment 1 is until in fluid state, then by the resist agent of fluid state according to mesh
Case of marking on a map is scratched in fresh cloth, waits to dye cloth after obtaining waxing after resist agent solidification.
It will wax to be soaked in wait dying cloth and be extracted by Asian puccoon after obtained coloring agent dyed for 18 hours, and pull out and dry
To siccative.
By heating the resist agent removed on siccative.
Embodiment 8
A kind of batik.Batik is to be formed by weaving cotton cloth of working out of cotton fiber by batik.
Preparing the method for batik includes：
After being cleaned to weaving cotton cloth with clear water, then it is soaked in water and boils, pulls out and fresh cloth is obtained after drying.
Resist agent prepared by embodiment 2 is diluted with water in fluid state, then by the resist agent of fluid state according to
Target pattern is printed on fresh cloth, makes to obtain waxing after resist agent solidification to wait to dye cloth by drying.
It will wax to be soaked in wait dying cloth and be extracted by Asian puccoon after obtained coloring agent dyed for 15 hours, and pull out and dry
To siccative.Wherein, sodium alginate is also added with coloring agent, the weight ratio of ultraviolet extract and sodium alginate is 60:1, marine alga
The viscosity of sour sodium is 1800mpas, acid number 330.
By being soaked in water by siccative, and heated to remove resist agent.
Embodiment 9
A kind of batik.Batik is to be formed by weaving cotton cloth of working out of cotton fiber by batik.
Preparing the method for batik includes：
Soaked to weaving cotton cloth with aqueous sodium carbonate, and be heated to 60 DEG C and be kept at this temperature after 8 days, pulled out after drying,
Again fresh cloth is obtained with diablement fort kneading within 10 minutes.
Resist agent prepared by embodiment 3 is diluted with water in fluid state, then by the resist agent of fluid state according to
Target pattern is applied to fresh cloth, makes to obtain waxing after resist agent solidification to wait to dye cloth by drying.
It will wax to be soaked in wait dying cloth and be extracted by wooden blue after obtained coloring agent dyed for 20 hours, and pull out and dry
To siccative.
By being soaked in water by siccative, and heated to remove resist agent.
Embodiment 10
A kind of batik.Batik is to be formed by weaving cotton cloth of working out of silk by batik.
Preparing the method for batik includes：
Cleaned to weaving cotton cloth with clear water, fresh cloth is obtained after drying.
Resist agent prepared by heating embodiment 4 is until in fluid state, then by the resist agent of fluid state according to mesh
Case of marking on a map is printed on fresh cloth, waits to dye cloth after obtaining waxing after resist agent solidification.
It will wax to be soaked in wait dying cloth and be extracted by Asian puccoon after obtained coloring agent dyed for 2 days, and pull out and dry and obtain
Siccative.Wherein, sodium alginate is also added with coloring agent, the weight ratio of ultraviolet extract and sodium alginate is 50:1, alginic acid
The viscosity of sodium is 1000mpas, acid number 300.
By heating the resist agent removed on siccative.
Embodiment 11
A kind of batik.Batik is to be formed by weaving cotton cloth of working out of cotton fiber by batik.
Preparing the method for batik includes：
Soaked to weaving cotton cloth with aqueous sodium carbonate, and be heated to 77 DEG C and be kept at this temperature after 40 minutes, pulled out and dry
After obtain fresh cloth.
Resist agent prepared by embodiment 6 is diluted with water in fluid state, then by the resist agent of fluid state according to
Target pattern is applied to fresh cloth, makes to obtain waxing after resist agent solidification to wait to dye cloth by drying.
It will wax to be soaked in wait dying cloth and be extracted by Asian puccoon after obtained coloring agent dyed for 2 days, and pull out and dry and obtain
Siccative.
By being soaked in water by siccative, and heated to remove resist agent.
Embodiment 12
A kind of batik.Batik is to be formed by weaving cotton cloth of working out of cotton fiber by batik.
Preparing the method for batik includes：
Soaked to weaving cotton cloth with aqueous sodium carbonate, and be heated to 90 DEG C and be kept at this temperature after 3 days, pulled out and obtained after drying
To fresh cloth.Resist agent prepared by embodiment 6 is diluted with water in fluid state, then by the resist agent of fluid state according to mesh
Case of marking on a map silk-screen printing makes to obtain waxing after resist agent solidification to wait to dye cloth in fresh cloth by drying.
It will wax to be soaked in wait dying cloth and be extracted by Asian puccoon after obtained coloring agent carries out dyeing 1 day, and pull out and dry and obtain
Siccative.
By being soaked in water by siccative, and heated to remove resist agent.
Comparative example 1
A kind of batik, its by the following method batik form.
It is wax liquor that cerate, which is melted,.Wax liquor is smeared into cotton according to target pattern.Using cabbage extract dyestuff to attachment
The cotton for having wax liquor carries out dyeing 50 hours.Cotton is pulled out, dried naturally.Wherein, cerate is by paraffin, beeswax, rosin, flower bulb
The main modified organic silicon of alkali, polyethers compares 70 with weight:16:8:5:2 mixing compositions.
Comparative example 2
A kind of batik, its by the following method batik form.
It is liquid that rosin, which is melted, and cotton is smeared according to target pattern.Using Flos Rosae Rugosae extract dyestuff to being attached with wax
The cotton of liquid carries out dyeing 2 days.Cotton is pulled out, dried naturally.
Comparative example 3
A kind of batik, its by the following method batik form.
It is wax liquor that cerate, which is melted,.Wax liquor is printed into cotton according to target pattern.Using cabbage extract dyestuff to attachment
The cotton for having wax liquor carries out dyeing 1 day.Cotton is pulled out, dried naturally.Wherein, cerate is by 5 kilograms of chlorinated paraffin, triethanolamine
0.05 kilogram, 6 kilograms of rosin, 15 kilograms of sodium dodecyl benzenylsulfonate are mixed.
Test example 1
The batik that the batik and comparative example 1 to 3 provided embodiment 7 to embodiment 12 is provided carries out batik effect
Fruit is evaluated.The batik provided compared to comparative example 1 to 3, the batik formation that the embodiment of the present invention 7 to embodiment 12 is provided
Batik pattern becomes apparent from, profile is more obvious, and the more smooth nature of feel.The dyeing for the batik that comparative example 1 to 3 is provided
The spot that the batik in decorative pattern spot, and comparative example 1 occurs in pattern is more serious.
In addition, the batik Buran provided compared to the batik embodiment 7 that comparative example 1 to 3 is provided to embodiment 12
Pattern color is denseer, vivid.Wherein, the pattern of the batik in comparative example 3 is more limited compared to comparative example 1 and 2.But
It is that the lack of homogeneity of the pattern of the batik in comparative example 3 is in comparative example 1 and 2.
Test example 2
Dyestuff coloring persistence to the batik of offer is evaluated.
Take the batik prepared in embodiment 7 to embodiment 12 and comparative example 1 to 3 respectively, 60 DEG C, it is relatively wet
In the enclosed environment of degree 30%, preserve 1 month.It is separately immersed in again in room temperature (25 DEG C) water 6 hours, observes its discoloration.
As a result show, the batik that the embodiment of the present invention 7 to embodiment 12 is provided does not occur obvious colour fading.Wax in comparative example 1 to 3
Colour fading of dying cloth is obvious, and its comparative example 2 fades more serious.
In the case of stirring, heating water is to 60 DEG C and continues immersion 36 and carries out after hour, embodiment 8 and embodiment 11
The batik of offer does not occur obvious colour fading, and slight fade occur in embodiment 7, embodiment 9,10 and 12.
There are the above results to understand, the resist agent that the present invention is provided has more preferable protection effect, it is possible to prevente effectively from batik
During there is piebald, and cloth is more compliant, not hardened.Secondly, by using above-mentioned resist agent, provided by the present invention
Batik method can obtain clear patterns, profile and understand, and vivid.
Although illustrate and describing the present invention with specific embodiment, but it will be appreciated that without departing substantially from the present invention's
Many other changes and modification can be made in the case of spirit and scope.It is, therefore, intended that in the following claims
Including belonging to all such changes and modifications in the scope of the invention.
Claims (10)
1. a kind of resist agent, it is characterised in that prepare the following components that the raw material of the resist agent includes counting by weight：Breast
60~80 parts of fossil waxes, 1~5 part of triethanolamine, 1~3 part of modified organic silicon, 1~5 part of alkyl-modified organosiloxane, poly- second
3~7 parts of alkene wax, 10~16 parts of neopelex.
2. resist agent according to claim 1, it is characterised in that the raw material is including peace parts by weight meter with the following group
Point：65~70 parts of emulsified wax, 2~4 parts of triethanolamine, 1~3 part of modified organic silicon, 2~4 parts of alkyl-modified organosiloxane,
4~7 parts of Tissuemat E, 12~14 parts of neopelex.
3. resist agent according to claim 1, it is characterised in that the raw material is including peace parts by weight meter with the following group
Point：72 parts of emulsified wax, 3 parts of triethanolamine, 2 parts of modified organic silicon, 4 parts of alkyl-modified organosiloxane, 5 parts of Tissuemat E,
13 parts of neopelex.
4. a kind of preparation method of resist agent as claimed any one in claims 1 to 3, it is characterised in that methods described bag
Include and mix the raw material.
5. resist agent according to claim 4, it is characterised in that the method for the mixing raw material includes：By the emulsification
Paraffin, the Tissuemat E are mixed and heated to molten condition and obtain the first batch mixing；By the triethanolamine, the modified organic silicon
And the alkyl-modified organosiloxane is mixed to get the second batch mixing；The detergent alkylate is added into second batch mixing
Sodium sulfonate, and add under conditions of stirring first batch mixing.
6. a kind of batik method, for being dyed to weaving cotton cloth, it is characterised in that using such as any one of claims 1 to 3 institute
State resist agent and carry out batik, the batik method includes：
The progress of weaving cotton cloth is pre-processed and obtains fresh cloth；In the resist agent of fluid state institute will be attached to according to target pattern
State fresh cloth and obtain waxing and wait to dye cloth；By it is described wax to wait to dye cloth to be soaked in the coloring agent obtained by plant extract is dyed
Afterwards, pull out and dry and obtain siccative；Remove the resist agent on the siccative.
7. batik method according to claim 6, it is characterised in that the method that is pre-processed of weaving cotton cloth is included：
Using being weaved cotton cloth described in dipping by lye 3~8 days, kneaded after being cleaned with clear water with linen-cotton cloth.
8. batik method according to claim 7, it is characterised in that 60~90 DEG C of the temperature of the alkali lye.
9. batik method according to claim 7, it is characterised in that contain sodium alginate in the coloring agent.
10. a kind of batik, it is characterised in that the batik is contaminated as the batik method any one of claim 6 to 9
Color is formed.
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| CN201710361621.6A CN107044058A (en) | 2017-05-19 | 2017-05-19 | Resist agent and preparation method, batik and batik method |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108755201A (en) * | 2018-05-07 | 2018-11-06 | 贵州西江阿幼民族文化博物馆有限公司 | A kind of preparation method of batik |
| CN109518486A (en) * | 2018-11-30 | 2019-03-26 | 镇宁自治县蚩尤布依民族服饰有限责任公司 | A kind of preparation method and applications using dragon fruit natural dye preparation batik cream |
| CN109518490A (en) * | 2018-11-25 | 2019-03-26 | 福泉市筑梦服装有限公司 | A kind of nationality's batik cerate and preparation method thereof |
| CN111876876A (en) * | 2020-06-30 | 2020-11-03 | 江苏金太阳纺织科技股份有限公司 | Regenerated cellulose fiber soft mat fabric and preparation method thereof |
| CN115142280A (en) * | 2022-08-03 | 2022-10-04 | 东莞长联新材料科技股份有限公司 | Water-based printing adhesive cement with anti-dyeing and anti-color-migration effects and preparation method and application thereof |
| CN115748272A (en) * | 2022-11-21 | 2023-03-07 | 广东溢达纺织有限公司 | Mottled fabric, dyeing method thereof and ready-made clothes |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108755201A (en) * | 2018-05-07 | 2018-11-06 | 贵州西江阿幼民族文化博物馆有限公司 | A kind of preparation method of batik |
| CN109518490A (en) * | 2018-11-25 | 2019-03-26 | 福泉市筑梦服装有限公司 | A kind of nationality's batik cerate and preparation method thereof |
| CN109518486A (en) * | 2018-11-30 | 2019-03-26 | 镇宁自治县蚩尤布依民族服饰有限责任公司 | A kind of preparation method and applications using dragon fruit natural dye preparation batik cream |
| CN111876876A (en) * | 2020-06-30 | 2020-11-03 | 江苏金太阳纺织科技股份有限公司 | Regenerated cellulose fiber soft mat fabric and preparation method thereof |
| CN115142280A (en) * | 2022-08-03 | 2022-10-04 | 东莞长联新材料科技股份有限公司 | Water-based printing adhesive cement with anti-dyeing and anti-color-migration effects and preparation method and application thereof |
| CN115142280B (en) * | 2022-08-03 | 2023-12-08 | 东莞长联新材料科技股份有限公司 | Water-based printing adhesive cement with anti-dyeing and anti-migration effects and preparation method and application thereof |
| CN115748272A (en) * | 2022-11-21 | 2023-03-07 | 广东溢达纺织有限公司 | Mottled fabric, dyeing method thereof and ready-made clothes |
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