CN107313270A - A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing - Google Patents
A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing Download PDFInfo
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- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
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- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
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- D06P1/67341—Salts or hydroxides of elements different from the alkaline or alkaline-earth metals or with anions containing those elements
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Abstract
The present invention relates to historical relic's protection field, a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing is disclosed, including：A）The kiginu system of beating；B）Jiao Fanshui is prepared；C）Gluing；D）Print paints pigment solution preparation；E）Painted to print and calcium hydroxide aqueous solution is gradually added in pigment solution until solution ph is neutral or alkalescent；F）Paint, gluing；G）Aging.The present invention not only can effectively simulate ancient times classical Chinese painting on silk; it is that ancient times classical Chinese painting on silk historical relic ageing research and protection work provide sample; there is very important realistic meaning to the precious traditional culture resource of protection China, and to this progress fixation treatment, it is had more durable firm characteristic.
Description
Technical field
Prepared the present invention relates to historical relic's protection field, more particularly to a kind of durable fixation classical Chinese painting on silk based on archaistic colored drawing
Method.
Background technology
Chinese silk goods are originating from the Neolithic Age before more than 5,000 years, in the paper uncreated very long years, silk
Fabric is always the carrier of drawing.Its middle ancient times classical Chinese painting on silk belongs to the higher class of researching value in silk fabric cultural relics, and classical Chinese painting on silk is also named
Painting on silk, finding as the unearthed Warring states such as Changsha in kind, Western Han Dynastry's painting on silk book copied on silk.But because spun silk is mainly made up of silk, silk fibroin
The attribute of dimension determines " tender constitution, the rapid wear, be difficult to ensure and deposit " of textile, at the same extremely easily by environmental factor it is for example moist, damp and hot,
The influence that improper ventilation, animals and plants disease corrode, the silk mainly constituted as thin,tough silk in addition is particularly quick to light, acid, alkali, salt etc.
Sense.And the pigment of ancient times classical Chinese painting on silk, then based on mineral pigment, phyteral pigment, pigment in humid conditions, can change in classical Chinese painting on silk
Acid-base property of the silk scroll at this, can accelerate the ager process of classical Chinese painting on silk.Unearthed classical Chinese painting on silk due to being imbedded in underground for a long time simultaneously, by each
The effect of the factor of kind, fiber has occurred and that different degrees of aging, and after being unearthed, the effect of light and other each factors can accelerate it
Aging, finally cause silk weaving historical relic change so much that one loses one's identity, some even serious embrittlement, efflorescence, touch powder, substantial amounts of cause
Make the presence of the factor of classical Chinese painting on silk historical relic aging, the protection and research to classical Chinese painting on silk bring very big difficulty.Therefore, for classical Chinese painting on silk
Protection is extremely urgent, and to this present situation, the research for carrying out its aging phenomenon is great to the Protection significance after it.Meanwhile, ancient times paint
Drawing skill and technique causes pigment to form one layer of membranoid substance on silk fabrics surface, and this layer of membranoid substance can completely cut off thin,tough silk and light, the contact of mould,
So that thin,tough silk is destroyed from it, the ager process of classical Chinese painting on silk slow down.
Witnessed very due to unearthed classical Chinese painting on silk historical relic rare numbers and as the preciousness material object of Chinese nation's successive dynasties civilized history
It is precious, it is impossible to easily for historical relic's protection research work, thus effectively simulate ancient times classical Chinese painting on silk study its agine mechaism and its
Protection has extremely important effect to ancient times classical Chinese painting on silk historical relic's protection.
The content of the invention
In order to solve the above-mentioned technical problem, the invention provides a kind of durable fixation classical Chinese painting on silk system based on archaistic colored drawing
Preparation Method.The raw material used in the inventive method using natural or ancient times, can more precisely simulate ancient times classical Chinese painting on silk
The preparation of historical relic.
The present invention concrete technical scheme be：A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, bag
Include following steps：
A）The kiginu system of beating：The alcoholic solution that white kiginu is less than 15wt% with concentration is cleaned, then natural air drying beats 8 ~ 12
Minute.
The silicone oil that can be cleaned in kiginu fabric with ethanol, ethanol water never excessive concentration, in order to avoid in cleaning process
In to the protein in silk fiber cause damage.Silk fiber is beaten into flat processed, naked eyes are beaten before system it is observed that comparing,
Cloth gap diminishes, but fabric tightness type after fibrous fracture, processing can not be made more preferably to be beneficial to fixation during upper dye.
B）Jiao Fanshui is prepared：According to mass ratio 2 ~ 4:1~2:100 ~ 200 measure gelatin, alum and deionized water respectively, so
Gelatin is mixed with water afterwards, and stirring to moisture is completely immersed in glue, is placed in 65-75 DEG C of water-bath carries out after expansion completely
Heating stirring, after heating terminates, gelatin melts completely, treats that solution is cooled to less than 50 DEG C, and alum is added in solution, stirring
It is completely dissolved to alum, Jiao Fanshui is made, is incubated in the water-bath for being subsequently placed in 25-35 DEG C standby.
C）Gluing：The kiginu that makes will be beaten to be fixed with picture frame, water spray processing is carried out to kiginu, Jiao Fanshui is uniformly brushed in
On kiginu cloth, brushed after one side, after cloth it is micro- it is dry after brush the second face, two sides is brushed finish after, cloth is placed in ventilation
Locate natural air drying, ripe thin,tough silk is made.
Water spray is sprayed water using watering can, to ensure that the water sprayed in watering can not mistake in vaporific and water spray amount during water spray
It is many.Kiginu is carried out after Jiao Fanshui brushings, it is easier to paint.
D）Print paints pigment solution preparation：By 1.5-2.5:Mineral pigments and attapulgite are mixed and gone forward side by side by 1 mass ratio
Row vibration, then stands 5-7 hours, obtains pigment composition；Then 1 is pressed:5-7 mass ratio adds air bladder denaturation extract
Into water, it is sufficiently stirred for, then adds pigment composition, is placed in 65-75 DEG C of water-bath and is incubated, it is standby.
The present invention is mixed using attapulgite with pigment, and advantage is the hybrid pigment of attapulgite preparation compared with other clays
Stability is protruded for mineral.The main component of air bladder extract is collagen, and its viscosity is very big, is highly suitable for system
Standby natural pigment adhesive.The adhesive derives from natural products, compared with organic synthesis adhesive, without formaldehyde, safe nothing
Poison, can more precisely simulate ancient times classical Chinese painting on silk historical relic.
E）Painted to print and calcium hydroxide aqueous solution is gradually added in pigment solution until solution ph is neutral or alkalescent.
The present invention adjusts pH to neutrality using calcium hydroxide aqueous solution, and advantage is so to have pigment excellent durable
Solid color.
F）The print modulated is painted into pigment solution painting to be plotted on ripe thin,tough silk, untill paint region pigment is substantially uniform, from
So air-dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, it is complete without repeating to brush
Into rear natural air drying, classical Chinese painting on silk is made.
In paint, never there is not molten pigment little particle.
Because the aging of ancient times ripe classical Chinese painting on silk is the result of the comprehensive functions such as thin,tough silk, glue alum and environment, thus must be to simulation
Classical Chinese painting on silk carry out applying glue alum processing, while herein simulate on the basis of durable fixation treatment is carried out to it, allow color more firmly and
For a long time.
G）By the classical Chinese painting on silk after paint, it is put into ultraviolet deterioration with moisture combined test chamber and carries out aging, setting humidity is 75-85%,
Temperature is 40-50 DEG C；Aging period, classical Chinese painting on silk needs daily turn-over once, and ageing time is 3-4 weeks.
Preferably, step D）In, the mineral pigments is ochre, malachite green, orpiment, indigo.
Preferably, step D）In, the preparation method of the air bladder denaturation extract is as follows：Fresh air bladder is taken to clean, will
It is immersed in water mesohigh boiling 1-2h, and taking-up removes moisture removal, is placed in container and stirs 0.5-1.5h, then add it to dense
Spend in the basic protein enzyme aqueous solution for 0.05-0.15wt% and digested, go out enzyme after enzymolysis at 110-130 DEG C, filter, it is dense
Contracting, dry after air bladder extract is made, air bladder extract is finally soaked into 0.5-1.5h in acetone soln, takes out and is made after drying
Obtain air bladder denaturation extract.
The present invention extracts the collagen in air bladder, fish made from above-mentioned specific process using hot water extraction and enzymatic isolation method
Fish glue extract viscosity is especially good.In order to further improve the stickiness of albumen, go out enzyme when use high temperature, make protein denaturation, then
It is soaked in again in acetone, further improves the stickiness of albumen.
Preferably, pH value of solution is 7.5-9, hydrolysis temperature is 30-40 DEG C, and enzymolysis time is 2-4h.
In order to further improve the stickiness of albumen, alkaline environment is specially used in enzymolysis, makes protein denaturation, improves it
Stickiness.
Preferably, step E）In, pH value of solution is adjusted to 7-8.5.
It is compared with the prior art, the beneficial effects of the invention are as follows：
1st, it can generally be simulated by the present invention and ancient times classical Chinese painting on silk is painted with mineral pigment, be ancient times classical Chinese painting on silk historical relic ageing research
Sample is provided with protection work, there is very important realistic meaning to the precious traditional culture resource of protection China.
2nd, the chemistry and physics and ancient times classical Chinese painting on silk that the classical Chinese painting on silk prepared by the present invention contains are basically identical, by right
It, which carries out deterioration research, can effectively inquire into out the degradation mechanism of ancient times classical Chinese painting on silk, and ageing research is carried out on this basis to be obtained
To more accurate result, have great importance to ancient records and relics protection.
3rd, developed by the present invention with the durable color-fixing method painted in mineral pigment on ancient times classical Chinese painting on silk, for from now on
The durable fixation of colored drawing classical Chinese painting on silk provides a good method.
Embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, comprises the following steps：
A）The kiginu system of beating：White kiginu is cleaned with concentration 10wt% alcoholic solution, then natural air drying is beaten 10 minutes.
B）Jiao Fanshui is prepared：According to mass ratio 3:1.5:150 measure gelatin, alum and deionized water respectively, then by gelatin with
Water is mixed, and stirring to moisture is completely immersed in glue, is placed at after expansion in 70 DEG C of water-bath carries out heating stirring completely, heated
After end, gelatin melts completely, treats that solution is cooled to less than 50 DEG C, and alum is added in solution, stirs completely molten to alum
Solution, is made Jiao Fanshui, is incubated in the water-bath for being subsequently placed in 30 DEG C standby.
C）Gluing：The kiginu that makes will be beaten to be fixed with picture frame, water spray processing is carried out to kiginu, Jiao Fanshui is uniformly brushed in
On kiginu cloth, brushed after one side, after cloth it is micro- it is dry after brush the second face, two sides is brushed finish after, cloth is placed in ventilation
Locate natural air drying, ripe thin,tough silk is made.
D）Print paints pigment solution preparation：By 2:1 mass ratio is by mineral pigments（Ochre）Gone forward side by side with attapulgite mixing
Row vibration, then stands 6 hours, obtains pigment composition；Then 1 is pressed:Air bladder denaturation extract is added to water by 6 mass ratio
In, it is sufficiently stirred for, then adds pigment composition, is placed in 70 DEG C of water-baths and is incubated, it is standby.
The preparation method of the air bladder denaturation extract is as follows：Take fresh air bladder to clean, be immersed in the steaming of water mesohigh
1.5h is boiled, taking-up removes moisture removal, is placed in container and stirs 1h, then add it to the alkali protease water that concentration is 0.1wt%
Digested in solution, pH value of solution is 8, hydrolysis temperature is 35 DEG C, and enzymolysis time is 3h.Go out enzyme, mistake after enzymolysis at 120 DEG C
Filter, concentration, dry after air bladder extract is made, air bladder extract is finally soaked into 1h in acetone soln, takes out and is made after drying
Obtain air bladder denaturation extract.
E）Painted to print and calcium hydroxide aqueous solution is gradually added in pigment solution until solution ph is 7.5.
F）The print modulated is painted into pigment solution painting to be plotted on ripe thin,tough silk, untill paint region pigment is substantially uniform, from
So air-dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, it is complete without repeating to brush
Into rear natural air drying, classical Chinese painting on silk is made.
G）By the classical Chinese painting on silk after paint, it is put into ultraviolet deterioration with moisture combined test chamber and carries out aging, it is 80% to set humidity, temperature
Spend for 45 DEG C；Aging period, classical Chinese painting on silk needs daily turn-over once, and ageing time is 25 days.
Embodiment 2
A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, comprises the following steps：
A）The kiginu system of beating：White kiginu is cleaned with concentration 12wt% alcoholic solution, then natural air drying is beaten 8 minutes.
B）Jiao Fanshui is prepared：According to mass ratio 2:1:100 measure gelatin, alum and deionized water respectively, then by gelatin and water
Mix, and stirring to moisture is completely immersed in glue, is placed at after expansion in 65 DEG C of water-bath carries out heating stirring completely, heating is tied
Shu Hou, gelatin melts completely, treats that solution is cooled to less than 50 DEG C, and alum is added in solution, and stirring to alum is completely dissolved,
Jiao Fanshui is made, is incubated in the water-bath for being subsequently placed in 25 DEG C standby.
C）Gluing：The kiginu that makes will be beaten to be fixed with picture frame, water spray processing is carried out to kiginu, Jiao Fanshui is uniformly brushed in
On kiginu cloth, brushed after one side, after cloth it is micro- it is dry after brush the second face, two sides is brushed finish after, cloth is placed in ventilation
Locate natural air drying, ripe thin,tough silk is made.
D）Print paints pigment solution preparation：By 1.5:1 mass ratio is by mineral pigments（Malachite green）With attapulgite mixing simultaneously
Vibrated, then stand 5 hours, obtain pigment composition；Then 1 is pressed:Air bladder denaturation extract is added to by 5 mass ratio
In water, it is sufficiently stirred for, then adds pigment composition, is placed in 65 DEG C of water-baths and is incubated, it is standby.
The preparation method of the air bladder denaturation extract is as follows：Take fresh air bladder to clean, be immersed in the steaming of water mesohigh
1h is boiled, taking-up removes moisture removal, is placed in container and stirs 0.5h, then add it to the alkali protease that concentration is 0.05wt%
Digested in the aqueous solution, pH value of solution is 7.5, hydrolysis temperature is 30 DEG C, and enzymolysis time is 4h.Go out enzyme after enzymolysis at 110 DEG C,
Filtering, concentration, dry after air bladder extract is made, air bladder extract is finally soaked into 0.5h in acetone soln, drying is taken out
Air bladder denaturation extract is made afterwards.
E）Painted to print and calcium hydroxide aqueous solution is gradually added in pigment solution until solution ph is 7.
F）The print modulated is painted into pigment solution painting to be plotted on ripe thin,tough silk, untill paint region pigment is substantially uniform, from
So air-dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, it is complete without repeating to brush
Into rear natural air drying, classical Chinese painting on silk is made.
G）By the classical Chinese painting on silk after paint, it is put into ultraviolet deterioration with moisture combined test chamber and carries out aging, it is 75% to set humidity, temperature
Spend for 40 DEG C；Aging period, classical Chinese painting on silk needs daily turn-over once, and ageing time is 3 weeks.
Embodiment 3
A kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, comprises the following steps：
A）The kiginu system of beating：White kiginu is cleaned with concentration 14wt% alcoholic solution, then natural air drying is beaten 12 minutes.
B）Jiao Fanshui is prepared：According to mass ratio 4:2:200 measure gelatin, alum and deionized water respectively, then by gelatin and water
Mix, and stirring to moisture is completely immersed in glue, is placed at after expansion in 75 DEG C of water-bath carries out heating stirring completely, heating is tied
Shu Hou, gelatin melts completely, treats that solution is cooled to less than 50 DEG C, and alum is added in solution, and stirring to alum is completely dissolved,
Jiao Fanshui is made, is incubated in the water-bath for being subsequently placed in 35 DEG C standby.
C）Gluing：The kiginu that makes will be beaten to be fixed with picture frame, water spray processing is carried out to kiginu, Jiao Fanshui is uniformly brushed in
On kiginu cloth, brushed after one side, after cloth it is micro- it is dry after brush the second face, two sides is brushed finish after, cloth is placed in ventilation
Locate natural air drying, ripe thin,tough silk is made.
D）Print paints pigment solution preparation：By 2.5:1 mass ratio is by mineral pigments（It is orpiment, indigo）It is mixed with attapulgite
Merging is vibrated, and then stands 7 hours, obtains pigment composition；Then 1 is pressed:7 mass ratio adds air bladder denaturation extract
Add in water, be sufficiently stirred for, then add pigment composition, be placed in 75 DEG C of water-baths and be incubated, it is standby.
The preparation method of the air bladder denaturation extract is as follows：Take fresh air bladder to clean, be immersed in the steaming of water mesohigh
2h is boiled, taking-up removes moisture removal, is placed in container and stirs 1.5h, then add it to the alkali protease that concentration is 0.15wt%
Digested in the aqueous solution, pH value of solution is 9, hydrolysis temperature is 40 DEG C, and enzymolysis time is 4h.Go out enzyme, mistake after enzymolysis at 130 DEG C
Filter, concentration, dry after air bladder extract is made, air bladder extract is finally soaked into 1.5h in acetone soln, taken out after drying
Air bladder denaturation extract is made.
E）Painted to print and calcium hydroxide aqueous solution is gradually added in pigment solution until solution ph is 8.5.
F）The print modulated is painted into pigment solution painting to be plotted on ripe thin,tough silk, untill paint region pigment is substantially uniform, from
So air-dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, it is complete without repeating to brush
Into rear natural air drying, classical Chinese painting on silk is made.
G）By the classical Chinese painting on silk after paint, it is put into ultraviolet deterioration with moisture combined test chamber and carries out aging, it is 85% to set humidity, temperature
Spend for 50 DEG C；Aging period, classical Chinese painting on silk needs daily turn-over once, and ageing time is 4 weeks.
Raw materials used in the present invention, equipment, is the conventional raw material, equipment of this area unless otherwise noted；In the present invention
Method therefor, is the conventional method of this area unless otherwise noted.
It is described above, only it is presently preferred embodiments of the present invention, not the present invention is imposed any restrictions, it is every according to the present invention
Any simple modification, change and equivalent transformation that technical spirit is made to above example, still fall within the technology of the present invention side
The protection domain of case.
Claims (5)
1. a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing, it is characterised in that comprise the following steps：
A）The kiginu system of beating：The alcoholic solution that white kiginu is less than 15wt% with concentration is cleaned, then natural air drying beats 8 ~ 12
Minute；
B）Jiao Fanshui is prepared：According to mass ratio 2 ~ 4:1~2:100 ~ 200 measure gelatin, alum and deionized water respectively, then will
Gelatin is mixed with water, and stirring to moisture is completely immersed in glue, is placed in 65-75 DEG C of water-bath is heated after expansion completely
Stirring, after heating terminates, gelatin melts completely, treats that solution is cooled to less than 50 DEG C, and alum is added in solution, stirs to bright
Alum is completely dissolved, and Jiao Fanshui is made, is incubated in the water-bath for being subsequently placed in 25-35 DEG C standby；
C）Gluing：The kiginu that makes will be beaten to be fixed with picture frame, water spray processing is carried out to kiginu, Jiao Fanshui is uniformly brushed in kiginu
On cloth, brushed after one side, after cloth it is micro- it is dry after brush the second face, two sides is brushed finish after, by cloth be placed in ventilation from
So air-dry, ripe thin,tough silk is made；
D）Print paints pigment solution preparation：By 1.5-2.5:Mineral pigments and attapulgite are mixed and shaken by 1 mass ratio
Swing, then stand 5-7 hours, obtain pigment composition；Then 1 is pressed:Air bladder denaturation extract is added to water by 5-7 mass ratio
In, it is sufficiently stirred for, then adds pigment composition, is placed in 65-75 DEG C of water-bath and is incubated, it is standby；
E）Painted to print and calcium hydroxide aqueous solution is gradually added in pigment solution until solution ph is neutral or alkalescent；
F）The print modulated is painted into pigment solution painting to be plotted on ripe thin,tough silk, untill paint region pigment is substantially uniform, natural wind
It is dry；Then the ripe thin,tough silk after coloring is brushed with Jiao Fanshui, same position is brushed once, without repeating to brush, after the completion of
Natural air drying, is made classical Chinese painting on silk；
G）By the classical Chinese painting on silk after paint, it is put into ultraviolet deterioration with moisture combined test chamber and carries out aging, setting humidity is 75-85%, temperature
For 40-50 DEG C；Aging period, classical Chinese painting on silk needs daily turn-over once, and ageing time is 3-4 weeks.
2. a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing as claimed in claim 1, it is characterised in that
Step D）In, the mineral pigments is ochre, malachite green, orpiment, indigo.
3. a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing as claimed in claim 1 or 2, its feature exists
In step D）In, the preparation method of the air bladder denaturation extract is as follows：Take fresh air bladder to clean, be immersed in water high
Boiling 1-2h is pressed, taking-up removes moisture removal, is placed in container and stirs 0.5-1.5h, then add it to concentration for 0.05-
Digested, go out enzyme after enzymolysis at 110-130 DEG C, filtered in 0.15wt% basic protein enzyme aqueous solution, after concentration, drying
Air bladder extract is made, air bladder extract is finally soaked into 0.5-1.5h in acetone soln, takes out and air bladder change is made after drying
Property extract.
4. a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing as claimed in claim 3, it is characterised in that
PH value of solution is 7.5-9, and hydrolysis temperature is 30-40 DEG C, and enzymolysis time is 2-4h.
5. a kind of durable fixation classical Chinese painting on silk preparation method based on archaistic colored drawing as claimed in claim 1, it is characterised in that
Step E）In, pH value of solution is adjusted to 7-8.5.
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| CN110328998A (en) * | 2019-08-13 | 2019-10-15 | 孙舜尧 | A kind of production method of Chinese realistic painting embroidery mural painting |
| CN113801495A (en) * | 2021-09-29 | 2021-12-17 | 浙江理工大学 | Preparation method of antibacterial composite pigment juice green based on high-energy ball milling method and freeze drying technology |
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