CN107258839A - A kind of composite disinfectant and preparation method thereof - Google Patents
A kind of composite disinfectant and preparation method thereof Download PDFInfo
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- CN107258839A CN107258839A CN201710563359.3A CN201710563359A CN107258839A CN 107258839 A CN107258839 A CN 107258839A CN 201710563359 A CN201710563359 A CN 201710563359A CN 107258839 A CN107258839 A CN 107258839A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/12—Iodine, e.g. iodophors; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/14—Boron; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/46—Stemonaceae [Stemona family], e.g. croomia
Abstract
The invention discloses a kind of composite disinfectant, include the raw material of following parts by weight：0.3~0.8 part of 0.5~2 part of 10~20 parts of paste bentonite, iodine, glacial acetic acid after acidifying, 2~5 parts of traditional Chinese medicine bactericide, 1~2 part of sodium ethylene diamine tetracetate, 0.2~0.6 part of double-chain quaternary ammonium salt, 3~12 parts of sodium cellulose glycolate, 0.4~0.9 part of quaternary ammonium salt synergist, 1~5 part of boric acid, 1~5 part of borax, 0.8~4 part of nano titanium oxide silver antibacterial agent, 0.1~5 part of nonionic surfactant, 40~80 parts of deionized water.Iodine, quaternary ammonium salt and traditional Chinese medicine bactericide are combined by the composite disinfectant, and Disinfection Effect is good, has a safety feature, and stability is strong.
Description
Technical field
The invention belongs to disinfectant technical field, and in particular to a kind of composite disinfectant and preparation method thereof.
Background technology
With the development and the raising of living standards of the people of aquaculture, food security and healthy aquaculture also receive much attention, green
Color aquaculture is more and more valued by the people, and researches and develops more high effects, low-residual, the prevention and health care medication to person poultry safety
It is current matter of utmost importance.Composite disinfectant is used as the necessity of cultivation, health and the success or failure cultivated of the animal directly affected.
Iodine class composite disinfectant is also good because of its has a broad antifungal spectrum, security short to the microorganism killing time, is widely used in medical science and faces
Bed, health, daily life, agriculture and animal husbandry aquaculture etc..But common Operand is big to Skin and mucosa irritation, color depth, stability
It is poor, oxidizable to lose bactericidal action, thus presently commercially available and clinical practice at most be chelated iodine.PVP-I, i.e. polyethylene pyrrole
Pyrrolidone, is the high-molecular compound that iodine is slowly discharged by molecular iodine and the PVP water soluble characteristic being combined into.The molten water of the product
Stability is good, can play a role the long period, but polyvinylpyrrolidone is a kind of macromolecular substances, be difficult naturally under bad border
Degraded, largely uses for long-range circumstances spraying disinfection or animal body surface, will threaten to human and livestock health, and PVP-I consumption
Larger, use cost is high, is the optimal selection of culturist absolutely not.
The content of the invention
The invention provides a kind of composite disinfectant and preparation method thereof, the problem of solving in above-mentioned background technology, institute
State composite disinfectant to be combined iodine, quaternary ammonium salt and traditional Chinese medicine bactericide, Disinfection Effect is good, has a safety feature, and stability is strong.
In order to solve the problem of prior art is present, adopt the following technical scheme that：
A kind of composite disinfectant, includes the raw material of following parts by weight：10~20 parts of paste bentonite, iodine 0.5~2 after acidifying
Part, 0.3~0.8 part of glacial acetic acid, 2~5 parts of traditional Chinese medicine bactericide, 1~2 part of sodium ethylene diamine tetracetate, double-chain quaternary ammonium salt 0.2~0.6
Part, 3~12 parts of sodium cellulose glycolate, 0.4~0.9 part of quaternary ammonium salt synergist, 1~5 part of boric acid, part, nanometer two of borax 1~5
0.8~4 part of titanium oxide silver antibacterial agent, 0.1~5 part of nonionic surfactant, 40~80 parts of deionized water.
It is preferred that, described composite disinfectant includes the raw material of following parts by weight：Paste bentonite 12~18 after acidifying
It is part, 0.7~1.3 part of iodine, 0.4~0.7 part of glacial acetic acid, 3~4 parts of traditional Chinese medicine bactericide, 1.1~1.9 parts of sodium ethylene diamine tetracetate, double
0.3~0.5 part of chain quaternary ammonium salt, 5~10 parts of sodium cellulose glycolate, 0.5~0.8 part of quaternary ammonium salt synergist, 2~4 parts of boric acid, boron
2~4 parts of sand, 1.6~3.2 parts of nano titanium oxide silver antibacterial agent, 1~4 part of nonionic surfactant, deionized water 50~70
Part.
It is preferred that, described composite disinfectant includes the raw material of following parts by weight：15 parts of paste bentonite after acidifying,
1.2 parts of iodine, 0.6 part of glacial acetic acid, 3.5 parts of traditional Chinese medicine bactericide, 1.7 parts of sodium ethylene diamine tetracetate, 0.4 part of double-chain quaternary ammonium salt, hydroxyl first
It is 8 parts of base sodium cellulosate, 0.7 part of quaternary ammonium salt synergist, 3 parts of boric acid, 3 parts of borax, 2.1 parts of nano titanium oxide silver antibacterial agent, non-
3 parts of ionic surface active agent, 60 parts of deionized water.
It is preferred that, the quaternary ammonium salt synergist is cetyl trimethylammonium bromide or hexadecyltrimethylammonium chloride.
It is preferred that, the nonionic surfactant is AEO, APES, aliphatic acid
One or more in macrogol ester, aliphatic amine polyoxyethylene ether and Tween 80.
It is preferred that, the double-chain quaternary ammonium salt is selected from double eight alkyl dimethyl ammonium chlorides, didecyl Dimethy ammonium chloride, double
Dodecyl dimethyl ammonium chloride, dioctadecyl dimethyl ammonium chloride, double eight alkyl dimethyls ammonium bromides, double ten alkyl-dimethyls
At least one of base ammonium bromide, didodecyldimethylammbromide bromide and DDA.
It is preferred that, the traditional Chinese medicine bactericide is made up of the raw material of following parts by weight：18~25 parts of aloe, kuh-seng 28~33
Part, 20~40 parts of oriental wormwood, 12~18 parts of cloves, 13~22 parts of Celastrus angulatus, 10~15 parts of honeysuckle, 17~22 parts of frutus cnidii, remove
10~15 parts of worm chrysanthemum, 18~26 parts of the tuber of stemona, 10~20 parts of talcum powder.
It is preferred that, the paste bentonite after the acidifying is obtained by following methods：By the swelling that water content is 70%~80%
Soil paste body and hydrochloric acid are uniformly mixed, and are placed in acidification 1~3 day in acidification pool, produce the paste bentonite after acidifying, institute
The mass ratio for stating hydrochloric acid and bentonite slurry is 1:9, the concentration of hydrochloric acid is 31%.
A kind of method for preparing the composite disinfectant, comprises the following steps：
（1）By above-mentioned formula weigh acidifying after paste bentonite, iodine, glacial acetic acid, traditional Chinese medicine bactericide, sodium ethylene diamine tetracetate,
Double-chain quaternary ammonium salt, sodium cellulose glycolate, quaternary ammonium salt synergist, boric acid, borax, nano titanium oxide silver antibacterial agent, nonionic
Surfactant, deionized water, it is standby；
（2）Each raw material is first put into mixer and is uniformly mixed, then is placed in ball mill ball milling into pasty mixture, then
It is placed in again in homogenizer and carries out high-speed stirred 1~2 hour, obtains composite disinfectant semi-finished product；
（3）By step（2）Obtained composite disinfectant semi-finished product carry out vacuum degassing process processing, produce the composite disinfecting
Agent.
It is preferred that, the mixing speed of the high-speed stirred is 2000~3000r/min.
Compared with prior art, it has the advantages that the present invention：
Iodine, quaternary ammonium salt and traditional Chinese medicine bactericide are combined by composite disinfectant of the present invention, and Disinfection Effect is good, security performance
Good, stability is strong, specific as follows：
（1）Composite disinfectant of the present invention is made with the paste bentonite after being acidified, iodine, traditional Chinese medicine bactericide and double-chain quaternary ammonium salt
For raw material, iodine, traditional Chinese medicine bactericide and double-chain quaternary ammonium salt three mutually act synergistically, the life of microorganism of quaternary ammonium salt material damage
Thing film, making the permeability of film increases, and is easy to the intrusion of iodine and traditional Chinese medicine bactericide and plays a role, Disinfection Effect is good, after acidifying
Paste bentonite changes the stability of the composite disinfectant containing iodine, extends the term of validity of composite disinfectant；
（2）Composite disinfectant of the present invention also added quaternary ammonium salt synergist, add cetyl trimethylammonium bromide/ten
After six alkyl trimethyl ammonium chlorides, the antibacterial activity of quaternary ammonium salt is greatly improved, with iodine coordinate after, enhance iodine Disinfection Effect and
The stability of iodine, also has stronger sterilizing ability to bacterial spore；
（3）Composite disinfectant high safety of the present invention, it is non-stimulated to skin, it can be used for band livestock and poultry sterilization.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1
The present embodiment is related to a kind of composite disinfectant, includes the raw material of following parts by weight：10 parts of paste bentonite, iodine after acidifying
0.5 part, 0.3 part of glacial acetic acid, 2 parts of traditional Chinese medicine bactericide, 1 part of sodium ethylene diamine tetracetate, 0.2 part of double-chain quaternary ammonium salt, hydroxylmethyl cellulose
Plain 3 parts of sodium, 0.4 part of quaternary ammonium salt synergist, 1 part of boric acid, 1 part of borax, 0.8 part of nano titanium oxide silver antibacterial agent, nonionic table
0.1 part of face activating agent, 40 parts of deionized water.
Wherein, the quaternary ammonium salt synergist is cetyl trimethylammonium bromide.
Wherein, the nonionic surfactant is AEO.
Wherein, the double-chain quaternary ammonium salt is double eight alkyl dimethyl ammonium chlorides.
Wherein, the traditional Chinese medicine bactericide is made up of the raw material of following parts by weight：18 parts of aloe, 28 parts of kuh-seng, 20 parts of oriental wormwood,
12 parts of cloves, 13 parts of Celastrus angulatus, 10 parts of honeysuckle, 17 parts of frutus cnidii, 10 parts of Dalmatian chrysanthemum, 18 parts of the tuber of stemona, 10 parts of talcum powder.
Wherein, the paste bentonite after the acidifying is obtained by following methods：By water content for 70% bentonite slurry and
Hydrochloric acid is uniformly mixed, and is placed in acidification 1 day in acidification pool, produces the paste bentonite after acidifying, the hydrochloric acid and swollen
The mass ratio of the native mud of profit is 1:9, the concentration of hydrochloric acid is 31%.
A kind of method for preparing the composite disinfectant, comprises the following steps：
（1）By above-mentioned formula weigh acidifying after paste bentonite, iodine, glacial acetic acid, traditional Chinese medicine bactericide, sodium ethylene diamine tetracetate,
Double-chain quaternary ammonium salt, sodium cellulose glycolate, quaternary ammonium salt synergist, boric acid, borax, nano titanium oxide silver antibacterial agent, nonionic
Surfactant, deionized water, it is standby；
（2）Each raw material is first put into mixer and is uniformly mixed, then is placed in ball mill ball milling into pasty mixture, then
It is placed in again in homogenizer and carries out high-speed stirred 1 hour, obtains composite disinfectant semi-finished product；
（3）By step（2）Obtained composite disinfectant semi-finished product carry out vacuum degassing process processing, produce the composite disinfecting
Agent.
Wherein, the mixing speed of the high-speed stirred is 2000r/min.
Embodiment 2
The present embodiment is related to a kind of composite disinfectant, includes the raw material of following parts by weight：20 parts of paste bentonite, iodine after acidifying
2 parts, 0.8 part of glacial acetic acid, 5 parts of traditional Chinese medicine bactericide, 2 parts of sodium ethylene diamine tetracetate, 0.6 part of double-chain quaternary ammonium salt, hydroxymethyl cellulose
12 parts of sodium, 0.9 part of quaternary ammonium salt synergist, 5 parts of boric acid, 5 parts of borax, 4 parts of nano titanium oxide silver antibacterial agent, non-ionic surface are lived
5 parts of agent of property, 80 parts of deionized water.
Wherein, the quaternary ammonium salt synergist is hexadecyltrimethylammonium chloride.
Wherein, the nonionic surfactant is APES.
Wherein, the double-chain quaternary ammonium salt is didecyl Dimethy ammonium chloride.
Wherein, the traditional Chinese medicine bactericide is made up of the raw material of following parts by weight：25 parts of aloe, 33 parts of kuh-seng, 40 parts of oriental wormwood,
18 parts of cloves, 22 parts of Celastrus angulatus, 15 parts of honeysuckle, 22 parts of frutus cnidii, 15 parts of Dalmatian chrysanthemum, 26 parts of the tuber of stemona, 20 parts of talcum powder.
Wherein, the paste bentonite after the acidifying is obtained by following methods：By water content for 80% bentonite slurry and
Hydrochloric acid is uniformly mixed, and is placed in acidification 3 days in acidification pool, produces the paste bentonite after acidifying, the hydrochloric acid and swollen
The mass ratio of the native mud of profit is 1:9, the concentration of hydrochloric acid is 31%.
A kind of method for preparing the composite disinfectant, comprises the following steps：
（1）By above-mentioned formula weigh acidifying after paste bentonite, iodine, glacial acetic acid, traditional Chinese medicine bactericide, sodium ethylene diamine tetracetate,
Double-chain quaternary ammonium salt, sodium cellulose glycolate, quaternary ammonium salt synergist, boric acid, borax, nano titanium oxide silver antibacterial agent, nonionic
Surfactant, deionized water, it is standby；
（2）Each raw material is first put into mixer and is uniformly mixed, then is placed in ball mill ball milling into pasty mixture, then
It is placed in again in homogenizer and carries out high-speed stirred 2 hours, obtains composite disinfectant semi-finished product；
（3）By step（2）Obtained composite disinfectant semi-finished product carry out vacuum degassing process processing, produce the composite disinfecting
Agent.
Wherein, the mixing speed of the high-speed stirred is 3000r/min.
Embodiment 3
The present embodiment is related to a kind of composite disinfectant, includes the raw material of following parts by weight：12 parts of paste bentonite, iodine after acidifying
0.7 part, 0.4 part of glacial acetic acid, 3 parts of traditional Chinese medicine bactericide, 1.1 parts of sodium ethylene diamine tetracetate, 0.3 part of double-chain quaternary ammonium salt, methylol it is fine
Plain 5 parts of the sodium of dimension, 0.5 part of quaternary ammonium salt synergist, 2 parts of boric acid, 2 parts of borax, 1.6 parts of nano titanium oxide silver antibacterial agent, nonionic
1 part of surfactant, 50 parts of deionized water.
Wherein, the quaternary ammonium salt synergist is cetyl trimethylammonium bromide.
Wherein, the nonionic surfactant is fatty acid polyethylene glycol ester.
Wherein, the double-chain quaternary ammonium salt be double dodecyl dimethyl ammonium chlorides, dioctadecyl dimethyl ammonium chloride with
The mixture of double eight alkyl dimethyls ammonium bromides.
Wherein, the traditional Chinese medicine bactericide is made up of the raw material of following parts by weight：20 parts of aloe, 30 parts of kuh-seng, 25 parts of oriental wormwood,
14 parts of cloves, 15 parts of Celastrus angulatus, 12 parts of honeysuckle, 19 parts of frutus cnidii, 11 parts of Dalmatian chrysanthemum, 20 parts of the tuber of stemona, 13 parts of talcum powder.
Wherein, the paste bentonite after the acidifying is obtained by following methods：By water content for 72% bentonite slurry and
Hydrochloric acid is uniformly mixed, and is placed in acidification 2 days in acidification pool, produces the paste bentonite after acidifying, the hydrochloric acid and swollen
The mass ratio of the native mud of profit is 1:9, the concentration of hydrochloric acid is 31%.
A kind of method for preparing the composite disinfectant, comprises the following steps：
（1）By above-mentioned formula weigh acidifying after paste bentonite, iodine, glacial acetic acid, traditional Chinese medicine bactericide, sodium ethylene diamine tetracetate,
Double-chain quaternary ammonium salt, sodium cellulose glycolate, quaternary ammonium salt synergist, boric acid, borax, nano titanium oxide silver antibacterial agent, nonionic
Surfactant, deionized water, it is standby；
（2）Each raw material is first put into mixer and is uniformly mixed, then is placed in ball mill ball milling into pasty mixture, then
It is placed in again in homogenizer and carries out high-speed stirred 1.2 hours, obtains composite disinfectant semi-finished product；
（3）By step（2）Obtained composite disinfectant semi-finished product carry out vacuum degassing process processing, produce the composite disinfecting
Agent.
Wherein, the mixing speed of the high-speed stirred is 2200r/min.
Embodiment 4
The present embodiment is related to a kind of composite disinfectant, includes the raw material of following parts by weight：18 parts of paste bentonite, iodine after acidifying
1.3 parts, 0.7 part of glacial acetic acid, 4 parts of traditional Chinese medicine bactericide, 1.9 parts of sodium ethylene diamine tetracetate, 0.5 part of double-chain quaternary ammonium salt, methylol it is fine
Plain 10 parts of the sodium of dimension, 0.8 part of quaternary ammonium salt synergist, 4 parts of boric acid, 4 parts of borax, 3.2 parts of nano titanium oxide silver antibacterial agent, nonionic
4 parts of surfactant, 70 parts of deionized water.
Wherein, the quaternary ammonium salt synergist is hexadecyltrimethylammonium chloride.
Wherein, the nonionic surfactant is the mixture of aliphatic amine polyoxyethylene ether and Tween 80.
Wherein, the double-chain quaternary ammonium salt is double eight alkyl dimethyl ammonium bromides, didecyl Dimethy ammonium bromide, double 12
The mixture of alkyl dimethyl ammonium bromide and DDA.
Wherein, the traditional Chinese medicine bactericide is made up of the raw material of following parts by weight：21 parts of aloe, 31 parts of kuh-seng, 30 parts of oriental wormwood,
15 parts of cloves, 17 parts of Celastrus angulatus, 13 parts of honeysuckle, 20 parts of frutus cnidii, 13 parts of Dalmatian chrysanthemum, 23 parts of the tuber of stemona, 15 parts of talcum powder.
Wherein, the paste bentonite after the acidifying is obtained by following methods：By water content for 75% bentonite slurry and
Hydrochloric acid is uniformly mixed, and is placed in acidification 2 days in acidification pool, produces the paste bentonite after acidifying, the hydrochloric acid and swollen
The mass ratio of the native mud of profit is 1:9, the concentration of hydrochloric acid is 31%.
A kind of method for preparing the composite disinfectant, comprises the following steps：
（1）By above-mentioned formula weigh acidifying after paste bentonite, iodine, glacial acetic acid, traditional Chinese medicine bactericide, sodium ethylene diamine tetracetate,
Double-chain quaternary ammonium salt, sodium cellulose glycolate, quaternary ammonium salt synergist, boric acid, borax, nano titanium oxide silver antibacterial agent, nonionic
Surfactant, deionized water, it is standby；
（2）Each raw material is first put into mixer and is uniformly mixed, then is placed in ball mill ball milling into pasty mixture, then
It is placed in again in homogenizer and carries out high-speed stirred 1.5 hours, obtains composite disinfectant semi-finished product；
（3）By step（2）Obtained composite disinfectant semi-finished product carry out vacuum degassing process processing, produce the composite disinfecting
Agent.
Wherein, the mixing speed of the high-speed stirred is 2500r/min.
Embodiment 5
The present embodiment is related to a kind of composite disinfectant, includes the raw material of following parts by weight：15 parts of paste bentonite, iodine after acidifying
1.2 parts, 0.6 part of glacial acetic acid, 3.5 parts of traditional Chinese medicine bactericide, 1.7 parts of sodium ethylene diamine tetracetate, 0.4 part of double-chain quaternary ammonium salt, methylol
8 parts of sodium cellulosate, 0.7 part of quaternary ammonium salt synergist, 3 parts of boric acid, 3 parts of borax, 2.1 parts of nano titanium oxide silver antibacterial agent, it is non-from
Sub- 3 parts of surfactant, 60 parts of deionized water.
Wherein, the quaternary ammonium salt synergist is hexadecyltrimethylammonium chloride.
Wherein, the nonionic surfactant is AEO, APES, fatty acid polyglycol
The mixture of glycol ester, aliphatic amine polyoxyethylene ether and Tween 80.
Wherein, the double-chain quaternary ammonium salt be double dodecyl dimethyl ammonium chlorides, it is dioctadecyl dimethyl ammonium chloride, double
Eight alkyl dimethyl ammonium bromides, didecyl Dimethy ammonium bromide, didodecyldimethylammbromide bromide and double octadecyls two
The mixture of methyl bromide ammonium.
Wherein, the traditional Chinese medicine bactericide is made up of the raw material of following parts by weight：22 parts of aloe, 31 parts of kuh-seng, 35 parts of oriental wormwood,
17 parts of cloves, 20 parts of Celastrus angulatus, 14 parts of honeysuckle, 20 parts of frutus cnidii, 14 parts of Dalmatian chrysanthemum, 22 parts of the tuber of stemona, 13 parts of talcum powder.
Wherein, the paste bentonite after the acidifying is obtained by following methods：By water content for 78% bentonite slurry and
Hydrochloric acid is uniformly mixed, and is placed in acidification 2 days in acidification pool, produces the paste bentonite after acidifying, the hydrochloric acid and swollen
The mass ratio of the native mud of profit is 1:9, the concentration of hydrochloric acid is 31%.
A kind of method for preparing the composite disinfectant, comprises the following steps：
（1）By above-mentioned formula weigh acidifying after paste bentonite, iodine, glacial acetic acid, traditional Chinese medicine bactericide, sodium ethylene diamine tetracetate,
Double-chain quaternary ammonium salt, sodium cellulose glycolate, quaternary ammonium salt synergist, boric acid, borax, nano titanium oxide silver antibacterial agent, nonionic
Surfactant, deionized water, it is standby；
（2）Each raw material is first put into mixer and is uniformly mixed, then is placed in ball mill ball milling into pasty mixture, then
It is placed in again in homogenizer and carries out high-speed stirred 1.8 hours, obtains composite disinfectant semi-finished product；
（3）By step（2）Obtained composite disinfectant semi-finished product carry out vacuum degassing process processing, produce the composite disinfecting
Agent.
Wherein, the mixing speed of the high-speed stirred is 2800r/min.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (10)
1. a kind of composite disinfectant, it is characterised in that include the raw material of following parts by weight：Paste bentonite 10~20 after acidifying
Part, 0.5~2 part of iodine, 0.3~0.8 part of glacial acetic acid, 2~5 parts of traditional Chinese medicine bactericide, 1~2 part of sodium ethylene diamine tetracetate, double-strand quaternary ammonium
0.2~0.6 part of salt, 3~12 parts of sodium cellulose glycolate, 0.4~0.9 part of quaternary ammonium salt synergist, 1~5 part of boric acid, borax 1~5
Part, 0.8~4 part of nano titanium oxide silver antibacterial agent, 0.1~5 part of nonionic surfactant, 40~80 parts of deionized water.
2. composite disinfectant according to claim 1, it is characterised in that include the raw material of following parts by weight：After acidifying
12~18 parts of paste bentonite, 0.7~1.3 part of iodine, 0.4~0.7 part of glacial acetic acid, 3~4 parts of traditional Chinese medicine bactericide, ethylenediamine tetrem
Sour 1.1~1.9 parts of sodium, 0.3~0.5 part of double-chain quaternary ammonium salt, 5~10 parts of sodium cellulose glycolate, quaternary ammonium salt synergist 0.5~
0.8 part, 2~4 parts of boric acid, 2~4 parts of borax, 1.6~3.2 parts of nano titanium oxide silver antibacterial agent, nonionic surfactant 1
~4 parts, 50~70 parts of deionized water.
3. composite disinfectant according to claim 1, it is characterised in that include the raw material of following parts by weight：After acidifying
15 parts of paste bentonite, 1.2 parts of iodine, 0.6 part of glacial acetic acid, 3.5 parts of traditional Chinese medicine bactericide, 1.7 parts of sodium ethylene diamine tetracetate, double-strand season
0.4 part of ammonium salt, 8 parts of sodium cellulose glycolate, 0.7 part of quaternary ammonium salt synergist, 3 parts of boric acid, 3 parts of borax, nano titanium oxide silver
2.1 parts of antiseptic, 3 parts of nonionic surfactant, 60 parts of deionized water.
4. composite disinfectant according to claim 1, it is characterised in that the quaternary ammonium salt synergist is cetyl front three
Base ammonium bromide or hexadecyltrimethylammonium chloride.
5. composite disinfectant according to claim 1, it is characterised in that the nonionic surfactant is poly alkyl alcohol
One kind in oxygen vinethene, APES, fatty acid polyethylene glycol ester, aliphatic amine polyoxyethylene ether and Tween 80 or
It is several.
6. composite disinfectant according to claim 1, it is characterised in that the double-chain quaternary ammonium salt is selected from double eight alkyl-dimethyls
Ammonium chloride, didecyl Dimethy ammonium chloride, double dodecyl dimethyl ammonium chlorides, dioctadecyl dimethyl ammonium chloride,
Double eight alkyl dimethyls ammonium bromides, didecyl Dimethy ammonium bromide, didodecyldimethylammbromide bromide and double octadecyls
At least one of ditallowdimethyl ammonium bromide.
7. composite disinfectant according to claim 1, it is characterised in that the traditional Chinese medicine bactericide by following parts by weight original
Material is made：18~25 parts of aloe, 28~33 parts of kuh-seng, 20~40 parts of oriental wormwood, 12~18 parts of cloves, 13~22 parts of Celastrus angulatus, gold
10~15 parts of honeysuckle flower, 17~22 parts of frutus cnidii, 10~15 parts of Dalmatian chrysanthemum, 18~26 parts of the tuber of stemona, 10~20 parts of talcum powder.
8. composite disinfectant according to claim 1, it is characterised in that the paste bentonite after the acidifying is by with lower section
Method is obtained：Water content is uniformly mixed for 70%~80% bentonite slurry and hydrochloric acid, acidification 1 in acidification pool is placed in
~3 days, the paste bentonite after acidifying is produced, the mass ratio of the hydrochloric acid and bentonite slurry is 1:9, the concentration of hydrochloric acid is
31%。
9. a kind of method for preparing any one of claim 1~8 composite disinfectant, it is characterised in that comprise the following steps：
（1）By above-mentioned formula weigh acidifying after paste bentonite, iodine, glacial acetic acid, traditional Chinese medicine bactericide, sodium ethylene diamine tetracetate,
Double-chain quaternary ammonium salt, sodium cellulose glycolate, quaternary ammonium salt synergist, boric acid, borax, nano titanium oxide silver antibacterial agent, nonionic
Surfactant, deionized water, it is standby；
（2）Each raw material is first put into mixer and is uniformly mixed, then is placed in ball mill ball milling into pasty mixture, then
It is placed in again in homogenizer and carries out high-speed stirred 1~2 hour, obtains composite disinfectant semi-finished product；
（3）By step（2）Obtained composite disinfectant semi-finished product carry out vacuum degassing process processing, produce the composite disinfecting
Agent.
10. preparation method according to claim 9, it is characterised in that the mixing speed of the high-speed stirred is 2000~
3000r/min。
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| CN108294069A (en) * | 2018-02-07 | 2018-07-20 | 合肥华盖生物科技有限公司 | A kind of disinfectant for animals and preparation method thereof |
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| WO2023027134A1 (en) * | 2021-08-25 | 2023-03-02 | アース製薬株式会社 | Composition |
| WO2023115446A1 (en) * | 2021-12-23 | 2023-06-29 | 泰波亚太有限公司 | Cleaning agent, and preparation method therefor and use thereof |
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