CN107213050A - A kind of floral water containing plant component and preparation method thereof - Google Patents
A kind of floral water containing plant component and preparation method thereof Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract
The invention belongs to daily chemical product technical field, and in particular to a kind of floral water containing plant component and preparation method thereof, and the floral water is mainly made up of the raw material of following parts by weight：5 10 parts of 40 50 parts of ethanol, 55 75 parts of deionized water, 47 parts of dipropylene glycol, 37 parts of sodium citrate, 26 parts of antioxidant, 5 10 parts of peppermint oil, 5 10 parts of lemonweed essential oil, 6 11 parts of crape myrtle extract solution, 48 parts of Verbena officinalis essential oil, 6 10 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution.The floral water of the present invention mainly has drawn from plant, with the bland feature of safety, there is good mosquito repellent, repellent antipruritic and relieving mental strain and helping sleep due to the addition of lemonweed essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution；Meanwhile, floral water material requested of the present invention is simple and easy to get, and preparation technology is simple, there is very big promotional value.
Description
Technical field
The invention belongs to daily chemical product technical field, and in particular to a kind of containing the floral water of plant component and its preparation side
Method.
Background technology
Mosquito needs to suck human blood to lay eggs, educate ovum, therefore brings many troubles to the mankind.Human body is by bite by mosquitos
Afterwards, skin can become red and swollen, and sufferings unbearably, have an effect on outward appearance.In addition, bite by mosquitos can also influence to sleep, propagate malaria,
Filariasis, Japanese Type-B encephalitis and leather step on the diseases such as heat, totally unfavorable to human body health.In order to take precautions against bite by mosquitos,
Most people can select the sprinkling floral water on one's body to carry out expelling mosquito.Tradition has the floral water of mosquito-repelling function, and its is main
Anophelifuge activity composition be generally the household pesticides compositions such as Metadelphene, dimethyl phthalate, mosquito repellent fat or dihydropyrone, belong to micro- malicious product,
And anaphylaxis irritant to the skin of contact.In addition, the reason for traditional floral water is in order in terms of preparation stabilization is usually contained
The ethanol of higher concentration（70% or so）, thus some side effects are brought, such as accelerate skin water loss, cause dry skin, appearance
Easy aging, generation wrinkle, the stimulation to the tender skin of infant are then more prominent.At the children particularly infant of less than 6 years old
In the vigorous stage of growing, skin absorbability is stronger, and respiratory tract resistivity is weaker, should avoid producing using chemical mosquito repellent
Product；And after bite by mosquitos, small wound can be left on skin, if at this moment using traditional floral water, ethanol therein, change
Learn the chemical substances such as culicifuge directly can enter deep skin by these small wounds, so as to produce stimulation pain, exacerbation
Inflammation, causes skin injury, particularly Metadelphene, such as long-term or a large amount of using it is also possible that neurological symptom is white with inducing
Blood disease etc..Therefore, the mosquito-repellent perfume of exploitation safety non-toxic has important social effect.
The content of the invention
It is an object of the present invention to have stimulation to human body for the chemical composition added in many floral water of above-mentioned in the market
There is provided a kind of floral water with mosquito repellent, repellent antipruritic and efficacy of tranquilizing mind and improving sleeping containing plant component with hypersensitive problem for property.
To reach above-mentioned purpose, the technical solution adopted in the present invention is：
A kind of floral water containing plant component, is mainly made up of the raw material of following parts by weight：40-50 parts of ethanol, deionized water 55-
75 parts, 4-7 parts of dipropylene glycol, 3-7 parts of sodium citrate, 2-6 parts of antioxidant, 5-10 parts of peppermint oil, 5-10 parts of lemonweed essential oil,
5-10 parts of 6-11 parts of crape myrtle extract solution, 4-8 parts of Verbena officinalis essential oil, 6-10 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution.
In the present invention, further instruction, the floral water is mainly made up of the raw material of following parts by weight：Ethanol 43-
47 parts, 60-70 parts of deionized water, 5-6 parts of dipropylene glycol, 4-6 parts of sodium citrate, 3-5 parts of antioxidant, 6-9 parts of peppermint oil, lemon
6-9 parts of vanilla essential oil, 7-10 parts of crape myrtle extract solution, 5-7 parts of Verbena officinalis essential oil, 7-9 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution
6-9 parts.
In the present invention, further instruction, the floral water is mainly made up of the raw material of following parts by weight：Ethanol 45
Part, 65 parts of deionized water, 5.5 parts of dipropylene glycol, 5 parts of sodium citrate, 4 parts of antioxidant, 8 parts of peppermint oil, lemonweed essential oil 7
Part, 8 parts of crape myrtle extract solution, 6 parts of Verbena officinalis essential oil, 8 parts of Radix Sophorae Flavescentis extractive liquid and 8 parts of Herba Andrographitis extract solution.
In the present invention, further instruction, described antioxidant is BHT.
In the present invention, further instruction, the concentration of the ethanol is 70%-75%.
A kind of method for preparing the floral water containing plant component, comprises the following steps：
（1）By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, it is standby；
（2）Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 85-95 DEG C, and mixture 1 is heated 1-2 hours under conditions of being maintained at 85-95 DEG C, is mixed
Thing 2；
（3）To step（2）Dipropylene glycol, peppermint oil, lemonweed essential oil, crape myrtle extract solution, horse are added in the mixture 2 of gained
Whip grass essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, and 8- is stirred with 1000-1200r/min mixing speed
10min, is well mixed each raw material, obtains mixture 3；
（4）By step（3）The mixture 3 of gained carries out refrigeration 3-5 hours under conditions of being placed in 0-6 DEG C, produces floral water.
In the present invention, further instruction, lemonweed essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid
Extracting method with Herba Andrographitis extract solution is as follows：
The extracting method of lemonweed essential oil：1）The carrying agent for accounting for lemonweed weight 0.3-0.5% is sprayed into lemonweed
In, then continuous cycling extraction, control extraction kettle temperature in lemonweed addition extraction kettle, will be carried out with supercritical carbon dioxide fluid
30-42 DEG C of degree, extracts pressure 15-25MPa, flow velocity is 15-20kg/h, extraction time 1.5-2.5h；The carrying agent is by following
The each component of mass fraction is mixed：50-55 parts of ethanol, 3-5 parts of triethanolamine, 0.3-0.5 parts of hexamethylene；（2）Will extraction
CO 2 fluid afterwards is separated into separator, and the flow of CO 2 fluid is 12-15kg/h, and separator pressure is
8-10MPa, temperature is 40-45 DEG C, extracts 1-3h, is released from separator bottom after extract, standing, lemon is obtained through water-oil separating
Lemon vanilla essential oil.
The extracting method of crape myrtle extract solution：First each constitutive material pick selecting pure, then claimed according to composition by weight
Take crape myrtle petal to be placed in ultrasonic extractor, add 2-4 times of weight than pure water, with 28KHz under 45-48 DEG C of constant temperature
Concussion filters to obtain crape myrtle extract solution after extracting 25-30 minutes under frequency.
The extracting method of Verbena officinalis essential oil：（1）The fresh Verbena officinalis strain body of harvesting, including stem, leaf, flower, clean up, get rid of
Solid carbon dioxide point；（2）With bruisher, by Verbena officinalis hand hay cutter, to be broken into diameter≤2cm small broken section；（3）Put Verbena officinalis of the hand hay cutter after broken into destilling tower
Steam distillation is carried out, 120 DEG C >=vapo(u)rizing temperature >=100 DEG C, boiler bottom will keep moisture, raw material to touch pot, in order to avoid production
Green coke is pasted；（4）The mixing gas distilled out is delivered directly to cooling tower, and 0 DEG C of -5 DEG C≤chilling temperature ＜ separates out ice cube, obtained
Pure Verbena officinalis essential oil.
The extracting method of Radix Sophorae Flavescentis extractive liquid：Weigh kuh-seng coarse powder appropriate, 75% alcohol solution dipping 0.15-0.8h, heating
Decoct and extract 3 times, the 1st time plus 11-15 times measure 75% ethanol solution, extract 1-2.5h, it is molten to measure 75% ethanol the 2nd time plus 9-11 times
Liquid, extracts 1-1.5h, and the 3rd time plus 6-9 times measure 75% ethanol solution, extracts 0.5-1.5h, every time filtration, merging filtrate, filtrate
Volume concentration to 4-8 times of kuh-seng weight, filtering produces Radix Sophorae Flavescentis extractive liquid.
The extracting method of Herba Andrographitis extract solution：Take Herba Andrographitis to go the removal of impurity, clean, add the ethanol of 10-16 times of its weight
Solution, under 230-270MPa, ultra high pressure treatment 1-4min；Then at 38-46 DEG C, ultrasonic wave extraction 12-24min；Centrifugation
Separation, takes supernatant, obtains Herba Andrographitis extract solution.
The present invention has the advantage that compared with prior art：
1. floral water of the present invention is using plant component as main component, with good mosquito repellent, repellent antipruritic and relieving mental strain and helping sleep
Effect.Lemonweed essential oil gives out light citrus scented, makes one spirit and QI cleaning, while its fragrance distributed has well
Mosquito repellent function；The fragrance that crape myrtle extract solution is distributed is harmless, while playing the role of to make mosquito hear its perfume and keep away from, two kinds of essences
Mixing can strengthen mosquito repellent function to oil in certain proportion.Verbena officinalis essential oil has fragrant and sweet lemon, there is the effect eased off the pressure
Really, it can make one to feel to loosen, and be fallen asleep under the atmosphere releived.Herba Andrographitis extract solution has clearing heat and detoxicating, anti-inflammatory, swelling and pain relieving
Effect, its addition can alleviate skin swelling and pain, the symptom of itch；Radix Sophorae Flavescentis extractive liquid is in addition to effect containing subdhing swelling and detoxicating, especially
Be good at desinsection antipruritic, there is significant curative effect for pruritic skin, after mosquito bite, skin occur local itch,
Swell and ache, the addition of Herba Andrographitis extract solution and Radix Sophorae Flavescentis extractive liquid can effectively alleviate this symptom.Dipropylene glycol is a class NMF, thorn
Swash property small, with good moisture-keeping efficacy, it, which is added, can alleviate the problem of alcohol volatilization causes dry skin in floral water.This hair
Bright middle lemonweed essential oil, crape myrtle extract solution, Verbena officinalis essential oil, the addition of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution not only make
Floral water smell is unique, also assigns the good mosquito repellent of floral water, effect of repellent antipruritic；Tradition flower is alleviated in the addition of dipropylene glycol
The problem of dry skin occurred after dew use.
1. the material source used in floral water of the present invention is in plant extract material, harmless, excitant is small, preparation side
Method is simple, and required equipment is common equipment, is well suited for large-scale production.
Embodiment
The invention provides providing a kind of floral water containing plant component and preparation method thereof, for make the purpose of the present invention,
Technical scheme and effect are clearer, clear and definite, and the present invention is described in more detail below.It should be appreciated that described herein
Specific embodiment only to explain the present invention, is not intended to limit the present invention.
In following examples, lemonweed essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis are carried
Take liquid and extracted with following extracting method：
The extracting method of lemonweed essential oil：1）The carrying agent for accounting for lemonweed weight 0.3-0.5% is sprayed into lemonweed
In, then continuous cycling extraction, control extraction kettle temperature in lemonweed addition extraction kettle, will be carried out with supercritical carbon dioxide fluid
30-42 DEG C of degree, extracts pressure 15-25MPa, flow velocity is 15-20kg/h, extraction time 1.5-2.5h；The carrying agent is by following
The each component of mass fraction is mixed：50-55 parts of ethanol, 3-5 parts of triethanolamine, 0.3-0.5 parts of hexamethylene；（2）Will extraction
CO 2 fluid afterwards is separated into separator, and the flow of CO 2 fluid is 12-15kg/h, and separator pressure is
8-10MPa, temperature is 40-45 DEG C, extracts 1-3h, is released from separator bottom after extract, standing, lemon is obtained through water-oil separating
Lemon vanilla essential oil.
The extracting method of crape myrtle extract solution：First each constitutive material pick selecting pure, then claimed according to composition by weight
Take crape myrtle petal to be placed in ultrasonic extractor, add 2-4 times of weight than pure water, with 28KHz under 45-48 DEG C of constant temperature
Concussion filters to obtain crape myrtle extract solution after extracting 25-30 minutes under frequency.
The extracting method of Verbena officinalis essential oil：（1）The fresh Verbena officinalis strain body of harvesting, including stem, leaf, flower, clean up, get rid of
Solid carbon dioxide point；（2）With bruisher, by Verbena officinalis hand hay cutter, to be broken into diameter≤2cm small broken section；（3）Put Verbena officinalis of the hand hay cutter after broken into destilling tower
Steam distillation is carried out, 120 DEG C >=vapo(u)rizing temperature >=100 DEG C, boiler bottom will keep moisture, raw material to touch pot, in order to avoid production
Green coke is pasted；（4）The mixing gas distilled out is delivered directly to cooling tower, and 0 DEG C of -5 DEG C≤chilling temperature ＜ separates out ice cube, obtained
Pure Verbena officinalis essential oil.
The extracting method of Radix Sophorae Flavescentis extractive liquid：Weigh kuh-seng coarse powder appropriate, 75% alcohol solution dipping 0.15-0.8h, heating
Decoct and extract 3 times, the 1st time plus 11-15 times measure 75% ethanol solution, extract 1-2.5h, it is molten to measure 75% ethanol the 2nd time plus 9-11 times
Liquid, extracts 1-1.5h, and the 3rd time plus 6-9 times measure 75% ethanol solution, extracts 0.5-1.5h, every time filtration, merging filtrate, filtrate
Volume concentration to 4-8 times of kuh-seng weight, filtering produces Radix Sophorae Flavescentis extractive liquid.
The extracting method of Herba Andrographitis extract solution：Take Herba Andrographitis to go the removal of impurity, clean, add the ethanol of 10-16 times of its weight
Solution, under 230-270MPa, ultra high pressure treatment 1-4min；Then at 38-46 DEG C, ultrasonic wave extraction 12-24min；Centrifugation
Separation, takes supernatant, obtains Herba Andrographitis extract solution.
Embodiment 1
A kind of floral water containing plant component that the present invention is provided is as follows：
A kind of floral water containing plant component, is mainly made up of the raw material of following parts by weight：40 parts of ethanol, 55 parts of deionized water,
4 parts of dipropylene glycol, 3 parts of sodium citrate, 2 parts of antioxidant, 5 parts of peppermint oil, 5 parts of lemonweed essential oil, 6 parts of crape myrtle extract solution, horse
5 parts of 4 parts of essential oil of whip grass, 6 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 70%；The antioxygen
Agent is BHT.
The preparation method of floral water is as follows：
（1）By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, it is standby；
（2）Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 85 DEG C, and mixture 1 is heated 1 hour under conditions of being maintained at 85 DEG C, obtains mixture 2；
（3）To step（2）Dipropylene glycol, peppermint oil, lemonweed essential oil, crape myrtle extract solution, horse are added in the mixture 2 of gained
Whip grass essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, and 8min is stirred with 1000r/min mixing speed, make each original
Material is well mixed, obtains mixture 3；
（4）By step（3）The mixture 3 of gained carries out refrigeration 3 hours under conditions of being placed in 0 DEG C, produces floral water.
Embodiment 2
A kind of floral water containing plant component that the present invention is provided is as follows：
A kind of floral water containing plant component, is mainly made up of the raw material of following parts by weight：45 parts of ethanol, 65 parts of deionized water,
5.5 parts of dipropylene glycol, 5 parts of sodium citrate, 4 parts of antioxidant, 8 parts of peppermint oil, 7 parts of lemonweed essential oil, 8 parts of crape myrtle extract solution,
8 parts of 6 parts of Verbena officinalis essential oil, 8 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 73%；It is described anti-
Oxygen agent is BHT.
The preparation method of floral water is as follows：
（1）By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, it is standby；
（2）Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 90 DEG C, and mixture 1 is heated 1.5 hours under conditions of being maintained at 90 DEG C, obtains mixture 2；
（3）To step（2）Dipropylene glycol, peppermint oil, lemonweed essential oil, crape myrtle extract solution, horse are added in the mixture 2 of gained
Whip grass essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, and 9min is stirred with 1100r/min mixing speed, make each original
Material is well mixed, obtains mixture 3；
（4）By step（3）The mixture 3 of gained carries out refrigeration 4 hours under conditions of being placed in 3 DEG C, produces floral water.
Embodiment 3
A kind of floral water containing plant component that the present invention is provided is as follows：
A kind of floral water containing plant component, is mainly made up of the raw material of following parts by weight：50 parts of ethanol, 75 parts of deionized water,
7 parts of dipropylene glycol, 7 parts of sodium citrate, 6 parts of antioxidant, 10 parts of peppermint oil, 10 parts of lemonweed essential oil, 11 parts of crape myrtle extract solution,
10 parts of 8 parts of Verbena officinalis essential oil, 10 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 75%；It is described
Antioxidant is BHT.
The preparation method of floral water is as follows：
（1）By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, it is standby；
（2）Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 95 DEG C, and mixture 1 is heated 2 hours under conditions of being maintained at 95 DEG C, obtains mixture 2；
（3）To step（2）Dipropylene glycol, peppermint oil, lemonweed essential oil, crape myrtle extract solution, horse are added in the mixture 2 of gained
Whip grass essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, and 10min is stirred with 1200r/min mixing speed, make each original
Material is well mixed, obtains mixture 3；
（4）By step（3）The mixture 3 of gained carries out refrigeration 5 hours under conditions of being placed in 6 DEG C, produces floral water.
Embodiment 4
A kind of floral water containing plant component that the present invention is provided is as follows：
A kind of floral water containing plant component, is mainly made up of the raw material of following parts by weight：43 parts of ethanol, 60 parts of deionized water,
5 parts of dipropylene glycol, 4 parts of sodium citrate, 3 parts of antioxidant, 6 parts of peppermint oil, 6 parts of lemonweed essential oil, 7 parts of crape myrtle extract solution, horse
6 parts of 5 parts of essential oil of whip grass, 7 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 71%；The antioxygen
Agent is BHT.
The preparation method of floral water is as follows：
（1）By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, it is standby；
（2）Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 87 DEG C, and mixture 1 is heated 1.2 hours under conditions of being maintained at 87 DEG C, obtains mixture 2；
（3）To step（2）Dipropylene glycol, peppermint oil, lemonweed essential oil, crape myrtle extract solution, horse are added in the mixture 2 of gained
Whip grass essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, and 8min is stirred with 1050r/min mixing speed, make each original
Material is well mixed, obtains mixture 3；
（4）By step（3）The mixture 3 of gained carries out refrigeration 3.5 hours under conditions of being placed in 2 DEG C, produces floral water.
Embodiment 5
A kind of floral water containing plant component that the present invention is provided is as follows：
A kind of floral water containing plant component, is mainly made up of the raw material of following parts by weight：47 parts of ethanol, 70 parts of deionized water,
6 parts of dipropylene glycol, 6 parts of sodium citrate, 5 parts of antioxidant, 9 parts of peppermint oil, 9 parts of lemonweed essential oil, 10 parts of crape myrtle extract solution, horse
9 parts of 7 parts of essential oil of whip grass, 9 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 74%；The antioxygen
Agent is BHT.
The preparation method of floral water is as follows：
（1）By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, it is standby；
（2）Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 93 DEG C, and mixture 1 is heated 1.8 hours under conditions of being maintained at 93 DEG C, obtains mixture 2；
（3）To step（2）Dipropylene glycol, peppermint oil, lemonweed essential oil, crape myrtle extract solution, horse are added in the mixture 2 of gained
Whip grass essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, and 10min is stirred with 1150r/min mixing speed, make each original
Material is well mixed, obtains mixture 3；
（4）By step（3）The mixture 3 of gained carries out refrigeration 4.5 hours under conditions of being placed in 5 DEG C, produces floral water.
Performance test
Performance test is carried out to the product obtained by embodiment 1-5, it is as a result as follows：
（1）Smell is checked：Sense organ, smell is pure and fresh；
（2）The repelling effect test of floral water
Some mosquitoes are caught with mosquito catcher and are put into mosquito cage, after " starvation " at a night cultivates, are divided into 6 groups, and 5 groups respectively with scribbling
The finger of embodiment 1-5 products obtained therefroms stretches into test in mosquito cage, and another group is with the finger test for being not coated with floral water, testing time
5 group fingers that product of the present invention is scribbled within 10min, 10min are all close without mosquito, and are not coated with being stung in the finger for floral water
Sting.Thus illustrate that floral water of the present invention has good repelling effect.
（3）Repellent antipruritic effect and inspection
The detumescence effect that embodiment 1-5 prepares floral water is evaluated by experiment on probation, the volunteer 120 of 20-60 Sui is elected,
Sex ratio is 1:1, cause red swelling of the skin itch using mosquito saliva is injected, they are randomly divided into 6 groups, every group 20, its
In have one group as a control group, daily sooner or later respectively apply a corresponding floral water of 1-5 products of the embodiment of the present invention once, compare institute
The floral water used is commercially available floral water, continuous to use a week, redness and the consulting user detected by an unaided eye on skin
The improvement situation of pruritis, counts repellent antipruritic effect efficiently individual quantity and the effective people of antipruritic effect of 6 group volunteers respectively
Count and be recorded in as in following table.Assay such as following table：
| Test group | Repellent antipruritic effect efficiently individual quantity | Antipruritic effect efficiently individual quantity |
| Embodiment 1 | 18 | 17 |
| Embodiment 2 | 19 | 19 |
| Embodiment 3 | 17 | 18 |
| Embodiment 4 | 16 | 17 |
| Embodiment 5 | 16 | 16 |
| Control group | 11 | 10 |
Embodiment 1-5 products have obvious repellent antipruritic effect to most people as seen from the above table, and commercially available floral water only has gently
Micro- repellent antipruritic effect.
Relieving mental strain and helping sleep effect, smell favorable comment degree and stimulation sex investigation：
Choose 80 volunteers and participate in experiment, volunteer is selected from odor-sensitive, the crowd that sleep quality easily influences, its age
Scope is at 20-60 Sui, and volunteer's number of this 4 age brackets of wherein 20-30 Sui, 30-40 Sui, 40-50 Sui and 50-60 Sui is
20 people, and the sex ratio of each age bracket is 1:1, this 80 volunteers are randomly divided into two test groups of A, B, every group 40
People.
Test group and subjects：A groups use floral water of the present invention, and B groups use commercially available floral water.
Test method：Floral water is sprayed on interior by volunteer before sleeping every night, and each volunteer uses the amount of floral water every time
It is identical, it is continuous to use 20 days, it is desirable to not used similar product in volunteer 20 days.
Evaluation criterion：Sensory evaluation is carried out for the smell of floral water, is divided into satisfied, general and dissatisfied three evaluations etc.
Level, statistics is satisfied with the percentage shared by the grade after 20 days, and is recorded in table；Excitant to floral water is evaluated, will
Hope person according to the excitant of floral water whether there is respectively favorable comment, in comment and difference comments three opinion ratings, counted after 20 days shared by favorable comment
Percentage, and be recorded in table；Relieving mental strain and helping sleep effect to floral water is evaluated, and volunteer comments respectively according to using effect
Comment, in comment and difference comments three opinion ratings, favorable comment percentage is counted after 20 days, and be recorded in table.
After 20 days, investigation statisticses result is as shown in the table：
| Experimental group number evidence | Smell | Excitant | Relieving mental strain and helping sleep effect |
| A groups | 88% | 90% | 89% |
| B groups | 67% | 65% | 27% |
Find out that liquid distilled from honeysuckle flowers or lotus leaves aqueous vapor of the present invention is received by most of consumer by data above, improved compared to commercially available prod, together
When there is the characteristics of stimulating small, the also effect with relieving mental strain and helping sleep.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair
The equal change or modification change completed under bright patent claim, the technical spirit suggested by all present invention, all should belong to
Cover the scope of the claims in the present invention.
Claims (6)
1. a kind of floral water containing plant component, it is characterised in that be mainly made up of the raw material of following parts by weight：Ethanol 40-50
Part, 55-75 parts of deionized water, 4-7 parts of dipropylene glycol, 3-7 parts of sodium citrate, 2-6 parts of antioxidant, 5-10 parts of peppermint oil, lemon
5-10 parts of vanilla essential oil, 6-11 parts of crape myrtle extract solution, 4-8 parts of Verbena officinalis essential oil, 6-10 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis are extracted
5-10 parts of liquid.
2. a kind of floral water containing plant component according to claim 1, it is characterised in that mainly by following parts by weight
Raw material is made：43-47 parts of ethanol, 60-70 parts of deionized water, 5-6 parts of dipropylene glycol, 4-6 parts of sodium citrate, 3-5 parts of antioxidant,
6-9 parts of peppermint oil, 6-9 parts of lemonweed essential oil, 7-10 parts of crape myrtle extract solution, 5-7 parts of Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid 7-9
6-9 parts of part and Herba Andrographitis extract solution.
3. a kind of floral water containing plant component according to claim 1, it is characterised in that mainly by following parts by weight
Raw material is made：45 parts of ethanol, 65 parts of deionized water, 5.5 parts of dipropylene glycol, 5 parts of sodium citrate, 4 parts of antioxidant, 8 parts of peppermint oil,
8 parts of 7 parts of lemonweed essential oil, 8 parts of crape myrtle extract solution, 6 parts of Verbena officinalis essential oil, 8 parts of Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution.
4. a kind of floral water containing plant component according to claim 1-3 any one, it is characterised in that：Described is anti-
Oxygen agent is BHT.
5. a kind of floral water containing plant component according to claim 1-3 any one, it is characterised in that：The ethanol
Concentration be 70%-75%.
6. a kind of prepare a kind of method of the floral water containing plant component described in claim 1-3 any one, it is characterised in that
Comprise the following steps：
（1）By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, crape myrtle extract solution, Verbena officinalis essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, it is standby；
（2）Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 85-95 DEG C, and mixture 1 is heated 1-2 hours under conditions of being maintained at 85-95 DEG C, is mixed
Thing 2；
（3）To step（2）Dipropylene glycol, peppermint oil, lemonweed essential oil, crape myrtle extract solution, horse are added in the mixture 2 of gained
Whip grass essential oil, Radix Sophorae Flavescentis extractive liquid and Herba Andrographitis extract solution, and 8- is stirred with 1000-1200r/min mixing speed
10min, is well mixed each raw material, obtains mixture 3；
（4）By step（3）The mixture 3 of gained carries out refrigeration 3-5 hours under conditions of being placed in 0-6 DEG C, produces floral water.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110638724A (en) * | 2019-11-06 | 2020-01-03 | 高小军 | Natural whitening floral water and preparation method thereof |
| CN111481455A (en) * | 2020-04-02 | 2020-08-04 | 广州市逸轩精细化工有限公司 | Floral water and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103006500A (en) * | 2011-09-28 | 2013-04-03 | 龚亚菊 | Herbal floral water |
| CN103655718A (en) * | 2012-08-30 | 2014-03-26 | 北京妙心堂医药科技有限公司 | Traditional Chinese medicine composition, preparation, and floral water and application method thereof |
| CN104921988A (en) * | 2015-06-03 | 2015-09-23 | 刘强 | Mosquito-repelling liquid |
| CN105395410A (en) * | 2015-12-03 | 2016-03-16 | 青岛新中新新材料有限公司 | Herbal floral water and preparation method thereof |
| CN106389238A (en) * | 2016-12-09 | 2017-02-15 | 申艾平 | Floral water |
-
2017
- 2017-04-24 CN CN201710272476.4A patent/CN107213050A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103006500A (en) * | 2011-09-28 | 2013-04-03 | 龚亚菊 | Herbal floral water |
| CN103655718A (en) * | 2012-08-30 | 2014-03-26 | 北京妙心堂医药科技有限公司 | Traditional Chinese medicine composition, preparation, and floral water and application method thereof |
| CN104921988A (en) * | 2015-06-03 | 2015-09-23 | 刘强 | Mosquito-repelling liquid |
| CN105395410A (en) * | 2015-12-03 | 2016-03-16 | 青岛新中新新材料有限公司 | Herbal floral water and preparation method thereof |
| CN106389238A (en) * | 2016-12-09 | 2017-02-15 | 申艾平 | Floral water |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110638724A (en) * | 2019-11-06 | 2020-01-03 | 高小军 | Natural whitening floral water and preparation method thereof |
| CN111481455A (en) * | 2020-04-02 | 2020-08-04 | 广州市逸轩精细化工有限公司 | Floral water and preparation method thereof |
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