KR20220005133A - Spray composition for blocking harmful substances wirh antifungal and antiviral - Google Patents

Abstract

The present invention relates to an antibacterial, antivirus, harmful material preventive, and safe natural spray composition capable of being harmless to a human body, and relates to a harmful material preventive and safe natural spray composition capable of being harmless to a human body, which comprises a natural extract exhibiting antibacterial, antivirus, and harmful material preventive effects as an active ingredient to exhibit a blocking effect of absorbing heavy metals, fine dust, pollen, and others, and prevent bad odor and bacteria propagation.

Description

A safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances {SPRAY COMPOSITION FOR BLOCKING HARMFUL SUBSTANCES WIRH ANTIFUNGAL AND ANTIVIRAL}

The present invention relates to a safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances. More specifically, it contains natural extracts that exhibit antibacterial, antiviral and harmful substance blocking effects as active ingredients, which can exhibit the effect of adsorbing heavy metals, fine dust, pollen, etc., and harmful substances that can prevent odor and bacterial propagation It relates to a safe natural spray composition harmless to the human body for barrier protection.

Microorganisms are living things that always exist around us, and there are beneficial microorganisms that help humans, but some pathogenic microorganisms such as bacteria, fungi, and viruses cause diseases and harm the human body, such as generating bad odors. Interest in sanitary care products to improve the unsanitary environment caused by such microorganisms is increasing.

In addition, as industrialization progresses, exhaust gases emitted from various industrial facilities such as power plants and incinerators include gases such as SOx, NOx, volatile organic compounds (VOC), odors, fine dust, and heavy metal particles. Recently, the influx of foreign air pollutants such as yellow dust and smog has increased, and since 2013, the number of diesel vehicles that emit a large amount of nitrogen oxide, a precursor of fine dust, has risen sharply due to the rapid increase in the generation of high-concentration fine dust. It is urgent to establish fine dust intensive management and reduction measures. In order to reduce fine dust and air pollution from automobiles, the main culprits of fine dust and air pollution in large cities, limiting the operation of old diesel vehicles is being promoted, but the amount of fine dust is still increasing.

However, because existing masks for blocking fine dust do not have an antibacterial function to prevent the growth of bacteria, the moisture contained in the user's breath causes bacteria to multiply more easily, causing odors when reused, and factors that cause infection with bacteria or bacteria can be,

Even in general homes, the indoor environment of the house is not free from human safety problems due to the state of being contaminated by various fungi such as bacteria and mold that cannot be identified by the human eye, sick house syndrome or fine dust, etc. As this issue is being raised, technology development is required.

In particular, due to the outbreak of epidemics such as SARS, avian influenza, and swine flu since the 2000s, interest in hygiene products that help prevent bacterial and viral infections is increasing.

On the other hand, in summer, when cooked food is stored, it is easily spoiled, and various bacteria easily multiply through food waste, and the odor generated not only gives discomfort but also adversely affects the health of people by various bacteria inhabiting it. For example, various germs and mites such as mold and bacteria inhabit the bed, and in the case of house dust mites, they feed on human dander or dead skin cells while standing in bed, and emit harmful excrement. Even in the case of shoes, sweat easily builds up inside them, so various bacteria easily multiply, and these bacteria are the cause of athlete's foot and the like.

In addition, in the case of clothing mold, mold is more likely to occur on carbon-based cotton fibers than on wool fibers, which are the main components of protein. It is the cause of this, so you need to be especially careful. In the case of washing clothes by normal washing, bacteria and microorganisms are removed along with contamination to some extent when washing is completed. When dried or stored, an unpleasant and unpleasant odor derived from bacteria is produced. In addition, since collection derived from sweat or sebum attaches to the fibers for clothes, towels, etc., it is not only unpleasant but also undesirable from a hygienic point of view.

However, conventional antibacterial agents mainly consist of organic antibacterial products using specific chemicals, so there is a safety problem with these compounds. In addition, low molecular weight compounds used in antibacterial agents have a disadvantage in that durability is poor because they are volatilized.

Therefore, inorganic antibacterial products using inorganic substances with antibacterial and deodorizing properties are being manufactured, and as such inorganic antibacterial products, a form in which a metal having antibacterial activity is dispersed in a solvent, or a form in which a metal is bonded to a porous support is manufactured. is becoming

As an example, antibacterial products in which metal ions with excellent antibacterial properties such as silver (Ag), copper (Cu), manganese (Mn), zinc (Zn), etc. are substituted for inorganic carriers such as zeolite, silica, alumina, etc. Because it has a three-dimensional skeletal structure, it has a large specific surface area and excellent heat resistance. However, there is still a need for improvement of a technology for stably supporting a metal having antibacterial properties on an inorganic carrier.

A typical metal for which the antibacterial activity is recognized is silver. Silver (Ag) is known as a powerful sterilizing agent that kills bacteria by incapacitating it by acting very little on the enzymes that function in the metabolism of single-celled bacteria (TN Kim, QL Feng, et al. J. Mater. Sci. Mater. Med. , 9, 129 (1998)). In addition to silver, metals such as copper and zinc can have the same effect, but among them, silver has the strongest antibacterial effect. Although silver (Ag) has excellent antibacterial activity, silver in an ionic state is unstable due to its high reactivity, so it is easily oxidized or reduced to metal depending on the surrounding environment and discolors itself or causes coloration in other materials. As the US EPA classifies silver nano-containing materials as “insecticides” and strictly restricts their use in household products, safety issues are being raised when nano silver particles are used.

In addition, silver nanoparticles have a strong sterilization power against bacteria, but there are problems in application such as safety problems because a high concentration of silver nanoparticles must be used to control fungi. Therefore, in what form and how silver is applied to antibacterial products remains a challenge.

As described above, daily life in modern cities is exposed to various pollutants such as automobile soot, living pollutants, and industrial waste dust. As fine dust floating in the air is a serious environmental problem, such as causing various respiratory diseases, it is urgent to develop hygiene products that help prevent bacterial and viral infections. development is needed.

KR 10-1397225 B1

It is an object of the present invention to contain natural extracts that exhibit antibacterial, antiviral and harmful substance blocking effects as an active ingredient to the human body for blocking antibacterial, antiviral and harmful substances, which have excellent effects of adsorbing and blocking heavy metals, fine dust, pollen, etc. To provide a harmless and safe natural spray composition.

Another object of the present invention is to provide an aqueous liquid-type spray composition so that it can be applied without limitation on the type, shape or structure of the substrate, and can be applied to various fields.

In order to achieve the above object, a safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances according to an embodiment of the present invention includes an aqueous ethanol solution, thistle (irsium japonicum) extract, New Green (Brassica oleracea var botrytis aut italiana L.) extract, gondalbi (Ligularia stenocephala) extract, dandelion (Taraxacum platycarpum), green tea extract, ginseng (Panax ginseng) extract, and a natural extract consisting of a mixture thereof.

The aqueous ethanol solution is an aqueous ethanol solution having a concentration of 60% to 70%.

The composition is gold and silver flower (Lonicera japonica), Angelica gigas, red ginseng, Astragalus propinquus, ginger (Zingiber officinale), soybean (Glycine max), rice bran, mulberry leaf (Tilia taquetii CKSchneid.), mugwort (Artemisia) , Prunus mume, Cynanchum bungei, Apple peel, Schisandra chinensis, Chlorella, Oregano (origanum vulgare), Sage (Salvia officinalis), Basil (Ocimum basilicum), Fennel (oeniculum) ), Garlic (Allium sativum), Lemon Balm (Melissa officinalis), Mint (Mentha canadensis), Rosemary (Salvia Rosmarinus), Echinacea (Echinacea), Sambucus (Sambucus), Licorice (Glycyrrhiza uralensis), Orchid (Eleutherococcus) , blueberry (Cyanococcus), and further comprises a natural extract selected from the group consisting of mixtures thereof.

The composition is to block fine dust and reduce airborne bacteria having a particle size of 0.03 um to 1.0 um.

The natural antibacterial agent according to another embodiment of the present invention includes the antibacterial, antiviral and safe natural spray composition harmless to the human body for blocking harmful substances.

The natural deodorant according to another embodiment of the present invention includes the antibacterial, antiviral and safe natural spray composition harmless to the human body for blocking harmful substances.

A natural cleaner according to another embodiment of the present invention is to include the antibacterial, antiviral and safe natural spray composition harmless to the human body for blocking harmful substances.

Hereinafter, the present invention will be described in more detail.

A safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances according to an embodiment of the present invention includes an aqueous ethanol solution, thistle (irsium japonicum) extract, New Green (Brassica oleracea var. botrytis aut italiana L.) extracts, natural extracts comprising Ligularia stenocephala extract, dandelion (Taraxacum platycarpum), green tea extract, Panax ginseng extract, and mixtures thereof.

The aqueous ethanol solution may include vegetable ethanol and distilled water made by fermenting grains. The grain is generally used to make vegetable ethanol in the art, and the type is not particularly limited, but, for example, fermented ones from rice, barley, sweet potato, corn, sugar cane, etc. may be used.

In addition, the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention is thistle (irsium japonicum) extract, New Green (Brassica oleracea var. botrytis aut italiana L.) extract, gondalbi (Ligularia) in the aqueous ethanol solution. stenocephala) extract, dandelion (Taraxacum platycarpum), green tea extract, ginseng (Panax ginseng) extract and a natural extract consisting of a mixture thereof. can be prevented

The thistle (irsium japonicum) is a dicotyledonous perennial plant of the order Asteraceae, branching a little at the upper part and growing upright, and a large one reaches about 1 m. The leaves are long oval in shape and have large and small thorns on the edge. The outpost or root is called Daegye and is used in oriental medicine. It is known to have blood clotting and liver detoxification effects.

The New Green (Brassica oleracea var. botrytis aut italiana L.) is a kind of broccoli in the cruciferous family, also called Toscano. Broccoli is edible with the flower buds and flower stalks, whereas New Green uses the leaves for food. The leaves are long oval, dark green in color, and have convex and convex irregularities on the front side.

The gondalbi (Ligularia stenocephala) is a perennial herb of the Asteraceae family, a double leaf plant, and grows in a wetland deep in the mountains. The whole grass is hairless and the rhizome is thick. The leaves attached to the roots remain until flowers bloom, and they are about 24cm long and 20cm wide. There are hairs along the veins on the underside of the leaves, and there are sharp sawtooths on the edges.

The dandelion (Taraxacum platycarpum) is a perennial plant of the Asteraceae family that grows in a sunny place in a field or vacant lot. In early spring, several leaves come out of the root and spread sideways like a cushion on the ground. The flowers are yellow and bloom one by one at the end of the peduncle in April-May. Hundreds of tongue flowers hang in a head inflorescence on a single flower. Each tongue flower has 5 stamens and 1 pistil. At the edge of the flower cluster, several inner and outer cells are running around, and the inflorescences are upright and have horn-like projections on the upper part. The fruit has umbrella-shaped hairs that are blown away by the wind.

Green tea is a tea made from unfermented tea leaves. The leaves are used as tea, the fruits are milked and used as oil, and the stems are used as buttons. It prevents the formation of blood clots and lowers cholesterol and blood sugar. It is also effective in preventing tooth decay. Green tea extract has antioxidant properties.

The ginseng (Panax ginseng) is a root of the Arboraceae family as it is, or a thin root and a cork layer have been removed. Ginseng restores vitality and is used for body weakness, malaise, fatigue, loss of appetite, vomiting, and diarrhea. Pharmacological action has been reported to include cortical excitability and inhibition, balance, anti-fatigue, anti-aging, immune enhancement, heart contraction, gonadotrophin, hyperglycemia suppression, protein synthesis promotion, homeostasis maintenance, anticancer, and detoxification.

Preferably, the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances is based on 100 parts by weight of an aqueous ethanol solution, 100 parts by weight of thistle extract, 100 parts by weight of New Green extract, 100 parts by weight of gondalbi extract, 100 parts by weight of dandelion extract parts, and 100 parts by weight of green tea extract and 100 parts by weight of ginseng extract.

According to the above range, the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention can obtain excellent antibacterial, antiviral and deodorizing effects without including harmful ingredients, and in particular, ammonia, It has excellent antibacterial properties that remove volatile harmful substances (VOSs) such as trimethylamine, hydrogen sulfide and methyl mercaptan.

The aqueous ethanol solution is an aqueous ethanol solution having a concentration of 60% to 70%.

The safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention can obtain a superior antibacterial effect by using an aqueous solution of ethanol at a concentration of 60% to 70%. In the case of an aqueous ethanol solution having a concentration of 70% or more, it contains too much ethanol and may be irritating to the human body. may not work out.

The composition is gold and silver flower (Lonicera japonica), Angelica gigas, red ginseng, Astragalus propinquus, ginger (Zingiber officinale), soybean (Glycine max), rice bran, mulberry leaf (Tilia taquetii CKSchneid.), mugwort (Artemisia) , Prunus mume, Cynanchum bungei, Apple peel, Schisandra chinensis, Chlorella, Oregano (origanum vulgare), Sage (Salvia officinalis), Basil (Ocimum basilicum), Fennel (oeniculum) ), Garlic (Allium sativum), Lemon Balm (Melissa officinalis), Mint (Mentha canadensis), Rosemary (Salvia Rosmarinus), Echinacea (Echinacea), Sambucus (Sambucus), Licorice (Glycyrrhiza uralensis), Orchid (Eleutherococcus) , blueberry (Cyanococcus), and further comprises a natural extract selected from the group consisting of mixtures thereof.

When the natural extract is further included, the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention may have stronger antibacterial, antiviral and deodorizing effects.

The gold and silver flower (Lonicera japonica) is a bud of honeysuckle, or a flower just starting to bloom, and belongs to the genus Honeysuckle. Pharmacological action has been reported to have antibacterial action, anti-inflammatory action, antipyretic action, increase leukocyte phagocytic action, central nervous system excitability action, serum cholesterol lowering effect, and ulcer prevention effect. The appearance is a mixture of a funnel-shaped bud and a lip-shaped flower. The outer surface of the flower is yellowish white or greenish white, and the longer it is stored, the darker the color. Light brown hairs are observed under a magnifying glass. The calyx is green, and the tip is split into 5 pieces, and the split piece has hairs and is about 2 mm long. There are 5 stamens, yellow, and 1 pistil, and the ovary has no hair.

The Angelica gigas is a representative medicinal plant, and it enjoys the subtle herbal scent that spreads from the roots and leaves of Angelica gigas and uses the leaves a lot as a healthy vegetable. You can taste a different flavor if you tear off the soft Angelica leaves and serve it with lettuce wrap. Although it is a perennial plant, all medicinal herbs must be dug up before flowering. The initial growth is very slow, and after June when it grows to a certain extent, it grows vigorously.

The red ginseng is ginseng having a light yellowish-brown or light reddish-brown color by carefully selecting 6-year-old fresh ginseng of good quality produced in a suitable growing area of ginseng, steaming it for a long time without peeling it, and then drying it.

The astragalus (Astragalus propinquus) is a perennial herbaceous plant belonging to the legume family, it grows in the mountains and reaches a height of 1 m and has fine hairs throughout. Efficacy is easily fatigued, weak strength, low voice, weak pulse, and shows remarkable efficacy for those who sweat a lot.

The ginger (Zingiber officinale) is a perennial herb of the ginger family, and the root is used for food and medicine. Flowers do not bloom in Korea, but in the tropics, in August, a 20-25 cm long peduncle wrapped in a leaf sheath appears and a spike of flowers hangs at the end of the flower. Flowers come out between bracts and are 4~7.6cm long. The calyx has a short tubular shape, and the tip of the corolla is split into 3 parts, and the split piece has a sharp tip. There is one stamen and the anther is yellow.

The soybean (Glycine max) is a seed of a legume plant and is also called a bean. Among soybeans, it is rich in protein and fatty acids, and contains protein (34.4%), carbohydrates (30%), lipids (18.6%), and various minerals and vitamins. It has a lot of high-quality protein that is comparable to meat, and serves as an important plant protein source for vegetarians. In addition, soybeans are rich in isoflavones, which prevent calcium loss from the bones and help calcium absorption to maintain bone health and prevent osteoporosis.

The rice bran refers to a pulverized mixture of pericarp, seed hull, and aloe layer produced when milling brown rice to make rice bran, and is called rice bran (米糠) in Chinese. Usually, 6-8% of the rice bran of brown rice is produced. If the degree of grinding of brown rice is increased, the amount increases, and the composition also changes according to the degree of grinding.

The mulberry leaf (Tilia taquetii C.K.Schneid.) is the leaf of the mulberry tree and is the second most protein-rich material after soybeans.

The mugwort (Artemisia) is a dicotyledonous perennial plant of the order Asteraceae, and grows to about 1 m in height in a sunny place. The whole is covered with cobweb-like hairs, and underground stems grow sideways. The leaves run alternately on the stem, and the stem leaves are oval and deeply divided like feathers. Flowers bloom from midsummer to autumn in cone-flower sequence. A cluster of flowers is stacked in a gun barrel. Young shoots are edible and mature ones are medicinal.

The plum (Prunus mume) is the fruit of the plum tree, has a round shape, and ripens to green from the end of May to the middle of June. About 80% of the fruit is the flesh, of which about 85% is water and about 10% sugar. It is rich in minerals, vitamins, and organic acids (citric acid, malic acid, succinic acid, tartaric acid), and also contains minerals such as calcium, phosphorus, potassium and carotene. Among them, citric acid promotes carbohydrate metabolism and relieves fatigue, and organic acid activates the action of the stomach and stimulates appetite.

The Cynanchum bungei is a dried tuber root of the genus Bacariaceae, which has a conical shape, a length of 5 to 10 cm, and a diameter of 1.5 to 3.5 cm. The outer surface is grayish-yellow to yellowish-brown, and there are many vertical wrinkles and the quality is hard. The cut side is white. It has no odor and tastes bitter, sweet, and astringent.

The apple peel is the peel of the fruit of an apple tree, which is a plant of the deciduous family Rosaceae, a dicotyledonous plant, and is an alkaline food, and the apple has a round shape with a diameter of about 5 to 10 cm, and the color is usually red or yellow.

The Schisandra chinensis is a fruit of a deciduous broad-leaved vine of the Magnolia family, and has a dark red color with a diameter of about 1 cm. It is called omija because it can taste sweet, sour, bitter, salty and spicy.

The chlorella (Chlorella) is a freshwater algae belonging to the green algae plant Chlorelladae, a kind of plankton. As it is rich in various nutrients such as protein, chlorophyll, vitamins, minerals, and amino acids, it has been studied by NASA as a food for astronauts and has become famous.

The oregano (origanum vulgare) is a perennial herb of the Lamiaceae family, also called flower mint, and has a pungent mint-like scent. It is an herb that is resistant to pests and diseases and cold, and shows the strength of wild flowers. The height is 30-60 cm, and the leaves are about 1.5 cm long.

The sage (Salvia officinalis) is a dicotyledonous perennial herb of the order Lamiaceae, also called medicinal salvia. The stem is rectangular, almost woody at the bottom, 30-90cm high, and the whole is fragrant. Leaves are opposite, petiole is short, long oval, dull end and flat edge. The underside of the leaf is gray-green with white hairs along with the stem, and the surface has fine wrinkles in the network.

The basil (Ocimum basilicum) is an annual plant of the dicotyledonous plant Lamiaceae, the origin is East Asia, and is an annual plant belonging to the mint family, and is widely used in Italian and French cuisine. Medicinal effects include headache, nervous irritability, stomatitis, tonic effect, health, calming, sterilization, insomnia and lactation.

The fennel (oeniculum vulgare) is a plant of the family Hemiaceae, and the phenolic compound of fennel has antioxidant and liver protective actions, and is mainly used as medicine, food, and spice.

The garlic (Allium sativum) is a monocotyledonous perennial plant of the Liliaceae family, and it is the most spicy plant among the Liliaceae native to Central Asia. are being cultivated

The lemon balm (Melissa officinalis) is a dicotyledonous perennial plant of the order Lamiaceae, a cold-resistant perennial plant growing about 60-150 cm in height, and the stem is square. The length of the leaves is about 8cm wide ovate, opposite, petiole and hairs, and strong lemon scent. Flowers are attached in white, yellow, and light blue rings in late summer. It contains eugenol, which has an anticonvulsant action, and is mainly used as an essential oil.

The peppermint (Mentha canadensis) is a dicotyledonous plant, a perennial plant of the Lamiaceae family, native to temperate regions, and the leaves and stems grown in cool climates have a strong fragrance. It tolerates the summer rainy season better than the mint type, which is Western mint, and it is good to eat the fragrance by using soft leaves or shoots sprouting in spring and autumn.

The rosemary (Salvia Rosmarinus) is an evergreen shrub of the Lamiaceae family of dicotyledonous plants, has excellent antibacterial and bactericidal action and is good for moisturizing effect. It is used as a cosmetic ingredient because it gently soothes the skin, and its unique fresh scent activates brain functions and is often used as a spice.

The Echinacea (Echinacea) is a plant of the genus Echinacea Asteraceae, and is one of the most commonly used medicinal herbs in the world. Originally used by Native Americans as a folk medicine, it was used by Comanche to treat toothache, sore throat, hand-foot rabies, snake bites, and sepsis.

The sambucus (Sambucus) is a genus of elderberry of the genus Lobsteraceae, and the fruit is called an elderberry. Elderberry is rich in anthocyanin, an antioxidant and antiviral component, and has excellent effects in enhancing immune function and preventing colds.

The licorice (Glycyrrhiza uralensis) is a perennial herb of the family Rosaceae, a medicinal plant. The roots are reddish-brown and go deep into the ground, and the stems are hairy and grow up to about 1m tall. In addition, the white hairs are dense and appear grayish-white, and there are scattered preoccupations. The leaves are alternate and odd pinnate compound leaves.

The Eleutherococcus senticosus is the bark of the roots, stems and branches of the Aleutherococcus senticosus or other plants of the family Araliaceae. Flowers bloom in August and September in purple, and the sepals are triangular and have hairs on the outside. The color of the medicinal material is yellowish brown or dark gray, flat, there are thorns or traces in some places, and there are grayish-white spots on the skin of relatively young branches.

The blueberry (Cyanococcus) is a dicotyledonous shrub of the Azalea family, the fruit is almost round and 1 to 1.5 g of one fruit is dark sky blue, reddish brown, black, and has white powder on the outside. Because it has a slightly sweet and sour taste, it is sometimes eaten raw or made into jam, juice, and canned food. Some of the fruits of the ginseng tree grown in Korea have large fruits depending on the individual.

The natural extract is extracted using an extraction solvent selected from the group consisting of water, C1 to C6 lower alcohols, and mixtures thereof.

Specifically, washing the natural product to prepare the extract; drying after washing; pulverizing the natural product after drying; leaching the pulverized product using an organic solvent; drying the sample after leaching; leaching with water; And including the step of leaching, it is possible to obtain a natural extract.

The natural extract extracted using the organic solvent may further comprise the step of performing fractionation using an organic solvent.

The method for preparing the extract may be a conventional extraction method in the art, such as an ultrasonic extraction method, a leaching method, and a reflux extraction method. Specifically, it may be an extract obtained by extracting a natural product from which foreign substances have been removed by washing and drying with water, alcohol having 1 to 6 carbon atoms, or a mixed solvent thereof, and may be an extract extracted by sequentially applying the solvents to the sample.

The reflux extraction method is water, based on 100 mL of an alcohol having 1 to 6 carbon atoms, 10 to 30 g of a pulverized product of a natural product, a reflux time of 1 to 3 hours, and 50 to 100% alcohol or water having 1 to 6 carbon atoms. More specifically, based on 100 mL of alcohol having 1 to 6 carbon atoms or 100 mL of water, 10 to 20 g of a pulverized product of a natural product, a reflux time of 1 to 2 hours, and 70 to 90% alcohol or water having 1 to 4 carbon atoms. .

The leaching method is carried out at 15 to 30° C. for 24 to 72 hours, and water or 50 to 100% alcohol having 1 to 6 carbon atoms is used as an extraction solvent. More specifically, the process is carried out at 20 to 25° C. for 30 to 54 hours, and the extraction solvent is water or 70 to 80% alcohol having 1 to 6 carbon atoms.

In the ultrasonic extraction method, the reaction is performed at 30 to 50° C. for 0.5 to 2.5 hours, and the extraction solvent is water or 50 to 100% alcohol having 1 to 6 carbon atoms. Specifically, extraction is performed at 40 to 50° C. for 1 to 2.5 hours, and the extraction solvent is water or 70 to 80% alcohol having 1 to 6 carbon atoms.

The extraction solvent may be used in an amount of 2 to 50 times, more specifically, 2 to 20 times, based on the weight of the sample. For extraction, the sample may be left for 1 to 72 hours for leaching in the extraction solvent, and more specifically, left for 24 to 48 hours.

After extraction, the extract may be fractionated by sequentially applying a fresh fractionation solvent. The fractionation solvent used for fractionation is any one or more selected from the group consisting of water, hexane, butanol, ethyl acetic acid, ethyl acetate, methylene chloride and mixtures thereof, preferably ethyl acetate or methylene chloride.

After obtaining the extract or fraction, a method such as concentration or freeze-drying may be additionally used.

Preferably, the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances is based on 100 parts by weight of an aqueous ethanol solution, 100 parts by weight of thistle extract, 100 parts by weight of New Green extract, 100 parts by weight of gondalbi extract, 100 parts by weight of dandelion extract parts, 100 parts by weight of green tea extract, 100 parts by weight of ginseng extract, 3 to 7 parts by weight of gold and silver extract, 3 to 7 parts by weight of Angelica keis extract, 3 to 7 parts by weight of red ginseng extract, 3 to 7 parts by weight of Astragalus extract, 3 to 7 parts by weight of ginger extract 7 parts by weight, 3 to 7 parts by weight of soybean extract, 3 to 7 parts by weight of rice bran extract, 3 to 7 parts by weight of mulberry leaf extract, 3 to 7 parts by weight of mugwort extract, 3 to 7 parts by weight of mesyl extract, 3 to 7 parts by weight of baeksuo extract parts by weight, apple peel extract 3-7 parts by weight, omija extract 3-7 parts by weight, chlorella extract 3-7 parts by weight, oregano extract 3-7 parts by weight, sage extract 3-7 parts by weight, basil extract 3-7 parts by weight parts, 3 to 7 parts by weight of fennel extract, 3 to 7 parts by weight of garlic extract, 3 to 7 parts by weight of lemon balm extract, 3 to 7 parts by weight of mint extract, 3 to 7 parts by weight of rosemary extract, 3 to 7 parts by weight of echinacea extract Parts, 3 to 7 parts by weight of sambucus extract, 3 to 7 parts by weight of licorice extract, 3 to 7 parts by weight of oleracea extract, and 3 to 7 parts by weight of blueberry extract.

When according to the above range, it is possible to exhibit high antibacterial and antiviral activity compared to simple mixing by the antistatic action of each extract. In particular, in the case of the above range, the deodorizing effect is excellent, and the antibacterial property of removing volatile harmful substances (VOSs) such as ammonia, trimethylamine, hydrogen sulfide and methyl mercaptan is very excellent, so it has excellent efficacy in indoor air purification. can have

More preferably, the antibacterial, antiviral and safe natural spray composition harmless to the human body for blocking harmful substances may further include one selected from the group consisting of grape peel extract, orange peel extract, and mixtures thereof.

Grape (Vitis vinifera) is the fruit of the vine, which is a berry and ripens to a brownish purple color in July to August. It is a widely used fruit because of its good flavor and abundant juice. As it matures, sugar increases and acid decreases, and sugar peaks at maturity. Sugar is usually 14-15%. There are various organic acids as flavor ingredients, with tartaric acid and malic acid occupying most of them. In particular, grape skins are rich in nutrients such as antioxidants.

Mandarin orange (Citrus unshiu) is the fruit of the tangerine tree. The tangerine tree is evergreen, 3~6m tall, like a thorn leaf, and has thorns sprouting between the stems, and white flowers bloom in early summer (mid/late May). Tangerines, a fruit, open in June-July, and ripen yellow in winter. In particular, the peel of tangerine is moist and has a good flavor, so it is good to dry it. In addition, it is not only rich in nutrients, but also helps in dieting by suppressing fat absorption.

When the grape skin extract and tangerine peel extract are additionally included in a safe natural spray composition that is harmless to the human body for antibacterial, antiviral and harmful substances blocking, antibacterial, antiviral, deodorizing and harmful substances blocking of natural extracts contained in the composition The effect can be increased, and even when it is dried and evaporated after spraying, the effect is excellent, so that the effect of antibacterial, antiviral, deodorizing and blocking harmful substances can be maintained for a long time.

More preferably, the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances is based on 100 parts by weight of an aqueous ethanol solution, 100 parts by weight of thistle extract, 100 parts by weight of New Green extract, 100 parts by weight of gondalbi extract, 100 parts by weight of dandelion extract Parts by weight, 100 parts by weight of green tea extract, 100 parts by weight of ginseng extract, 3 to 7 parts by weight of ginseng extract, 3 to 7 parts by weight of angelicae extract, 3 to 7 parts by weight of red ginseng extract, 3 to 7 parts by weight of Astragalus extract, 3 parts by weight of ginger extract to 7 parts by weight, 3 to 7 parts by weight of soybean extract, 3 to 7 parts by weight of rice bran extract, 3 to 7 parts by weight of mulberry leaf extract, 3 to 7 parts by weight of mugwort extract, 3 to 7 parts by weight of mesyl extract, 3 to 7 parts by weight of baeksuo extract 7 parts by weight, 3 to 7 parts by weight of apple peel extract, 3 to 7 parts by weight of Schisandra extract, 3 to 7 parts by weight of chlorella extract, 3 to 7 parts by weight of oregano extract, 3 to 7 parts by weight of sage extract, 3 to 7 parts by weight of basil extract Parts by weight, 3 to 7 parts by weight of fennel extract, 3 to 7 parts by weight of garlic extract, 3 to 7 parts by weight of lemon balm extract, 3 to 7 parts by weight of mint extract, 3 to 7 parts by weight of rosemary extract, 3 to 7 parts by weight of echinacea extract Parts by weight, 3 to 7 parts by weight of sambucus extract, 3 to 7 parts by weight of licorice extract, 3 to 7 parts by weight of oleracea extract, 3 to 7 parts by weight of blueberry extract, 10 to 20 parts by weight of grape skin extract and 10 parts by weight of tangerine peel extract to 20 parts by weight.

According to the above range, the antibacterial, antiviral, deodorizing and harmful substances blocking effect is enhanced by including the grape skin extract and the orange peel extract, and the degree of increase in the effect is excellent.

The composition is to block fine dust and reduce airborne bacteria having a particle size of 0.03 um to 1.0 um.

Currently, yellow dust masks and quarantine masks are being used to block the fine dust and airborne bacteria, and the Ministry of Food and Drug Safety has approved these yellow dust masks and quarantine mask performance standards by labeling them as KF.

KF94 (mask for quarantine) blocks more than 94% of particles with an average size of 0.4㎛, and KF80 (mask for sulfur) means that it blocks more than 80% of particles with an average size of 0.6㎛.

The safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention can reduce fine dust and airborne bacteria having a particle size of 0.03 um to 1.0 um, and has the same particle size as KF 80. It can exhibit the effect of blocking the fine dust and airborne bacteria by adsorbing more than 80% of harmful substances.

In addition, when the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention is sprayed on the yellow dust mask and quarantine mask, the blocking effect of fine dust and airborne bacteria can be increased, and the mask is in use It can effectively block odorous substances such as dust, fine dust, ultra-fine dust, formaldehyde, and ammonia entering the mask by maintaining normal blocking power without being affected by moisture caused by inhalation.

In particular, the performance of the cotton mask made of cotton fiber is evaluated to be less than a quarter of that of the KF80 mask. According to the Seoul Institute of Health and Environment, as a result of measuring the main dust collection efficiency that filters out fine particles, it was found that the droplet particle blocking rate of commercial cotton masks and homemade cotton masks with static filters removed was 16% to 22%. It is less than a quarter of the KF80 mask, which can filter out more than 80% of particles with a size of 0.6㎛.

However, when a safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention is sprayed on the cotton mask, it is possible to block fine dust having a particle size of 0.03 um to 1.0 um, so the KF80 mask It is possible to filter out particles of a better size.

Even in the case of a conventional dental mask, the effect of blocking harmful substances is lower than that of a mask including a melt-brown filter in the form of a non-woven outer and lining attached.

Specifically, a non-woven mask called a dental mask does not use a melt-brown filter, but uses a non-woven fabric as an outer and lining. there is

In addition, when spraying on the dental mask using the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention, the composition is coated on one or both sides of the nonwoven fabric so that the composition is equivalent to or equal to the melt brown filter It exhibits more harmful substances blocking effect.

In addition, compared to the conventional KF80 or KF94 mask, it is excellent in blocking effect of harmful substances, and can exhibit a significant difference from the conventional mask in that it can simultaneously exhibit antibacterial, antiviral and deodorizing effects.

As such, KF80 or KF94 masks are superior in blocking harmful substances compared to cotton masks, dental masks, and non-woven masks. By spraying and using the spray composition of the present invention, it can be usefully used because it exhibits more excellent antibacterial, antiviral and deodorizing effects.

The safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention is to be sprayed on the front surface of the cotton mask, dental mask, non-woven mask, and KF80 or KF94 mask. In other words, it is possible to purify the contaminated air introduced into the interior by inhalation from the user's mouth and nose, so that the user can breathe with clean air.

In addition, when the safe natural spray composition harmless to the human body for blocking the antibacterial, antiviral and harmful substances is sprayed, the adsorption capacity of metal ions is excellent, ^{and heavy metals such as Cd 2+} , Ni ²⁺ can be adsorbed, and other It can block by adsorbing fine dust and pollen contained in the polluted air.

Cadmium (cd) is a soft and toxic transition metal that is blue and white, and poisoning with this substance can cause itai-itai disease. The Itai-itai disease is a typical symptom of cadmium poisoning, and is a cadmium pollution disease occurring in the downstream of the Jinzu River in Toyama Prefecture, Japan. In the early stage, there are no obvious symptoms, so you may not feel any danger, but the main symptom is bone brittleness as calcium accumulates in the bones instead of calcium. In addition, shortness of breath, chest tightness, and cardiopulmonary dysfunction appear, and if continued, death may occur. Zinc has the effect of removing lead, which is a harmful heavy metal, and when cadmium accumulates, zinc cannot function properly in the nervous system, causing itai-itai disease.

Nickel (Ni) is a silver-white transition metal with a hard, metallic luster. Exposure to this substance can cause skin diseases, diarrhea, gastritis, vomiting, indigestion, duodenitis, insomnia, anemia, headache, rhinitis, bronchitis, asthma, and mild It can cause fibrosis and various respiratory-related diseases. According to some studies, it can also cause myocardial infarction, stroke, respiratory cancer, and kidney failure.

In addition, there is an advantage that the mask can be used for a long time by effectively blocking and removing odor substances such as formaldehyde and ammonia.

In particular, a safe natural spray composition that is harmless to the human body for blocking antibacterial, antiviral and harmful substances is sprayed on the front side of the mask and comes into contact with the user's face when used, thereby preventing skin irritation.

The material from which the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances is sprayed may be a mask sheet made of at least one of a polyester-based nonwoven fabric and a polyethylene-based nonwoven fabric, but antibacterial , It is a material that can be used in the field to exhibit antiviral, deodorizing and harmful substance blocking effects, and its size and shape are not limited.

The harmful substances include volatile harmful substances (VOSs) such as ammonia, trimethylamine, hydrogen sulfide and methyl mercaptan, pathogenic microorganisms, allergens such as pollen, industrial dust such as coal and metal powder, fine dust caused by yellow dust, viruses , means air containing bacteria, and if you do not use the safe natural spray that is harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention, harmful components of air polluted by breathing penetrate into the body, the present invention It is possible to prevent the harmful substances from penetrating through the respiration by the spray composition exhibiting the antibacterial, antiviral and harmful substance blocking effect of the.

Therefore, the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention can be used in various applications, such as medical, industrial, and daily life antibacterial agents and deodorants caused by fine dust and yellow dust.

The safe natural spray composition for blocking antibacterial, antiviral and harmful substances of the present invention has antibacterial, antiviral and deodorizing effects, as well as heavy metals and fine dust, even when applied to clothing, bathroom products, curtains, blinds, bedding and wallpaper. It can show the effect of blocking harmful substances such as

In particular, in the case of clothing, bathroom products, and bedding, when the safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances of the present invention is applied, the growth of fungi on keratin accumulated in direct contact with human skin is prevented. It is possible to suppress the occurrence of odors caused by the smell of sweat in summer.

In addition, since clothing, including T-shirts and socks, is vulnerable to harmful substances present in the external atmosphere, a preparation for removing harmful substances is required, and the present invention is a safe and natural material that is harmless to the human body for blocking antibacterial, antiviral and harmful substances. The spray composition can be used for absorbent fabric or cloth, and can exhibit antibacterial, antiviral, deodorizing and harmful substance blocking effects through the spray composition.

Examples of the bathroom products include towels and handkerchiefs, and examples of bedding include pillows and blankets.

The natural antibacterial agent according to another embodiment of the present invention includes the antibacterial, antiviral and safe natural spray composition harmless to the human body for blocking harmful substances.

The natural deodorant according to another embodiment of the present invention includes the antibacterial, antiviral and safe natural spray composition harmless to the human body for blocking harmful substances.

A natural cleaner according to another embodiment of the present invention is to include the antibacterial, antiviral and safe natural spray composition harmless to the human body for blocking harmful substances.

The present invention contains a natural extract that exhibits antibacterial, antiviral and harmful substance blocking effect as an active ingredient. A natural spray composition is provided.

In addition, the present invention can be applied without limitation on the type, shape or structure of the substrate by providing it as an aqueous liquid type spray composition, and can be applied to various fields.

1 shows the heavy metal adsorption capacity of a safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances according to an embodiment of the present invention.
Figure 2 shows the antibacterial effect of a safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances according to an embodiment of the present invention.
Figure 3 shows the antiviral effect of a safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances according to an embodiment of the present invention.
Figure 4 shows the deodorizing effect of a safe natural spray composition harmless to the human body for blocking antibacterial, antiviral and harmful substances according to an embodiment of the present invention.

Hereinafter, embodiments of the present invention will be described in detail so that those of ordinary skill in the art can easily carry out the present invention. However, the present invention may be embodied in several different forms and is not limited to the embodiments described herein.

[Preparation Example 1: Preparation of a spray composition for blocking antibacterial, antiviral and harmful substances]

One. Preparation of natural extracts

First, Lonicera japonica was washed, dried, and then pulverized. The pulverized product was mixed with ethanol and extracted for 2 hours, cooled and filtered with Whatman filter paper to obtain the filtrate, which was prepared as an extract of gold and silver coins (LEE).

Milk thistle extract (YEE), New green extract (NEE), gondalbi extract (DEE), dandelion extract (MEE), green tea extract (TEE), ginseng extract (PE), Angelica asiatica extract (AE) in the same manner as the ginseng extract (LEE). ), red ginseng extract (HE), astragalus extract (ME), ginger extract (ZE), soybean extract (GE), rice bran extract (EE), mulberry leaf extract (FE), mugwort extract (IE), mesyl extract (SE), baeksuo extract (VE), apple peel extract (XE), omija extract (KE), chlorella extract (CE), oregano extract (OE), sage extract (BE), basil extract (JE), fennel extract (RE), Garlic Extract (TE), Lemon Balm Extract (UE), Peppermint Extract (WE), Rosemary Extract (DE), Echinacea Extract (QE), Sambucus Extract (LE), Licorice Extract (NE), Orchid Extract (YE) , blueberry extract (bE), grape peel ethanol extract (GSE) and orange peel ethanol extract (OSE) were prepared.

2. Preparation of a spray composition for blocking antibacterial, antiviral and harmful substances

Based on 100 parts by weight of a 70% concentration ethanol aqueous solution in a reagent bottle cleanly sterilized at room temperature, 100 parts by weight of an extract of gold and silver leaf (LEE), 100 parts by weight of thistle extract (YEE), 100 parts by weight of New Green extract (NEE), gondalbi extract ( DEE) 100 parts by weight, dandelion extract (MEE) 100 parts by weight, and green tea extract (TEE) 100 parts by weight were mixed and aged for 24 hours at room temperature to prepare a natural composition for spraying (HC1).

The prepared antibacterial natural composition (HC1) and natural extract were mixed in the content range as shown in [Table 1] and [Table 2] to prepare a spray composition for blocking antibacterial, antiviral and harmful substances.

AX1 AX2 AX3 AX4 AX5 AX6 AX7 AX8 AX9 AX10 AX11 AX12 AX13 AX14 AX15 HC1 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 PE - 5 - - - - - - - - - - - - - AE - - 5 - - - - - - - - - - - - HE - - - 5 - - - - - - - - - - - ME - - - - 5 - - - - - - - - - - ZE - - - - - 5 - - - - - - - - - GE - - - - - - 5 - - - - - - - - EE - - - - - - - 5 - - - - - - - FE - - - - - - - - 5 - - - - - - IE - - - - - - - - - 5 - - - - - SE - - - - - - - - - - 5 - - - - VE - - - - - - - - - - - 5 - - - XE - - - - - - - - - - - - 5 - - KE - - - - - - - - - - - - - 5 - CE - - - - - - - - - - - - - - 5

(Unit: parts by weight)

AX16 AX17 AX18 AX19 AX20 AX21 AX22 AX23 AX24 AX25 AX26 AX27 AX28 AX29 AX30 HC1 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 CE 5 - - - - - - - - - - - - - - OE - 5 - - - - - - - - - - - - - BE - - 5 - - - - - - - - - - - - JE - - - 5 - - - - - - - - - - - RE - - - - 5 - - - - - - - - - - TE - - - - - 5 - - - - - - - - - UE - - - - - - 5 - - - - - - - - WE - - - - - - - 5 - - - - - - - DE - - - - - - - - 5 - - - - - - QE - - - - - - - - - 5 - - - - - LE - - - - - - - - - - 5 - - - - NE - - - - - - - - - - - 5 - - - YE - - - - - - - - - - - - 5 - - bE - - - - - - - - - - - - - 5 - GSE - - - - - - - - - - - - - - 15 OSE - - - - - - - - - - - - - - 15

(Unit: parts by weight)

With respect to the antibacterial, antiviral and harmful substance blocking spray composition AX30, 5 parts by weight of ginseng extract (PE), 5 parts by weight of Angelicae extract (AE), 5 parts by weight of red ginseng extract (HE), 5 parts by weight of Astragalus extract (ME) part, ginger extract (ZE) 5 parts by weight, soybean extract (GE) 5 parts by weight, rice bran extract (EE) 5 parts by weight, mulberry leaf extract (FE), mugwort extract (IE) 5 parts by weight, mesyl extract (SE) 5 parts by weight, baeksuo extract (VE) 5 parts by weight, apple peel extract (XE) 5 parts by weight, omija extract (KE) 5 parts by weight, chlorella extract (CE) 5 parts by weight, oregano extract (OE) 5 parts by weight, 5 parts by weight of sage extract (BE), 5 parts by weight of basil extract (JE), 5 parts by weight of fennel extract (RE), 5 parts by weight of garlic extract (TE), 5 parts by weight of lemon balm extract (UE), mint extract (WE) ) 5 parts by weight, rosemary extract (DE) 5 parts by weight, echinacea extract (QE) 5 parts by weight, sambucus extract (LE) 5 parts by weight, licorice extract (NE) 5 parts by weight, oleracea extract (YE) 5 parts by weight Part and 5 parts by weight of blueberry extract (bE) were mixed to prepare a spray composition AX31 for blocking antibacterial, antiviral and harmful substances.

[Preparation Example 2: Preparation of a face mask coated with the spray composition of the present invention]

Comparative Example of 32 commercially available cotton masks coated with the antibacterial, antiviral and harmful substance blocking spray compositions AX1 to AX31 prepared in Preparation Example 1 (MS1 to MS31) and non-coated cotton masks (MS0).

[Experimental Example 1: Hazardous Substance Blocking Effect Test]

Heavy metal adsorption capacity test

The adsorption amount of the heavy metal cadmium and nickel of 32 cotton masks (MS0 to MS31) prepared in Preparation Example 2 was evaluated.

After preparing 34 each of the aqueous solution samples each containing 10 mmol of cadmium and nickel, 32 cotton masks (MS0 to MS31) were placed in 100 mL of cadmium aqueous solution and nickel aqueous solution samples, respectively, and left for 24 hours, As a control, 0.1 g of a commercially available KF 80 mask adsorption sheet and 0.1 g of a non-woven mask sheet were also allowed to adsorb cadmium and nickel in aqueous solution.

The cadmium and nickel-adsorbed cotton masks MS0 to MS31, the KF 80 mask absorption sheet and the non-woven mask sheet are recovered, and the cotton masks MS0 to MS31, KF 80 mask absorption sheet and the non-woven mask sheet are removed. By back titration, the adsorption amount of cadmium and nickel adsorbed by each adsorption member was calculated.

The results are shown in FIG. 1, and as shown in FIG. 1, the cotton masks MS0 to MS31 of the present invention show superior adsorption efficiency compared to the commercially available KR 80 mask adsorption sheet and nonwoven mask sheet. Confirmed.

In particular, it was confirmed that the spray compositions (AX1 to AX31) for blocking antibacterial, antiviral and harmful substances of the present invention exhibited superior adsorption performance in the coated cotton masks MS1 to MS31 compared to the uncoated cotton mask (MS0).

In addition, it was confirmed that the cotton masks MS1, MS30 and MS31 coated with the antibacterial, antiviral and harmful substances blocking spray compositions AX1, AX30 and AX31 of the present invention exhibited excellent adsorption performance.

Instantaneous fine dust collection efficiency

In order to measure the fine dust collection efficiency of the cotton masks MS1, MS30 and MS31, which showed an excellent effect in the heavy metal adsorption capacity test, 1 wt % of potassium chloride was dissolved in distilled water and the particle generator was operated to obtain an average particle diameter of 0.03 μm to 0.1 μm. Mixed particles in which the particles were mixed were prepared.

Using the mixed particles, the fine dust collection efficiency for the present invention was measured.

The particles were injected into the cotton masks MS1, MS30 and MS31 to measure the potassium chloride capture efficiency according to the weight method of ASHRAE STANDARD 52.1 at a test wind speed of 1.0 m/s and an end pressure loss of 76 mmAq.

For the relative evaluation, as a control, a commercially available absorption sheet for a KF 80 mask and an untreated cotton mask (MS0) were used. did

The results are shown in Table 3 below.

Control 1
(sheet for KF 80 mask) Control 2
(Untreated face mask) MS1 MS30 MS31 Fine dust collection efficiency 5 2 6 9 8

(Unit: Index)

As shown in Table 3 above, compared to the KF 80 mask sheet that blocks 80% of fine dust with a particle size of 0.04 um to 1.0 um, the spray composition for blocking antibacterial, antiviral and harmful substances of the present invention is applied. It was confirmed that the cotton masks MS1, MS30 and MS31 were excellent in the effect of collecting particles having an average particle diameter of 0.03 μm to 0.1 μm.

In addition, the untreated cotton mask (MS0) had lower fine dust collection efficiency compared to the KF 80 mask sheet, but the cotton masks MS1, MS30 and In the case of MS31, it was confirmed that the fine dust collection efficiency was superior to that of the KF 80 mask sheet.

[Experimental Example 2: Antibacterial, antiviral and deodorizing effect test]

Antibacterial effect test

In order to examine the antibacterial effect of the comparative example cotton mask MS0 prepared in Preparation Example 2 and the cotton masks MS1 to MS31 coated with antibacterial, antiviral and harmful substance blocking spray compositions (AX1 to AX31), KS 0693 - 1990 test According to the law, Staphylococcus aureus, which is generally present on the skin and nasal surfaces of humans, ^{was inoculated with 10 6} strains, and the antibacterial level of the fabrics for cotton masks MS0 to MS31 was measured.

For the relative evaluation, a commercially available KF 80 mask sheet was used as a control, and the comparative example cotton mask MS0 and KF 80 mask sheet were untreated with the antibacterial, antiviral and harmful substance blocking spray composition.

The antibacterial effect was shown in FIG. 2 by measuring the amount of microorganisms, and as shown in FIG. 2, cotton masks MS1, MS30 and It was confirmed that MS31 exhibited high antimicrobial activity in which the amount of microorganisms ^{decreased to 10 3} or less, and in particular, in contrast to the cotton mask MS0 to which the antibacterial, antiviral and harmful substance blocking spray composition of the present invention was not applied, the applied MS1 to MS30 showed an excellent antibacterial effect compared to the KF 80 mask sheet.

Antiviral effect test

In order to examine the antiviral effect of the comparative example cotton mask MS0 prepared in Preparation Example 2 and the cotton masks MS1 to MS31 coated with antibacterial, antiviral and harmful substance blocking spray compositions (AX1 to AX31), influenza (influenza) After infiltrating the virus, the virus value was measured after a certain period of time.

For the relative evaluation, a commercially available KF 80 mask sheet was used as a control, and the comparative example cotton mask MS0 and KF 80 mask sheet were untreated with the antibacterial, antiviral and deodorizing composition, and after a certain period of time Later virus values were measured.

The results are shown in FIG. 3, and the virus reduction rate after a certain time has elapsed.

As shown in FIG. 3 , a high antiviral effect that reduces influenza virus values by 90% or more in the cotton masks MS1, MS30 and MS31 coated with the antibacterial, antiviral and harmful substance blocking spray composition of the present invention compared to the untreated group It was confirmed that the

In particular, the antibacterial, antiviral and harmful substance blocking spray composition of the present invention was not applied to the mask MS0, whereas the applied MS1 to MS30 showed an excellent antiviral effect compared to the KF 80 mask sheet.

Deodorization effect test

Using the KS M 0062:2004 test method, the deodorizing effect of the comparative example cotton mask MS0 and the cotton masks MS1 to MS31 coated with antibacterial, antiviral and harmful substances blocking spray compositions (AX1 to AX31) were investigated. Specifically, the cotton masks MS0 to MS31 were injected with a certain amount of ammonia in a 5L chamber, and then the concentration of residual ammonia over time was analyzed to calculate the deodorization rate.

For the relative evaluation, a commercially available KF 80 mask sheet was used as a control, and the comparative example cotton mask MS0 and KF 80 mask sheet were untreated with the antibacterial, antiviral and deodorizing composition.

The results are shown in FIG. 4 below.

As a result of the measurement, as shown in FIG. 4 below, the cotton masks MS1, MS30 and MS31 coated with the antibacterial, antiviral and harmful substance blocking spray composition of the present invention contained ammonia, the main culprit of living odor, from 60 to 90 with respect to the initial concentration. It was confirmed that the deodorization effect was exhibited by removing more than %.

In particular, the antibacterial, antiviral and harmful substance blocking spray composition of the present invention was not applied to the cotton mask MS0, whereas the applied MS1 to MS30 showed an excellent deodorizing effect compared to the KF 80 mask sheet.

[Experimental Example 3: Efficacy of spray composition for blocking antibacterial, antiviral and harmful substances]

In order to check whether the cotton mask coated with the antibacterial, antiviral and harmful substance blocking spray composition of the present invention confirmed in Experimental Examples 1 and 2 shows a significant effect on clothes and bathroom products, clothes, towels and After preparing a handkerchief and proceeding in the same manner as in the cotton mask experiment, the effects are shown in Table 4 below.

For the relative evaluation, the cotton mask MS30, which showed the best effect in Experimental Examples 1 and 2, was set to an index of 5, and the effect on the antibacterial, antiviral and harmful substance blocking spray composition of the present invention was measured.

MS30 dress Towel handkerchief Hazardous Substance Blocking Effect 5 5 6 6 antibacterial 5 5 5 5 antiviral 5 5 6 5 deodorization 5 6 6 5

(Unit: Index)

As shown in Table 4, the antibacterial, antiviral, and harmful substance blocking spray composition of the present invention has the effect of blocking harmful substances, antibacterial, antiviral and deodorizing even when applied to clothes, towels and handkerchiefs as well as a cotton mask. It was confirmed that it was excellent by equivalent or more.

[Experimental Example 4: Taste Test]

Skin irritation test

Thirty 20-year-old women who are sensitive to skin irritation were selected and divided into 5 groups of 6 each. Dilute the spray compositions AX1, AX30 and AX31 for blocking antibacterial, antiviral and harmful substances of the present invention in water and use them for 10 days. After that, a survey was conducted on whether or not skin irritation occurred, and the results are shown in Table 5 below.

[Evaluation standard]

◎: No irritation at all

○: Almost no stimulation

△: There is slight irritation, so it is not recommended to use it on sensitive mucous membranes

Х: Extremely irritating, unusable

AX1 AX30 AX31 1 group ◎ ◎ ◎ 2 groups ○ ◎ ○ 3 groups ○ ○ ○ 4 groups ◎ ◎ ◎ 5 groups ◎ ◎ ◎

According to Table 5, it was confirmed that when the spray compositions AX1, AX30 and AX31 for blocking antibacterial, antiviral and harmful substances of the present invention were used, there was almost no skin irritation. In particular, it was confirmed that the composition according to AX30 hardly felt skin irritation.

Although preferred embodiments of the present invention have been described in detail above, the scope of the present invention is not limited thereto, and various modifications and improvements by those skilled in the art using the basic concept of the present invention as defined in the following claims are also provided. is within the scope of the

Claims (7)

an aqueous solution of ethanol,
Natural thistle (irsium japonicum) extract, New Green (Brassica oleracea var. botrytis aut italiana L.) extract, Ligularia stenocephala extract, Dandelion (Taraxacum platycarpum), Green tea extract, Panax ginseng extract and mixtures thereof containing extracts
A safe natural spray composition that is harmless to the human body for blocking antibacterial, antiviral and harmful substances. The method of claim 1,
The ethanol aqueous solution is an ethanol aqueous solution having a concentration of 60% to 70%
A safe natural spray composition that is harmless to the human body for blocking antibacterial, antiviral and harmful substances. The method of claim 1,
The composition is gold and silver (Lonicera japonica), Angelica gigas, red ginseng, Astragalus propinquus, ginger (Zingiber officinale), soybean (Glycine max), rice bran, mulberry leaf (Tilia taquetii CKSchneid.), mugwort (Artemisia), Plum (Prunus mume), Cynanchum bungei, Apple peel, Schisandra chinensis, Chlorella, Oregano (origanum vulgare), Sage (Salvia officinalis), Basil (Ocimum basilicum), Fennel (oeniculum) , Garlic (Allium sativum), Lemon Balm (Melissa officinalis), Mint (Mentha canadensis), Rosemary (Salvia Rosmarinus), Echinacea (Echinacea), Sambucus (Sambucus), Licorice (Glycyrrhiza uralensis), Orchid (Eleutherococcus) senticosus, Blueberry (Cyanococcus) and further comprising a natural extract selected from the group consisting of mixtures thereof
A safe natural spray composition that is harmless to the human body for blocking antibacterial, antiviral and harmful substances. According to claim 1,
The composition blocks fine dust having a particle size of 0.03 um to 1.0 um and reduces airborne bacteria.
A safe natural spray composition that is harmless to the human body for blocking antibacterial, antiviral and harmful substances. Claims 1 to 4, comprising a safe natural spray composition that is harmless to the human body for blocking antibacterial, antiviral and harmful substances according to any one of claims 1 to 4
natural antibacterial agent. Claims 1 to 4, comprising a safe natural spray composition that is harmless to the human body for blocking antibacterial, antiviral and harmful substances according to any one of claims 1 to 4
Natural deodorant. Claims 1 to 4, comprising a safe natural spray composition that is harmless to the human body for blocking antibacterial, antiviral and harmful substances according to any one of claims 1 to 4
natural cleanser.

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