KR101260371B1 - Antibiotic deodorant composition including mulberry extract - Google Patents

Abstract

PURPOSE: An antibiotic deodorant composite including a mulberry extract is provided to implement an antibiotic effect on skin bacteria, to restrain ammonia odor, and to freshen air. CONSTITUTION: An antibiotic deodorant composite including a mulberry extract comprises 7 to 30 wt% of a mulberry leaf extract, 7 to 30 wt% of a mulberry root extract, 5 to 25 wt% of a chamaecyparis obtuse extract, 3 to 20 wt% of a cinnamomum japonicum siebold extract, 0.1 to 3 wt% of a liquid olive, 10 to 25 wt% of ethanol, and 20 to 40 wt% of water. The composite further includes 3 to 20 wt% of a persimmon extract and 0.01 to 5 wt% of at least one liquid chamaecyparis obtuse extract which is selected from a group of essential oil of chamaecyparis obtuse and the floral water of chamaecyparis obtuse.

Description

Antibacterial deodorant composition comprising mulberry extract {ANTIBIOTIC DEODORANT COMPOSITION INCLUDING MULBERRY EXTRACT}

The present invention relates to an antimicrobial deodorant composition comprising the mulberry extract as a main component, more specifically, the leaf and root extract of the mulberry as a main ingredient and the skin is parasitic to the skin of the mandarin extract and dalberry extract The present invention relates to an antibacterial deodorizing composition having an antimicrobial activity against bacteria and suppressing odors such as ammonia generated while aging and having aromaticity.

According to the analysis of the National Statistical Office, Korea entered into an aging society in 2000, and by 2026, it has become an aging society, and the number of aging population exceeds the number of childhood population, and the change of domestic population pyramid is expected due to the increase of aging population. As the elderly population increases, the necessity and diversity of well-being silver household products are required.

Aging is the main cause of aging, the human body has been eating, digesting, and excreted for decades, the body's metabolism is not smooth, making a lot of waste material, unsaturated fatty acids are decomposed, non-non-aldehyde (C ₉ H ₁₆ O) smells bad. In particular, areas where the secretory glands are gathered, such as ammonia, sweat glands, armpits, and the genital area due to poor functioning of urination, do not leave a cloudy and smoky smell unless washed well.

Smell of old people may cause discomfort to family and neighbors, create feelings of isolation and discomfort from children and grandchildren, and cause severe depression.In group life in nursing homes, complaints of headache, loss of appetite, sleep disorders, etc. There is a situation.

Commercially available deodorant deodorant is mainly used a lot of aromatic masking agent and there are perfumes that are deodorant used to control the body odor and the like for home, car air freshener, various workplaces, such as deodorant in the bathroom. These forms also include volatilization of frankincense components solidified with aerosols, spray sprays, gelatin, agar, etc. by inert gas such as freon, divergence by sublimation, evaporation from powder surface, silica, etc. There are many kinds of products such as adsorption type, but most of them are synthetic fragrances and ingredients.

The deodorant currently developed in Korea includes deodorant and deodorant using a powerful aroma masking effect, but research and development on deodorant and deodorant beauty products that can remove or improve the odor from the body of the elderly is almost done. In addition, due to the characteristics that need to be in direct contact with the human body, there is an urgent need for the development of herbal products that exclude chemical ingredients or beauty products that can be deodorized and deodorized using natural herbal materials.

Thus, the inventor of the present invention can effectively remove the ammonia odor from the body of the elderly by selecting a deodorant material (condensed tannin, polyphenols) from the aromas that are native to Korea and the herbal herbs with a unique aroma. The deodorant composition was developed to arrive at the present invention.

It is an object of the present invention to provide an antibacterial deodorizing composition having a mulberry leaf and root extract as a main component, has antibacterial activity against the skin bacteria parasitic on the skin, inhibits ammonia odor and has aroma.

Deodorizing composition of the present invention,

7 to 30% by weight of mulberry leaf extract, 7 to 30% by weight of mulberry root extract, 5 to 25% by weight of cypress extract, 3 to 20% by weight of rhododendron extract, 0.1 to 3% by weight of olive liquid, ethanol 10 To 25 wt%, and 20 to 40 wt% of water.

The antimicrobial deodorant composition of the present invention has a mulberry leaves and roots as a main component has an antimicrobial activity against skin bacteria and can effectively remove the odor of ammonia. In addition, the cypress and dalberry extract is properly mixed to give a good fragrance, and the high content of polyphenolic compounds has an antioxidant ability to prevent skin aging when applied to the skin.

The antimicrobial deodorant composition of the present invention can minimize side effects on the human body by using natural medicines such as mulberry, cypress, hawthorn.

Antibacterial deodorant composition of the present invention,

7 to 30% by weight of mulberry leaf extract, 7 to 30% by weight of mulberry root extract, 5 to 25% by weight of cypress extract, 3 to 20% by weight of rhododendron extract, 0.1 to 3% by weight of olive liquid, ethanol 10 To 25 wt%, and 20 to 40 wt% of water.

First, the properties of the main components constituting the deodorizing composition of the present invention.

Mulberry has traditionally been used as a medicine to reduce blood sugar and lower blood pressure in herbal medicine, and has recently been used as a health tea.

Mulberry leaves are known to have a hypoglycemic effect, and also lower and stabilize blood pressure in hypertensive patients, lower triglyceride levels and cholesterol content in blood, and in particular, increase HDL-cholesterol levels and lower harmful LDL-cholesterol levels. Seems. Mulberry leaves have been reported to treat arteriosclerosis, improve blood flow, increase the number of beneficial bacteria in the intestinal bacteria and inhibit aging due to its antioxidant effect.

It is known that the mulberry tree's root bark, baekbaekpi, contains more than 100 substances. Among them, efficacy is known as moran A, which lowers blood sugar, and mulberrofuran F, G, which lowers blood pressure. This is good for preventing adult diseases. Also, Kuwanon A ~ H (morusinol), Moracin, Demoracin, which kills bacteria in the body and is good for high blood pressure, etc. Morucin (cyclomorusin: a kind of anticancer ingredient) that kills tumors This is known.

Cypress, Chamaecyparis obtusa , is a cypress plant known to produce large amounts of pyhtoncide. Phytoncide is a substance that plants release or secrete to resist pathogens. Phytoncide is well absorbed by the human body, and the absorbed phytoncide is responsible for killing or driving away the germs that are harassing the cell by boosting its vitality and boosting immunity.

The known effects of herbal medicine of cypress is to stop the bleeding and abdominal pain caused by gastrointestinal bleeding and to use the cough caused by respiratory diseases.

Cinnamomum japonicum Siebold ( Cinnamomum japonicum Siebold ) is a camphor tree and is always a blue evergreen tree, and it is known that it can be extracted as a natural fragrance with good fragrance by rubbing it. Birch fruit is used as an additive fragrance to make edible oil and to make bread. It is also used as a soap material or medicine. In oriental medicine, it is used as a bark and a medicine called Cheonggye-gye (天 효능). It is said to be effective for cold abdominal pain, limbs and painful symptoms. Birch essential oil contains phellandrene, eugenol, methyleugenol, safrole, cineole and the like.

Mulberry leaves and roots having the above characteristics, extracts, such as cypress, hawthorn is used in the antimicrobial deodorant composition of the present invention.

In the deodorizing composition of the present invention, each component is extracted with ethanol and then using an extract obtained by extracting a useful component using ethyl acetate.

In the antimicrobial deodorizing composition of the present invention, if the content of the mulberry leaf extract is less than 7% by weight relative to the total weight of the composition, there is a problem in that the removal efficiency of ammonia (NH ₃ ) is insufficient, and the content of the mulberry leaf extract is 30% by weight relative to the total weight of the composition. If it exceeds the high taste (bitter flavor) is a strong flying problem.

In the antibacterial and deodorant composition of the present invention, if the content of the mulberry root extract is less than 7% by weight relative to the total weight of the composition, there is a problem in that the antimicrobial and whitening effects are insufficient, and the content of the mulberry root extract is more than 30% by weight relative to the total weight of the composition. There is a problem that high flavor is strong.

In the deodorizing composition of the present invention, if the content of the cypress extract is less than 5% by weight relative to the total weight of the composition, there is a problem in that the aromatic effect is insufficient, and if the content of the cypress extract exceeds 25% by weight relative to the total weight of the composition, such as mulberry extract Due to the low content of other components of the antimicrobial and deodorant effect is insufficient.

In the deodorizing composition of the present invention, at least one cypress extract selected from the group consisting of cypress essential oil and cypress floral water may further comprise 0.01 to 5% by weight based on the total weight of the composition.

The method of obtaining the cypress essential oil and the cypress floral water is as follows: The leaves and branches of the cypress are put into water and distilled using a conventional steam distillation apparatus. The essential oil is distilled and collected in the upper layer. What is collected is floral water.

In the deodorizing composition of the present invention, when cypress essential oil and cypress floral water are used together, it is preferable to further include 0.01 to 1 wt% of cypress essential oil and 0.1 to 3 wt% of cypress floral water based on the total weight of the composition. .

In the deodorizing composition of the present invention, there is a problem that the fragrance effect is insufficient if the content of the barberry extract is less than 3% by weight relative to the total weight of the composition, the mulberry extract, etc., if the content of the barberry extract exceeds 20% by weight relative to the total weight of the composition Due to the low content of other components of the antimicrobial and deodorant effect is insufficient.

In the deodorizing composition of the present invention, at least one selected from the group consisting of essential oils and wild bilberry floral water may be 0.01 to 5% by weight based on the total weight of the composition.

The method of obtaining the essential oil of rhododendron and the flower of the wild tree is the same as the method of obtaining the essential oil of the cypress and the cypress floral water.

In the deodorizing composition of the present invention, when used with both wild and essential oil floral water, it is preferable to further include 0.01 to 1% by weight of wild essential oil and 0.1 to 3% by weight of wild wood floral water based on the total weight of the composition. .

In the antimicrobial deodorant composition of the present invention, the olive liquid (Liquid Olive) acts as an emulsifier to mix the essential oil in the composition well.

In the deodorizing composition of the present invention, ethanol and water serve as a solvent.

In the deodorizing composition of the present invention, distilled water is preferably used for water.

In addition, in the deodorizing composition of the present invention, persimmon extract may be made to further comprise 3 to 20% by weight based on the total weight of the composition. Persimmon contains a lot of tannins (polyphenols), it is known to remove the active oxygen and have an antioxidant effect, deodorizing effect.

In the deodorizing composition of the present invention, if the content of the persimmon extract is less than 3% by weight relative to the total weight of the composition, there is a problem that the deodorizing effect is inadequate, and when the content of the persimmon extract exceeds 20% by weight based on the total weight of the composition, other components are less There is a problem that the antimicrobial effect is insufficient.

The antimicrobial deodorant composition of the present invention may be prepared by being included in cosmetics, and may be prepared in formulations such as toner (skin), lotion, and other deodorant mists.

Hereinafter, the antimicrobial deodorant composition of the present invention will be described in more detail with reference to the following examples.

Example 1 Extract Preparation

Mulberry leaves and roots, rhododendron leaves, cypress leaves and persimmons were prepared and washed thoroughly. Each plant was cut to a certain size and extracted by administering ethanol to each plant, and then extract extraction concentrate was prepared using a reduced pressure concentrator. Distilled water was added to each of the concentrates obtained above to make a suspension, hexane was added to separate the oily layer, ethyl acetate was separated to the separated aqueous layer, and the fractionated layer was separated. Solid phase extracts were obtained.

Example 2 Extraction and Separation of Essential Oil and Floral Water

Cypress leaves and sprigs were prepared, washed thoroughly, cut to a certain size, 100 g of the cut cypress leaves and branches were placed in a circular flask, 500 g of distilled water was added to the flask, and steam distilled for 5 hours using a steam distillation apparatus. . The oil refined | distilled and collected in the upper layer and the floral water of the lower layer were isolate | separated, respectively. Birch leaves and sprigs were prepared and the essential oil and floral water were separated in the same manner as above.

Example 3 Preparation of Antimicrobial Deodorant Composition

15g of mulberry leaf extract prepared in Examples 1 and 2, mulberry root extract 15g, cypress extract 10g, 5g olive extract, 0.5g olive liquid, 25g ethanol was mixed and distilled water was administered to prepare a 100g antibacterial deodorizing composition.

Example 4 Preparation of Antimicrobial Deodorant Composition

Mulberry leaf extract 15g prepared in Examples 1 and 2, mulberry root extract 15g, cypress extract 10g, wild tree extract 5g, persimmon extract 5g, olive liquid 0.5g, ethanol 25g mixed and administered with distilled water 100g of antibacterial deodorant composition Was prepared.

Example 5 Preparation of Antimicrobial Deodorant Composition

10g mulberry leaf extract prepared in Examples 1 to 2, mulberry root extract 10g, cypress extract 6g, wild tree extract 5g, persimmon extract 5g, cypress essential oil 0.02g, cypress floral water 2g, olive liquid 0.5g, ethanol 25g 100 g of antimicrobial deodorant composition was prepared by mixing and administering distilled water.

Example 6 Preparation of Antibacterial Deodorant Composition

10g mulberry leaf extract prepared in Examples 1 to 2, mulberry root extract 10g, cypress extract 6g, wild berry extract 5g, persimmon extract 5g, cypress essential oil 0.02g, cypress floral water 2g, wild grape essential oil 0.02g, raw moon 2 g of wood floral water, 0.5 g of olive liquid, and 25 g of ethanol were mixed and distilled water was administered to prepare 100 g of an antibacterial deodorizing composition.

≪ Comparative Example 1 &

The mulberry leaf extract prepared in Example 1 35g, cypress extract 10g, wild ginseng extract 7g, olive liquid 0.5g, ethanol 25g was mixed and distilled water was administered to prepare a 100g antibacterial deodorizing composition.

Comparative Example 2

5g of mulberry leaf extract prepared in Example 1, mulberry root extract 5g, cypress extract 10g, raw ginseng extract 25g, olive liquid 0.5g, ethanol 25g was mixed and distilled water was administered to prepare a 100g antibacterial deodorizing composition.

The following tests were carried out using the antibacterial and deodorant compositions prepared in Examples and Comparative Examples.

Test Example 1 Deodorizing Force Test

The KCL-FIR 1085 method was used using the analysis equipment FT-IR (Model name: MIDAC I2004) of the Korea Institute of Construction Test. 20 mL of the liquid sample prepared in Examples and Comparative Examples was placed in a test chamber (size 5L) of FT-IR (gas cell temperature 60 ° C., pressure 14.57 psi, path length 10 m). The deodorization rate for NH ₃ ) gas was analyzed. Deodorization rate was calculated as [(blank concentration over time-sample concentration over time) / blank concentration over time] X 100.

sample % Deodorization by Time 0 min 30 minutes 60 minutes 90 minutes 120 minutes Example 3 0.0 95.3 96.5 97.2 97.6 Example 4 0.0 95.8 96.7 97.3 98.0 Example 5 0.0 97.9 97.9 98.4 98.4 Example 6 0.0 98.0 98.0 98.5 98.5 Comparative Example 1 0.0 80.0 81.8 82.4 82.7 Comparative Example 2 0.0 71.3 72.4 72.3 72.4

As shown in the results of Table 1, it was confirmed that the deodorizing compositions of the Example has a higher deodorization rate for ammonia than the deodorizing compositions of the comparative example.

Test Example 2 Antibacterial Activity Test

Antimicrobial activity assay was determined by the disk agar plate diffusion method. The agar medium diffusion method is to filter the sample solution at a concentration of 10 µg / disk with a 0.45 µm membrane filter (Milipore, USA) to sterilize and sterilize filter paper disks (Toyo, 8 mm, Japan). After 20 µl absorption, the solvent was completely volatilized, placed on a test plate medium to be in close contact with each other, and left in a 4 ° C. refrigerator for 1 hour. The diameter of the clear zone was measured.

Antibacterial activity (inhibition ring mm / 2mg) Example 3 14.87 Example 4 15.01 Example 5 15.56 Example 6 15.98 Comparative Example 1 8.56 Comparative Example 2 8.28

As shown in the results of Table 2, it was confirmed that the deodorizing compositions of the Example has a higher antimicrobial range than the deodorizing compositions of the Comparative Example.

<Test Example 3> Deodorization sensory test

The following tests were performed on 20 inspectors with sensory ability. A sample containing 5 μl of non-aldehyde (trans-2-nonenal, 97%) in 100 ml of distilled water was sprayed twice on the tissue of Y company, and then twice the deodorizing composition prepared in Examples and Comparative Examples was sprayed thereon. The examiner sniffed the tissue and evaluated the deodorizing effect olfactory and the results are shown in Table 3.

The evaluation criteria are as follows:

0. Odorless

Almost indistinguishable odor (minimum detected value)

2. Odor that can distinguish what smell (minimum value)

3. Easy to feel odor

4. Strong odor

5. Unbearable intense odor

Deodorizing power Example 3 2.5 Example 4 2.3 Example 5 2.2 Example 6 2.0 Comparative Example 1 3.8 Comparative Example 2 4.2

As shown in the results of Table 3, it was confirmed that the deodorizing compositions of the Example compared to the deodorizing compositions of the comparative example weakens the smell of non-aldehyde aldehyde.

Test Example 4 Aroma Preference Test

The following tests were performed on 20 inspectors with sensory ability. After spraying the compositions prepared in Examples and Comparative Examples twice on tissues of Y company, the tissues adsorbed onto the tissues were examined to examine the degree of preference for olfactory sensation and the results are shown in Table 4. Evaluation criteria were based on the 10-point scale method (1 (bad) to 10 (good)).

Incense preference Example 3 8.9 Example 4 9.0 Example 5 9.4 Example 6 9.4 Comparative Example 1 5.6 Comparative Example 2 4.8

As shown in the results of Table 4, it was confirmed that the deodorant compositions of the Example has a higher affinity than the deodorant compositions of the comparative example.

While the present invention has been described in connection with certain exemplary embodiments, it is to be understood that the invention is not limited to the disclosed exemplary embodiments, but, on the contrary, is intended to cover various modifications and equivalent arrangements included within the spirit and scope of the appended claims.

Claims (6)

7 to 30% by weight of mulberry leaf extract, 7 to 30% by weight of mulberry root extract, 5 to 25% by weight of cypress extract, 3 to 20% by weight of rhododendron extract, 0.1 to 3% by weight of olive liquid, ethanol 10 To 25 wt%, and 20 to 40 wt% of water. The method according to claim 1,
Antimicrobial deodorant composition, characterized in that it further comprises 3 to 20% by weight relative to the total weight of the composition. The method according to claim 1 or 2,
Antibacterial and deodorant composition, characterized in that the cypress extract is at least one selected from the group consisting of essential oil and cypress floral water, 0.01 to 5% by weight based on the total weight of the composition. The method according to claim 1 or 2,
Antibacterial and deodorant composition, characterized in that it further comprises 0.01 to 1% by weight of cypress essential oil and 0.1 to 3% by weight of cypress floral water, based on the total weight of the composition. The method according to claim 1 or 2,
Antibacterial and deodorant composition, characterized in that at least one selected from the group consisting of essential oils and wild tree floral water is 0.01 to 5% by weight based on the total weight of the composition. The method according to claim 1 or 2,
Antibacterial and deodorant composition, characterized in that it further comprises 0.01 to 1% by weight essential oil and 0.1 to 3% by weight of the wild tree flower relative to the total weight of the composition.