CN107137264A - A kind of floral water and preparation method thereof - Google Patents
A kind of floral water and preparation method thereof Download PDFInfo
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- CN107137264A CN107137264A CN201710271934.2A CN201710271934A CN107137264A CN 107137264 A CN107137264 A CN 107137264A CN 201710271934 A CN201710271934 A CN 201710271934A CN 107137264 A CN107137264 A CN 107137264A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/02—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
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Abstract
The invention belongs to daily chemical product technical field, and in particular to a kind of floral water and preparation method thereof, and the floral water is mainly made up of the raw material of following parts by weight:5 10 parts of 40 50 parts of ethanol, 50 70 parts of deionized water, 36 parts of dipropylene glycol, 37 parts of sodium citrate, 26 parts of antioxidant, 48 parts of peppermint oil, 5 10 parts of lemonweed essential oil, 6 11 parts of thyme essential oil, 48 parts of schizonepeta extract solution, 6 10 parts of windproof extract solution and Herba Andrographitis extract solution.The addition of Chinese medicine extract not only makes floral water smell unique in the present invention, also assigns the good mosquito repellent of floral water, effect of repellent antipruritic;The problem of dry skin occurred after traditional floral water use is alleviated in the addition of dipropylene glycol, and floral water preparation method of the present invention is simple, there is very big promotional value.
Description
Technical field
The invention belongs to daily chemical product technical field, and in particular to a kind of floral water and preparation method thereof.
Background technology
Mosquito needs to suck human blood to lay eggs, educate ovum, therefore brings many troubles to the mankind.Human body is by bite by mosquitos
Afterwards, skin can become red and swollen, and sufferings unbearably, have an effect on outward appearance.In addition, bite by mosquitos can also influence to sleep, propagate malaria,
Filariasis, Japanese Type-B encephalitis and leather step on the diseases such as heat, totally unfavorable to human body health.In order to take precautions against bite by mosquitos,
Most people can select the sprinkling floral water on one's body to carry out expelling mosquito.Tradition has the floral water of mosquito-repelling function, and its is main
Anophelifuge activity composition be generally the household pesticides compositions such as Metadelphene, dimethyl phthalate, mosquito repellent fat or dihydropyrone, belong to micro- malicious product,
And anaphylaxis irritant to the skin of contact.In addition, the reason for traditional floral water is in order in terms of preparation stabilization is usually contained
The ethanol of higher concentration(70% or so), thus some side effects are brought, such as accelerate skin water loss, cause dry skin, appearance
Easy aging, generation wrinkle, the stimulation to the tender skin of infant are then more prominent.At the children particularly infant of less than 6 years old
In the vigorous stage of growing, skin absorbability is stronger, and respiratory tract resistivity is weaker, should avoid producing using chemical mosquito repellent
Product;And after bite by mosquitos, small wound can be left on skin, if at this moment using traditional floral water, ethanol therein, change
Learn the chemical substances such as culicifuge directly can enter deep skin by these small wounds, so as to produce stimulation pain, exacerbation
Inflammation, causes skin injury, particularly Metadelphene, such as long-term or a large amount of using it is also possible that neurological symptom is white with inducing
Blood disease etc..Therefore, the mosquito-repellent perfume of exploitation safety non-toxic has important social effect.
The content of the invention
It is an object of the present invention to have stimulation to human body for the chemical composition added in many floral water of above-mentioned in the market
Property with hypersensitive problem there is provided it is a kind of without harmful chemical component have mosquito repellent, repellent antipruritic effect floral water.
To reach above-mentioned purpose, the technical solution adopted in the present invention is:
A kind of floral water, is mainly made up of the raw material of following parts by weight:It is 40-50 parts of ethanol, 50-70 parts of deionized water, double third sweet
3-6 parts of alcohol, 3-7 parts of sodium citrate, 2-6 parts of antioxidant, 4-8 parts of peppermint oil, 5-10 parts of lemonweed essential oil, thyme essential oil 6-
11 parts, 4-8 parts of schizonepeta extract solution, windproof extract solution 6-10 parts and 5-10 parts of Herba Andrographitis extract solution.
In the present invention, further instruction, the floral water is mainly made up of the raw material of following parts by weight:Ethanol 42-
48 parts, 55-65 parts of deionized water, 4-5 parts of dipropylene glycol, 4-6 parts of sodium citrate, 3-5 parts of antioxidant, 5-7 parts of peppermint oil, lemon
6-9 parts of vanilla essential oil, 7-10 parts of thyme essential oil, 5-7 parts of schizonepeta extract solution, windproof extract solution 7-9 parts and Herba Andrographitis extract solution
6-9 parts.
In the present invention, further instruction, the floral water is mainly made up of the raw material of following parts by weight:Ethanol 45
Part, 60 parts of deionized water, 4.5 parts of dipropylene glycol, 5 parts of sodium citrate, 4 parts of antioxidant, 6 parts of peppermint oil, lemonweed essential oil 7
Part, 9 parts of thyme essential oil, 6 parts of schizonepeta extract solution, 8 parts of windproof extract solution and 7 parts of Herba Andrographitis extract solution.
In the present invention, further instruction, described antioxidant is BHT.
In the present invention, further instruction, the concentration of the ethanol is 70%-75%.
A kind of method for preparing floral water, comprises the following steps:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, thyme essential oil, schizonepeta extract solution, windproof extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 85-95 DEG C, and mixture 1 is heated 1-2 hours under conditions of being maintained at 85-95 DEG C, is mixed
Thing 2;
(3)To step(2)Dipropylene glycol, peppermint oil, lemonweed essential oil, thyme essential oil, chaste tree are added in the mixture 2 of gained
Mustard extract solution, windproof extract solution and Herba Andrographitis extract solution, and 8- is stirred with 1000-1200r/min mixing speed
10min, is well mixed each raw material, obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 3-5 hours under conditions of being placed in 0-6 DEG C, produces floral water.
In the present invention, lemonweed essential oil, thyme essential oil, schizonepeta extract solution, windproof extract solution and Herba Andrographitis extract solution
Extracting method it is as follows:
The extracting method of lemonweed essential oil:(1)The carrying agent for accounting for lemonweed weight 0.3-0.5% is sprayed into lemonweed
In, then continuous cycling extraction, control extraction kettle temperature in lemonweed addition extraction kettle, will be carried out with supercritical carbon dioxide fluid
30-42 DEG C of degree, extracts pressure 15-25MPa, flow velocity is 15-20kg/h, extraction time 1.5-2.5h;The carrying agent is by following
The each component of mass fraction is mixed:50-55 parts of ethanol, 3-5 parts of triethanolamine, 0.3-0.5 parts of hexamethylene;(2)Will extraction
CO 2 fluid afterwards is separated into separator, and the flow of CO 2 fluid is 12-15kg/h, and separator pressure is
8-10MPa, temperature is 40-45 DEG C, extracts 1-3h, is released from separator bottom after extract, standing, lemon is obtained through water-oil separating
Lemon vanilla essential oil.
The extracting method of thyme essential oil:The acetone cold soaking of the 15-40 times of quality of thyme first 1-7 days, then use concentration
For the H for 1%-5%2SO4Acidifying, filtering, obtains extract solution, then is extracted with ethyl acetate 2-3 times, extract is filtered, in 0.04-
Solvent is recovered under reduced pressure under conditions of 0.06MPa, extract is produced.
The extracting method of schizonepeta extract solution:Schizonepeta is crushed, 30-50 mesh sieves is crossed, is placed in glass container, weight 5- is added
8 times of distilled water, is extracted using ultrasonic-microwave, control ultrasonic wave 600W(It is normally opened), microwave power 500-800W is continuous
2-5h is extracted, filtering extracts filtrate 2-4 times with organic solvent, combining extraction liquid, anhydrous sodium sulfate drying is concentrated under reduced pressure, i.e.,
Obtain schizonepeta extract solution.
The extracting method of windproof extract solution:After windproof crushing, soak 1-3 hours, the addition of water is windproof
10-20 times, then ultrasonic wave extraction 10-15 minutes, filter, centrifugation discards precipitation, by supernatant concentration, obtained windproof extract solution.
The extracting method of Herba Andrographitis extract solution:Take Herba Andrographitis to go the removal of impurity, clean, add the ethanol of 10-16 times of its weight
Solution, under 230-270MPa, ultra high pressure treatment 1-4min;Then at 38-46 DEG C, ultrasonic wave extraction 12-24min;Centrifugation
Separation, takes supernatant, obtains Herba Andrographitis extract solution.
The present invention has the advantage that compared with prior art:
1. floral water of the present invention has good mosquito repellent function and repellent antipruritic effect.Lemonweed essential oil gives out light
Citrus scented, makes one spirit and QI cleaning, while its fragrance distributed has good mosquito repellent function;The fragrance that thyme essential oil is distributed
Mosquito repellent, the effect of sterilization can be effectively acted as, two kinds of essential oils mix can strengthen mosquito repellent function in certain proportion.Schizonepeta have and
Blood anastalsis, for rubella pruigo, can be used for pruitus with windproof compatibility, therefore, schizonepeta extract solution and anti-in floral water
The addition of wind extract solution can alleviate the itch problem occurred after mosquito bite.After mosquito bite, skin occur local itch,
Swell and ache, and Herba Andrographitis extract solution has clearing heat and detoxicating, anti-inflammatory, swelling and pain relieving effect, it, which is added, can alleviate skin swelling and pain, itch
Symptom.Dipropylene glycol is a class NMF, and excitant is small, and with good moisture-keeping efficacy, its addition can alleviate wine in floral water
The problem of essence volatilization causes dry skin.Lemonweed essential oil, thyme essential oil, schizonepeta extract solution, windproof extraction in the present invention
The addition of liquid and Herba Andrographitis extract solution not only makes floral water smell unique, also assigns the good mosquito repellent of floral water, repellent antipruritic
Effect;The problem of dry skin occurred after traditional floral water use is alleviated in the addition of dipropylene glycol.
2. the material source used in floral water of the present invention is in plant extract material, harmless, excitant is small, preparation side
Method is simple, and required equipment is common equipment, is well suited for large-scale production.
Embodiment
The invention provides a kind of floral water is provided, to make the purpose of the present invention, technical scheme and effect clearer, bright
Really, the present invention is described in more detail below.It should be appreciated that specific embodiment described herein is only to explain this hair
It is bright, it is not intended to limit the present invention.
In following examples, lemonweed essential oil, thyme essential oil, schizonepeta extract solution, windproof extract solution and Herba Andrographitis are carried
Take liquid and extracted with following extracting method:
The extracting method of lemonweed essential oil:(1)The carrying agent for accounting for lemonweed weight 0.3-0.5% is sprayed into lemonweed
In, then continuous cycling extraction, control extraction kettle temperature in lemonweed addition extraction kettle, will be carried out with supercritical carbon dioxide fluid
30-42 DEG C of degree, extracts pressure 15-25MPa, flow velocity is 15-20kg/h, extraction time 1.5-2.5h;The carrying agent is by following
The each component of mass fraction is mixed:50-55 parts of ethanol, 3-5 parts of triethanolamine, 0.3-0.5 parts of hexamethylene;(2)Will extraction
CO 2 fluid afterwards is separated into separator, and the flow of CO 2 fluid is 12-15kg/h, and separator pressure is
8-10MPa, temperature is 40-45 DEG C, extracts 1-3h, is released from separator bottom after extract, standing, lemon is obtained through water-oil separating
Lemon vanilla essential oil.
The extracting method of thyme essential oil:The acetone cold soaking of the 15-40 times of quality of thyme first 1-7 days, then use concentration
For the H for 1%-5%2SO4Acidifying, filtering, obtains extract solution, then is extracted with ethyl acetate 2-3 times, extract is filtered, in 0.04-
Solvent is recovered under reduced pressure under conditions of 0.06MPa, extract is produced.
The extracting method of schizonepeta extract solution:Schizonepeta is crushed, 30-50 mesh sieves is crossed, is placed in glass container, weight 5- is added
8 times of distilled water, is extracted using ultrasonic-microwave, control ultrasonic wave 600W(It is normally opened), microwave power 500-800W is continuous
2-5h is extracted, filtering extracts filtrate 2-4 times with organic solvent, combining extraction liquid, anhydrous sodium sulfate drying is concentrated under reduced pressure, i.e.,
Obtain schizonepeta extract solution.
The extracting method of windproof extract solution:After windproof crushing, soak 1-3 hours, the addition of water is windproof
10-20 times, then ultrasonic wave extraction 10-15 minutes, filter, centrifugation discards precipitation, by supernatant concentration, obtained windproof extract solution
The extracting method of Herba Andrographitis extract solution:Take Herba Andrographitis to go the removal of impurity, clean, add the ethanol solution of 10-16 times of its weight,
Under 230-270MPa, ultra high pressure treatment 1-4min;Then at 38-46 DEG C, ultrasonic wave extraction 12-24min;Centrifuge,
Supernatant is taken, Herba Andrographitis extract solution is obtained.
Embodiment 1
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:40 parts of ethanol, 50 parts of deionized water, 3 parts of dipropylene glycol,
3 parts of sodium citrate, 2 parts of antioxidant, 4 parts of peppermint oil, 5 parts of lemonweed essential oil, 6 parts of thyme essential oil, 4 parts of schizonepeta extract solution,
5 parts of 6 parts of windproof extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 70%;The antioxidant is di-t-butyl
Paracresol.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, thyme essential oil, schizonepeta extract solution, windproof extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 85 DEG C, and mixture 1 is heated 1 hour under conditions of being maintained at 85 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, lemonweed essential oil, thyme essential oil, chaste tree are added in the mixture 2 of gained
Mustard extract solution, windproof extract solution and Herba Andrographitis extract solution, and 8min is stirred with 1000r/min mixing speed, make each original
Material is well mixed, obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 3 hours under conditions of being placed in 0 DEG C, produces floral water.
Embodiment 2
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:45 parts of ethanol, 60 parts of deionized water, dipropylene glycol 4.5
Part, 5 parts of sodium citrate, 4 parts of antioxidant, 6 parts of peppermint oil, 7 parts of lemonweed essential oil, 9 parts of thyme essential oil, schizonepeta extract solution 6
7 parts of part, 8 parts of windproof extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 73%;The antioxidant is two tertiary fourths
Base paracresol.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, thyme essential oil, schizonepeta extract solution, windproof extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 90 DEG C, and mixture 1 is heated 1.5 hours under conditions of being maintained at 90 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, lemonweed essential oil, thyme essential oil, chaste tree are added in the mixture 2 of gained
Mustard extract solution, windproof extract solution and Herba Andrographitis extract solution, and 9min is stirred with 1100r/min mixing speed, make each original
Material is well mixed, obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 4 hours under conditions of being placed in 3 DEG C, produces floral water.
Embodiment 3
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:50 parts of ethanol, 70 parts of deionized water, 6 parts of dipropylene glycol,
7 parts of sodium citrate, 6 parts of antioxidant, 8 parts of peppermint oil, 10 parts of lemonweed essential oil, 11 parts of thyme essential oil, schizonepeta extract solution 8
10 parts of part, 10 parts of windproof extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 75%;The antioxidant is two uncles
Butyl paracresol.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, thyme essential oil, schizonepeta extract solution, windproof extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 95 DEG C, and mixture 1 is heated 2 hours under conditions of being maintained at 95 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, lemonweed essential oil, thyme essential oil, chaste tree are added in the mixture 2 of gained
Mustard extract solution, windproof extract solution and Herba Andrographitis extract solution, and 10min is stirred with 1200r/min mixing speed, make each original
Material is well mixed, obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 5 hours under conditions of being placed in 6 DEG C, produces floral water.
Embodiment 4
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:42 parts of ethanol, 55 parts of deionized water, 4 parts of dipropylene glycol,
4 parts of sodium citrate, 3 parts of antioxidant, 5 parts of peppermint oil, 6 parts of lemonweed essential oil, 7 parts of thyme essential oil, 5 parts of schizonepeta extract solution,
6 parts of 7 parts of windproof extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 71%;The antioxidant is di-t-butyl
Paracresol.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, thyme essential oil, schizonepeta extract solution, windproof extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 87 DEG C, and mixture 1 is heated 1.2 hours under conditions of being maintained at 87 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, lemonweed essential oil, thyme essential oil, chaste tree are added in the mixture 2 of gained
Mustard extract solution, windproof extract solution and Herba Andrographitis extract solution, and 8min is stirred with 1050r/min mixing speed, make each original
Material is well mixed, obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 3.5 hours under conditions of being placed in 2 DEG C, produces floral water.
Embodiment 5
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:48 parts of ethanol, 65 parts of deionized water, 5 parts of dipropylene glycol,
6 parts of sodium citrate, 5 parts of antioxidant, 7 parts of peppermint oil, 9 parts of lemonweed essential oil, 10 parts of thyme essential oil, 7 parts of schizonepeta extract solution,
9 parts of 9 parts of windproof extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 74%;The antioxidant is di-t-butyl
Paracresol.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, thyme essential oil, schizonepeta extract solution, windproof extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 93 DEG C, and mixture 1 is heated 1.8 hours under conditions of being maintained at 93 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, lemonweed essential oil, thyme essential oil, chaste tree are added in the mixture 2 of gained
Mustard extract solution, windproof extract solution and Herba Andrographitis extract solution, and 10min is stirred with 1150r/min mixing speed, make each original
Material is well mixed, obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 4.5 hours under conditions of being placed in 5 DEG C, produces floral water.
Performance test
Performance test is carried out to the product obtained by embodiment 1-5, it is as a result as follows:
(1)Smell is checked:Sense organ, smell is pure and fresh;
(2)The repelling effect test of floral water
Some mosquitoes are caught with mosquito catcher and are put into mosquito cage, after " starvation " at a night cultivates, are divided into 6 groups, and 5 groups respectively with scribbling
The finger of embodiment 1-5 products obtained therefroms stretches into test in mosquito cage, and another group is with the finger test for being not coated with floral water, testing time
5 group fingers that product of the present invention is scribbled within 10min, 10min are all close without mosquito, and are not coated with being stung in the finger for floral water
Sting.Thus illustrate that floral water of the present invention has good repelling effect.
(3)Repellent antipruritic validity check
The detumescence effect that embodiment 1-5 prepares floral water is evaluated by experiment on probation, the volunteer 120 of 20-60 Sui is elected,
Sex ratio is 1:1, cause red swelling of the skin itch using mosquito saliva is injected, they are randomly divided into 6 groups, every group 20, its
In have one group as a control group, daily sooner or later respectively apply a corresponding floral water of 1-5 products of the embodiment of the present invention once, compare institute
The floral water used is commercially available floral water, continuous to use a week, redness and the consulting user detected by an unaided eye on skin
The improvement situation of pruritis, counts repellent antipruritic effect efficiently individual quantity and the effective people of antipruritic effect of 6 group volunteers respectively
Count and be recorded in as in following table.Assay such as following table:
Test group | Repellent antipruritic effect efficiently individual quantity | Antipruritic effect efficiently individual quantity |
Embodiment 1 | 18 | 17 |
Embodiment 2 | 19 | 19 |
Embodiment 3 | 17 | 18 |
Embodiment 4 | 16 | 17 |
Embodiment 5 | 16 | 16 |
Control group | 11 | 10 |
Embodiment 1-5 products have obvious repellent antipruritic effect to most people as seen from the above table, and commercially available floral water only has gently
Micro- repellent antipruritic effect.
Smell favorable comment degree and stimulation sex investigation:
Choose 80 volunteers and participate in experiment, volunteer is selected from the crowd to odor-sensitive, its range of age at 20-60 Sui, its
Volunteer's number of this 4 age brackets of middle 20-30 Sui, 30-40 Sui, 40-50 Sui and 50-60 Sui is 20 people, and each age
The sex ratio of section is 1:1, this 80 volunteers are randomly divided into two test groups of A, B, every group of 40 people.
Test group and subjects:A groups use floral water of the present invention, and B groups use commercially available floral water.
Test method:Floral water is sprayed on interior by volunteer before sleeping every night, and each volunteer uses the amount of floral water every time
It is identical, it is continuous to use 20 days, it is desirable to not used similar product in volunteer 20 days.
Evaluation criterion:Sensory evaluation is carried out for the smell of floral water, is divided into satisfied, general and dissatisfied three evaluations etc.
Level, statistics is satisfied with the percentage shared by the grade after 20 days, and is recorded in table;Excitant to floral water is evaluated, will
Hope person according to the excitant of floral water whether there is respectively favorable comment, in comment and difference comments three opinion ratings, positive rating is counted after 20 days, and
It is recorded in table.
After 20 days, investigation statisticses result is as shown in the table:
Experimental group number evidence | Smell | Excitant positive rating |
A groups | 91% | 90% |
B groups | 66% | 57% |
Find out that liquid distilled from honeysuckle flowers or lotus leaves aqueous vapor of the present invention is received by most of consumer by data above, improved compared to commercially available prod, together
When have stimulate it is small the characteristics of.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair
The equal change or modification change completed under bright patent claim, the technical spirit suggested by all present invention, all should belong to
Cover the scope of the claims in the present invention.
Claims (6)
1. a kind of floral water, it is characterised in that be mainly made up of the raw material of following parts by weight:40-50 parts of ethanol, deionized water
50-70 parts, 3-6 parts of dipropylene glycol, 3-7 parts of sodium citrate, 2-6 parts of antioxidant, 4-8 parts of peppermint oil, lemonweed essential oil 5-10
Part, 6-11 parts of thyme essential oil, 4-8 parts of schizonepeta extract solution, windproof extract solution 6-10 parts and 5-10 parts of Herba Andrographitis extract solution.
2. a kind of floral water according to claim 1, it is characterised in that be mainly made up of the raw material of following parts by weight:Second
42-48 parts of alcohol, 55-65 parts of deionized water, 4-5 parts of dipropylene glycol, 4-6 parts of sodium citrate, 3-5 parts of antioxidant, peppermint oil 5-7
Part, 6-9 parts of lemonweed essential oil, 7-10 parts of thyme essential oil, 5-7 parts of schizonepeta extract solution, windproof extract solution 7-9 parts and Herba Andrographitis
6-9 parts of extract solution.
3. a kind of floral water according to claim 1, it is characterised in that be mainly made up of the raw material of following parts by weight:Second
45 parts of alcohol, 60 parts of deionized water, 4.5 parts of dipropylene glycol, 5 parts of sodium citrate, 4 parts of antioxidant, 6 parts of peppermint oil, lemonweed essence
7 parts of 7 parts of oil, 9 parts of thyme essential oil, 6 parts of schizonepeta extract solution, 8 parts of windproof extract solution and Herba Andrographitis extract solution.
4. a kind of floral water according to claim 1-3 any one, it is characterised in that:Described antioxidant is two tertiary fourths
Base paracresol.
5. a kind of floral water according to claim 1-3 any one, it is characterised in that:The concentration of the ethanol is 70%-
75%。
6. a kind of prepare a kind of method of floral water described in claim 1-3 any one, it is characterised in that including following step
Suddenly:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, lemonweed are taken respectively
Essential oil, thyme essential oil, schizonepeta extract solution, windproof extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right
Mixture 1 carries out being heated to 85-95 DEG C, and mixture 1 is heated 1-2 hours under conditions of being maintained at 85-95 DEG C, is mixed
Thing 2;
(3)To step(2)Dipropylene glycol, peppermint oil, lemonweed essential oil, thyme essential oil, chaste tree are added in the mixture 2 of gained
Mustard extract solution, windproof extract solution and Herba Andrographitis extract solution, and 8- is stirred with 1000-1200r/min mixing speed
10min, is well mixed each raw material, obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 3-5 hours under conditions of being placed in 0-6 DEG C, produces floral water.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110251435A (en) * | 2019-07-24 | 2019-09-20 | 黑龙江省科学院高技术研究院 | A kind of essential oil with mosquito-expelling and antipruritic effect is spraying and preparation method thereof |
CN110638724A (en) * | 2019-11-06 | 2020-01-03 | 高小军 | Natural whitening floral water and preparation method thereof |
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CN1548028A (en) * | 2003-05-13 | 2004-11-24 | 上海家化联合股份有限公司 | Mosquito-repellent toilet water |
CN102579288A (en) * | 2012-04-06 | 2012-07-18 | 厦门鼎嘉奇投资管理有限公司 | Natural plant essential oil composition capable of directly serving as mosquito repellent |
CN105534871A (en) * | 2016-02-17 | 2016-05-04 | 广西大学 | Mosquito-repelling and itching-relieving floral water and preparation method thereof |
CN106389238A (en) * | 2016-12-09 | 2017-02-15 | 申艾平 | Floral water |
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2017
- 2017-04-24 CN CN201710271934.2A patent/CN107137264A/en not_active Withdrawn
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1548028A (en) * | 2003-05-13 | 2004-11-24 | 上海家化联合股份有限公司 | Mosquito-repellent toilet water |
CN102579288A (en) * | 2012-04-06 | 2012-07-18 | 厦门鼎嘉奇投资管理有限公司 | Natural plant essential oil composition capable of directly serving as mosquito repellent |
CN105534871A (en) * | 2016-02-17 | 2016-05-04 | 广西大学 | Mosquito-repelling and itching-relieving floral water and preparation method thereof |
CN106389238A (en) * | 2016-12-09 | 2017-02-15 | 申艾平 | Floral water |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110251435A (en) * | 2019-07-24 | 2019-09-20 | 黑龙江省科学院高技术研究院 | A kind of essential oil with mosquito-expelling and antipruritic effect is spraying and preparation method thereof |
CN110251435B (en) * | 2019-07-24 | 2022-01-11 | 黑龙江省科学院高技术研究院 | Essential oil spray with mosquito-repelling and itching-relieving effects and preparation method thereof |
CN110638724A (en) * | 2019-11-06 | 2020-01-03 | 高小军 | Natural whitening floral water and preparation method thereof |
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Application publication date: 20170908 |