CN107213049A - A kind of repellent antipruritic floral water - Google Patents

A kind of repellent antipruritic floral water Download PDF

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CN107213049A
CN107213049A CN201710272467.5A CN201710272467A CN107213049A CN 107213049 A CN107213049 A CN 107213049A CN 201710272467 A CN201710272467 A CN 201710272467A CN 107213049 A CN107213049 A CN 107213049A
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parts
extract solution
floral water
solution
antioxidant
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何新霞
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Guangxi University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/02Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82Preparation or application process involves sonication or ultrasonication

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
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Abstract

The invention belongs to daily chemical product technical field, and in particular to a kind of repellent antipruritic floral water, and the floral water is mainly made up of the raw material of following parts by weight:5 10 parts of 40 50 parts of ethanol, 50 70 parts of deionized water, 36 parts of dipropylene glycol, 37 parts of sodium citrate, 26 parts of antioxidant, 48 parts of peppermint oil, 5 10 parts of crape myrtle extract solution, 6 11 parts of Rosemary Oil, 48 parts of Flos Lonicerae extractive solution, 6 10 parts of stringy stonecrop extract solution and Herba Andrographitis extract solution.The floral water of the present invention has good repelling effect, because the material source of use is in plant, small effect is stimulated with safety, while having the effect of repellent antipruritic.Swollen and ache for caused itch after bite by mosquitos with significant mitigation;And floral water preparation method of the present invention is simple, there is very big promotional value.

Description

A kind of repellent antipruritic floral water
Technical field
The invention belongs to daily chemical product technical field, and in particular to a kind of repellent antipruritic floral water.
Background technology
Mosquito needs to suck human blood to lay eggs, educate ovum, therefore brings many troubles to the mankind.Human body is by bite by mosquitos Afterwards, skin can become red and swollen, and sufferings unbearably, have an effect on outward appearance.In addition, bite by mosquitos can also influence to sleep, propagate malaria, Filariasis, Japanese Type-B encephalitis and leather step on the diseases such as heat, totally unfavorable to human body health.In order to take precautions against bite by mosquitos, Most people can select the sprinkling floral water on one's body to carry out expelling mosquito.Tradition has the floral water of mosquito-repelling function, and its is main Anophelifuge activity composition be generally the household pesticides compositions such as Metadelphene, dimethyl phthalate, mosquito repellent fat or dihydropyrone, belong to micro- malicious product, And anaphylaxis irritant to the skin of contact.In addition, the reason for traditional floral water is in order in terms of preparation stabilization is usually contained The ethanol of higher concentration(70% or so), thus some side effects are brought, such as accelerate skin water loss, cause dry skin, appearance Easy aging, generation wrinkle, the stimulation to the tender skin of infant are then more prominent.At the children particularly infant of less than 6 years old In the vigorous stage of growing, skin absorbability is stronger, and respiratory tract resistivity is weaker, should avoid producing using chemical mosquito repellent Product;And after bite by mosquitos, small wound can be left on skin, if at this moment using traditional floral water, ethanol therein, change Learn the chemical substances such as culicifuge directly can enter deep skin by these small wounds, so as to produce stimulation pain, exacerbation Inflammation, causes skin injury, particularly Metadelphene, such as long-term or a large amount of using it is also possible that neurological symptom is white with inducing Blood disease etc..Therefore, the mosquito-repellent perfume of exploitation safety non-toxic has important social effect.
The content of the invention
It is an object of the present invention to have stimulation to human body for the chemical composition added in many floral water of above-mentioned in the market Property with hypersensitive problem there is provided a kind of floral water without harmful chemical component, while having the work(of mosquito repellent, repellent antipruritic Effect.
To reach above-mentioned purpose, the technical solution adopted in the present invention is:
A kind of floral water, is mainly made up of the raw material of following parts by weight:It is 40-50 parts of ethanol, 50-70 parts of deionized water, double third sweet 3-6 parts of alcohol, 3-7 parts of sodium citrate, 2-6 parts of antioxidant, 4-8 parts of peppermint oil, 5-10 parts of crape myrtle extract solution, Rosemary Oil 6-11 Part, 4-8 parts of Flos Lonicerae extractive solution, 6-10 parts of stringy stonecrop extract solution and 5-10 parts of Herba Andrographitis extract solution.
In the present invention, further instruction, the floral water is mainly made up of the raw material of following parts by weight:Ethanol 42- 48 parts, 55-65 parts of deionized water, 4-5 parts of dipropylene glycol, 4-6 parts of sodium citrate, 3-5 parts of antioxidant, 5-7 parts of peppermint oil, crape myrtle 6-9 parts of extract solution, 7-10 parts of Rosemary Oil, 5-7 parts of Flos Lonicerae extractive solution, 7-9 parts of stringy stonecrop extract solution and Herba Andrographitis are extracted 6-9 parts of liquid.
In the present invention, further instruction, the floral water is mainly made up of the raw material of following parts by weight:Ethanol 45 Part, 60 parts of deionized water, 4.5 parts of dipropylene glycol, 5 parts of sodium citrate, 4 parts of antioxidant, 6 parts of peppermint oil, 7 parts of crape myrtle extract solution, 7 parts of 9 parts of Rosemary Oil, 6 parts of Flos Lonicerae extractive solution, 8 parts of stringy stonecrop extract solution and Herba Andrographitis extract solution.
In the present invention, further instruction, described antioxidant is BHT.
In the present invention, further instruction, the concentration of the ethanol is 70%-75%.
A kind of method for preparing floral water, comprises the following steps:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, crape myrtle is taken to extract respectively Liquid, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right Mixture 1 carries out being heated to 85-95 DEG C, and mixture 1 is heated 1-2 hours under conditions of being maintained at 85-95 DEG C, is mixed Thing 2;
(3)To step(2)Dipropylene glycol, peppermint oil, crape myrtle extract solution, Rosemary Oil, gold and silver are added in the mixture 2 of gained Flower extract solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, and 8- is stirred with 1000-1200r/min mixing speed 10min, is well mixed each raw material, obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 3-5 hours under conditions of being placed in 0-6 DEG C, produces floral water.
In the present invention, crape myrtle extract solution, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis are extracted The extracting method of liquid is as follows:
The extracting method of crape myrtle extract solution:First each constitutive material pick selecting pure, then weigh purple according to composition by weight Common vetch petal is placed in ultrasonic extractor, add 2-4 times of weight than pure water, with 28KHz frequencies under 45-48 DEG C of constant temperature Lower concussion filters to obtain crape myrtle extract solution after extracting 25-30 minutes.
The extracting method of Rosemary Oil:Component weighs fresh rosemary petal by weight, clean be put into distiller every Water is distilled, and big fire is heated 2-3 hours, produces mixed gas, and mixed gas enters in condenser pipe along conduit, is condensed into mixing former Liquid, mixing stoste is poured into separatory funnel, water-oil separating removes moisture and obtains Rosemary Oil.
The extracting method of Flos Lonicerae extractive solution:Flower, Ye Hezhi are opened with deionized water cleaning Lonicera japonica, honeysuckle, And dry to below water content 8-15%;In terms of quality parts ratio, 60-70 parts of Lonicera japonica, gold and silver are added into distilling apparatus The flowers are in blossom let off fireworks 10-20 parts, 5-10 parts of leaf, 12-20 DEG C of deionized water of 5-10 parts of branch and 200-300 mass parts be mixed into distillation body System;Control distillation system to keep 12-20 DEG C of immersion 2-6h, be then warming up to 50-70 DEG C, keep 6-15h, evaporation is collected in condensation Thing, obtains Flos Lonicerae extractive solution.
The extracting method of stringy stonecrop extract solution:It will crush, weigh through garbled stringy stonecrop, be soaked with 5 times of extraction solvents Repeated after stain 3d, filtering 3 times, merging filtrate produces corresponding stringy stonecrop crude extract;Crude extract is added to Rotary Evaporators In Claisen flask, the temperature of ethanol, chloroform, petroleum ether is controlled, at 60-70 DEG C, 50-60 DEG C, 40-50 DEG C, to be concentrated under reduced pressure respectively Obtain stringy stonecrop extract solution.
The extracting method of Herba Andrographitis extract solution:Take Herba Andrographitis to go the removal of impurity, clean, add the ethanol of 10-16 times of its weight Solution, under 230-270MPa, ultra high pressure treatment 1-4min;Then at 38-46 DEG C, ultrasonic wave extraction 12-24min;Centrifugation Separation, takes supernatant, obtains Herba Andrographitis extract solution.
The present invention has the advantage that compared with prior art:
1. floral water of the present invention has good mosquito repellent function and repellent antipruritic effect.The fragrance that crape myrtle extract solution is distributed is to people Body is harmless, while playing the role of to make mosquito hear its perfume and keep away from;The smell that Rosemary Oil is distributed is special, has to mosquito certain Expeling effect, two kinds of essential oils mix can strengthen mosquito repellent function in certain proportion.Flos Lonicerae extractive solution is to because of mosquito bite and insect bite Caused pruitus has obvious inhibitory action;Stringy stonecrop extract solution plays the role of clearing heat and detoxicating, bactericidal antiphlogistic, controls pyogenic infections, For itch caused by after summer bite by mosquitos, swell and ache play the role of rapid detumescence, it is antipruritic;And Herba Andrographitis extract solution has heat-clearing Removing toxic substances, anti-inflammatory, swelling and pain relieving effect, its addition can alleviate skin swelling and pain, the symptom of itch, and Flos Lonicerae extractive solution, stringy stonecrop carry The use of arranging in pairs or groups according to a certain percentage of liquid and Herba Andrographitis extract solution is taken to strengthen repellent antipruritic effect of floral water.Dipropylene glycol is one Class NMF, excitant is small, with good moisture-keeping efficacy, and its addition, which can alleviate alcohol volatilization in floral water, causes dry skin The problem of.Crape myrtle extract solution, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis are extracted in the present invention The addition of liquid not only makes floral water smell unique, also assigns the good mosquito repellent of floral water, effect of repellent antipruritic;Dipropylene glycol The problem of dry skin occurred after traditional floral water use is alleviated in addition.
2. the material source used in floral water of the present invention is in plant extract material, harmless, excitant is small, preparation side Method is simple, and required equipment is common equipment, is well suited for large-scale production.
Embodiment
The invention provides a kind of floral water is provided, to make the purpose of the present invention, technical scheme and effect clearer, bright Really, the present invention is described in more detail below.It should be appreciated that specific embodiment described herein is only to explain this hair It is bright, it is not intended to limit the present invention.
In following examples, crape myrtle extract solution, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis Extract solution is extracted with following extracting method:
The extracting method of crape myrtle extract solution:First each constitutive material pick selecting pure, then weigh purple according to composition by weight Common vetch petal is placed in ultrasonic extractor, add 2-4 times of weight than pure water, with 28KHz frequencies under 45-48 DEG C of constant temperature Lower concussion filters to obtain crape myrtle extract solution after extracting 25-30 minutes.
The extracting method of Rosemary Oil:Component weighs fresh rosemary petal by weight, clean be put into distiller every Water is distilled, and big fire is heated 2-3 hours, produces mixed gas, and mixed gas enters in condenser pipe along conduit, is condensed into mixing former Liquid, mixing stoste is poured into separatory funnel, water-oil separating removes moisture and obtains Rosemary Oil.
The extracting method of Flos Lonicerae extractive solution:Flower, Ye Hezhi are opened with deionized water cleaning Lonicera japonica, honeysuckle, And dry to below water content 8-15%;In terms of quality parts ratio, 60-70 parts of Lonicera japonica, gold and silver are added into distilling apparatus The flowers are in blossom let off fireworks 10-20 parts, 5-10 parts of leaf, 12-20 DEG C of deionized water of 5-10 parts of branch and 200-300 mass parts be mixed into distillation body System;Control distillation system to keep 12-20 DEG C of immersion 2-6h, be then warming up to 50-70 DEG C, keep 6-15h, evaporation is collected in condensation Thing, obtains Flos Lonicerae extractive solution.
The extracting method of stringy stonecrop extract solution:It will crush, weigh through garbled stringy stonecrop, be soaked with 5 times of extraction solvents Repeated after stain 3d, filtering 3 times, merging filtrate produces corresponding stringy stonecrop crude extract;Crude extract is added to Rotary Evaporators In Claisen flask, the temperature of ethanol, chloroform, petroleum ether is controlled, at 60-70 DEG C, 50-60 DEG C, 40-50 DEG C, to be concentrated under reduced pressure respectively Obtain stringy stonecrop extract solution.
The extracting method of Herba Andrographitis extract solution:Take Herba Andrographitis to go the removal of impurity, clean, add the ethanol of 10-16 times of its weight Solution, under 230-270MPa, ultra high pressure treatment 1-4min;Then at 38-46 DEG C, ultrasonic wave extraction 12-24min;Centrifugation Separation, takes supernatant, obtains Herba Andrographitis extract solution.
Embodiment 1
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:40 parts of ethanol, 50 parts of deionized water, 3 parts of dipropylene glycol, 3 parts of sodium citrate, 2 parts of antioxidant, 4 parts of peppermint oil, 5 parts of crape myrtle extract solution, 6 parts of Rosemary Oil, 4 parts of Flos Lonicerae extractive solution, 5 parts of 6 parts of stringy stonecrop extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 70%;The antioxidant is two tertiary fourths Base paracresol.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, crape myrtle is taken to extract respectively Liquid, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right Mixture 1 carries out being heated to 85 DEG C, and mixture 1 is heated 1 hour under conditions of being maintained at 85 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, crape myrtle extract solution, Rosemary Oil, gold and silver are added in the mixture 2 of gained Flower extract solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, and 8min is stirred with 1000r/min mixing speed, make each Raw material is well mixed, and obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 3 hours under conditions of being placed in 0 DEG C, produces floral water.
Embodiment 2
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:45 parts of ethanol, 60 parts of deionized water, dipropylene glycol 4.5 Part, 5 parts of sodium citrate, 4 parts of antioxidant, 6 parts of peppermint oil, 7 parts of crape myrtle extract solution, 9 parts of Rosemary Oil, Flos Lonicerae extractive solution 6 7 parts of part, 8 parts of stringy stonecrop extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 73%;The antioxidant is two uncles Butyl paracresol.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, crape myrtle is taken to extract respectively Liquid, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right Mixture 1 carries out being heated to 90 DEG C, and mixture 1 is heated 1.5 hours under conditions of being maintained at 90 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, crape myrtle extract solution, Rosemary Oil, gold and silver are added in the mixture 2 of gained Flower extract solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, and 9min is stirred with 1100r/min mixing speed, make each Raw material is well mixed, and obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 4 hours under conditions of being placed in 3 DEG C, produces floral water.
Embodiment 3
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:50 parts of ethanol, 70 parts of deionized water, 6 parts of dipropylene glycol, 7 parts of sodium citrate, 6 parts of antioxidant, 8 parts of peppermint oil, 10 parts of crape myrtle extract solution, 11 parts of Rosemary Oil, Flos Lonicerae extractive solution 8 10 parts of part, 10 parts of stringy stonecrop extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 75%;The antioxidant is two Butylated Hydroxytoluene.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, crape myrtle is taken to extract respectively Liquid, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right Mixture 1 carries out being heated to 95 DEG C, and mixture 1 is heated 2 hours under conditions of being maintained at 95 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, crape myrtle extract solution, Rosemary Oil, gold and silver are added in the mixture 2 of gained Flower extract solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, and 10min is stirred with 1200r/min mixing speed, make each Raw material is well mixed, and obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 5 hours under conditions of being placed in 6 DEG C, produces floral water.
Embodiment 4
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:42 parts of ethanol, 55 parts of deionized water, 4 parts of dipropylene glycol, 4 parts of sodium citrate, 3 parts of antioxidant, 5 parts of peppermint oil, 6 parts of crape myrtle extract solution, 7 parts of Rosemary Oil, 5 parts of Flos Lonicerae extractive solution, 6 parts of 7 parts of stringy stonecrop extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 71%;The antioxidant is two tertiary fourths Base paracresol.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, crape myrtle is taken to extract respectively Liquid, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right Mixture 1 carries out being heated to 87 DEG C, and mixture 1 is heated 1.2 hours under conditions of being maintained at 87 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, crape myrtle extract solution, Rosemary Oil, gold and silver are added in the mixture 2 of gained Flower extract solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, and 8min is stirred with 1050r/min mixing speed, make each Raw material is well mixed, and obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 3.5 hours under conditions of being placed in 2 DEG C, produces floral water.
Embodiment 5
A kind of floral water that the present invention is provided is as follows:
A kind of floral water, is mainly made up of the raw material of following parts by weight:48 parts of ethanol, 65 parts of deionized water, 5 parts of dipropylene glycol, 6 parts of sodium citrate, 5 parts of antioxidant, 7 parts of peppermint oil, 9 parts of crape myrtle extract solution, 10 parts of Rosemary Oil, 7 parts of Flos Lonicerae extractive solution, 9 parts of 9 parts of stringy stonecrop extract solution and Herba Andrographitis extract solution.Wherein, the concentration of the ethanol is 74%;The antioxidant is two tertiary fourths Base paracresol.
The preparation method of floral water is as follows:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, crape myrtle is taken to extract respectively Liquid, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right Mixture 1 carries out being heated to 93 DEG C, and mixture 1 is heated 1.8 hours under conditions of being maintained at 93 DEG C, obtains mixture 2;
(3)To step(2)Dipropylene glycol, peppermint oil, crape myrtle extract solution, Rosemary Oil, gold and silver are added in the mixture 2 of gained Flower extract solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, and 10min is stirred with 1150r/min mixing speed, make each Raw material is well mixed, and obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 4.5 hours under conditions of being placed in 5 DEG C, produces floral water.
Performance test
Performance test is carried out to the product obtained by embodiment 1-5, it is as a result as follows:
(1)Smell is checked:Sense organ, smell is pure and fresh;
(2)The repelling effect test of floral water
Some mosquitoes are caught with mosquito catcher and are put into mosquito cage, after " starvation " at a night cultivates, are divided into 6 groups, and 5 groups respectively with scribbling The finger of embodiment 1-5 products obtained therefroms stretches into test in mosquito cage, and another group is with the finger test for being not coated with floral water, testing time 5 group fingers that product of the present invention is scribbled within 10min, 10min are all close without mosquito, and are not coated with being stung in the finger for floral water Sting.Thus illustrate that floral water of the present invention has good repelling effect.
(3)Repellent antipruritic validity check
The detumescence effect that embodiment 1-5 prepares floral water is evaluated by experiment on probation, the volunteer 120 of 20-60 Sui is elected, Sex ratio is 1:1, cause red swelling of the skin itch using mosquito saliva is injected, they are randomly divided into 6 groups, every group 20, its In have one group as a control group, daily sooner or later respectively apply a corresponding floral water of 1-5 products of the embodiment of the present invention once, compare institute The floral water used is commercially available floral water, continuous to use a week, redness and the consulting user detected by an unaided eye on skin The improvement situation of pruritis, counts repellent antipruritic effect efficiently individual quantity and the effective people of antipruritic effect of 6 group volunteers respectively Count and be recorded in as in following table.Assay such as following table:
Test group Repellent antipruritic effect efficiently individual quantity Antipruritic effect efficiently individual quantity
Embodiment 1 19 18
Embodiment 2 18 17
Embodiment 3 18 19
Embodiment 4 17 17
Embodiment 5 17 17
Control group 9 10
Embodiment 1-5 products have obvious repellent antipruritic effect to most people as seen from the above table, and commercially available floral water only has gently Micro- repellent antipruritic effect.
Smell favorable comment degree and stimulation sex investigation:
Choose 80 volunteers and participate in experiment, volunteer is selected from the crowd to odor-sensitive, its range of age at 20-60 Sui, its Volunteer's number of this 4 age brackets of middle 20-30 Sui, 30-40 Sui, 40-50 Sui and 50-60 Sui is 20 people, and each age The sex ratio of section is 1:1, this 80 volunteers are randomly divided into two test groups of A, B, every group of 40 people.
Test group and subjects:A groups use floral water of the present invention, and B groups use commercially available floral water.
Test method:Floral water is sprayed on interior by volunteer before sleeping every night, and each volunteer uses the amount of floral water every time It is identical, it is continuous to use 20 days, it is desirable to not used similar product in volunteer 20 days.
Evaluation criterion:Sensory evaluation is carried out for the smell of floral water, is divided into satisfied, general and dissatisfied three evaluations etc. Level, statistics is satisfied with the percentage shared by the grade after 20 days, and is recorded in table;Excitant to floral water is evaluated, will Hope person according to the excitant of floral water whether there is respectively favorable comment, in comment and difference comments three opinion ratings, counted after 20 days shared by favorable comment Percentage, and be recorded in table.
After 20 days, investigation statisticses result is as shown in the table:
Experimental group number evidence Smell Excitant
A groups 90% 89%
B groups 65% 58%
Find out that liquid distilled from honeysuckle flowers or lotus leaves aqueous vapor of the present invention is received by most of consumer by data above, improved compared to commercially available prod, together When have stimulate it is small the characteristics of.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair The equal change or modification change completed under bright patent claim, the technical spirit suggested by all present invention, all should belong to Cover the scope of the claims in the present invention.

Claims (6)

1. a kind of floral water, it is characterised in that be mainly made up of the raw material of following parts by weight:40-50 parts of ethanol, deionized water 50-70 parts, 3-6 parts of dipropylene glycol, 3-7 parts of sodium citrate, 2-6 parts of antioxidant, 4-8 parts of peppermint oil, 5-10 parts of crape myrtle extract solution, 5-10 parts of 6-11 parts of Rosemary Oil, 4-8 parts of Flos Lonicerae extractive solution, 6-10 parts of stringy stonecrop extract solution and Herba Andrographitis extract solution.
2. a kind of floral water according to claim 1, it is characterised in that be mainly made up of the raw material of following parts by weight:Second 42-48 parts of alcohol, 55-65 parts of deionized water, 4-5 parts of dipropylene glycol, 4-6 parts of sodium citrate, 3-5 parts of antioxidant, peppermint oil 5-7 Part, 6-9 parts of crape myrtle extract solution, 7-10 parts of Rosemary Oil, 5-7 parts of Flos Lonicerae extractive solution, 7-9 parts of stringy stonecrop extract solution and punching 6-9 parts of lotus extract solution.
3. a kind of floral water according to claim 1, it is characterised in that be mainly made up of the raw material of following parts by weight:Second 45 parts of alcohol, 60 parts of deionized water, 4.5 parts of dipropylene glycol, 5 parts of sodium citrate, 4 parts of antioxidant, 6 parts of peppermint oil, crape myrtle extract solution 7 Part, 9 parts of Rosemary Oil, 6 parts of Flos Lonicerae extractive solution, 8 parts of stringy stonecrop extract solution and 7 parts of Herba Andrographitis extract solution.
4. a kind of floral water according to claim 1-3 any one, it is characterised in that:Described antioxidant is two tertiary fourths Base paracresol.
5. a kind of floral water according to claim 1-3 any one, it is characterised in that:The concentration of the ethanol is 70%- 75%。
6. a kind of prepare a kind of method of floral water described in claim 1-3 any one, it is characterised in that including following step Suddenly:
(1)By weight, ethanol, deionized water, dipropylene glycol, sodium citrate, antioxidant, peppermint oil, crape myrtle is taken to extract respectively Liquid, Rosemary Oil, Flos Lonicerae extractive solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, it is standby;
(2)Ethanol, deionized water, sodium citrate and antioxidant are mixed and mixture 1 is uniformly mixing to obtain, it is then right Mixture 1 carries out being heated to 85-95 DEG C, and mixture 1 is heated 1-2 hours under conditions of being maintained at 85-95 DEG C, is mixed Thing 2;
(3)To step(2)Dipropylene glycol, peppermint oil, crape myrtle extract solution, Rosemary Oil, gold and silver are added in the mixture 2 of gained Flower extract solution, stringy stonecrop extract solution and Herba Andrographitis extract solution, and 8- is stirred with 1000-1200r/min mixing speed 10min, is well mixed each raw material, obtains mixture 3;
(4)By step(3)The mixture 3 of gained carries out refrigeration 3-5 hours under conditions of being placed in 0-6 DEG C, produces floral water.
CN201710272467.5A 2017-04-24 2017-04-24 A kind of repellent antipruritic floral water Withdrawn CN107213049A (en)

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CN103655718A (en) * 2012-08-30 2014-03-26 北京妙心堂医药科技有限公司 Traditional Chinese medicine composition, preparation, and floral water and application method thereof
CN105434261A (en) * 2015-12-21 2016-03-30 青岛克立克信息技术有限公司 Mosquito repellent toilet water
CN106389238A (en) * 2016-12-09 2017-02-15 申艾平 Floral water

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CN101632725A (en) * 2009-06-04 2010-01-27 深圳帕雷特科技有限公司 Liquid for relieving itching and eliminating swelling
CN103655718A (en) * 2012-08-30 2014-03-26 北京妙心堂医药科技有限公司 Traditional Chinese medicine composition, preparation, and floral water and application method thereof
CN103520512A (en) * 2013-11-01 2014-01-22 山东省千佛山医院 Method for preparing traditional Chinese medicine lotion used for treating red face type back carbuncle
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CN110638724A (en) * 2019-11-06 2020-01-03 高小军 Natural whitening floral water and preparation method thereof

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